US3096234A - Continuous digesting system - Google Patents

Continuous digesting system Download PDF

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US3096234A
US3096234A US770424A US77042458A US3096234A US 3096234 A US3096234 A US 3096234A US 770424 A US770424 A US 770424A US 77042458 A US77042458 A US 77042458A US 3096234 A US3096234 A US 3096234A
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liquor
pulp
digester
press
dilution tank
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Armstrong Bruce
William J Nolan
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NOLAN
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    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21CPRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C3/00Pulping cellulose-containing materials
    • D21C3/22Other features of pulping processes
    • D21C3/24Continuous processes

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  • This invention relates to a continuous digester system for producing pulp and, more particularly, to a continuous digester system lhav-ing improved mechanisms for introducing the chips to Ithe digester and withdrawing the cooked pulp therefrom.
  • the liquor ratio that is, the ratio of the weight of chemical solution to weight o-f dry wood has always been kept at a minimum, and, more specifically, ⁇ a liquor ratio of between 3.0:1 and 4.011 has in the past been used in order to minimize both the heat required to bring the ⁇ digester charge to cooking temperature and the heat required to evaporate the spent black liquor.
  • the second serious fault inherent in low liquor ratios is the necessarily high concentration of digestion chemicals needed at the start of the cook in order to insure a sufficiently high 4concentration near the end of the cook to supply driving force for the digestion reaction. If the liquor ratio can be increased without economic penalty, the .initial concentration of digestion chemicals therein can be markedly reduced, the strength of the liquor near the end of the cook being just ⁇ as high as if -a high ⁇ chemical concentration, low liquor ratio cook were performed. It the digester can be designed to permit the use of high liquor ratios, any suitable low initial concentration may be used. This provides .a lchoice of various combinations of concentrations and temperatures not available with low liquor-wood ratios.
  • the invention provides .a means of changing the liquor/wood ratio at each successive step so that each step in the process is performed at the most favorable consistency.
  • the mixture of cooking liquor and Wood is pumped at approximately 4% consistency because pumps for this service perform best at this consistency.
  • the mixture of liquor and chips requires steam to bring the mixture up to digester temperature.
  • Four percent consistency is equivalent to 24 lbs. liquor per lb. of oven-dry wood. This would require an excessive amount of steam.
  • the No. 1 liquor transfer press removes liquor from the mixture until there remains only that liquor required to provide suicient chemical to react with and remove substantially all the lignin and leave a small residual of chemical to force the reaction right up to the end of the cook.
  • the chips are moved through the digester during which time the pulping reaction occurs.
  • the cooked pulp exi-ting from the digester is fed through a How sensing device and then to a second press where some of the spent digestion liquor is expressed therefrom. Part of this spent liquor is returned and mixed with 4the chips entering the digester and ⁇ the balance is sent to the recovery system.
  • the pulp ⁇ and spent liquor mixed therewith exiting from the press define the external liquor ratio which is la measure of the heat leaving the system and which, in any event, will be much less than the internal liquor ratio.
  • Suitable pressures are maintained on the streams entering and leaving the digester so that the chips are continuously fed thereinto and cooked pulp is removed therefrom while a suitable digesting pressure is maintained within the digester.
  • the transfer is designed to have an output consistency ranging from 20% to 40% As there are 24 pounds of liquor per pound of ovendry wood at 4% consistency, and from 4 pounds to 1'1/2 pounds at 20 and 40% respectively, the transfer will remove from 20 pounds to 221/2 pounds of liquor per pound of wood.
  • Heating up only 21/2 to 5 pounds of mixture of wood and cooking liquor to digester temperature would constitute an ⁇ attractive steam ⁇ demand but presents 1a diiiicult material handling problem; and does not provide la sufficient volume of yliquor to effectively wet :all Kthe chips in tlrir passage through the system.
  • spent black liquor from the second liquor transfer press 36 is re- 5 cycled to the digester and added to the high consistency mixture to dilute it to the desired liquor ratio.
  • This new liquor ratio may range from a low of 5 to 1 up to a high of to 1.
  • the recycle black liquor may be introduced by means of an injector which not only provides the necessary energy to inject the liquor but also provides the heat necessary to bring the mixture of chips and cooking liquor up to digester temperature plus the heat losses in the system.
  • the recycle black liquor and steam may be added directly to the digester or, preferably, mixed with the output of the liquor transfer press just prior to entering the digester.
  • a concentration for the original cooking liquor is selected so that the mixture of wood, cooking liquor, steam and recycle black liquor will give the desired starting concentration for the liquor ratio selected and (at the end of the cook) will give the required minimum residual concentration.
  • the cellulosic material which may be shredded chips prepared in accordance with the disclosures of application Serial No. 578,378, iled April 16, 1956, now abandoned, or ⁇ application Serial No. 369,740, tiled July 22, 1953, now U.S. Patent No.
  • 2,904,460 is fed, usually after being weighed, onto aV conveyor 10.
  • the chips are fed by the conveyor into a mixing tank 11 and yfresh digestion liquor, sometimes hereinafter referred to .as white liquor, is added thereto.
  • the white liquor is ordinarily at the temperature at which it is pumped from the causticizing system, usually in a range of 150l80 F.
  • the white liquor is pumped :by a pump 13, through a meter 14 Iand a valve 15, into the tank.
  • the valve 15 is controlled by a liquid level control 16.
  • Sullicient White liquor is added to the tank 11A so that the chips therein can be kept in uniform suspension by the agitator 12 and can be read-ily pumped.
  • the quantity of white liquor may be varied to provide a consistency within the range of 2-10% and is not critical, since ⁇ all excess :over digester requirements is removed by the first liquor transfer press 18 and is returned to the mixing tank, No. 11.
  • the chip suspension discharged from the tank 11 passes through a pump 17 to the first liquor transfer press 18.
  • la primary purpose of the pump 17 is to provide a hydrostatic pressure sullicient to equalize or slightly exceed the steam pressure in the -digester plus what ever friction is developed in the system.
  • Many types of pumps may be used for this purpose, such as a high-head centrifugal, a multi-stage centrifugal or a progressive cavity pump.
  • the rst liquor transfer press 18 may be substantially the same as that shown in U.S. Patent No. 2,664,814 and consists yof Ia screw of decreasing pitch, said screw rotating in a perforated barrel.
  • the annular area of the press decreases from the entrance lto the exit thereof.
  • the amount lof white liquor in contact with the chips as the chips leave the press determines the external liquor ratio and is so selected that it is sutiicient to insure completion of the desired pulping reaction.
  • the press 18 does not operate against digester pressure. Rather, there is la hydrostatic pressure built up by the pump 17 equal to or slightly greater than the steam pressure in the digester i9.
  • the pressed chips, entering the digester 19, are mixed with spent liquor from the ⁇ discharge end of the digester.
  • the spent liquor is substantially at full digester pressure, for example, at 150 pounds per square inch and 366 F.
  • the chips and their accompanying white liquor, before mixing with the spent liquor are at a temperature in the range of about 150 to 180 F. Since the spent liquor mixed at this point is substantially at digester temperature and pressure the only ⁇ steam required will be that amount necessary to heat the chips and white liquor from the press 18 to the digester temperature, in this example, 366 F. plus the heat losses of the system. Thus, steam requirements are held .to a minimum.
  • the spent liquor substanatially yat full digester Itemperature and pressure, is forwarded from :the spent liquor storage tank 2l through the conduit 22.
  • a valve 23 is provided in conduit 22 and the setting of said valve is controlled by .a metering device 24 in order to maintain the proper rate of ilow of the spent black liquor.
  • the black liquor then passes into an injector unit 26 where steam is fed thereinto and then the mixture is injected into and mixed with the chips' exiting from the press.
  • the steam not only serves to -inject the ⁇ spent liquor into the digester but also serves to 4heat the chips and the white liquor to the ⁇ digester temperature.
  • the mixture of the white liquor and the chips from the press, the spent liquor and the condensed steam determinees the internal :liquor ratio, that is, the liquor to wood ratio within Ithe digester. It is obvious that the internal liquor ratio is h-igher than the external ratio and may be set at any desired value by adding more or less spent liquor without yany substantial penalty to steam economy. The only effect of increases in .the internal liquor ratio will be to decrease the pulp capacity of the digester.
  • the digester i9 may take a variety of dierent forms.
  • the ⁇ digester includes a cylindrical tank 28 having an inlet opening 29 at the bottom thereof ⁇ and an outlet opening 30 at the top thereof.
  • the diameter and length of the digester are adjusted so that a suiiicient volume will be provided to insure the required tonnage of production at the liquor-to-wood ratio selected and the proper retention time for the cook.
  • a slowly rotating screw 31 is disposed within the digester and is driven by a suitable motor 32, preferably having a ⁇ suitable variable speed driving mechanism.
  • the angle of the helix and the speed of rotation of the screw are selected so that the vertical component just equals the upward bul-k flow rate of the ⁇ suspension of chips and liquor in the digester.
  • This llow rate is a function of the net area of the digester and the volume of the suspension per unit of time.
  • Some of the chips may contain sufficient entrained air to cause them to tend to float rapidly to the top of the digester. However, the settling rate of over half of the chips in the suspension will normally be greater than the bulk liow rate and they will tend to settle out of suspension toward-s the bottom ⁇ of the digester. Either phenomenon would adversely aiect the uniformity of the iinished pulp.
  • a relief line 33 ⁇ is provided at the top of the digester for ⁇ drawing olf air, noncondensible gases and volatile organic compounds su-ch as turpentine, etc.
  • the capacity of the digester system may be increased by using one or more ⁇ of these digester bodies in series. For example, if the digester is of such dimensions and the pitch and speed of the screw are so designed to provide one hundredtons of pulp per ⁇ day at a cooking time of thirtyfive minutes and an internal liquor ratio of ten to one, production may be doubled by using two digester bodies in series. The speed of the pump 17, and transfer screw in this .case must be doubled so that the total retention time of the chips in the two ⁇ digesters together will be equal to the total cooking time of thirty-live m-inutes.
  • the cooked pulp leaves through the exit opening 30 and passes through a conduit 34.
  • the conduit has a suitable flow sensing ldevice 35, such as a magnetic flow meter, a venturi meter or a similar instrument, for providing a signal, either electrical, mechanical or fluid pressure, proportional tol the flow through the conduit 34.
  • a second liquor transfer press 36 which is similar to the transfer press 1S previously described.
  • the decreasing annular space and ⁇ decreasing axial pitch of the screw squeeze out the excess spent liquor which passes through the perforations in the barrel. Since the pulp and spent liquor are still at the digester temperature and pressure, the expressed spent liquor is also at the digester temperature and pressure, and it flows into the strong spent liquor storage tank 21.
  • a liquid level controller 37 in the strong liquor tank 2l insures that all of the spent liquor entering the tank, in excess of that used yfor recirculation, will be drawn oit through the conduit 38 to the recovery system. Since the liquor sent to the recovery system is also at digester temperature and pressure, its heat content can be used effectively in the evaporators of the recovery system.
  • the squeezed pulp will leave the liquor transfer press 36 at a consistency determined by the design of the press, for example, ranging from about 20 to about 40 percent dry liber.
  • the pulp is then fed to a ⁇ dilution tank 39 where a suitable diluent, such as dilute black liquor yfrom the pulp washers, normally at a temperature of 4to 150 F. is flowed thereinto and is mixed therewith by an agitator 41.
  • a suitable diluent such as dilute black liquor yfrom the pulp washers, normally at a temperature of 4to 150 F.
  • the quantity of black liquor from the washing system can be Ivaried to ygive any desired linal pulp consistency, such as from 240%, for 4pumping purposes.
  • the equilibrium temperature within the dilution tank 39 is always kept below 212 F.
  • a suitable gas pressure source is connected -thereto by a conduit 42, said ⁇ conduit having a control valve 43 therein.
  • the gas pressure source may be either air or some other non-condensible gas and, as shown, is usually compressed air.
  • the rate of flow being determined by the pressure differential between the pressure in lthe digester and the pressure in the dilution tank 39.
  • the ilow meter 35 in the conduit 34 is made to control the .rate of flow of the pulp into the dilution tank 39.
  • the meter transmits a signal to the pressure control valve 43 and this, in turn, increases the gas pressure in the dilution tank. This increase in gas pressure decreases the rate of pulp ilow.
  • the flow meter transmits a reverse signal to the gas pressure control valve 43, thereby reducing the pressure in the dilution tank 39 to provide an increase in pulp flow.
  • the pressure Within the dilution tank 39 controls the flow of pulp thereinto and by properly coordinating the flow sensing device 35 and valve 43 it is possible to attain a substantially steady continuous flow of pulp into said tank while maintaining proper pressure within the digester.
  • a liquid level controller 44 maintains a constant level of pulp suspension in the dilution tank 39. This level may be located in la portion of reduced cross-section of the tank so that a minimum, still surface of the suspension will :be presented to the gas phase, insuring a minimum of gas solution into the hot pulp suspension.
  • the liquid level controller 44 is used to vary the speed of the final stock pump 46 if a positive displacement pump is used; -or it may 'be utilized to Vary the opening of the throttling valve for adjustable orifice.
  • the pump 46 transports the dilute pulp suspension through a consistency regulator 47, thence to the pulp washing system.
  • a iiow meter 48 may, i-f desired, be used after the consistency regulator to indicate and record the pulp flow. lFrom this pulp iiow rate and the consistency provided by the regulator it is possible to compute the Weight of dry pulp being produced during a unit of time. At the other end of the digester system, the combination of recorded weight of chips and the moisture content of the chips as determined from lan automatic chip sampling device make it possible to calculate the weight of dry chips -fed to the digester system per unit of time. From these data a true value of pulp yield and tonnage may be obtained continuously making it possible to adjust the digester controls as required to insure uniformity of yield and production.
  • the digester system can be adapted for use with any suitable cellulosic raw material, such as wood, bagasse, cotton or flax stalks, bamboo stalks and other annuals.
  • the digesting liquor may be alkaline -White liquor as used in the kraft process, caustic soda as used in the soda process, lbisulphite liquor with a soda, magnesium, ammonium or calcium base; sodium sulphite and carbonate as used in the neutral sulphite semichemical process, or any other suitable digestant.
  • the end product may be a fully cooked pulp, a high yield pulp, or a semichemical pulp requiring further mechanical subdivision.
  • the pulping reaction is obliged to start in the digester at the outside surface of the chip and progress in a radial direction toward the center of the chip.
  • a continuous digestion system including: a digester, said digester having an entrance opening adjacent the lower end thereof and an exit opening adjacent the upper end thereof; a ro-tatable screw within said digester forming continuously upward moving compartments controlling the movement of the -chips suspended inl liquor fed into said digester through said entrance opening upwardly at the same rate as the liquor to said exit opening; a feed mechanism for feeding chips of cellulosic material to said digester, said feeding mechanism including a mixing tank for receiving chips and mixing same with digestion liquor to iform a pumpa'ole slurry, a pump connected for withdrawing the slurry from said mixing tank and pressurizing same to a value in excess of the pressure within said digester, a -rst liquor transfer press connected for receiving the pressurized slurry from said pump, said -first press including means for expressing liquid from the slurry as same passes therethrough without substantially changing the pressure on said -chips so that the chips exiting from said press are at a high consistency and are acted upon by
  • a .continuous digester system for cooking cellulosic material comprising:
  • ya iirst liquor transfer press for receiving material from said pump and for squeezing out liquor therefrom without changing the pressure thereon;
  • control device for produoing'a signal proportional to the rate of ilow of material therethrough and means for feeding the material exiting 4from the top of the di-gester through said control device to produce a signal therefrom;
  • a second liquor transfer press for receiving the material from the control device to express the hot spent liquor therefrom;
  • a continuous digestion system including:
  • a feed mechanism for continuously feeding chips of cellulosic material to said digester, said feeding mechanism including a mixing tank for receiving chips and mixing same with 4digestion liquor to form a pumpable slurry;
  • a pump connected for withdrawing the slurry from said mixing tank and pressurizing same to a value in excess ofthe pressure within said digester
  • a iirst liquor transfer press connected for receiving the pressurized slurry from said pump, said rst press including means for expressing liquid ⁇ from the slurry as same passes therethrough without substantially changing the pressure on said chips so that .the chips exiting from said press are at a high consistency ⁇ and are acted upon by pressure in excess of that necessary to move same into the digester;
  • a discharge mechanism for continuously withdrawing pulp from said digester, said discharge mechanism including a conduit connected to the discharge end of said digester;
  • a second liquor transfer press connected to said conduit for receiving pulp flowing therethrough, s-aid second press including means ⁇ for expressing digestion liquor from the pulp las same passes therethrough so that the pulp exiting ⁇ from said second press is at a high consistency;
  • a high pressure storage tank for receiving expressed liquor
  • control means for controlling the pressure within said dilution tank
  • liquid llevel controller connected to said dilution tank for maintain-ing a substantially constant liquid level therein;
  • a continuous digestion system including:
  • a digester said digester having an entrance opening ladjacent the lower end thereof and an exit opening adjacent .the upper end thereof;
  • a feed mechanism for feeding chips of cellulosic material t-o said digester, said feeding mechanism including a mixing tank for receiving chips and mixing same with digestion liquor to form a pumpable slurry;
  • a pump connected for withdrawing the slurry from said mixing tank and pressurizing same to a value in excess of the pressure within said digester
  • a first liquor transfer press ⁇ connected for receiving the pressurized slurry from said pump, said rst press including means for expressing liquid ⁇ from the slurry as same passes therethrough without substa-ntially changing the pressure on said chips so that the chips exiting from said press are at a high consistency and are acted upon by pressure suicient to move same intothe digester;
  • a .discharge mechanism for continuously withdrawing pulp from said digester, said discharge mechanism including a conduit connected to the discharge end of said digester;
  • a second liquid transfer press connected to said conduit ⁇ for receiving pulp flowing therethrough, said second press including means for expressing digestion liquor from the pulp as same passes therethrough so that the pulp exiting from said second press is ⁇ at a high consistency;
  • I control means for controlling the pressure of the nonicondensable gas applied to said ⁇ dilution tank
  • liquid level controller connected to said dilution tank for maintaining a substantially constant liquid level therein;
  • Y and pump means for withdrawing diluted pulp from the dilution tank in such a manner as to cause ⁇ a smooth controllable llow of pulp and a release Iof the dilution tank pressure thereon.

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July 2, 1963 B. ARMSTRONG ETAL 3,096,234
CONTINUOUS DIGESTING SYSTEM Filed Oct. 29, 1958 mm Nm INVENTORS 5PZ/Cf ARMSTRONG [4f/L //W J. NOM/V NODO: OZ-PmmO-D 'BY wwwa/MQW A TTOE/VE VS 3,96,234 CNTINUUS DllGESTNG SYSTEM Bruce Armstrong and William J. Nolan, Gainesville, Fla.; said Armstrong assigner to said Nolan Filed Get. 29, 1953, Ser. No. 770,424 6 Claims. (Cl. 162-237) This invention relates to a continuous digester system for producing pulp and, more particularly, to a continuous digester system lhav-ing improved mechanisms for introducing the chips to Ithe digester and withdrawing the cooked pulp therefrom.
|In :the past, digester design has been controlled by the economics of chemical recovery. The liquor ratio, that is, the ratio of the weight of chemical solution to weight o-f dry wood has always been kept at a minimum, and, more specifically, `a liquor ratio of between 3.0:1 and 4.011 has in the past been used in order to minimize both the heat required to bring the `digester charge to cooking temperature and the heat required to evaporate the spent black liquor.
This low ratio of between 3.0:1 and 4.0:1 creates conditions which re-sult in poor quality and lack of uniformity in the pulp. First, with t-his low ratio, there is not quite enough liquor to cover the chips in the `digester. Since fresh liquor enters into the chips and reaction products leave the chips and return to the main body of liquor by diiusional processes, the availability of fresh,
chemical tothe chips will vary with the degree of packing of the chips in a digesten Many digesters are equipped with devices rfor effecting lcirculation of the liquor in `rder to improve the chip-liquor contact. However, in these cases channeling often occurs in the digester, supplying 4an excess of liquor at some points and a deficiency at others. This channeling of liquor also results in hot and cold spots and thus causes a lack of uniformity in the temperature of the digester charge.
The second serious fault inherent in low liquor ratios is the necessarily high concentration of digestion chemicals needed at the start of the cook in order to insure a sufficiently high 4concentration near the end of the cook to supply driving force for the digestion reaction. If the liquor ratio can be increased without economic penalty, the .initial concentration of digestion chemicals therein can be markedly reduced, the strength of the liquor near the end of the cook being just `as high as if -a high `chemical concentration, low liquor ratio cook were performed. It the digester can be designed to permit the use of high liquor ratios, any suitable low initial concentration may be used. This provides .a lchoice of various combinations of concentrations and temperatures not available with low liquor-wood ratios.
However, high liquor ratios are prohibited by economic considerations in both batch digesters `and in the continuous digesters presently available. If, for example, twice as much liquor is placed in the digester with the chips, twice as much steam is needed to heat the digester charge. Also, if twice as much spent liquor leaves the digester with the blown pulp, evaporator steam consumption Will double. Chemical losses will also increase because twice as much of the chemical must be handled in the recovery system. It can thus be seen that `a high external liquor ratio, that is, `a high ratio of liquor to wood entering the digester system, cannot now be tolerated because of cost. Therefore, :the advantages of uniformity of cooking and low initial concentration characteristic of high liquor ratios, cannot be utilized eilectively in the prior art batch and continuous digester systems.
Accordingly, it is aan object of this invention to proH vide `an improved digester system for continuously producing pulp of uniform, high quality from wood or other cellules-ic material.
'ice
It is |a further object of this invention to provide an improved digester system, as aforesaid, in which two distinct liquor ratios are used, one of which is a high ratio of liquor to wood inside the digester to provide a uni-form pulp while the other is a low ratio of liquor to wood outside the 4digester to insure operation economy.
It is a further object of this invention to provide an improved digester system, as aforesaid, in which the pulp is discharge from the d-igester without the use of a blow, that is, a reduction of digester pressure to atmospheric, which normally causes high heat loss due to the sudden ash of steam created thereby.
It is a further object of the invention to provide an improved digester system which utilizes either standard, commercially available equipment or equipment which may be .easily and inexpensively fabricated.
Other objects and yadvantages of this invention will become apparent to those acquainted wi-th systems of this type upon reading the following disclosure and inspecting the accompanying drawing, which is la schematic diagram of the system to which the invention relates.
The invention provides .a means of changing the liquor/wood ratio at each successive step so that each step in the process is performed at the most favorable consistency.
Thus the mixture of cooking liquor and Wood is pumped at approximately 4% consistency because pumps for this service perform best at this consistency. The mixture of liquor and chips requires steam to bring the mixture up to digester temperature. Four percent consistency is equivalent to 24 lbs. liquor per lb. of oven-dry wood. This would require an excessive amount of steam. Accordingly the No. 1 liquor transfer press removes liquor from the mixture until there remains only that liquor required to provide suicient chemical to react with and remove substantially all the lignin and leave a small residual of chemical to force the reaction right up to the end of the cook.
The chips are moved through the digester during which time the pulping reaction occurs. The cooked pulp exi-ting from the digester is fed through a How sensing device and then to a second press where some of the spent digestion liquor is expressed therefrom. Part of this spent liquor is returned and mixed with 4the chips entering the digester and `the balance is sent to the recovery system. The pulp `and spent liquor mixed therewith exiting from the press define the external liquor ratio which is la measure of the heat leaving the system and which, in any event, will be much less than the internal liquor ratio. This mixture of pulp and liquor exiting the press at digested temperature is fed into =a dilution tank where it is mixed with a siutable diluent and is then fed to the pulp washing system. This diluent is usually dilute black liquor from the washing system. Suitable pressures are maintained on the streams entering and leaving the digester so that the chips are continuously fed thereinto and cooked pulp is removed therefrom while a suitable digesting pressure is maintained within the digester.
With the mixture of cooking liquor entering at 4% consistency, the transfer is designed to have an output consistency ranging from 20% to 40% As there are 24 pounds of liquor per pound of ovendry wood at 4% consistency, and from 4 pounds to 1'1/2 pounds at 20 and 40% respectively, the transfer will remove from 20 pounds to 221/2 pounds of liquor per pound of wood.
Heating up only 21/2 to 5 pounds of mixture of wood and cooking liquor to digester temperature would constitute an `attractive steam `demand but presents 1a diiiicult material handling problem; and does not provide la sufficient volume of yliquor to effectively wet :all Kthe chips in tlrir passage through the system.
27.4-12.0=l5.4 grams Na20 at. the end of the oook tion of yapparatus fo-r carrying out the invention.
Accordingly, referring to the drawing spent black liquor from the second liquor transfer press 36, still substantially at digester temperature and pressure, is re- 5 cycled to the digester and added to the high consistency mixture to dilute it to the desired liquor ratio. This new liquor ratio may range from a low of 5 to 1 up to a high of to 1. The recycle black liquor may be introduced by means of an injector which not only provides the necessary energy to inject the liquor but also provides the heat necessary to bring the mixture of chips and cooking liquor up to digester temperature plus the heat losses in the system. The recycle black liquor and steam may be added directly to the digester or, preferably, mixed with the output of the liquor transfer press just prior to entering the digester.
.There is =a residual active chemical in the recycle black liquor which must -be taken into account. A concentration for the original cooking liquor is selected so that the mixture of wood, cooking liquor, steam and recycle black liquor will give the desired starting concentration for the liquor ratio selected and (at the end of the cook) will give the required minimum residual concentration.
Example No. 1:-Calculation of White Liquor and 25 Residual Liquor Concentrations Assume:
Then:
Per 100 grams of wood, oven-dry- 100 50%=50 grams wood dissolved 50 0.24=l2 grams NazO consumed At start yof cook, the moisture in the wood is trapped in the hollow lumens. Therefore, this moisture is not part of Ithe liquor at the start of the cook.
X35=27.4 grams Na2O at start of cook At the end of the cook, the moisture in the wood is part of the total liquor, and:
l-QX-llQ-Fosro um man liquor '150x O0 per 100 grams oven-dry wood 15.4 @TO-17.7 grams per liter 1n resldual liquor 55 After leaving No. 1 liquor transfer there will remain 100 ygrams oven-dry wood, 100 grams moisture and 200 grams white liquor. Similarly, on a 100 pound oven- `dry vwood basis, there will be 100 pounds moisture and 200 pounds White liquor. To heat this from 150 F. to 365 F. will require:
(B65-150)[100x1+100 0.34-|-200 0.94] :67,100 B.t.u. Y 67,100/857=78 lb. steam at 365 F. (150 pounds per square inch) per 100 lb. wood, or 78 grams er 100 grams wood To the 400 grams of wood, moisture and white liquor 4 200 grams of white liquor from No. 1 liquor transfer E 200/(1000 1 111)=0.180 liter 17.9/0.180=99.4 grams per liter required in the white liquor This is normally `available in the average white liquor coming from the recovery system. If this -concentration is higher than required, it is diluted with black liquor to the desired concentration. If the concentration from recovery is lower than required, a new internal liquor ratio is selected Iand the calculation repeated until a suitable set of conditions has been achieved.
Example N0. 2.-Calculati0n of Temperature in Dilution Tank Assume:
Liquor ratio of 3 to 1 from transfer No. 2 at 365 F. 4% consistency in 1dilution tank. 24 to l liquor ratio. 2li-3:21 pounds dilution liquor required at 150 F. Let x=equilibrium temperature of the mix-ture in dilution tank 0.34)| (30016.94) (265 x) =(x-)(2100x.94) x=177 F. (Using la speoilc heat of 0.34 for pulp and 0.94 specic heat of black liquor).
Referring to the drawing, the cellulosic material, which may be shredded chips prepared in accordance with the disclosures of application Serial No. 578,378, iled April 16, 1956, now abandoned, or `application Serial No. 369,740, tiled July 22, 1953, now U.S. Patent No.
2,904,460, is fed, usually after being weighed, onto aV conveyor 10. The chips are fed by the conveyor into a mixing tank 11 and yfresh digestion liquor, sometimes hereinafter referred to .as white liquor, is added thereto. The white liquor is ordinarily at the temperature at which it is pumped from the causticizing system, usually in a range of 150l80 F. The white liquor is pumped :by a pump 13, through a meter 14 Iand a valve 15, into the tank. The valve 15 is controlled by a liquid level control 16. Sullicient White liquor is added to the tank 11A so that the chips therein can be kept in uniform suspension by the agitator 12 and can be read-ily pumped. The quantity of white liquor may be varied to provide a consistency within the range of 2-10% and is not critical, since `all excess :over digester requirements is removed by the first liquor transfer press 18 and is returned to the mixing tank, No. 11.
The chip suspension discharged from the tank 11 passes through a pump 17 to the first liquor transfer press 18. In 'addition to moving the chips, la primary purpose of the pump 17 is to provide a hydrostatic pressure sullicient to equalize or slightly exceed the steam pressure in the -digester plus what ever friction is developed in the system. Many types of pumps may be used for this purpose, such as a high-head centrifugal, a multi-stage centrifugal or a progressive cavity pump.
The rst liquor transfer press 18 may be substantially the same as that shown in U.S. Patent No. 2,664,814 and consists yof Ia screw of decreasing pitch, said screw rotating in a perforated barrel. The annular area of the press decreases from the entrance lto the exit thereof. Thus, the chips 'are pressed together and the white liquor therein is expelled therefrom through the perforations in the barrel. It is possible to remove sufficient liquid such that the chips exiting from the press will be at a consistency of between 20 'and about 40 percent. The amount lof white liquor in contact with the chips as the chips leave the press determines the external liquor ratio and is so selected that it is sutiicient to insure completion of the desired pulping reaction. It should be pointed out that the press 18 does not operate against digester pressure. Rather, there is la hydrostatic pressure built up by the pump 17 equal to or slightly greater than the steam pressure in the digester i9. The excess liquor, expelled from the vbarrel of the liquor transfer press 18, flows through a throttle valve 4Ztl to prevent loss of pressure in the press and thence back to the mixing tank 11 whereupon it is mixed with fresh chips and is used to transport such chips from the tank ll through the pump 17 to the press 18.
The pressed chips, entering the digester 19, are mixed with spent liquor from the `discharge end of the digester. The spent liquor is substantially at full digester pressure, for example, at 150 pounds per square inch and 366 F. The chips and their accompanying white liquor, before mixing with the spent liquor, are at a temperature in the range of about 150 to 180 F. Since the spent liquor mixed at this point is substantially at digester temperature and pressure the only `steam required will be that amount necessary to heat the chips and white liquor from the press 18 to the digester temperature, in this example, 366 F. plus the heat losses of the system. Thus, steam requirements are held .to a minimum. The spent liquor, substanatially yat full digester Itemperature and pressure, is forwarded from :the spent liquor storage tank 2l through the conduit 22. A valve 23 is provided in conduit 22 and the setting of said valve is controlled by .a metering device 24 in order to maintain the proper rate of ilow of the spent black liquor. The black liquor then passes into an injector unit 26 where steam is fed thereinto and then the mixture is injected into and mixed with the chips' exiting from the press.
The steam not only serves to -inject the `spent liquor into the digester but also serves to 4heat the chips and the white liquor to the `digester temperature.
The mixture of the white liquor and the chips from the press, the spent liquor and the condensed steam :determines the internal :liquor ratio, that is, the liquor to wood ratio within Ithe digester. It is obvious that the internal liquor ratio is h-igher than the external ratio and may be set at any desired value by adding more or less spent liquor without yany substantial penalty to steam economy. The only effect of increases in .the internal liquor ratio will be to decrease the pulp capacity of the digester.
The digester i9 may take a variety of dierent forms. In the perferred form of the digester shown in the `drawing, the `digester includes a cylindrical tank 28 having an inlet opening 29 at the bottom thereof `and an outlet opening 30 at the top thereof. The diameter and length of the digester are adjusted so that a suiiicient volume will be provided to insure the required tonnage of production at the liquor-to-wood ratio selected and the proper retention time for the cook. A slowly rotating screw 31 is disposed within the digester and is driven by a suitable motor 32, preferably having a `suitable variable speed driving mechanism.
The angle of the helix and the speed of rotation of the screw are selected so that the vertical component just equals the upward bul-k flow rate of the `suspension of chips and liquor in the digester. This llow rate is a function of the net area of the digester and the volume of the suspension per unit of time.
Some of the chips may contain sufficient entrained air to cause them to tend to float rapidly to the top of the digester. However, the settling rate of over half of the chips in the suspension will normally be greater than the bulk liow rate and they will tend to settle out of suspension toward-s the bottom `of the digester. Either phenomenon would adversely aiect the uniformity of the iinished pulp.
As the suspension enters the bottom of the digester it is encompassed by a pair of upper and lower flights which may be considered as a continuously moving compartment. Any chips tending to iioat would be held back b-y the upper iiight and any chips tending to settle out of suspension would be lifted by the bottom llight and cause all the -chips to remain with the liquid with which they entered the digester until discharged at the top, thus assuring a uniform dwell time in the digester and preventing the admixture of one layer of suspension with an adjacent layer.
Assuming an entering liquor ratio of .10 pounds liquor to l pound oven-dry wood, and a yield of 50%, one halfV the wood will have reacted and been taken into solution in the liquor. The liquor ratio at the discharge end of the digester would then be fl/z pound wood to lul/2 parts liquor, or 21:1, equivalent to a pulp consistency at discharge of 4.55% which is suitable `for flowing through the :balance of the system.
A relief line 33 `is provided at the top of the digester for `drawing olf air, noncondensible gases and volatile organic compounds su-ch as turpentine, etc. The capacity of the digester system may be increased by using one or more `of these digester bodies in series. For example, if the digester is of such dimensions and the pitch and speed of the screw are so designed to provide one hundredtons of pulp per `day at a cooking time of thirtyfive minutes and an internal liquor ratio of ten to one, production may be doubled by using two digester bodies in series. The speed of the pump 17, and transfer screw in this .case must be doubled so that the total retention time of the chips in the two `digesters together will be equal to the total cooking time of thirty-live m-inutes.
The cooked pulp leaves through the exit opening 30 and passes through a conduit 34. The conduit has a suitable flow sensing ldevice 35, such as a magnetic flow meter, a venturi meter or a similar instrument, for providing a signal, either electrical, mechanical or fluid pressure, proportional tol the flow through the conduit 34. After passing through the meter 35, the pulp flows into a second liquor transfer press 36 which is similar to the transfer press 1S previously described. In this press, the decreasing annular space and `decreasing axial pitch of the screw squeeze out the excess spent liquor which passes through the perforations in the barrel. Since the pulp and spent liquor are still at the digester temperature and pressure, the expressed spent liquor is also at the digester temperature and pressure, and it flows into the strong spent liquor storage tank 21. The required amount of this spent liquor is returned to the digester 19 through the conduit 22 in the manner previously described to provide the proper internal liquor ratio as `discussed above. lt can be seen that any part of this spent liquor may be circulated back to the digester without the need of any heating other than that required to make up for heat losses.
A liquid level controller 37 in the strong liquor tank 2l insures that all of the spent liquor entering the tank, in excess of that used yfor recirculation, will be drawn oit through the conduit 38 to the recovery system. Since the liquor sent to the recovery system is also at digester temperature and pressure, its heat content can be used effectively in the evaporators of the recovery system.
Returning lnow to the pulp stream, the squeezed pulp will leave the liquor transfer press 36 at a consistency determined by the design of the press, for example, ranging from about 20 to about 40 percent dry liber. The pulp is then fed to a `dilution tank 39 where a suitable diluent, such as dilute black liquor yfrom the pulp washers, normally at a temperature of 4to 150 F. is flowed thereinto and is mixed therewith by an agitator 41. The quantity of black liquor from the washing system can be Ivaried to ygive any desired linal pulp consistency, such as from 240%, for 4pumping purposes. The equilibrium temperature within the dilution tank 39 is always kept below 212 F. and, thus, the liquor will not -llash into steam lbut will remain in the liquid phase in the dilution tank. In order to maintain pressure equilibrium in the system and to control the lflow of the pulp into the dilution tank, it is necessary that the dilution tank be pressurized. Accordingly, a suitable gas pressure source is connected -thereto by a conduit 42, said `conduit having a control valve 43 therein. The gas pressure source may be either air or some other non-condensible gas and, as shown, is usually compressed air. When the gas pressure within the `tank 39 is main- 'tained at the same pressure as the digester, no flow of pulp can occur. As the gas pressure is decreased outward ow from the digester to the dilution tank occurs, the rate of flow being determined by the pressure differential between the pressure in lthe digester and the pressure in the dilution tank 39. The ilow meter 35 in the conduit 34 is made to control the .rate of flow of the pulp into the dilution tank 39. Thus, las the iow meter senses an increase in tlow over the desired rate, the meter transmits a signal to the pressure control valve 43 and this, in turn, increases the gas pressure in the dilution tank. This increase in gas pressure decreases the rate of pulp ilow. Conversely, if pulp flow falls below the predetermined -desired rate, the flow meter transmits a reverse signal to the gas pressure control valve 43, thereby reducing the pressure in the dilution tank 39 to provide an increase in pulp flow. Thus the pressure Within the dilution tank 39 controls the flow of pulp thereinto and by properly coordinating the flow sensing device 35 and valve 43 it is possible to attain a substantially steady continuous flow of pulp into said tank while maintaining proper pressure within the digester.
A liquid level controller 44 maintains a constant level of pulp suspension in the dilution tank 39. This level may be located in la portion of reduced cross-section of the tank so that a minimum, still surface of the suspension will :be presented to the gas phase, insuring a minimum of gas solution into the hot pulp suspension. The liquid level controller 44 is used to vary the speed of the final stock pump 46 if a positive displacement pump is used; -or it may 'be utilized to Vary the opening of the throttling valve for adjustable orifice. The pump 46 transports the dilute pulp suspension through a consistency regulator 47, thence to the pulp washing system.
A iiow meter 48 may, i-f desired, be used after the consistency regulator to indicate and record the pulp flow. lFrom this pulp iiow rate and the consistency provided by the regulator it is possible to compute the Weight of dry pulp being produced during a unit of time. At the other end of the digester system, the combination of recorded weight of chips and the moisture content of the chips as determined from lan automatic chip sampling device make it possible to calculate the weight of dry chips -fed to the digester system per unit of time. From these data a true value of pulp yield and tonnage may be obtained continuously making it possible to adjust the digester controls as required to insure uniformity of yield and production.
it is apparent that the digester system can be adapted for use with any suitable cellulosic raw material, such as wood, bagasse, cotton or flax stalks, bamboo stalks and other annuals. The digesting liquor may be alkaline -White liquor as used in the kraft process, caustic soda as used in the soda process, lbisulphite liquor with a soda, magnesium, ammonium or calcium base; sodium sulphite and carbonate as used in the neutral sulphite semichemical process, or any other suitable digestant. Similarly, the end product may be a fully cooked pulp, a high yield pulp, or a semichemical pulp requiring further mechanical subdivision.
While the vertical upilow type of digester equipped with a vertical, rotatable, helical screw disclosed in the drawing, is the preferred type of digester for use in the system, it is apparent that the system can also Ibe -used to advantage with existing types of conventional stationary, vertical, downflow type digesters or continuous, horizontal tube digesters.
It has been found that subdivided chips prepared as disclosed in applications Serial Nos. 369,740, now U.S. Patent No. 2,904,460 and 578,378, tiled April 16, 1956, now abandoned, which have a large specific surface, require an increase in the liquor-to-wood ratio to properly Wet all the surface and insure an ample supply of chemical for each particle. By providing the digestion chemical at a high concentration and subsequently diluting this with recycled spent liquor as the chips enter the digester, a high liquor ratio can be achieved without substantially increasing the steam requirements as the recycled spent liquor is already at substantially dgester temperature. Since the prevailing temperature in the liquor-transfer press 18 is below 212 F., the conditions are unfavorable to either penetration of the digesting liquor into the structure of the chips or an active reaction between the digesting chemicals and the lignin in the wood. Consequently, the pulping 'reaction cannot start until the chips and liquor enter the digester and their temperature is rapidly raised therein. Therefore, the pulping reaction is obliged to start in the digester at the outside surface of the chip and progress in a radial direction toward the center of the chip.
While -a particular preferred embodiment of -the invention has been referred to hereinabove, the invention contemplates such modi'cations or changes therein as lie within the scope of the appended claims.
What is claimed is:
1. A system for continuously discharging pulp from a digester, including: a conduit connected to the discharge end of said digester; control means in said conduit responsive to the flow of pulp in said conduit for providing a signal proportional thereto; a liquor transfer press connected to said conduit for receiving pulp ilowing therethrough, said press including means for expressing digestion liquor, at digester temperature, from the pulp as same passes therethrough so that the expressed liquor can Ibe stored in a pressurized tank for reuse and the pulp exiting from said press is at a high consistency; a pressurized dilution tank connected for receiving pulp exiting from said press, said dilution tank being closed; means connected to said dilution tank for continuously supplying a non-condensible gas under pressure into said dilution tank to provide pressure on the pulp in said dilution tank and on the discharge end of said press, said last-named means being connected for responding to. a signal from said control means so that the pressure within said tank will be proportional to the ilow of pulp through said conduit; means for feeding a dilution liquid into said dilution tank `and mixing same with the pulp therein; a liquid level controller connected to said dilution tank for maintaining a substantially constant liquid level therein; and pump means for withdrawing diluted pulp from said dilution tank in such a manner as to cause a smooth controllable flow of pulp and a release of the dilution tank pressure thereon.
2. A continuous digestion system, including; a digester; a feed mechanism for continuously feeding chips of cellulosic material to said digester, said feeding mechanism including a mixing tank yfor receiving chips and mixing same with digestion liquor to form a pumpable slurry, a pump connected for withdrawing the slurry from said mixing tank and pressurizing same to a value in excess of the pressure within said digester, a Aiirst liquor transfer press connected for receiving the pressurized slurry from said pump, said yfirst press including means for expressing liquid from the slurry as same passes therethrough without substantially changing the pressure on said chips so that the chips exiting from said press are at a high consistency and are acted upon by a pressure rin excess of that necessary to move same into the digester; means for mixing steam and spent digestion liquor with the chips exiting from said first press while maintaining the pressure thereon so that the chips and liquor entering ysaid digester are at substantially the same pressure and temperature as the contents of said digester and are in a iluid condition; a discharge mechanism for continuously withdrawing pulp from said digester, said discharge mechanism including a conduit connected to the discharge end of said digester, control means in said conduit responsive to the ow of pulp therethrough for providing a signal proportional to such flow, a second liquor transfer press connected to said conduit for receiving pulp ilowing therethrough, said second press including means for expressing digestion liquor from the pulp as same passes therethrough so that the pulp ex- :iting from said second press is at a high consistency; a high pressure storage tank lfor receiving expressed liquor; a pressurized dilution tank connected for receiving pulp exiting from said second press, said dilution tank being closed and pressure tight, means connected to said dilution tank for continuously supplying a noncondensible gas under pressure into said dilution tank to provide pressure on the pulp in said dilution tank and on the discharge end of said second press, said lastnarned means being connected for responding to a signal from said control means so that the pressure within said dilution tank will be proportional to the ilow of pulp through said conduit, means for feeding a dilution liquid into said dilution tank and mixing same with the pulp therein, a liquid level controller connected to said dilution tank for maintaining a substantially constant liquid level therein; and pulp means for withdrawing diluted pulp from said dilution tank in such a manner as to cause a smooth controllable ilow of pulp and a release of the dilution tank pressure thereon.
3. A continuous digestion system, including: a digester, said digester having an entrance opening adjacent the lower end thereof and an exit opening adjacent the upper end thereof; a ro-tatable screw within said digester forming continuously upward moving compartments controlling the movement of the -chips suspended inl liquor fed into said digester through said entrance opening upwardly at the same rate as the liquor to said exit opening; a feed mechanism for feeding chips of cellulosic material to said digester, said feeding mechanism including a mixing tank for receiving chips and mixing same with digestion liquor to iform a pumpa'ole slurry, a pump connected for withdrawing the slurry from said mixing tank and pressurizing same to a value in excess of the pressure within said digester, a -rst liquor transfer press connected for receiving the pressurized slurry from said pump, said -first press including means for expressing liquid from the slurry as same passes therethrough without substantially changing the pressure on said -chips so that the chips exiting from said press are at a high consistency and are acted upon by a pressure suiiicient to move same into the digester, means for conducting the liquid expressed 'by said iirst press back to said mixing tank, means for mixing steam and spent `digestion liquor with the -chips exiting from said first press while maintaining the pressure thereon so that the chips entering said digester are at substantially the sarne pressure and temperature as the contents of said digester; a discharge mechanism for continuously w-ithdrawing pulp from said digester, said discharge mechanism including a conduit connected to the discharge end of said digester, contr-ol means in said conduit responsive to the flow of pulp therethrough for providing a signal proportional thereto, a second liquor transfer press connected to said conduit for receiving pulp ilowing therethrough, said second press including means for expressing `digestion liquor from the pulp as same passes therethrough so that the pulp exiting from said second press is at a high consistency, means for conducting the liquor expressed by said second press and injecting same with steam into the chips after they exit from said iirst press, a pressurized dilution tank connected for receiving pulp exiting from said second press, said dilution tank being closed and pressure tight, means connected to said dilution tank for continuously supplying a non-condensible gas under pressure into said dilution tank to provide pressure on the pulp in said dilution tank and on the ydischarge end of said second press, said last-named means being connected for responding to a signal from said control means so that the pressure Within said dilution tank will be proportional to the flow of pulp through said conduit, means for feeding a dilution liquor into said dilution tank and means 'for mixing same with the pulp in said dilution tank; a liquid level controller connected to said dilution tank for maintaining a substantially constant liquid level therein; and pump means for withdrawing diluted pulp yfrom said dilution tank in such a manner as to cause a smooth controllable ilow of pulp and a release of the dilution tank pressure thereon. t
4. A .continuous digester system for cooking cellulosic material comprising:
a mixing tank;
`a pump for feeding cellulosic material mixed with an excess lof digestion liquor from said tank at ya hydraulic pressure slightly greater than the pressure at lthe discharge end 4of the hereinafter-mentioned lirst press and greater than the steam pressure in the hereinafter-mentioned digester;
ya iirst liquor transfer press for receiving material from said pump and for squeezing out liquor therefrom without changing the pressure thereon;
means for conducting the liquor expressed by said rst press back to said mixing tank, the cellulosic material leaving the press with only sumcient liquor to supply slightly more chemicals lthan is required by the digestion reaction, means for mixing the material leaving `said first press with steam and sufoient hot recirculatted, spent liquor to provide `a lluid condition at a pressure slightly higher than that in the hereinafter-mentioned digester;
a vertical, cylindrical digester `and means for admitting sai-d material into the bottom thereof;
a screw in said digester for forwarding said material through said digester at such a speed that said material will not settle out of its liquor but will travel at the same speed as the liquor;
a control device for produoing'a signal proportional to the rate of ilow of material therethrough and means for feeding the material exiting 4from the top of the di-gester through said control device to produce a signal therefrom;
a second liquor transfer press for receiving the material from the control device to express the hot spent liquor therefrom;
a pressurized dilution tank for receiving the'pressed material from 'the second press 'and means for dilutingkand cooling the pressed material in the dilution tan g means to continuously supply =a non-condensable gas under pressure .to said dilution tank which in turn will provide a hydraulic pressure on the `diluted material and on the discharge end of the second liquor transfer press;
means for varying the pressure of said gas in said dilution tank in response to said control device to control the rate of flow of material through the system;
`a liquid level control device in said dilution tank tor maintaining a substantially constant liquid level in the dilution tank, means for withdrawing the material from the dilution tank to cause a smooth, controllable iiow of material therefrom and a release of the dilution tank pressure on said material.
5. A continuous digestion system, including:
a digester;
a feed mechanism for continuously feeding chips of cellulosic material to said digester, said feeding mechanism including a mixing tank for receiving chips and mixing same with 4digestion liquor to form a pumpable slurry;
a pump connected for withdrawing the slurry from said mixing tank and pressurizing same to a value in excess ofthe pressure within said digester;
a iirst liquor transfer press connected for receiving the pressurized slurry from said pump, said rst press including means for expressing liquid `from the slurry as same passes therethrough without substantially changing the pressure on said chips so that .the chips exiting from said press are at a high consistency `and are acted upon by pressure in excess of that necessary to move same into the digester;
means for mixing steam and spent digestion liquor with the chips exiting from said iirst press While maintaining the pressure thereon so -that the chips and liquor entering said digester are at substantially the same pressure and temperature as the contents as said digester and are in a fluid condition;
a discharge mechanism for continuously withdrawing pulp from said digester, said discharge mechanism including a conduit connected to the discharge end of said digester;
a second liquor transfer press connected to said conduit for receiving pulp flowing therethrough, s-aid second press including means `for expressing digestion liquor from the pulp las same passes therethrough so that the pulp exiting `from said second press is at a high consistency;
a high pressure storage tank for receiving expressed liquor;
-a pressurized dilution tank connected for receiving pulp exiting from said second press, said .dilution tank being cl-osed and pressure tight;
. means connected to said `dilution -tank for continuously supplying a noncondens-able gas under pressure into said dilution `tank to provide pressure on the pulp in said dilution tank and on the .discharge end of said second press;
control means for controlling the pressure within said dilution tank;
means for feeding a dilution liquid into said dilution tank and mixing same with the pulp therein;
a liquid llevel controller connected to said dilution tank for maintain-ing a substantially constant liquid level therein;
and pump means for withdrawing diluted pulp from said dilution tank in such a manner Ias to cause a smooth controllable flow of pulp and a release of dilution tank pressure thereon.
6. A continuous digestion system, including:
a digester, said digester having an entrance opening ladjacent the lower end thereof and an exit opening adjacent .the upper end thereof;
la rotatable screw Within 'said digester forming continuously upwardly moving compartments controlling the movement lof the chips suspended in liquor fed into said digester through said entrance opening and moving said chips upwardly at the same rate as the liquor to said exit opening;
a feed mechanism for feeding chips of cellulosic material t-o said digester, said feeding mechanism including a mixing tank for receiving chips and mixing same with digestion liquor to form a pumpable slurry;
a pump connected for withdrawing the slurry from said mixing tank and pressurizing same to a value in excess of the pressure within said digester;
a first liquor transfer press `connected for receiving the pressurized slurry from said pump, said rst press including means for expressing liquid `from the slurry as same passes therethrough without substa-ntially changing the pressure on said chips so that the chips exiting from said press are at a high consistency and are acted upon by pressure suicient to move same intothe digester;
means for conducting the liquid expressed by said first press back to said mixing tank;
means for mixing steam and `spent digestion liquor with Ithe chips exiting from -said rst press while maintaining the pressure thereon so that the chips entering said digester `are at substantially the same pressure land temperature as the contents of said digester;
a .discharge mechanism for continuously withdrawing pulp from said digester, said discharge mechanism including a conduit connected to the discharge end of said digester;
a second liquid transfer press connected to said conduit `for receiving pulp flowing therethrough, said second press including means for expressing digestion liquor from the pulp as same passes therethrough so that the pulp exiting from said second press is `at a high consistency;
means for conducting the liquor expressed by said second press and injecting same with steam into the `chips after they exit from said first press;
`a pressurized dilution tank connected for receiving pulp exiting from said second press, -said .dilution tank being closed and pressure tight;
means connected to said dilution tank 'for continuously supplying a noncondensable gas under pressure into said dilution tank to provide a pressure on the pulp in said dilution tank and on the discharge end of said second press;
I control means for controlling the pressure of the nonicondensable gas applied to said `dilution tank;
means for feeding a dilution liquor into said dilution tank and means for mixing same with the pulp in said dilution tank;
a liquid level controller connected to said dilution tank for maintaining a substantially constant liquid level therein;
Y and pump means for withdrawing diluted pulp from the dilution tank in such a manner as to cause `a smooth controllable llow of pulp and a release Iof the dilution tank pressure thereon.
References Cited in the le of this patent UNITED STATES PATENTS 1,954,012 Lemberger et al Apr. 10, 1934 1,982,130 Wollenberg Nov. 27, 1934 2,038,925 Dunbar Apr. 28, 1936 2,542,801 De La Roza Feb. 20, 1951 2,607,680 Weiss et al Aug. 19, 1952 2,673,690 Segl Mar. 30, 1954 2,858,213 Durant et al. Oct. 28, 1958 FOREIGN PATENTS 852,892 France Nov. 9, 1939

Claims (1)

1. A SYSTEM FOR CONTINUOUSLY DISCHARGING PULP FROM A DIGESTER, INCLUDING: A CONDUIT CONNECTED TO THE DISCHARGE END OF SAID DIGESTER, CONTROL MEANS IN SAID CONDUIT RESPONSIVE TO THE FLOW OF PULP IN SAID CONDUIT FOR PROVIDING A SIGNAL PROPORTIONAL THERETO; A LIQUOR TRANSFER PRESS CONNECTED TO SAID CONDUIT FOR RECEIVING PULP FLOWING THERETHROUGH, SAID PRESS INCLUDING MEANS FOR EXPRESSING DIGESTION LIQUOR, AT DIGESTER TEMPERATURTE, FROM THE PULP AS SAME PASSES THERETHROUGH SO THAT THE EXPRESSED LIQUOR CAN BE STORED IN A PRESSURIZED TANK FOR REUSE AND THEP PULP EXITING FROM SAID PRESS IS AT A HIGH CONSISTENCY; A PRESSURIZED DILUTION TANK CONNECTED FOR RECEIVING PULP EXITING FROM SAID PRESS, SAID DILUTION TANK BEING CLOSED; MEANS CONNECTED TO SAID DILUTION TANK FOR CONTINUOUSLY SUPPLYING A NON-CONDENSIBLE GAS UNDER PRESSURE INTO SAID DILUTION TANK TO PROVIDE PRESSURE ON THE PULP IN SAID DILUTION TANK AND ON THE DISCHARGE END OF SAID PRESS, SAID LAST-NAMED MEANS BEING CONNECTED FOR RESPONDING TO A SIGNAL FROM SAID CONTROL MEANS SO THAT THE PRESSURE WITHIN SAID TANK WILL BE PROPORTIONAL TO THE FLOW OF PULP THROUGH SAID CONDUIT; MEANS FOR FEEDING A DILUTION LIQUID INTO SAID DILUTION TANK AND MIXING SAME WITH THE PULP THEREIN; A LIQUID LEVEL CONTROLLER CONNECTED TO SAID DILUTION TANK FOR MAINTAINIG A SUBSTANTIALLY CONSTANT LIQUID LEVEL THEREIN; AND PUMP MEANS FOR WITHDRAWING DILUTED PULP FROM SAID DILUTION TANK IN SUCH A MANNER AS TO CAUSE A SMOOTH CONTROLLABLE FLOW OF PULP AND A RELEASE OF THE DILUTION TANK PRESSURE THEREON.
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DE1267076B (en) 1968-04-25
FI40851B (en) 1969-02-28

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