US3395307A - Method and apparatus for producing an electrically conductive particle beam in a container under vacuum - Google Patents

Method and apparatus for producing an electrically conductive particle beam in a container under vacuum Download PDF

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US3395307A
US3395307A US317012A US31701263A US3395307A US 3395307 A US3395307 A US 3395307A US 317012 A US317012 A US 317012A US 31701263 A US31701263 A US 31701263A US 3395307 A US3395307 A US 3395307A
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particle beam
under vacuum
particles
electrically conductive
producing
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US317012A
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Haegi Marcel
Maisonnier Charles
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European Atomic Energy Community Euratom
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European Atomic Energy Community Euratom
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    • HELECTRICITY
    • H05ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
    • H05HPLASMA TECHNIQUE; PRODUCTION OF ACCELERATED ELECTRICALLY-CHARGED PARTICLES OR OF NEUTRONS; PRODUCTION OR ACCELERATION OF NEUTRAL MOLECULAR OR ATOMIC BEAMS
    • H05H1/00Generating plasma; Handling plasma
    • H05H1/54Plasma accelerators
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C14/00Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
    • C23C14/22Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
    • C23C14/24Vacuum evaporation
    • C23C14/32Vacuum evaporation by explosion; by evaporation and subsequent ionisation of the vapours, e.g. ion-plating
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01FMAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
    • H01F6/00Superconducting magnets; Superconducting coils
    • H01F6/06Coils, e.g. winding, insulating, terminating or casing arrangements therefor
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J27/00Ion beam tubes
    • H01J27/02Ion sources; Ion guns
    • H01J27/16Ion sources; Ion guns using high-frequency excitation, e.g. microwave excitation
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J37/00Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
    • H01J37/32Gas-filled discharge tubes
    • H01J37/32009Arrangements for generation of plasma specially adapted for examination or treatment of objects, e.g. plasma sources

Definitions

  • the instant invention relates to a method and an apparatus for producing, in a container under vacuum, an electrically conductive particle beam.
  • this beam may be obtained from the substance under study in the solid state if the thermodynamic conditions corresponding to this state are satisfactory; for absolute densities small than 10- g./cm. the rectilinear beams may be obtained by means of molecular beams.
  • a supersonic gaseous jet may be used the length of which before collapse is rigidly limited as it is practically impossible to obtain a Mach number greater than about 10 and the absolute density of which may only be small in view of the limited pumping speed of the vacuum pumps evacuating the system. It is also possible to use a number of fine solid or liquid particles in which case the desired absolute density is obtained by a judicial choice in the dimension and the concentration of the particles.
  • Particle beams having a density located between 10- and 10 g./crn. have been obtained or ways to obtain them suggested, by the condensation of a gas as it passes through a cooled nozzle followed by a separation of the mixture gas-droplets, the jet of droplets then forming said particle beam of a mean density of 10- to 10' g./cm.
  • Such particle beams may also be obtained by condensation of a gas on ionized centers followed by shooting of the gas-droplet mixture and then separation of the gas from the droplets, the jet of droplets forming the particle beam which has a mean absolute density of between 10- and 10- g./cm.
  • the invention relates to the production of conducting beams having an absolute density smaller than about 10' g./cm
  • a method of producing United States Patent 3,395,307 Patented July 30, 1968 an electrically conductive particle beam under vacuum consists in spreading the material which will constitute the beam in the form of a powder on a conducting electrode, in subjecting the said powder to an electrical field produced by the application of an electrical voltage between the electrode carrying the powder and a second electrode whereby the action of the field causes movement of the electrified powder grains insuch a way as to eject them from between the electrodes, in irradiating the powder grains by means of electromagnetic waves the frequency of which corresponds to maximum absorption of the waves by the powder grains whereby the action of the waves produces almost instantaneous volatilization of the grains and ionization of the material which thus becomes electrically conductive.
  • the ejection of the powder between the electrodes may also take place through an opening in one of the electrodes.
  • Ionization of the material may be increased by allowing an auxiliary electric current to flow through the particle beam.
  • a device for the production of an electrically conducting particle beam comprises a tight enclosure and pumping means connected thereto to create a vacuum; at least two conducting electrodes wherein one has an area adapted to support a powder of the material which will constitute the beam; these electrodes being connected to a high voltage electric source and being provided with means to throw the electrified powder grains inwardly of the space between the electrodes; the electrode which carries the powder having a substantially central aperture for the discharge of the electrified powder grains; and means to create an intense electrical are inside the said enclosure adjacent the passage of the electrified particles.
  • the drawing illustrates a tight casing or enclosure I placed under vacuum by a vacuum pump 2.
  • Casing 1 7 contains two flat electrodes 3 and 4 facing two tight and insulating passages 5 and 6 for connections joining plates 3 and 4 to a high voltage source 7 of, for instance 2x10 volts. Electrodes 3 and 4 are provided with convex peripheral rims 8 and 9 the purpose of which is explained below.
  • the lower electrode 3, over which the powder 10 to be ionized is spread, is provided with a central aperture 11.
  • the powder may, for instance, be grains of lithium aluminum hydride (LiAlH having a diameter of 10' cm.
  • a pair of electrodes 12, 13 Adjacent the axis of aperture 11 is mounted a pair of electrodes 12, 13 made of aluminum for instance, as this metal is included in the powder. Means is provided for the projection of an arc 14 between electrodes .12 and 13, the are having a very high intensity as, for instance, 2x10 amps. The are is energized through two tight and isolating passages 15, 16 by the discharge of a condenser 17 the circuit of which is closed by a spark-gap 18. Condenser 17 has a capacity of the order of one microfarad and is loaded under a voltage of approximately 20 kilovolts. Energization of arc 14 under vacuum is obtained by emission of cold electrons.
  • the operation of the device is as follows: the powder grains 10 loaded by contact with electrode 3 are attracted by the other electrode 4 over which they change their polarity and rebound.
  • a stationary condition prevails wherein, at each moment, the number of particles which come down per unit of time is equal to that which rises (see arrows f).
  • Rims 8 and 9 of the electrodes electrostatically and mechanically push back in the space between the electrodes the particles which would tend to escape from the ends.
  • the intense radiation-s 20 emitted by are 14 volatilize and ionize the jet-formed by a constellation of insulated powder grains-thus transforming it into an electrically conducting beam in such a brief period of time that the gaseous diffusion has not suffi-cient time to destroy the beam.
  • the invention finds numerous applications in the field of research:
  • the particle jet obtained may be used in the feeding of fusion nuclear reactors, for propulsion and compression of magnetic fields of great intensity, for the production of the UH radio frequencies, in plasma guns, in spacial propulsion, etc.
  • the industrial applications are equally quite interesting; it is used for high voltage switches, high current switches and high speed switches.
  • the invention is not limited to the embodiment which has just been described but also comprises various modificationssuch as, for instance, curving of the path of the particle jet 19 by subjecting it to the action of an auxiliary electric field in the case where a non-rectilinear beam is required.
  • a method for producing an electrically conducting beam of particles in vacuum which comprises spreading a powder of particles made of the material which is to constitute the beam on a first horizontal conducting electrode having a small aperture therein; subjecting the said powder to an electric field produced by applying an electrical voltage between the said first electrode carrying the powder and a second electrode whereby action of this field moves the electrified particles between the electrodes and ejects them through the said aperture; ir-
  • An apparatus for the production of an electricall conducting beam of particles comprising:
  • An apparatus as claimed in claim 3, comprising a rim on the edge of each electrode to prevent escape of the particles.

Description

July 30, 1968 M. HAEGI ET AL 3,395,307
METHOD AND APPARATUS FOR PRODUCING AN ELECTRICALLY CONDUCTIVE PARTICLE BEAM IN A CONTAINER UNDER VACUUM Filed on. 17, 1963 INVENTORS Marcel HAEGI Charles MAISDNNIER 3,395,307 METHOD AND APPARATUS FOR PRODUCING AN ELECTRICALLY CONDUCTIVE PARTICLE BEAM IN A CONTAINER UNDER VACUUM Marcel Haegi, Frascati, and Charles Maisonnier, Frascati- Grottaferrata, Italy, assignors to European Atomic Energy Community-Euratom Filed Oct. 17, 1963, Ser. No. 317,012 Claims priority, application Belgium, Oct. 29, 1962,
4 Claims. (51. 313-231 ABSTRACT OF THE DISCLOSURE The instant invention relates to a method and an apparatus for producing, in a container under vacuum, an electrically conductive particle beam.
In numerous scientific and industrial applications it is necessary to produce, in an enclosure under vacuum, a particle beam whose form, electric conductivity, density, chemical and isotopic composition must have predetermined values.
Particularly, for absolute densities of the order of 1 g./cm. this beam may be obtained from the substance under study in the solid state if the thermodynamic conditions corresponding to this state are satisfactory; for absolute densities small than 10- g./cm. the rectilinear beams may be obtained by means of molecular beams.
Between these two limits, a supersonic gaseous jet may be used the length of which before collapse is rigidly limited as it is practically impossible to obtain a Mach number greater than about 10 and the absolute density of which may only be small in view of the limited pumping speed of the vacuum pumps evacuating the system. It is also possible to use a number of fine solid or liquid particles in which case the desired absolute density is obtained by a judicial choice in the dimension and the concentration of the particles.
Particle beams having a density located between 10- and 10 g./crn. have been obtained or ways to obtain them suggested, by the condensation of a gas as it passes through a cooled nozzle followed by a separation of the mixture gas-droplets, the jet of droplets then forming said particle beam of a mean density of 10- to 10' g./cm. Such particle beams may also be obtained by condensation of a gas on ionized centers followed by shooting of the gas-droplet mixture and then separation of the gas from the droplets, the jet of droplets forming the particle beam which has a mean absolute density of between 10- and 10- g./cm.
Belgian Patent No. 611,449 has already been granted on a Methode pour produire des faisceaux rectilignes de matiere a linterieur (1 un espace ferme au sein duquel regne unvide pousse (Method for Producing Rectilinear Beams of Matter Inside a Closed Space Under High Vacuum).
It is an object of the present invention to widen the scope of the absolute density of these particle beams and to make them conductors of electricity; particularly, the invention relates to the production of conducting beams having an absolute density smaller than about 10' g./cm
According to the invention, a method of producing United States Patent 3,395,307 Patented July 30, 1968 an electrically conductive particle beam under vacuum consists in spreading the material which will constitute the beam in the form of a powder on a conducting electrode, in subjecting the said powder to an electrical field produced by the application of an electrical voltage between the electrode carrying the powder and a second electrode whereby the action of the field causes movement of the electrified powder grains insuch a way as to eject them from between the electrodes, in irradiating the powder grains by means of electromagnetic waves the frequency of which corresponds to maximum absorption of the waves by the powder grains whereby the action of the waves produces almost instantaneous volatilization of the grains and ionization of the material which thus becomes electrically conductive.
The ejection of the powder between the electrodes may also take place through an opening in one of the electrodes.
Ionization of the material may be increased by allowing an auxiliary electric current to flow through the particle beam.
Again in accordance with the invention, a device for the production of an electrically conducting particle beam comprises a tight enclosure and pumping means connected thereto to create a vacuum; at least two conducting electrodes wherein one has an area adapted to support a powder of the material which will constitute the beam; these electrodes being connected to a high voltage electric source and being provided with means to throw the electrified powder grains inwardly of the space between the electrodes; the electrode which carries the powder having a substantially central aperture for the discharge of the electrified powder grains; and means to create an intense electrical are inside the said enclosure adjacent the passage of the electrified particles.
A specific, although non-limitative, embodiment of the invention will now be described with reference to the annexed drawing containing a single figure which is a transverse cross-sectional view of an apparatus for the production of an electrically conductive particle beam according to the invention.
The drawing illustrates a tight casing or enclosure I placed under vacuum by a vacuum pump 2. Casing 1 7 contains two flat electrodes 3 and 4 facing two tight and insulating passages 5 and 6 for connections joining plates 3 and 4 to a high voltage source 7 of, for instance 2x10 volts. Electrodes 3 and 4 are provided with convex peripheral rims 8 and 9 the purpose of which is explained below. The lower electrode 3, over which the powder 10 to be ionized is spread, is provided with a central aperture 11. The powder may, for instance, be grains of lithium aluminum hydride (LiAlH having a diameter of 10' cm.
Adjacent the axis of aperture 11 is mounted a pair of electrodes 12, 13 made of aluminum for instance, as this metal is included in the powder. Means is provided for the projection of an arc 14 between electrodes .12 and 13, the are having a very high intensity as, for instance, 2x10 amps. The are is energized through two tight and isolating passages 15, 16 by the discharge of a condenser 17 the circuit of which is closed by a spark-gap 18. Condenser 17 has a capacity of the order of one microfarad and is loaded under a voltage of approximately 20 kilovolts. Energization of arc 14 under vacuum is obtained by emission of cold electrons.
The operation of the device is as follows: the powder grains 10 loaded by contact with electrode 3 are attracted by the other electrode 4 over which they change their polarity and rebound. A stationary condition prevails wherein, at each moment, the number of particles which come down per unit of time is equal to that which rises (see arrows f). Rims 8 and 9 of the electrodes electrostatically and mechanically push back in the space between the electrodes the particles which would tend to escape from the ends.
Finally, the descending particles escape through the aperture 11 and constitute the rectilinear jet 19. The intense radiation-s 20 emitted by are 14 volatilize and ionize the jet-formed by a constellation of insulated powder grains-thus transforming it into an electrically conducting beam in such a brief period of time that the gaseous diffusion has not suffi-cient time to destroy the beam.
The invention finds numerous applications in the field of research: The particle jet obtained may be used in the feeding of fusion nuclear reactors, for propulsion and compression of magnetic fields of great intensity, for the production of the UH radio frequencies, in plasma guns, in spacial propulsion, etc. The industrial applications are equally quite interesting; it is used for high voltage switches, high current switches and high speed switches.
It is to be understood that the invention is not limited to the embodiment which has just been described but also comprises various modificationssuch as, for instance, curving of the path of the particle jet 19 by subjecting it to the action of an auxiliary electric field in the case where a non-rectilinear beam is required.
We claim:
1, A method for producing an electrically conducting beam of particles in vacuum which comprises spreading a powder of particles made of the material which is to constitute the beam on a first horizontal conducting electrode having a small aperture therein; subjecting the said powder to an electric field produced by applying an electrical voltage between the said first electrode carrying the powder and a second electrode whereby action of this field moves the electrified particles between the electrodes and ejects them through the said aperture; ir-
radiatingthe ejected particles by means of electromagnetic waves the frequency of which corresponds to the frequency of the waves having the maximum absorption by the particles whereby the action of the waves produces an almost instantaneous volatilization of the particles and ionization of the material so that it becomes electrically conducting.
2. A method according to claim 1, wherein ionization of the material is increased by subjecting the beam of particles to an auxiliary electric current.
3. An apparatus for the production of an electricall conducting beam of particles comprising:
(a) a tight enclosure;
(b) means connected to said enclosure for creating a vacuum therein;
(c) at least two horizontally spaced conducting electrodes having facing surfaces, the lower electrode having a small aperture therein;
(d) a powder of particles made of the material which is to constitute the beam, spread over the lower electrode;
(e) a high voltage source for providing an electric field across the electrodes and for ejecting the electrified particles through said aperture; and
(f) a high intensity electromagnetic wave source within said enclosure for irradiating the ejected particles, the frequency of the said wave corresponding to the frequency of the waves having the maximum absorption by the said particles.
4. An apparatus as claimed in claim 3, comprising a rim on the edge of each electrode to prevent escape of the particles.
References Cited UNITED STATES PATENTS 3,239,717 3/1966 Peterson 3l73 JAMES W. LAWRENCE, Primary Examiner.
P. C. DEMEO, Assistant Examiner.
US317012A 1962-10-29 1963-10-17 Method and apparatus for producing an electrically conductive particle beam in a container under vacuum Expired - Lifetime US3395307A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3806763A (en) * 1971-04-08 1974-04-23 S Masuda Electrified particles generating apparatus

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RU2566620C2 (en) * 2013-12-24 2015-10-27 Сергей Николаевич Зубов Method and fuel for compound-synthesis, air jet engine running on compound-synthesis and turbomachine unit to this end (versions)

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3239717A (en) * 1962-02-26 1966-03-08 Goodrich High Voltage Astronau Method and apparatus for dispersing glomerate particles

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3239717A (en) * 1962-02-26 1966-03-08 Goodrich High Voltage Astronau Method and apparatus for dispersing glomerate particles

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3806763A (en) * 1971-04-08 1974-04-23 S Masuda Electrified particles generating apparatus

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