US3078685A - Method of charging carbon dioxide cylinders - Google Patents

Method of charging carbon dioxide cylinders Download PDF

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US3078685A
US3078685A US112060A US11206061A US3078685A US 3078685 A US3078685 A US 3078685A US 112060 A US112060 A US 112060A US 11206061 A US11206061 A US 11206061A US 3078685 A US3078685 A US 3078685A
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carbon dioxide
charging
cylinder
cylinders
particles
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John H Flournoy
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SOUTH LAB Inc
SOUTH LABORATORIES Inc
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    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17—STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17C—VESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C5/00—Methods or apparatus for filling containers with liquefied, solidified, or compressed gases under pressures

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  • the present invention relates to a method of charging small carbon dioxide cylinders having narrow necks by employing finely ground solid carbon dioxide. More broadly, the invention entails a unique method of conveying solid carbon dioxide.
  • a further object of the invention is to provide a carbon dioxide cylinder charging technique wherein the transfer of a carbon dioxide charge to a cylinder interior may be accomplished without refrigeration or high pressure equipment and wherein the charged cylinder may be sealed under atmospheric pressure.
  • An additional and highly significant object of the present invention is to provide a new and improved method of conveying carbon dioxide in solid form which is of particular value in effecting the entry of solid carbon dioxide into narrow necked receptacles.
  • a final object of the present invention is to provide a method of charging O0 cylinders whereby light and in-' expensive equipment may be employed.
  • a carbon dioxide cylinder charging technique wherein finely ground particles of solid carbon dioxide are passed through a relatively restricted passage to a cylinder to be charged. During movement of the particles through the passage, the particles are agitated while a vacuum is concurrently applied to the discharge end of the passage to both assist in the movement of the particles and to effect withdrawal of sublimed gas formed in the charging member or in the cylinder being charged. The charged cylinder is then sealed in the presence of atmospheric pressure.
  • each charge of solid carbon dioxide particles is measured and'individually placed within the charging member to effect charging of a cylinder, it is anticipated that a continuous supply of particles may be conveyed to the charging member.
  • FIG. 1 is a partially sectioned side elevational view of the apparatus.
  • FIG. 2 is a sectioned view of a portion of a cylinder which is to be charged by the method of the present invention.
  • the apparatus employed in carrying out the present invention comprises a stationary base member 1 and a pair of vertically disposed resilient brackets 2 which are adapted to support a charge receiving receptacle, i.e., hopper 3.
  • Hopper 3 is positioned above the base member and terminates in a relatively restricted outlet or passage 3a.
  • a conventional electro-mechanical vibrating device 4 is affixed to one of the resilient brackets to impart horizontal vibratory motion to the bracket and the bracket supported hopper 3.
  • a vertically disposed hollow charging member 5 is employed to form an elongated continuation of passage 3a.
  • Charging member 5 is adapted to be secured within an axial bore of a coupling member 6 by any suitable means such as welding or a press lit at a connecting point 7. Obviously this member could alternatively be made integral with the hopper 3 or the coupling 6.
  • the upwardly extending portion of the coupling 6 is adapted to be received in threaded engagement with a downwardly extending sleeve member 8 afiixed to the bottom of the hopper.
  • the cylindrical, narrow necked portion 9 of a cylinder to be charged is adapted to be slideably and sealingly received in engagement with the inner tubular wall 11 of a downwardly opening recess 12 in the bore of the coupling 6.
  • annular enlargement or chamber 13 communicating with a laterally extending opening 14. Opening 14, as illustrated, is threadedly adapted to receive a tube 15 connected to a conventional source of vacuum, not shown.
  • the narrow necked portion 9 of the cylinder is internally threaded at 16 to receive a closure member in the form of a threaded cap 17.
  • Cap 17, at its upper surface, has a frangible seal portion 18.
  • Sealing means in the form of a resilient O-ring 19 may be provided to etfect a hermetic seal between the cap 17 and the cylinder necked portion 9.
  • the diameter of the hollow charging member 5 is sufficiently small to permit the member to be received within the narrow necked portion 9 of the cylinder 10 so as to leave an annular space therebetween communicating the interior of the cylinder with the chamber 13. With the charging member thus positioned, it is insured that the ground carbon dioxide will enter the cylinder 10 and not be drawn into the vacuum hose 15.
  • the narrow necked portion of the cylinder to be charged is manually held or mechanically secured as by a friction fit within the recess 12 of the coupling 6.
  • a measured charge of finely ground particles of solid carbon dioxide is placed within the charge receiving hopper 3.
  • the vibrating device 4 is energized and vacuum is applied to the discharge end of the hollow charging member 5 and the interior of the cylinder 10 through the passage defined by the tubing 15, the annular chamber 13, and the annular space between the charging member 5 and threaded necked portion 16 of the cylinder.
  • the combined actions of vibrating the charging member by means of vibrator 4 and subjecting the discharge end of the charging member to vacuum greatly facilitates the passage of carbon dioxide particles through the hopper passage and charging member and prevents bridging or blocking of these areas. Additionally, the imposed vacuum acts to withdraw from the cylinder and charging member any sublimed carbon dioxide gas contained therein which would tend to impede the particle fiow.
  • the cylinder is removed from the charging apparatus and sealed in the presence of atmospheric pressure.
  • the vacuum and vibration filling technique enables the conveying of solid carbon dioxide in a powdered or finely ground form through passages or conduits of a highly constricted character. It has been found, for example, that the vibration and vacuum filling method may be successfully employed in filling small cylinders of the type used with inflatable life vests or belts which have neck openings onthe order of /8 inch in diameter.
  • the method in question may be accomplished without the cumbersome and expensive equipment previously associated with carbon dioxide charging operations.
  • the equipment required is structurally simple, easy tooperate, and easy to maintain.
  • the charging member of the apparatus although disclosed as a separate elongate tube, might well be an integral portion of the charge receiving receptacle. While the illustrated member is elongate in character to prevent the passage of solid carbon dioxide into the vacuum creating line, it is apparent that thecharge hopper may be arranged such that its discharge passage or outlet communicates directly with the vacuumized interior of cylinders to be charged.
  • the transfer of finely ground carbon dioxide to a charging unit may be mechanized such that a continuous flow of charging material is provided.
  • a measured charge transfer may be accomplished by timing the period of engagement of cylinders with the unit.
  • vibrators may be utilized to impart a multi-direction vibration to the charge receiving receptacles and attached cylinder or direct mechanical agitators may be located within the mass of charged material.
  • a method of charging a receptacle comprising the passing of a charge offinely ground particles of solid carbon dioxide into said receptacle through a restricted passage while concurrently agitating said particles and exposing said passage to vacuum to assist in the movement of said particles and to concurrently withdraw sub- .limed carbon dioxide gas.
  • a method of charging a narrow necked CO cylinder comprising the steps of passing a charge of finely ground particles of solid carbon dioxide into said cylinder through a hollow charging member while concurrently agitating said particles and exposing the discharge end of said charging member to vacuum to assist in the movement of said particules and to concurrently withdraw sublimed carbon dioxide gas, and subsequently sealing said cylinder.
  • a method of charging a narrow necked CO cylinder comprising the steps of placing a measured charge of finely ground particles of solid carbon dioxide within a charge receiving receptacle, transferring said charge into said cylinder from said receptacle member while concurrently agitating said particles and exposing the interior of .:said cylinder to vacuum to assist in the movement of said -partlcies and to concurrently withdraw sublimed carbon dioxide gas, and subsequently sealing said cylinder.
  • a method of charging a narrow necked CO cylinder comprising the steps of placing a measured charge of finelyground particles of solid carbon dioxide within a charge receiving receptacle, transferring said charge into said cylinder from said receptacle while concurrently vibrating said receptacle and said cylinder and exposing the'interior of said cylinder to vacuum to assist in the movement of said particles and to concurrently withdraw sublimed carbon dioxide gas, and subsequently sealing said cylinder in the presence of atmospheric pressure.
  • a method of conveying solid carbon dioxide through i a conduit comprising the steps of introducing small par- 'eles of solid carbon dioxide into said conduit, and vibrating said conduit and exposing said particles to vacuum to assist in the movement or" said particles through said conduit and to concurrently withdraw sublimed carbon dioxide gas from said conduit.

Description

Feb. 26, 1963 J. H. FLOURNOY METHOD OF CHARGING CARBON DIOXIDE CYLINDERS Filed May 23, 1961 INVENTOR John H. F/oumay I I'll ATTORNEYS United States Patent Ofiice 3,078,685 Patented Feb. 26, 1963 3,078,685 METHOD OF CHARGING CARBON DIOXIDE CYLINDERS John H. Flournoy, Huntington, W. Va., assignor to South Laboratories, Inc., Huntington, W. Va., a corporation of West Virginia Filed May 23, 1961, Ser. 'No. 112,060 Claims. (Cl. 62-47) The present invention relates to a method of charging small carbon dioxide cylinders having narrow necks by employing finely ground solid carbon dioxide. More broadly, the invention entails a unique method of conveying solid carbon dioxide.
It has heretofore been the practice to charge narrow necked carbon dioxide receptacles or cylinders by introducing liquefied carbon dioxide into such cylinders and then hermetically sealing the cylinders while maintaining the liquefied carbon dioxide under pressure. An obvious disadvantage of practicing this prior art method resides in the need for complex and expensive pressure maintaining equipment to handle the liquefied carbon dioxide. While the pressure equipment requirement can be somewhat reduced by refrigerating the liquefied carbon dioxide, the refrigeration operation itself imposes substantial equipment demands. During the charging and sealing of charged cylinders, complex pumping and charging apparatus is required. In addition, it has been found to be difficult to control the exact amount of liquid placed within cylinders being charged.
Recognizing the distinct need for a less cumbersome technique for charging carbon dioxide cylinders, it is an object of this invention to present a charging method which may be eifected without the complex liquid carbon dioxide handling apparatus previously employed.
It is a particular object of the invention to provide a cylinder charging method wherein carbon dioxide is employed in a conveniently manipulatable solid form during the charging operation.
A further object of the invention is to provide a carbon dioxide cylinder charging technique wherein the transfer of a carbon dioxide charge to a cylinder interior may be accomplished without refrigeration or high pressure equipment and wherein the charged cylinder may be sealed under atmospheric pressure.
An additional and highly significant object of the present invention is to provide a new and improved method of conveying carbon dioxide in solid form which is of particular value in effecting the entry of solid carbon dioxide into narrow necked receptacles.
A final object of the present invention is to provide a method of charging O0 cylinders whereby light and in-' expensive equipment may be employed.
To accomplish the foregoing objects there is contemplated a carbon dioxide cylinder charging technique wherein finely ground particles of solid carbon dioxide are passed through a relatively restricted passage to a cylinder to be charged. During movement of the particles through the passage, the particles are agitated while a vacuum is concurrently applied to the discharge end of the passage to both assist in the movement of the particles and to effect withdrawal of sublimed gas formed in the charging member or in the cylinder being charged. The charged cylinder is then sealed in the presence of atmospheric pressure.
While in a preferred form of the invention, each charge of solid carbon dioxide particles is measured and'individually placed within the charging member to effect charging of a cylinder, it is anticipated that a continuous supply of particles may be conveyed to the charging member.
In describing the invention reference will be made to an exemplary apparatus illustrated in the accompanying drawings wherein:
FIG. 1 is a partially sectioned side elevational view of the apparatus; and
FIG. 2 is a sectioned view of a portion of a cylinder which is to be charged by the method of the present invention.
The apparatus employed in carrying out the present invention comprises a stationary base member 1 and a pair of vertically disposed resilient brackets 2 which are adapted to support a charge receiving receptacle, i.e., hopper 3. Hopper 3 is positioned above the base member and terminates in a relatively restricted outlet or passage 3a. A conventional electro-mechanical vibrating device 4, the purpose of which is hereinafter described, is affixed to one of the resilient brackets to impart horizontal vibratory motion to the bracket and the bracket supported hopper 3.
A vertically disposed hollow charging member 5 is employed to form an elongated continuation of passage 3a. Charging member 5 is adapted to be secured within an axial bore of a coupling member 6 by any suitable means such as welding or a press lit at a connecting point 7. Obviously this member could alternatively be made integral with the hopper 3 or the coupling 6. To position the charging member 5 in axial alignment with a downwardly opening hole 3a in the bottom of the material receiving hopper 3, the upwardly extending portion of the coupling 6 is adapted to be received in threaded engagement with a downwardly extending sleeve member 8 afiixed to the bottom of the hopper.
The cylindrical, narrow necked portion 9 of a cylinder to be charged is adapted to be slideably and sealingly received in engagement with the inner tubular wall 11 of a downwardly opening recess 12 in the bore of the coupling 6.
Intermediate of the length of the coupling bore there is provided an annular enlargement or chamber 13 communicating with a laterally extending opening 14. Opening 14, as illustrated, is threadedly adapted to receive a tube 15 connected to a conventional source of vacuum, not shown.
As shown in FIGURE 2 the narrow necked portion 9 of the cylinder is internally threaded at 16 to receive a closure member in the form of a threaded cap 17. Cap 17, at its upper surface, has a frangible seal portion 18. Sealing means in the form of a resilient O-ring 19 may be provided to etfect a hermetic seal between the cap 17 and the cylinder necked portion 9. I 1
From FIGURE 1 it will be noted that the diameter of the hollow charging member 5 is sufficiently small to permit the member to be received within the narrow necked portion 9 of the cylinder 10 so as to leave an annular space therebetween communicating the interior of the cylinder with the chamber 13. With the charging member thus positioned, it is insured that the ground carbon dioxide will enter the cylinder 10 and not be drawn into the vacuum hose 15.
In practicing the present invention, the narrow necked portion of the cylinder to be charged is manually held or mechanically secured as by a friction fit within the recess 12 of the coupling 6. A measured charge of finely ground particles of solid carbon dioxide is placed within the charge receiving hopper 3. Either concurrently with the charging or immediately thereafter, the vibrating device 4 is energized and vacuum is applied to the discharge end of the hollow charging member 5 and the interior of the cylinder 10 through the passage defined by the tubing 15, the annular chamber 13, and the annular space between the charging member 5 and threaded necked portion 16 of the cylinder. The combined actions of vibrating the charging member by means of vibrator 4 and subjecting the discharge end of the charging member to vacuum greatly facilitates the passage of carbon dioxide particles through the hopper passage and charging member and prevents bridging or blocking of these areas. Additionally, the imposed vacuum acts to withdraw from the cylinder and charging member any sublimed carbon dioxide gas contained therein which would tend to impede the particle fiow. Upon completion of the charging step the cylinder is removed from the charging apparatus and sealed in the presence of atmospheric pressure.
In describing the operation of a preferred apparatus which may be utilized in charging narrow necked carbon. dioxide cylinders, the several advantages inherent in the method of this invention have been demonstrated. The use of powdered carbon dioxide as opposed to liquid carbon dioxide permits the charging operation to be con-- ducted at room temperature and with charging receptacles exposed to atmospheric pressure. Likewise, charged cylinders may be sealed under atmospheric pressure at the:
completion of the charging operation without any appreciable loss of carbon dioxide content.
The vacuum and vibration filling technique enables the conveying of solid carbon dioxide in a powdered or finely ground form through passages or conduits of a highly constricted character. it has been found, for example, that the vibration and vacuum filling method may be successfully employed in filling small cylinders of the type used with inflatable life vests or belts which have neck openings onthe order of /8 inch in diameter.
Of particular significance, it is to be noted that the method in question may be accomplished without the cumbersome and expensive equipment previously associated with carbon dioxide charging operations. The equipment required is structurally simple, easy tooperate, and easy to maintain.
While the invention has been described in relation to the operation of a particular apparatus, it is apparent that its scope is not limited to the use of this particular equipment. The charging member of the apparatus, although disclosed as a separate elongate tube, might well be an integral portion of the charge receiving receptacle. While the illustrated member is elongate in character to prevent the passage of solid carbon dioxide into the vacuum creating line, it is apparent that thecharge hopper may be arranged such that its discharge passage or outlet communicates directly with the vacuumized interior of cylinders to be charged.
Where desired, the transfer of finely ground carbon dioxide to a charging unit may be mechanized such that a continuous flow of charging material is provided. With such an arrangement, a measured charge transfer may be accomplished by timing the period of engagement of cylinders with the unit.
It is likewise evident that a variety of structures and techniques may be employed in securing cylinders in communication with charging units. In this connection, a variety of sealing arrangements may be employed between cylinders and the units.
In lieu of the electro-mechanical device described for agitation of the powdered carbon dioxide, other transducers or mechanical agitators may be employed. For
4 example, vibrators may be utilized to impart a multi-direction vibration to the charge receiving receptacles and attached cylinder or direct mechanical agitators may be located within the mass of charged material.
Other modifications of the invention will readily occur to those skilled in the art, the scope of which is defined in the appended claims.
I claim:
1 A method of charging a receptacle comprising the passing of a charge offinely ground particles of solid carbon dioxide into said receptacle through a restricted passage while concurrently agitating said particles and exposing said passage to vacuum to assist in the movement of said particles and to concurrently withdraw sub- .limed carbon dioxide gas.
2. A method of charging a narrow necked CO cylinder comprising the steps of passing a charge of finely ground particles of solid carbon dioxide into said cylinder through a hollow charging member while concurrently agitating said particles and exposing the discharge end of said charging member to vacuum to assist in the movement of said particules and to concurrently withdraw sublimed carbon dioxide gas, and subsequently sealing said cylinder.
3. A method of charging a narrow necked CO cylinder comprising the steps of placing a measured charge of finely ground particles of solid carbon dioxide within a charge receiving receptacle, transferring said charge into said cylinder from said receptacle member while concurrently agitating said particles and exposing the interior of .:said cylinder to vacuum to assist in the movement of said -partlcies and to concurrently withdraw sublimed carbon dioxide gas, and subsequently sealing said cylinder.
4. A method of charging a narrow necked CO cylinder comprising the steps of placing a measured charge of finelyground particles of solid carbon dioxide within a charge receiving receptacle, transferring said charge into said cylinder from said receptacle While concurrently vibrating said receptacle and said cylinder and exposing the'interior of said cylinder to vacuum to assist in the movement of said particles and to concurrently withdraw sublimed carbon dioxide gas, and subsequently sealing said cylinder in the presence of atmospheric pressure.
5. A method of conveying solid carbon dioxide through i a conduit comprising the steps of introducing small par- 'eles of solid carbon dioxide into said conduit, and vibrating said conduit and exposing said particles to vacuum to assist in the movement or" said particles through said conduit and to concurrently withdraw sublimed carbon dioxide gas from said conduit.
References Cited in the file of this patent UNITED STATES PATENTS 1,546,682 Slate July 21, 1925 1,967,294 Deming July 24, 1934 2,l06,492 Adams Ian. 25, 1938 2,570,074 Rupp Oct. 2, 1951 2,779,510 Wilson et al Jan. 29, 1957

Claims (1)

1. A METHOD OF CHARGING A RECEPTACLE COMPRISING THE PASSING OF A CHARGE OF FINELY GROUND PARTICLES OF SOLID CARBON DIOXIDE INTO SAID RECEPTACLE THROUGH A RESTRICTED PASSAGE WHILE CONCURRENTLY AGITATING SAID PARTICLES AND
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Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3875980A (en) * 1973-05-14 1975-04-08 Melvin R Getz Extinguisher charging system
US4240472A (en) * 1972-03-07 1980-12-23 Srinivas Srivas R Apparatus for cleaning and coating capillary tubes useful in gas chromatography
US4967814A (en) * 1988-09-19 1990-11-06 Westvaco Corporation Apparatus for filling high pressure gas storage bottles with powdered activated carbon
US6003547A (en) * 1997-08-04 1999-12-21 Tippmann Pneumatics, Inc. Valve and filling arrangement
US6065509A (en) * 1995-07-26 2000-05-23 Glaxo Wellcome Inc. Method and apparatus for filling cavities
WO2000070263A1 (en) * 1999-05-13 2000-11-23 Alexei Borisovich Shipachev Gas cylinder and method for filling the same
US20060011653A1 (en) * 2002-10-31 2006-01-19 Ivan-William Fontaine Apparatus for accurate powder metering
US20070102058A1 (en) * 2003-08-06 2007-05-10 Houzego Peter J Method and apparatus for filling a container
US20080190513A1 (en) * 2007-02-13 2008-08-14 Mettler-Toledo Ag Dosage-dispensing device with a tapping mechanism
US20170137154A1 (en) * 2015-11-15 2017-05-18 Xerox Corporation Single dose screening for particulate materials

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1546682A (en) * 1924-01-10 1925-07-21 Thomas B Slate Method and apparatus for producing carbon-dioxide snow and for separating same from the gas
US1967294A (en) * 1932-03-22 1934-07-24 Air Reduction Gas generator
US2106492A (en) * 1936-02-26 1938-01-25 Charles F Adams Vacuum and pressure filling apparatus for fluid, plastic, or various other materials
US2570074A (en) * 1949-06-30 1951-10-02 Standard Oil Dev Co Dry ice manufacture
US2779510A (en) * 1954-09-27 1957-01-29 Union Carbide & Carbon Corp Vibrational dispenser for forming solid gas mixtures

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1546682A (en) * 1924-01-10 1925-07-21 Thomas B Slate Method and apparatus for producing carbon-dioxide snow and for separating same from the gas
US1967294A (en) * 1932-03-22 1934-07-24 Air Reduction Gas generator
US2106492A (en) * 1936-02-26 1938-01-25 Charles F Adams Vacuum and pressure filling apparatus for fluid, plastic, or various other materials
US2570074A (en) * 1949-06-30 1951-10-02 Standard Oil Dev Co Dry ice manufacture
US2779510A (en) * 1954-09-27 1957-01-29 Union Carbide & Carbon Corp Vibrational dispenser for forming solid gas mixtures

Cited By (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4240472A (en) * 1972-03-07 1980-12-23 Srinivas Srivas R Apparatus for cleaning and coating capillary tubes useful in gas chromatography
US3875980A (en) * 1973-05-14 1975-04-08 Melvin R Getz Extinguisher charging system
US4967814A (en) * 1988-09-19 1990-11-06 Westvaco Corporation Apparatus for filling high pressure gas storage bottles with powdered activated carbon
US6065509A (en) * 1995-07-26 2000-05-23 Glaxo Wellcome Inc. Method and apparatus for filling cavities
US6003547A (en) * 1997-08-04 1999-12-21 Tippmann Pneumatics, Inc. Valve and filling arrangement
US6378570B1 (en) 1999-05-13 2002-04-30 Aleksei Borisovich Shipachev Gas cylinder and a method for filling the same
WO2000070263A1 (en) * 1999-05-13 2000-11-23 Alexei Borisovich Shipachev Gas cylinder and method for filling the same
US20060011653A1 (en) * 2002-10-31 2006-01-19 Ivan-William Fontaine Apparatus for accurate powder metering
US7284574B2 (en) * 2002-10-31 2007-10-23 Mettler-Toledo Flexilab Sas Apparatus for accurate powder metering
US20070102058A1 (en) * 2003-08-06 2007-05-10 Houzego Peter J Method and apparatus for filling a container
US8201590B2 (en) * 2003-08-06 2012-06-19 Pfizer, Limited Method and apparatus for filling a container
US20080190513A1 (en) * 2007-02-13 2008-08-14 Mettler-Toledo Ag Dosage-dispensing device with a tapping mechanism
US8191587B2 (en) * 2007-02-13 2012-06-05 Mettler-Toledo Ag Dosage-dispensing device with a tapping mechanism
US20170137154A1 (en) * 2015-11-15 2017-05-18 Xerox Corporation Single dose screening for particulate materials
US10029810B2 (en) * 2015-11-15 2018-07-24 Xerox Corporation Single dose screening for particulate materials

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