US3328125A - Reactive selectively sorptive silica materials and process of producing them - Google Patents

Reactive selectively sorptive silica materials and process of producing them Download PDF

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Publication number
US3328125A
US3328125A US149964A US14996461A US3328125A US 3328125 A US3328125 A US 3328125A US 149964 A US149964 A US 149964A US 14996461 A US14996461 A US 14996461A US 3328125 A US3328125 A US 3328125A
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particles
acid
materials
reaction
surface area
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US149964A
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Robert K Mays
Bertorelli Orlando Leonard
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JM Huber Corp
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JM Huber Corp
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Priority to US149964A priority Critical patent/US3328125A/en
Priority to GB3710062A priority patent/GB1020282A/en
Priority to DE19621467063 priority patent/DE1467063A1/de
Priority to FR913379A priority patent/FR1338067A/fr
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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09CTREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/40Compounds of aluminium
    • C09C1/42Clays
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N25/00Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
    • A01N25/08Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing solids as carriers or diluents
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/10Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/10Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
    • B01J20/103Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate comprising silica
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00Silicon; Compounds thereof
    • C01B33/113Silicon oxides; Hydrates thereof
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00Use of inorganic substances as compounding ingredients
    • C08K3/34Silicon-containing compounds
    • C08K3/36Silica
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/01Particle morphology depicted by an image
    • C01P2004/03Particle morphology depicted by an image obtained by SEM
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/54Particles characterised by their aspect ratio, i.e. the ratio of sizes in the longest to the shortest dimension
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/61Micrometer sized, i.e. from 1-100 micrometer
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/62Submicrometer sized, i.e. from 0.1-1 micrometer
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/12Surface area
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/14Pore volume
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/16Pore diameter
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/19Oil-absorption capacity, e.g. DBP values
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/60Optical properties, e.g. expressed in CIELAB-values
    • C01P2006/64Optical properties, e.g. expressed in CIELAB-values b* (yellow-blue axis)
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/80Compositional purity
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/80Compositional purity
    • C01P2006/82Compositional purity water content

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Analytical Chemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Agronomy & Crop Science (AREA)
  • Dispersion Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Medicinal Chemistry (AREA)
  • Pest Control & Pesticides (AREA)
  • Plant Pathology (AREA)
  • Toxicology (AREA)
  • Engineering & Computer Science (AREA)
  • Dentistry (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Silicon Compounds (AREA)
US149964A 1961-11-03 1961-11-03 Reactive selectively sorptive silica materials and process of producing them Expired - Lifetime US3328125A (en)

Priority Applications (4)

Application Number Priority Date Filing Date Title
US149964A US3328125A (en) 1961-11-03 1961-11-03 Reactive selectively sorptive silica materials and process of producing them
GB3710062A GB1020282A (en) 1961-11-03 1962-10-01 Reactive selectively sorptive silica materials and process for producing them
DE19621467063 DE1467063A1 (de) 1961-11-03 1962-10-20 Selektiv absorptionsfaehiges SiO2-haltiges Material und Verfahren zu seiner Herstellung
FR913379A FR1338067A (fr) 1961-11-03 1963-10-25 Matière siliceuse réactive et procédé de préparation

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US149964A US3328125A (en) 1961-11-03 1961-11-03 Reactive selectively sorptive silica materials and process of producing them
US62323167A 1967-03-15 1967-03-15

Publications (1)

Publication Number Publication Date
US3328125A true US3328125A (en) 1967-06-27

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US (1) US3328125A (fr)
FR (1) FR1338067A (fr)

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3437441A (en) * 1967-03-15 1969-04-08 Huber Corp J M Process of producing highly porous and reactive silica materials
US4230765A (en) * 1975-03-25 1980-10-28 Kabushiki Kaisha Osaka Packing Seizosho Novel amorphous silica, and products thereof
EP0165646A2 (fr) * 1984-06-22 1985-12-27 Mizusawa Industrial Chemicals Ltd. Phyllosilicate de magnésium lamellaire synthétique et procédé pour sa préparation
EP0165647A2 (fr) * 1984-06-22 1985-12-27 Mizusawa Industrial Chemicals Ltd. Procédé de préparation de minéral de silicate de zinc cristallin synthétique
US4780297A (en) * 1987-04-06 1988-10-25 J. M. Huber Corporation Low brightness magnesium silicate filler and methods
US5201950A (en) * 1987-04-06 1993-04-13 J. M. Huber Corporation Low brightness magnesium silicate SLR filler low brightness paper containing the filler and methods to produce the filler and use it in low brightness papers
US20060243164A1 (en) * 2002-11-22 2006-11-02 Dominique Dupuis Bituminous product and process for preparing it
US20070009751A1 (en) * 2005-07-05 2007-01-11 Chang Chun Plastics Co., Ltd. Polyamic acid resin composition modified with laminate nanometer silica sheet and polyimide prepared therefrom
US20170182514A1 (en) * 2015-12-25 2017-06-29 Tokyo Electron Limited Method for forming a protective film

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2027948A (en) * 1932-11-04 1936-01-14 Gen Chemical Corp Adsorbent
US2477639A (en) * 1947-10-04 1949-08-02 Houdry Process Corp Process of activating kaolin clay
US2485626A (en) * 1947-06-24 1949-10-25 Houdry Process Corp Catalytic conversion of hydrocarbons
US2731326A (en) * 1951-08-31 1956-01-17 Du Pont Process of preparing dense amorphous silica aggregates and product
US2879136A (en) * 1954-10-22 1959-03-24 Maloney Mabel Process of producing high bulking finely divided silica
US2940830A (en) * 1955-08-23 1960-06-14 Columbia Southern Chem Corp Method of preparing silica pigments

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2027948A (en) * 1932-11-04 1936-01-14 Gen Chemical Corp Adsorbent
US2485626A (en) * 1947-06-24 1949-10-25 Houdry Process Corp Catalytic conversion of hydrocarbons
US2477639A (en) * 1947-10-04 1949-08-02 Houdry Process Corp Process of activating kaolin clay
US2731326A (en) * 1951-08-31 1956-01-17 Du Pont Process of preparing dense amorphous silica aggregates and product
US2879136A (en) * 1954-10-22 1959-03-24 Maloney Mabel Process of producing high bulking finely divided silica
US2940830A (en) * 1955-08-23 1960-06-14 Columbia Southern Chem Corp Method of preparing silica pigments

Cited By (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3437441A (en) * 1967-03-15 1969-04-08 Huber Corp J M Process of producing highly porous and reactive silica materials
US4230765A (en) * 1975-03-25 1980-10-28 Kabushiki Kaisha Osaka Packing Seizosho Novel amorphous silica, and products thereof
US4330519A (en) * 1975-03-25 1982-05-18 Kabushiki Kaisha Osaka Packing Seizosho Novel amorphous silica
EP0165647A3 (fr) * 1984-06-22 1988-12-14 Mizusawa Industrial Chemicals Ltd. Procédé de préparation de minéral de silicate de zinc cristallin synthétique
JPH0513889B2 (fr) * 1984-06-22 1993-02-23 Mizusawa Industrial Chem
JPS6110019A (ja) * 1984-06-22 1986-01-17 Mizusawa Ind Chem Ltd ソーコナイト、ヘミモルファイト、或いはウィレマイト構造の合成結晶性ケイ酸亜鉛鉱物の製法
US4681749A (en) * 1984-06-22 1987-07-21 Mizusawa Industrial Chemicals, Ltd. Process for preparation of synthetic crystalline zinc silicate mineral having a sauconite, willemite or hemimorphite structure
EP0165647A2 (fr) * 1984-06-22 1985-12-27 Mizusawa Industrial Chemicals Ltd. Procédé de préparation de minéral de silicate de zinc cristallin synthétique
EP0165646A2 (fr) * 1984-06-22 1985-12-27 Mizusawa Industrial Chemicals Ltd. Phyllosilicate de magnésium lamellaire synthétique et procédé pour sa préparation
EP0165646A3 (en) * 1984-06-22 1989-03-08 Mizusawa Industrial Chemicals Ltd. Synthetic lamellar magnesium phyllosilicate and process for preparation thereof
US4780297A (en) * 1987-04-06 1988-10-25 J. M. Huber Corporation Low brightness magnesium silicate filler and methods
US5201950A (en) * 1987-04-06 1993-04-13 J. M. Huber Corporation Low brightness magnesium silicate SLR filler low brightness paper containing the filler and methods to produce the filler and use it in low brightness papers
US5300147A (en) * 1987-04-06 1994-04-05 J. M. Huber Corporation Low brightness magnesium silicate SLR filler, low-brightness paper containing the filler and methods to produce the filler and use it in low brightness papers
US20060243164A1 (en) * 2002-11-22 2006-11-02 Dominique Dupuis Bituminous product and process for preparing it
US20070009751A1 (en) * 2005-07-05 2007-01-11 Chang Chun Plastics Co., Ltd. Polyamic acid resin composition modified with laminate nanometer silica sheet and polyimide prepared therefrom
US20170182514A1 (en) * 2015-12-25 2017-06-29 Tokyo Electron Limited Method for forming a protective film
US10458016B2 (en) * 2015-12-25 2019-10-29 Tokyo Electron Limited Method for forming a protective film

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Publication number Publication date
FR1338067A (fr) 1963-09-20

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