US3406736A - Mold for sampling molten iron - Google Patents

Mold for sampling molten iron Download PDF

Info

Publication number
US3406736A
US3406736A US539999A US53999966A US3406736A US 3406736 A US3406736 A US 3406736A US 539999 A US539999 A US 539999A US 53999966 A US53999966 A US 53999966A US 3406736 A US3406736 A US 3406736A
Authority
US
United States
Prior art keywords
mold
sample
iron
sampling
molten iron
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
US539999A
Inventor
Robert W Jett
James I Mcnelis
Sowa Steven
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Ford Motor Co
Original Assignee
Ford Motor Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ford Motor Co filed Critical Ford Motor Co
Priority to US539999A priority Critical patent/US3406736A/en
Application granted granted Critical
Publication of US3406736A publication Critical patent/US3406736A/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Images

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/10Devices for withdrawing samples in the liquid or fluent state
    • G01N1/12Dippers; Dredgers
    • G01N1/125Dippers; Dredgers adapted for sampling molten metals
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S249/00Static molds
    • Y10S249/04Test mold

Definitions

  • ABSTRACT OF THE DISCLOSURE A sampling device for removing an analytical sample from a fiow stream of molten metal such as gray or pig iron. This sampling device is fabricated from a highly conductive, high melting point metal.
  • This invention relates to the ferrous metal production field and is more specifically concerned with a process and apparatus for more elfectively correlating the operations of a conventional blast furnace and a basic Oxygen furnace for the production of steel from the iron produced by the blast furnace.
  • This invention is more particularly concerned with a process of accurately and quickly sampling the blast furnace iron as it is tapped from the blast furnace and with an apparatus for executing this sampling method.
  • the usual basic Oxygen charge is approximately seventy percent molten blast furnace iron and is charged as received from the blast furnace.
  • An essentially immediate knowledge of the chemistry of this lmolten iron is necessary to the intelligent and most effective operation of the basic Oxygen furnace into which this iron is charged.
  • the process and apparatus taught by this invention enables a sarnple of this iron to be taken quickly, economically and without contamination.
  • FIGURE 1 is an exploded perspective view of the essentials of the sampling apparatus with a similar showing of a finished sample
  • FIGURE 2 is a perspective view of the actual sampling operation showing pictorially the preferred Way of obtaining a sample from a stream of molten iron as it fiows from the blast furnace.
  • FIGURE 1 clearly shows the mold employed for casting the sample.
  • the particular device illustrated has been machined from a copper rod four inches (10.2 cm.) long and two and one eighth inches (5.4 cm.) in diameter. Copper has been chosen for its combination of very high conductivity and reasonably high melting point.
  • the invention is not limited to the use of copper but may obviously by carried out in a mold of silver, or any other metal of similar thermal characteristics.
  • the mold employed in this invention may well take the form of a cylinder split upon a longitudinal axis, with the halves so produced provided with keying recesses and tapered dowel pins to assure proper assembly.
  • a circular passage one half inch (1.3 cm.) in diameter and one and one quarter inches (3.18 cm.) deep is drilled axially from each end of the mold assembly. That portion of the mold 3,406,736 Patented Oct. 22, 1968 ICC between the ends of these passages is machined to produe a sample cavity which will produce a sample one and one quarter inches (3.18 cm.) in diameter and about three sixteenths (0.48 cm.) of an inch thick. This sample 5 cavity is connected at each end to the circular passages.
  • the mold described supra is secured in refractory coated tongs (not shown) and placed in the fiowing stream of iron with the upstream mold passage immersed in the molten iron and the downstream passage held out of the iron stream.
  • the high thermal conductivity of the copper mold protects it from attack by the molten iron for a period of time sufficient to permit a sample to be secured.
  • the particular mold form shown provides, if necessary, for an initial brief fiow of iron through the mold if a rapid iron stream is conducted through the mold and also for the freezing of a sample promptly in the sample cavity when the fiow is retarded.
  • the rate of fiow is regulated by the inclination of the mold.
  • the finished sample is promptly obtained by separating the two halves of the mold and removing the cast sample.
  • the sample in the sample cavity is available for chemical analysis With only minor surface preparation.
  • This invention is clearly applicable to the sampling of metals from molten streams other than cast iron.
  • Molten finished steel is an obvious example.

Landscapes

  • Life Sciences & Earth Sciences (AREA)
  • Hydrology & Water Resources (AREA)
  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Sampling And Sample Adjustment (AREA)
  • Investigating And Analyzing Materials By Characteristic Methods (AREA)

Description

Oct. 22, 1968 R. w. JETT ETAL MOLD FOR SAMPLING MOLTEN IRON Filed April 4, 1966 F/G. Z
////U/ /UU /z/ ROBERT W JE 77' JAMES Mc/VE IS STEVEN SOWA INVENTORS United States Patent O 3,406,736 MOLD FOR SAMPLING MOLTEN IRON Robert W. Jett, Sonthgate, James I. McNelis, Trenton,
and Steven Sowa, Lincoln Park, Mlich., assignors to Ford Motor Company, Dearborn, Mich., a corporation of Delaware Filed Apr. 4, 1966, Ser. No. 539,999 4 Clairns. (Cl. 164-4) ABSTRACT OF THE DISCLOSURE A sampling device for removing an analytical sample from a fiow stream of molten metal such as gray or pig iron. This sampling device is fabricated from a highly conductive, high melting point metal.
This invention relates to the ferrous metal production field and is more specifically concerned with a process and apparatus for more elfectively correlating the operations of a conventional blast furnace and a basic Oxygen furnace for the production of steel from the iron produced by the blast furnace. This invention is more particularly concerned with a process of accurately and quickly sampling the blast furnace iron as it is tapped from the blast furnace and with an apparatus for executing this sampling method.
The usual basic Oxygen charge is approximately seventy percent molten blast furnace iron and is charged as received from the blast furnace. An essentially immediate knowledge of the chemistry of this lmolten iron is necessary to the intelligent and most effective operation of the basic Oxygen furnace into which this iron is charged. The process and apparatus taught by this invention enables a sarnple of this iron to be taken quickly, economically and without contamination.
This invention is explained in connection with the drawings in which:
FIGURE 1 is an exploded perspective view of the essentials of the sampling apparatus with a similar showing of a finished sample, and
FIGURE 2 is a perspective view of the actual sampling operation showing pictorially the preferred Way of obtaining a sample from a stream of molten iron as it fiows from the blast furnace.
FIGURE 1 clearly shows the mold employed for casting the sample. The particular device illustrated has been machined from a copper rod four inches (10.2 cm.) long and two and one eighth inches (5.4 cm.) in diameter. Copper has been chosen for its combination of very high conductivity and reasonably high melting point. The invention is not limited to the use of copper but may obviously by carried out in a mold of silver, or any other metal of similar thermal characteristics.
The mold employed in this invention may well take the form of a cylinder split upon a longitudinal axis, with the halves so produced provided with keying recesses and tapered dowel pins to assure proper assembly. A circular passage one half inch (1.3 cm.) in diameter and one and one quarter inches (3.18 cm.) deep is drilled axially from each end of the mold assembly. That portion of the mold 3,406,736 Patented Oct. 22, 1968 ICC between the ends of these passages is machined to produe a sample cavity which will produce a sample one and one quarter inches (3.18 cm.) in diameter and about three sixteenths (0.48 cm.) of an inch thick. This sample 5 cavity is connected at each end to the circular passages.
The actual sampling operation is seen in FIGURE 2.
The mold described supra is secured in refractory coated tongs (not shown) and placed in the fiowing stream of iron with the upstream mold passage immersed in the molten iron and the downstream passage held out of the iron stream. The high thermal conductivity of the copper mold protects it from attack by the molten iron for a period of time sufficient to permit a sample to be secured. The particular mold form shown provides, if necessary, for an initial brief fiow of iron through the mold if a rapid iron stream is conducted through the mold and also for the freezing of a sample promptly in the sample cavity when the fiow is retarded. The rate of fiow is regulated by the inclination of the mold.
The finished sample is promptly obtained by separating the two halves of the mold and removing the cast sample. The sample in the sample cavity is available for chemical analysis With only minor surface preparation.
This invention is clearly applicable to the sampling of metals from molten streams other than cast iron. Molten finished steel is an obvious example.
We clairn as our invention:
1. The process of obtaining a clean and representative analytieal sample from a stream of molten metal comprising supporting a highly conductive metallic mold in the stream of molten metal, said mold having a pair of passages each of which start at an end of the mold and terminate in an intermediate sample cavity which sample cavity has one dimension much less than the smallest dimension of the passages, fiowing the molten metal through one of the passages into the sample cavity and freezing the sample in the cavity to provide the solid sample.
' 2. The process recited in claim 1 in which the sample is taken with the axis of the passages arranged so that the outer termination of the upstream passage is immersed in molten metal and the outer termination of the downstream passage is at least partially above the adjacent fiowing metal.
3. The process recited in claim 1 in which the arrangement of the mold in the stream is such that the first metal entering the mold fiows past the sample cavity without solidifying therein.
4. The process recited in claim 1 in which the small dimension of the sample cavity is approximately Vertical. 50
References Cited J. SPENCER OVERI-IOLSER, Primary Examiner. E. MAR, Assistant Examner.
US539999A 1966-04-04 1966-04-04 Mold for sampling molten iron Expired - Lifetime US3406736A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
US539999A US3406736A (en) 1966-04-04 1966-04-04 Mold for sampling molten iron

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US539999A US3406736A (en) 1966-04-04 1966-04-04 Mold for sampling molten iron

Publications (1)

Publication Number Publication Date
US3406736A true US3406736A (en) 1968-10-22

Family

ID=24153542

Family Applications (1)

Application Number Title Priority Date Filing Date
US539999A Expired - Lifetime US3406736A (en) 1966-04-04 1966-04-04 Mold for sampling molten iron

Country Status (1)

Country Link
US (1) US3406736A (en)

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3583236A (en) * 1969-12-05 1971-06-08 United States Steel Corp Sampling mold and method of obtaining samples of molten metal
US3656347A (en) * 1970-06-24 1972-04-18 William J Collins Device and method for sampling molten metal
US3996803A (en) * 1974-11-26 1976-12-14 Falk Richard A Molten metal sampling apparatus
US6454459B1 (en) * 1998-02-26 2002-09-24 Novacast Ab Device and process for thermal analysis of molten metals
EP2781607A1 (en) 2013-03-20 2014-09-24 Heraeus Electro-Nite International N.V. Sampler for molten iron
EP3336513A1 (en) 2016-12-13 2018-06-20 Heraeus Electro-Nite International N.V. Sampler for hot metal

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2189238A (en) * 1938-05-23 1940-02-06 Israel J Benjamin Sampling dipper
US3188565A (en) * 1962-03-29 1965-06-08 Shell Oil Co Drum shaped fluid stream analysis detector having vortical flow of the fluid therein
US3236103A (en) * 1963-09-12 1966-02-22 United States Steel Corp Method for sampling molten metal
US3289069A (en) * 1962-07-30 1966-11-29 Trygon Electronics Inc Phase controlled voltage regulating system
US3295171A (en) * 1964-06-16 1967-01-03 Jones & Laughlin Steel Corp Frangible ceramic test mold
US3302919A (en) * 1965-11-12 1967-02-07 Abex Corp Apparatus for casting metal wheels

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2189238A (en) * 1938-05-23 1940-02-06 Israel J Benjamin Sampling dipper
US3188565A (en) * 1962-03-29 1965-06-08 Shell Oil Co Drum shaped fluid stream analysis detector having vortical flow of the fluid therein
US3289069A (en) * 1962-07-30 1966-11-29 Trygon Electronics Inc Phase controlled voltage regulating system
US3236103A (en) * 1963-09-12 1966-02-22 United States Steel Corp Method for sampling molten metal
US3295171A (en) * 1964-06-16 1967-01-03 Jones & Laughlin Steel Corp Frangible ceramic test mold
US3302919A (en) * 1965-11-12 1967-02-07 Abex Corp Apparatus for casting metal wheels

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3583236A (en) * 1969-12-05 1971-06-08 United States Steel Corp Sampling mold and method of obtaining samples of molten metal
US3656347A (en) * 1970-06-24 1972-04-18 William J Collins Device and method for sampling molten metal
US3996803A (en) * 1974-11-26 1976-12-14 Falk Richard A Molten metal sampling apparatus
US6454459B1 (en) * 1998-02-26 2002-09-24 Novacast Ab Device and process for thermal analysis of molten metals
EP2781607A1 (en) 2013-03-20 2014-09-24 Heraeus Electro-Nite International N.V. Sampler for molten iron
EP3336513A1 (en) 2016-12-13 2018-06-20 Heraeus Electro-Nite International N.V. Sampler for hot metal
US10495551B2 (en) 2016-12-13 2019-12-03 Heraeus Electro-Nite International N.V. Sampler for hot metal

Similar Documents

Publication Publication Date Title
JPS5573445A (en) Device for manufacturing metal slurry
JPS5293621A (en) Production of copper alloy containing graphite
US3406736A (en) Mold for sampling molten iron
DE2057962A1 (en) Lance for taking samples from a metal melt
EP0132643A1 (en) Temperature-measuring device
GB1283141A (en) Method of hardsoldering or brazing
Thomson et al. Evaluation of Grain Refinement of Leaded Yellow Brass(C 85800) and EnviroBrass III(C 89550) using Thermal Analysis
US895535A (en) Method of casting hollow metal bodies.
SU1686543A1 (en) Method for production of cable lugs from bimetal material
DE1015989B (en) Electrode arrangement in glass melting furnaces
SU862040A1 (en) Specimen for metal and alloy spectral analysis
JPS56114638A (en) Connecting rod manufacturing method
JPS5558396A (en) Copper plated steel plate excelling in lubricity
JPS6440142A (en) Continuous casting method for long hollow raw metal
ES461726A1 (en) Pouring of molten metal from a teeming vessel
Remaly et al. Brass Cartridge Case Flaw Detection
JPS5295503A (en) Production of alloy dispersed with metal particles
JPS5728669A (en) Method for manufacturing thin as-cated spheroidal graphite cast iron casting
KR19980022945U (en) Sampling Sampler for Charter Component Analysis
GB840584A (en) Method of making longitudinally perforated metal plates
DE9301069U1 (en) Temperature measuring device for internal measurement of hollow bodies
JPS5281003A (en) Equipment handling probe for molten metal
Gueussier Rotary Continuous Casting and its Possibilities
Protzer The Sampling of Alloys Subject to Segregation
JPS5645260A (en) Production of sendust-base alloy billet for hot working