US3461506A - Die for hot-pressing powdered metal - Google Patents

Die for hot-pressing powdered metal Download PDF

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Publication number
US3461506A
US3461506A US633779A US3461506DA US3461506A US 3461506 A US3461506 A US 3461506A US 633779 A US633779 A US 633779A US 3461506D A US3461506D A US 3461506DA US 3461506 A US3461506 A US 3461506A
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United States
Prior art keywords
die
powdered metal
hot
dies
pressing powdered
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Expired - Lifetime
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US633779A
Inventor
Richard E Rice
George Warren Webb
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Comstock and Wescott Inc
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Comstock and Wescott Inc
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B30PRESSES
    • B30BPRESSES IN GENERAL
    • B30B15/00Details of, or accessories for, presses; Auxiliary measures in connection with pressing
    • B30B15/02Dies; Inserts therefor; Mounting thereof; Moulds
    • B30B15/022Moulds for compacting material in powder, granular of pasta form
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F3/00Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
    • B22F3/12Both compacting and sintering
    • B22F3/14Both compacting and sintering simultaneously
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S425/00Plastic article or earthenware shaping or treating: apparatus
    • Y10S425/026High pressure

Definitions

  • Objects of this invention are to overcome the aforesaid ditiiculty and to provide a die in which there is no tendency to weld, gall or score either the die or the compacted article.
  • the present invention involves the discovery that titanium carbide is unique in that it affords dies which avoid all tendency to adhere to the compacted articles.
  • the titanium car-bide is preferably bonded with small amounts of nickel or cobalt or both, e.g., to the extent of about 3 to 12 percent by weight.
  • the walls of the dies may consist of titanium carbide, the dies would then be unduly costly. Consequently the walls are preferably made of some other material, such as tungsten carbide, and then lined with titanium carbide. This can be done by making a thin liner to fit the die or by vapor disposition in well-known manner.
  • FIG. 1 is a longitudinal axial section
  • FIG. 2 is an end view.
  • the particular embodiment chosen for the purpose of illustration comprises a cylinder made of tungsten carbide 3,461,506 Patented Aug. 19, 1969 "ice in three sections 1, 2 and 3 to facilitate finishing the inner surface of the die before the sections are assembled.
  • Wire 4 having a thermal expansion coefiicient closely matching that of the die, such as tungsten or molybdenum, as disclosed and claimed in the copending application of Richard E. Rice, Sr., No. 633,780, tiled on even date herewith.
  • the inner surfaces of the sections are lined with surfaces 5 of titanium carbide as above described.
  • the powdered metal is compressed between two plungers 6 and 7 in usual manner.
  • the upper plunger 6 is Withdrawn as shown in FIG. l, and to expel the compacted article the upper plunger is Withdrawn and the lower plunger is advanced.
  • a die having an inner surface consisting principally of titanium carbide.
  • a die according to claim 1 wherein said surface also comprises nickel or cobalt or both.

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  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Physical Vapour Deposition (AREA)
  • Chemical Vapour Deposition (AREA)
  • Powder Metallurgy (AREA)

Description

Aug. 19, 1969 R E. mcg ETAL 3,461,506
DIE FOR HOTITPRESSING POWDERED METAL I med April 2e. 1967 eo hfarre l yz M law United States Patent O U.S. Cl. 18-47 5 Claims ABSTRACT OF THE DISCLOSURE A die having an inner surface which does not adhere to powdered metal when compressed under high pressure and temperature.
In the use of powdered metal for making articles it is customary to compress the powder in dies under high pressure and temperature. However difculty has been experienced due to the powder sticking to the inner surfaces of the dies even when the dies are made of tungsten carbide. This results not only in imperfect articles but also in rapid deterioration of the dies.
Objects of this invention are to overcome the aforesaid ditiiculty and to provide a die in which there is no tendency to weld, gall or score either the die or the compacted article.
The present invention involves the discovery that titanium carbide is unique in that it affords dies which avoid all tendency to adhere to the compacted articles. The titanium car-bide is preferably bonded with small amounts of nickel or cobalt or both, e.g., to the extent of about 3 to 12 percent by weight.
While the walls of the dies may consist of titanium carbide, the dies would then be unduly costly. Consequently the walls are preferably made of some other material, such as tungsten carbide, and then lined with titanium carbide. This can be done by making a thin liner to fit the die or by vapor disposition in well-known manner.
For the purpose of illustration a typical embodiment of the invention is shown in the accompanying drawings in which FIG. 1 is a longitudinal axial section; and
FIG. 2 is an end view.
The particular embodiment chosen for the purpose of illustration comprises a cylinder made of tungsten carbide 3,461,506 Patented Aug. 19, 1969 "ice in three sections 1, 2 and 3 to facilitate finishing the inner surface of the die before the sections are assembled. To hold the sections together the die is wound with Wire 4 having a thermal expansion coefiicient closely matching that of the die, such as tungsten or molybdenum, as disclosed and claimed in the copending application of Richard E. Rice, Sr., No. 633,780, tiled on even date herewith. The inner surfaces of the sections are lined with surfaces 5 of titanium carbide as above described.
In use the powdered metal is compressed between two plungers 6 and 7 in usual manner. To charge the die with powdered metal the upper plunger 6 is Withdrawn as shown in FIG. l, and to expel the compacted article the upper plunger is Withdrawn and the lower plunger is advanced.
It should be understood that the present disclosure is for the purpose of illustration only and that this invention includes all modifications and equivalents which fall within the scope of the appended claims.
We claim:
1. For making articles by hot-pressing powdered metal, a die having an inner surface consisting principally of titanium carbide.
2. A die according to claim 1` wherein said surf-ace comprises a liner.
3. A die according to claim 1 wherein said surface comprises a vapor deposition.
4. A die according to claim 1 wherein said surface also comprises nickel or cobalt or both.
5. A die according to claim 3 wherein the body of the die consists of tungsten carbide.
References Cited UNITED STATES PATENTS 3,067,465 12/ 1962 Giardini et al. 3,061,877 11/1962 Custers et al. 3,084,388 4/ 1963 Ballhausen 18-16.5 3,085,291 4/1963 Hals etal 18-16.5 3,088,170 5/ 1963 Strong. 3,213,491 10/1965 Craig. 3,329,513 7/1967 Murata et al 264-332 X I. HOWARD FLINT, JR., Primary Examiner U.S. C1. X.R.
US633779A 1967-04-26 1967-04-26 Die for hot-pressing powdered metal Expired - Lifetime US3461506A (en)

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US63377967A 1967-04-26 1967-04-26

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Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US28574A (en) * 1860-06-05 Improvement jn core-boxes
US3810382A (en) * 1969-06-25 1974-05-14 Sandvik Ab Moulds
USRE28574E (en) * 1967-12-15 1975-10-21 Fiber reinforced hot pressing molds
US4142888A (en) * 1976-06-03 1979-03-06 Kelsey-Hayes Company Container for hot consolidating powder
US4340350A (en) * 1978-10-20 1982-07-20 Austung Proprietary Limited Process and apparatus for the manufacture of sintered tungsten carbide tool tips
US4380421A (en) * 1980-11-10 1983-04-19 Institut Cerac S.A. Die for compaction of powder
USRE31355E (en) * 1976-06-03 1983-08-23 Kelsey-Hayes Company Method for hot consolidating powder
US5308232A (en) * 1988-12-20 1994-05-03 Institut Strukturnoi Makrokinetiki Akademii Nauk Sssr Apparatus for making products from powdered materials
RU207524U1 (en) * 2021-04-05 2021-11-01 Федеральное государственное бюджетное учреждение науки "Дагестанский федеральный исследовательский центр Российской академии наук" HOT PRESS MOLD

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3061877A (en) * 1959-11-05 1962-11-06 Adamant Lab Proprietary Ltd High-pressure die
US3067465A (en) * 1961-04-05 1962-12-11 Armando A Giardini Pressure and temperature sensing device for high pressure apparatus
US3084388A (en) * 1959-03-18 1963-04-09 Ballhausen Carl Method of and a device for generating high pressures
US3085291A (en) * 1960-10-31 1963-04-16 Philips Corp Device for manufacturing magnetically anisotropic bodies
US3088170A (en) * 1961-08-02 1963-05-07 Gen Electric Two-terminal end cap for high pressure, high temperature reaction vessels
US3213491A (en) * 1961-12-18 1965-10-26 United Aircraft Corp Hardcoated mold press die
US3329513A (en) * 1965-11-08 1967-07-04 Carborundum Co Ceramic compositions and process of making same

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3084388A (en) * 1959-03-18 1963-04-09 Ballhausen Carl Method of and a device for generating high pressures
US3061877A (en) * 1959-11-05 1962-11-06 Adamant Lab Proprietary Ltd High-pressure die
US3085291A (en) * 1960-10-31 1963-04-16 Philips Corp Device for manufacturing magnetically anisotropic bodies
US3067465A (en) * 1961-04-05 1962-12-11 Armando A Giardini Pressure and temperature sensing device for high pressure apparatus
US3088170A (en) * 1961-08-02 1963-05-07 Gen Electric Two-terminal end cap for high pressure, high temperature reaction vessels
US3213491A (en) * 1961-12-18 1965-10-26 United Aircraft Corp Hardcoated mold press die
US3329513A (en) * 1965-11-08 1967-07-04 Carborundum Co Ceramic compositions and process of making same

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US28574A (en) * 1860-06-05 Improvement jn core-boxes
USRE28574E (en) * 1967-12-15 1975-10-21 Fiber reinforced hot pressing molds
US3810382A (en) * 1969-06-25 1974-05-14 Sandvik Ab Moulds
US4142888A (en) * 1976-06-03 1979-03-06 Kelsey-Hayes Company Container for hot consolidating powder
USRE31355E (en) * 1976-06-03 1983-08-23 Kelsey-Hayes Company Method for hot consolidating powder
US4340350A (en) * 1978-10-20 1982-07-20 Austung Proprietary Limited Process and apparatus for the manufacture of sintered tungsten carbide tool tips
US4380421A (en) * 1980-11-10 1983-04-19 Institut Cerac S.A. Die for compaction of powder
US5308232A (en) * 1988-12-20 1994-05-03 Institut Strukturnoi Makrokinetiki Akademii Nauk Sssr Apparatus for making products from powdered materials
RU207524U1 (en) * 2021-04-05 2021-11-01 Федеральное государственное бюджетное учреждение науки "Дагестанский федеральный исследовательский центр Российской академии наук" HOT PRESS MOLD

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