US2968837A - Super-high pressure apparatus - Google Patents

Super-high pressure apparatus Download PDF

Info

Publication number
US2968837A
US2968837A US804546A US80454659A US2968837A US 2968837 A US2968837 A US 2968837A US 804546 A US804546 A US 804546A US 80454659 A US80454659 A US 80454659A US 2968837 A US2968837 A US 2968837A
Authority
US
United States
Prior art keywords
crossheads
crosshead
frame
units
pressure generating
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
US804546A
Inventor
Zeitlin Alexander
Herman Harry
Brayman Jacob
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
ENGINEERING SUPERVISION Co
ENGINEERING SUPERVISION COMPAN
Original Assignee
ENGINEERING SUPERVISION COMPAN
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by ENGINEERING SUPERVISION COMPAN filed Critical ENGINEERING SUPERVISION COMPAN
Priority to US804546A priority Critical patent/US2968837A/en
Application granted granted Critical
Publication of US2968837A publication Critical patent/US2968837A/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Images

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J3/00Processes of utilising sub-atmospheric or super-atmospheric pressure to effect chemical or physical change of matter; Apparatus therefor
    • B01J3/06Processes using ultra-high pressure, e.g. for the formation of diamonds; Apparatus therefor, e.g. moulds or dies
    • B01J3/065Presses for the formation of diamonds or boronitrides
    • B01J3/067Presses using a plurality of pressing members working in different directions
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B30PRESSES
    • B30BPRESSES IN GENERAL
    • B30B11/00Presses specially adapted for forming shaped articles from material in particulate or plastic state, e.g. briquetting presses, tabletting presses
    • B30B11/004Presses specially adapted for forming shaped articles from material in particulate or plastic state, e.g. briquetting presses, tabletting presses involving the use of very high pressures
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B30PRESSES
    • B30BPRESSES IN GENERAL
    • B30B11/00Presses specially adapted for forming shaped articles from material in particulate or plastic state, e.g. briquetting presses, tabletting presses
    • B30B11/007Presses specially adapted for forming shaped articles from material in particulate or plastic state, e.g. briquetting presses, tabletting presses using a plurality of pressing members working in different directions

Definitions

  • This invention relates to apparatus for producing superhigh pressures, including pressures as great as 100,000 atmospheres or more. More particularly, this invention relates to mounting means for the pressure generating units in such apparatus and to improved pressure generating units.
  • Another object of the invention is to provide super-high pressure apparatus wherein undesired moments of force will not be communicated from one part to another of the mounting frame for the ram units.
  • Another object of the invention is to provide super-high pressure apparatus wherein reactive forces operably exerted by ram units on a mounting frame will tend to bring into better alignment the center lines of action of the ram units.
  • Another object of the invention is to provide improved pressure generating units for super-high pressure appa ratus.
  • a further object of the invention is to provide superhigh pressure apparatus having a mounting frame which permits convenient access to the interior of the apparatus, and which is characterized by case of disassembly, transportation in disassembled state, and reassembly.
  • the invention may be embodied in apparatus having a plurality of pressure generating units disposed at various angles about a central position and adapted to exert on an object at such position a plurality of pressure producing forces.
  • the pressure generating units may operate by hydraulic, pneumatic, mechanical or other action, and may be cylinder and piston ram units or of other form.
  • the pressure generating units may be provided with means for adjusting the angular alignment between the front ends and rear ends thereof, and, in the event that such units are fluid operated, they may embody certain features of construction which will minimize leakage.
  • the invention may be applied in instances where the center lines of action of all pressure generating units lie in a common plane. More frequently, however, in superhigh pressure work, the center lines of action of the pressure generating units will be disposed in three dimensions about the object. In that case, the center lines of action may be considered as approximating or corresponding to perpendiculars from the centers of the faces of a polyhedron which enclosesthe ram units and the object to be compressed, such perpendiculars ideally intersecting at a common central point.
  • This polyhedron may be a regular polyhedron as say, a tetrahedron, cube or octahedron (all of which have faces which, on each polyhedron, are regular polygons all of the same size and shape), or the polyhedron may be of an irregular configuration in one or more dimensions. If the polyhedron is irregular, the forces exerted by the pressure generating units on the object to be compressed are usually not all equal, but are adjusted relative to each other to satisfy the equations of static equilibrium that the net sum of all forces on the object be zero in all three dimensions and that the net sum of all moments of force on the object be zero in all three dimensions.
  • a plurality of crossheads which mount the pressure generating units to project inwardly from such crossheads toward the central object to be compressed.
  • Each crosshead is disposed in relation to the associated ram unit to have the major extent of the crosshead transverse to the center line of action of such unit and to have such line of action intersect the crosshead at a central point in the major extent thereof.
  • the crossheads are each marginally connected to abutting crossheads to form a frame which encloses and supports the pressure generating units.
  • each pressure generating unit By mounting each pressure generating unit on a crosshead having the described disposition in relation to the center line of action of the unit, and, further, by connecting the so disposed crossheads together to form a trame, as hereinafter described, the stresses developed by the reactive forces of the pressure generating units may be controlled and their tendency to deform the frame and misalign the pressure units may be substantially reduced.
  • the crossheads may, preferably, be connected with each other by hinges, such hinges comprising a hinge pin which connects ad acent crossheads by passing through a series of interspersed clevises projecting from the crossheads. Assemoly and disassembly of the frame is thereby greatly facilitated, and there are operational advantages which are hereinafter explained.
  • Fig. l is an isometric view of an embodiment of the invention wherein the configuration of the embodiment corresponds to a regular six-sided polyhedron, Le, a cube;
  • Fig. 2 is a plan view of the embodiment of Fig. 1 taken partly in cross section in a horizontal plane passing through the vertical center of the Fig. 1 embodiment;
  • Figs. 3 and 4 are schematic explanatory diagrams of forces and moments which are operative in the Fig. l embodiment
  • Fig. 5 is an isometric view of an embodiment according to the present invention wherein the embodiment corresponds in configuration to a regular tetrahedron, and;
  • Fig. 6 is a view in cross section of a preferred form of binge pin.
  • the reference numeral 10 designates (Fig. 2) a sample of material, workpiece or other object which is to be subjected to superhigh pressure.
  • the object 10 is encased in a solid block 11 of pyrophillite in the shape of a cube.
  • the elements 10 and 11 are not shown in Fig. 1.
  • Corresponding to the six faces of the pyrophillite cube 11 are six pressure generating units 12-17 (Fig. 1) which,
  • ram units 12-17 take the form of hydraulically actuated, cylinder and piston ram units. All of the ram units 12-17 are comprised of substantially identical parts. Therefore, only the ram unit 12 will be described in detail.
  • the front end of ram unit 12 comprises a cylindrical anvil 20 which has a rear face 21, and which is characterized by a slight inward conical taper 22 for a distance forward of the rear face.
  • This slight conical taper gives way at the front end of the anvil to a sharp inward taper 23 which is produced by chamfering the front end of the anvil at 90 intervals around its circumference in such manner that, in the chamfered region, the anvil will have a square cross section of diminishing size as the front face 24 of the anvil is approached.
  • This front face 24 is of square configuration and of slightly smaller size than the registering square face of the pyrophillite cube 11.
  • the sides of its front face 24 will be parallel to the sides of the corresponding square of the pyrophillite cube 11, the center of the front face 24 of the anvil will coincide with the center of the corresponding face of cube 11 when the anvil and the cube are in contact, and the center line of action of the pressure exerted by the anvil on the cube will pass through those coincident centers perpendicularly to the plane of contact between anvil and cube.
  • the rear face 21 of the anvil 20 is seated against the forwardly disposed, circular face of a radially projecting, forward flange portion 30 of a stand 31 having a conically tapered center portion 33 and a radially projecting, rear flange portion 34.
  • the anvil 20 is locked to the stand 31 by a collar 32 which, at its front end, grips the conical taper 22 of the anvil 20, and which, at its rear end, threadedly engages the periphery of the flange portion 30 of the stand. By rotating collar 32 in the appropriate direction, the anvil 20 may be uncoupled from the stand 31 or may be brought into tight fitting relation therewith.
  • the circular rear face of the rear flange portion 34 of stand 31 is seated against the forwardmost of two axially aligned cylindrical shoes 35 and 36.
  • The'rearmost shoe 36 is seated in turn against the cylindrical end face 37 of a hydraulic piston 38.
  • Each of the shoes 35 and 36 has a slight diametral taper. Therefore, by relatively rotating the shoes 35 and 36, it is possible to make slight angular adjustment between the central axis of the piston 38 and the center line of action of the assembly comprised of stand 31 and anvil 20.
  • the stand 31, shoes 35, 36 and piston 38 are clamped together by a sleeve 39 having an inwardly projecting annular lip 40 which fits over and engages the rear flange 34 of the stand 31.
  • the sleeve 39 is secured to the front end of the piston 38 by screws 41 which are distributed at angular intervals around the sleeve, and which axially extend through apertures (not shown) in the sleeve to be received in threaded holes (not shown) in the piston.
  • the hydraulic piston 38 comprises a larger diameter forward portion 45, a smaller diameter rearward portion 46, and a bearing ring 47 which is an integral part of the piston, and which is of greater diameter than either the forward portion 45, or the rearward portion 46.
  • the piston 38 ' is received within a cylinder 48 formed in a cylinder block 49 of circular cross section.
  • the forward portion 45 of the piston is encircled by an annular packing ring 50 disposed in an annular recess 51 which radially enlarges the forward end of the cylinder, and which provides an annular shoulder 52 at right angles to the cylinder axis. The p-acking.
  • ring-50 is'forced against the shoulder 52 by a gland 53 having a sleeve portion 54 which is inserted into recess 51 to bear against the packing ring.
  • the gland 53 also has a radially projecting, annular flange 54a seated against the forward surface of cylinder block 49.
  • the gland is secured to the cylinder block 44 by screws (not shown) passing through flange 54a to be received in threaded holes in the cylinder block.
  • the rearward portion 46 of the piston 38 is encircled by a bushing 55 and by an annular packing ring 56 which is interposed between the bushing and the bearing ring 47.
  • a circular plate 57 is disposed to the rear of piston portion 46, and is secured thereto by axially extending screws (not shown). The periphery of plate 57 axially registers with the bushing 55. Accordingly, when the screws which attach plate 57 to piston portion 46 are turned to draw the plate towards the piston portion, the plate 57 will press against the bushing 55 to thereby squeeze the packing ring 56 between the bushing and the bearing ring 47. As will be evident, the plate 57, bushing 55 and packing ring 56 will travel with the piston 38.
  • the rear end of the cylinder 48 is characterized by a circular hub 60 which extends axially into the cylinder, and which is of smaller radius than the cylinder.
  • An expandible diaphragm 61 of Buna rubber or the like is stretched over the front of the hub with the margins of the diaphragm being folded back over the axially extending, peripheral surface of the hub to lie flat against such peripheral surface. The diaphragm 61 is clamped in.
  • annular ring 62 which is inserted into the annular space between the hub and the cylinder wall, and which is thereafter drawn towards the rear end of the cylinder by the turning of screws (not shown) which pass axially through the ring 62 to be received in threaded apertures (not shown) in the cylinder block 49.
  • the drawing of the ring, as described, towards the rear end of the cylinder will cause the periphery of the diaphragm 61 to be tightly clamped between the hub 60 and the ring 62 to thereby form a fluid tight space between the diaphragm and the hub.
  • hydraulic fluid under pressure is inrodued into the space between the front end surface of the hub 60 and the expandible diaphragm 61 by a conduit 70 passing through the cylinder block 49 and hub 60.
  • the presence of the diaphragm precludes the leakage of hydraulic fluid which would otherwise occur if the high pressure fluid were permitted to flow freely into contact with the rear end of piston and thereby be subject to extrusion out of the ram unit through the clearance space between the piston and the cy'inder.
  • the diaphragm 61 expands to displace forwardly the piston 38, and to thereby cause the piston to exert pressure through, the anvil 20 on the pyrophillite block 11 and on the object 16 encased thereby.
  • the piston 38 is returned to its normal rearward position by injecting air into the space between bearing ring 47 and stationary packing ring 50 by way of a conduit 71 which runs diagonally from the front surface of cylinder block 49 to the said space.
  • the entire ram unit 12 is supported in place by having the cylinder block 49 received within a cylindrical well 74 formed in the reinforced central portion of a crosshead 82.
  • the cylinder block 49 has at its forward end a radially projecting flange portion 75' which is received within an annular recess 76a radially enlarging the front end of well 74 and providing an an nular shoulder 76 against which the flange 75 bears.
  • the cylinder block 49 is secured to crosshead 82 by screws (not shown) which pass throughrpertures (not shown) in flange 74 to be received in threaded holes in the cylinder block. If desired, the cylinder block 49 and the crosshead 82 may beformed. from one unitary.
  • the central reinforced portion of the crosshead 82 has formed therein a cylindrical bore 77 which is concentric with but of smaller radial size than the cylindrical well 74.
  • each crosshead is disposed to have its major extent lie transverse to the center line of action of the associated ram unit, and to have such line of action pass approximately or, preferably, exactly through the geometric center of the major extent of the crosshead.
  • each crosshead has margins which are each parallel to and adjacent to a margin of an adjacent crosshead, and the crossheads are each marginally connected to adjacent crossheads to form a polyhedral frame enclosing the ram units and supporting the ram units in substantially predetermined spaced position relative to each other.
  • the frame is completely self-supporting and high pressures are not exerted against any bad or other foundation support.
  • the frame may also be constructed with a minimum number of major or heavy components.
  • the ram units are balanced in pairs and directly oppose each other. Such arrangement facilitates an optimum alignment and balance of forces on the central object and reduces the angular moments which during operation tend to deform the frame and cause misalignment of the pressure generating units.
  • each of the crossheads 82-87 lie in the surfaces of a cube and each of the crossheads might, if desired, be of square configuration, in which case the frame would he cubical in form. In practice, however, it is preferable to cut away the corners of each crosshead to shape each such crosshead in the form of a cross and produce a frame with a configuration substantially like that shown in Fig. 1.
  • the cruciform configuration of the crossheads 82-87 provides openings for convenient access to the interior of the apparatus and also reduces the overall weight of the frame, while retaining the required mechanical strength.
  • Such a frame is produced by having the crossheads connected through joints which offer relatively low resistance to angular movement between adjacent crossheads and permit self-alignment of the frame under the stresses deveoped in operation.
  • hinges may be employed to connect each crosshead to its contiguous crossheads. As shown in Fig.
  • the hinges may be comprised of a set of clevises 89, 90, 91 projecting from the left-hand margin of crosshead 85 and interleaved with a second set of clevises 92, 93, 94 projecting from the right-hand margin of crosshead 82 to provide a continuous central bore through both sets of clevises and a hinge pin 95 which passes through such central bore, to join the crossheads 82 and 85.
  • Similar hinges may be employed, as shown in Fig. 1, to connect each crosshead with each of the four other crossheads which are adjacent thereto.
  • the frame formed of the crossheads may be easily disassembled and reassembled by the simple procedure of driving the hinge pins out of and back into the bores provided by the interleaved sets of clevises. No turning or other manipulation of connecting elements is required.
  • the hinge pin 95 may be constructed to be expandible by using as a pin the combination (Fig. 6) of an outer cylindrical collet 99 having: a conically tapered bore 99a and an inner mandrel 100 fitted into bore 99a at one end of the collet, and having a conical taper matching that of the bore.
  • the collet is split at one end by one or more axially running slots 9% extending from one end of the collet.
  • the collet may be substan.ia.ly uniformly expanded in diameter by driving the mandrel into the bore of the collet, and play between the hinge pin and the clevises may thereby be eliminated.
  • a tension or compression forceacting thereon from one of the connected crossheads will be distributed among the clevises on that crosshead, to be divided into separate smaller stresses which are aliquot fractions of the tension or compression force, and which act in shear against a corresponding number of cross sections of the hinge pin.
  • the total holding strength of the hinge is thus equal to the sum of the holding strengths of the individual cross sections thereof which are subjected to shearing stress.
  • a total holding strength is thereby provided which is several times greater than the holding strength which would be provided if an equal cross sectional area of the pin or other connector were subjected to a stress acting in tension.
  • the hinge pin and clevis arrangement thereby provides the required holding strength with the minimum of bulk and weight. Also, disassembly and reassembly of the frame is facilitated.
  • Figs. 3 and 4 illustrate some of the forces and moments acting in the Fig. 1 embodiment and show schematically some principal elements involved in the production of such moments and forces, namely crossheads 82-85, connectors 95-98 for joining the crossheads together into a frame, ram units 12 and 15, and the central cubic block 11 of pyrophillite.
  • the point x marks the center of cubic block 11, the rams 12 and 15 act upon the block 11 with forces represented by the arrows P and the same ram units 12 and 15 simultaneously react upon their respective crossheads 83 and with forces represented by the arrows F
  • the dotted line a-a through the center point x is the line with which the center lines of action of the rams 12 and 15 will coincide when such ram units are aligned to act with maximum elficiency upon the block 11.
  • Fig. 3 represents (with much exaggeration) a situation in which the frame is not quite true so that the crossheads as, 84 are not, as desired, exactly at right angles to the crossheads 83, 85, but, instead, are inclined at an angle to the last named crossheads.
  • the center line of action of each of ram units 12 and 15 is a line which forwardly passes through the center of the square face of block 11 which is presented thereto, and which rearwardly passes through the center point of the associated crosshead, it will be seen from Fig. 3 that the rams 12 and 15 will act upon the block 11 with respective forces F which do not pass through the center point x, and are not in alignment with each other.
  • the rams 12 and 15 will exert on crossheads 83, 85 reactive forces F which are not at right angles to the crossheads. Because of this lack of right angle relation, the force F on'the crosshead 83 will have a component f in line with the lie of crosshead 83 and directed away from the crosshead 82. Also, the force F, on crosshead 85 will have a component f in line with the crosshead 85 and directed towards crosshead 82. These two components f will act as a moment of force. If the connector elements 95-98 are of such character as to rigidly connect together the crossheads 82-85, the mentioned moment of force will be communicated to both of crossheads 82 and 84, and will set up substantial stresses thereon. Such stresses might be so great as to cause intolerable deformation or mechanical failure of the frame.
  • Fig. 5 there is shown another embodiment in which the frame is in the form of a tetrahedron.
  • the pyrophillite block (not shown) is in the form of a tetrahedron, and the four triangular faces of the tetrahedral block are acted upon by four ram units 161-104 whose center lines of action pass through the said four faces at right angles thereto and through the centers thereof to intersect at a common point marking the center of the pyrophillite block.
  • the front faces of the anvils of the ram units are in the shape of equilateral triangles of smaller size than the registering equilateral triangular faces of the tetrahedral pyrophillite block.
  • the mountings for the four ram units 1014M are provided by four crosshead plates -108.
  • Each crosshead plate is disposed to have the plane of its major extent perpendicular to the center line of action of the associated ram unit, and to have such line of action pass through the center of the crosshead.
  • each crosshead is connected to every other crosshead by a plurality of hinge means disposed at the margins of the crossheads. The crossheads 105-108 are thus joined in swingable relation to form an articulated tetrahedral frame.
  • the crossheads HTS-1% are not of the triangular configuration which would conform to the corresponding triangular faces of a perfect geometric tetrahedron.
  • the configuration of the crossheads is that of the triangular faces of a geometric tetrahedron when such triangular faces have been modified by having the vertex portions thereof cut away.
  • Such crossheads permit convenient access through the frame to the interior of the apparatus, and permit a reduction in weight while maintaining the required mechanical strength.
  • the Fig. 5 embodiment is similar to the embodiment shown in Figs. 1 and 2.
  • the frame may also be in the form of an octahedron.
  • example eight of the quasi-triangular crossheads shown in Fig. 5 may be joined into an octahedral frame in which each crosshead centrally supports one of eight ram units.
  • the front faces of the anvils would be in the shape of equilateral triangles and would press on a central pyrophillite block formed in the shape of a regular octahedron.
  • Such octahedral disposition of the ram units would be similar to the cubic disposition shown in Fig. 1 in that the ram units would be balanced in pairs.
  • the octahedral disposition like the cubic disposition, permits a greater volume of material in the pyrophillite block than could be provided in the tetra hedral arrangement shown in Fig. 5.
  • apparatus having a plurality of pressure generating units adapted to exert pressures on a centrally located object, a polyhedral arrangement of crossheads, each crosshead supporting one of said pressure generating units, said crossheads forming an articulated selfaligning polyhedral frame supporting said pressure generating units in mutually spaced relation.
  • Apparatus for applying high pressure to an object comprising a plurality of pressure generating units and crossheads, each pressure generating unit being centrally mounted on one of said crossheads to project inwardly toward said object and each crosshead being connected through movable joints with adjacent crossheads to form an articulated frame enclosing and supporting said pressure generating units.
  • each crosshead being disposed in relation to its associated pressure generating unit to have the major extent of the crosshead lie transverse to the center line of action of the unit and to have such line of action intersect the crosshead at a central location in the major extent thereof, and each crosshead haying margins which are each contiguous to a margin of an adjacent crosshead, the said crosshead being each connected with adjacent crossheads at such contiguous margins to form a frame enclosing said pressure generating units and supporting said units in mutually spaced relation.
  • apparatus having a plurality of pressure generating units disposed about a centrally located object and adapted to exert on said object a plurality of pressure producing forces
  • the combination therewith comprising, a plurality of crossheads each mounting one of said units to project inwardly from such crosshead towards said object, each crosshead being disposed in relation to its associated pressure generating unit to have the major extent of the crosshead lie transverse to the center line of action of the unit and to have such line of action intersect the crosshead at a central location in the major extent thereof, the said crossheads being each yieldably connected through joints with adjacent crossheads to form an articulated frame supporting said pressure generating units in mutually spaced relation.
  • crossheads are connected by hinges each comprised of a set of clevises extending outward from one of two adjacent crossheads interleaved with a set of clevises extending outward from the other of said two crossheads to form a central bore through both sets of clevises, and a hinge pin traversing said central bore and connecting in swingable relation said two sets of clevises.
  • said hinge pin is a combination comprising, an outer cylindrical member which is split at one end and which has a conically tapered bore extending axially into said pin from said one end and diminishing in diameter with progress away from said end, and an inner cylindrical member having a conically tapered portion which matches the taper of said bore and which is received therein, the said inner member being adapted to selectively adjust the effective diameter of said outer member by adjustment in axial position of said inner member relative to said outer member.
  • Apparatus for applying high pressure at a central region thereof to a test body comprised of an object to be compressed and a casing therefor of pressure-transmitting material comprising, a plurality of at least three units of which each is operative to generate pressure on said object, and of which each is comprised at least of an anvil having a smaller front face than rear face, the anvils of said units being disposed with their front faces towards and rear faces away from said region and being distributed about said region to enclose it in at least two dimensions excepting for gaps left between each anvil and the ones adjacent thereto to permit movement of said anvils relative to and towards the center of said region, and a plurality of crossheads of which each has a central portion backing a respective one of said units, and of which each crosshead is connected with adjacent crossheads to form a frame enclosing and supporting said pressure generating units.
  • Apparatus for applying high pressure at a central region thereof to a test body comprised of an object to be compressed and a casing therefor of pressure-transmitting material comprising, a plurality of at least three units of which each is operative to generate pressure on said object, and of which each is comprised at least of an anvil having a smaller front face than rear face, the anvils of said units being disposed with their front faces towards and rear faces away from said region and being distributed about said region to enclose it in at least two dimensions excepting for gaps left between each anvil and the ones adjacent thereto to permit movement of said anvils relative to and towards the center of said region, and a plurality of crossheads of which each has a central portion backing a respective one of said units, and of which each crosshead is connected through movable joints with adjacent crossheads to form an articulated frame enclosing and supporting said pressure generating units.

Landscapes

  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Press Drives And Press Lines (AREA)

Description

Jan. 24, 1961 A. ZElTLlN ETAL SUPER-HIGH PRESSURE APPARATUS Filed A ril 6, 1959 s Sheets-Sheei 1 m lmu N wZ N M ERR EE DH IA HY R ER LA AH N A m A R B B O C A J BY 8 'Knm,
THEIR ATTORNEYS Jan. 24, 1961 A. ZElTLlN ETAL 2,968,837
SUPER-HIGH PRESSURE APPARATUS Filed April 6, 1959 3 Sheets-Sheet 2 F|G.4. A I lni x i Fa R INVENTORS M akzwazmzi JACOB BRAYMAN BY 85 98 @MWQK-|*JM W THEIR ATTORNEYS Jan. 24, 1961 A. ZElTL lN ETl'AL SUPER-HIGH PRESSURE APPARATUS 5 Sheets-Sheet 3 Filed April 6, 1959 FIG.
INVENTORS m; E m m A O n .N A T l N A T E A M A Z M Y m Rmm AI 5% N Y T A B X R O mum A H J SUPER-HIGH PRESSURE APPARATUS Alexander Zeitlin, White Plains, N.Y., Harry Herman, Glen Rock, N.J., and Jacob Brayman, Staten Island,
N.Y., assignors to Engineering Supervision Company,
This invention relates to apparatus for producing superhigh pressures, including pressures as great as 100,000 atmospheres or more. More particularly, this invention relates to mounting means for the pressure generating units in such apparatus and to improved pressure generating units.
In the operation of such apparatus, very large reactive forces are produced by the pressure generating units, and, heretofore, such reactive forces have tended to deform the apparatus, resulting in breakdown or misalignment of the pressure generating units and deterioration in overall performance. Eccentric loads have often been present, and it has been a common occurrence for the pressure generating units to buckle or break.
It is an object of the invention disclosed herein to provide apparatus for producing super-high pressure wherein the reactive forces exerted by the ram units on the mounting frame will not set up stresses and moments to deform the frame and misalign the ram units.
Another object of the invention is to provide super-high pressure apparatus wherein undesired moments of force will not be communicated from one part to another of the mounting frame for the ram units.
Another object of the invention is to provide super-high pressure apparatus wherein reactive forces operably exerted by ram units on a mounting frame will tend to bring into better alignment the center lines of action of the ram units.
Another object of the invention is to provide improved pressure generating units for super-high pressure appa ratus.
A further object of the invention is to provide superhigh pressure apparatus having a mounting frame which permits convenient access to the interior of the apparatus, and which is characterized by case of disassembly, transportation in disassembled state, and reassembly.
The invention may be embodied in apparatus having a plurality of pressure generating units disposed at various angles about a central position and adapted to exert on an object at such position a plurality of pressure producing forces. The pressure generating units may operate by hydraulic, pneumatic, mechanical or other action, and may be cylinder and piston ram units or of other form. As hereinafter disclosed, the pressure generating units may be provided with means for adjusting the angular alignment between the front ends and rear ends thereof, and, in the event that such units are fluid operated, they may embody certain features of construction which will minimize leakage.
The invention may be applied in instances where the center lines of action of all pressure generating units lie in a common plane. More frequently, however, in superhigh pressure work, the center lines of action of the pressure generating units will be disposed in three dimensions about the object. In that case, the center lines of action may be considered as approximating or corresponding to perpendiculars from the centers of the faces of a polyhedron which enclosesthe ram units and the object to be compressed, such perpendiculars ideally intersecting at a common central point. This polyhedron may be a regular polyhedron as say, a tetrahedron, cube or octahedron (all of which have faces which, on each polyhedron, are regular polygons all of the same size and shape), or the polyhedron may be of an irregular configuration in one or more dimensions. If the polyhedron is irregular, the forces exerted by the pressure generating units on the object to be compressed are usually not all equal, but are adjusted relative to each other to satisfy the equations of static equilibrium that the net sum of all forces on the object be zero in all three dimensions and that the net sum of all moments of force on the object be zero in all three dimensions.
In accordance with the invention, there is provided a plurality of crossheads which mount the pressure generating units to project inwardly from such crossheads toward the central object to be compressed. Each crosshead is disposed in relation to the associated ram unit to have the major extent of the crosshead transverse to the center line of action of such unit and to have such line of action intersect the crosshead at a central point in the major extent thereof. The crossheads are each marginally connected to abutting crossheads to form a frame which encloses and supports the pressure generating units. By mounting each pressure generating unit on a crosshead having the described disposition in relation to the center line of action of the unit, and, further, by connecting the so disposed crossheads together to form a trame, as hereinafter described, the stresses developed by the reactive forces of the pressure generating units may be controlled and their tendency to deform the frame and misalign the pressure units may be substantially reduced.
The crossheads may, preferably, be connected with each other by hinges, such hinges comprising a hinge pin which connects ad acent crossheads by passing through a series of interspersed clevises projecting from the crossheads. Assemoly and disassembly of the frame is thereby greatly facilitated, and there are operational advantages which are hereinafter explained.
We have discovered that a cubic configuration for super-high pressure apparatus provides advantages not provided by the tetrahedral configuration. Accordingly, the invention will hereinafter be described primarily in terms of apparatus having such cubic configuration.
For a better understanding of the invention, reference is made to the following description of exemplary embodiments thereof, and to the accompanying drawings wherein:
Fig. l is an isometric view of an embodiment of the invention wherein the configuration of the embodiment corresponds to a regular six-sided polyhedron, Le, a cube;
Fig. 2 is a plan view of the embodiment of Fig. 1 taken partly in cross section in a horizontal plane passing through the vertical center of the Fig. 1 embodiment;
Figs. 3 and 4 are schematic explanatory diagrams of forces and moments which are operative in the Fig. l embodiment;
Fig. 5 is an isometric view of an embodiment according to the present invention wherein the embodiment corresponds in configuration to a regular tetrahedron, and;
Fig. 6 is a view in cross section of a preferred form of binge pin.
Referring now to Figs. 1 and 2, the reference numeral 10 designates (Fig. 2) a sample of material, workpiece or other object which is to be subjected to superhigh pressure. The object 10 is encased in a solid block 11 of pyrophillite in the shape of a cube. For convenience, the elements 10 and 11 are not shown in Fig. 1. Corresponding to the six faces of the pyrophillite cube 11 are six pressure generating units 12-17 (Fig. 1) which,
in the present instance, take the form of hydraulically actuated, cylinder and piston ram units. All of the ram units 12-17 are comprised of substantially identical parts. Therefore, only the ram unit 12 will be described in detail.
As shown in Fig. 2, the front end of ram unit 12 comprises a cylindrical anvil 20 which has a rear face 21, and which is characterized by a slight inward conical taper 22 for a distance forward of the rear face. This slight conical taper gives way at the front end of the anvil to a sharp inward taper 23 which is produced by chamfering the front end of the anvil at 90 intervals around its circumference in such manner that, in the chamfered region, the anvil will have a square cross section of diminishing size as the front face 24 of the anvil is approached. This front face 24 is of square configuration and of slightly smaller size than the registering square face of the pyrophillite cube 11. When anvil 20 is in proper alignment, the sides of its front face 24 will be parallel to the sides of the corresponding square of the pyrophillite cube 11, the center of the front face 24 of the anvil will coincide with the center of the corresponding face of cube 11 when the anvil and the cube are in contact, and the center line of action of the pressure exerted by the anvil on the cube will pass through those coincident centers perpendicularly to the plane of contact between anvil and cube.
The rear face 21 of the anvil 20 is seated against the forwardly disposed, circular face of a radially projecting, forward flange portion 30 of a stand 31 having a conically tapered center portion 33 and a radially projecting, rear flange portion 34. The anvil 20 is locked to the stand 31 by a collar 32 which, at its front end, grips the conical taper 22 of the anvil 20, and which, at its rear end, threadedly engages the periphery of the flange portion 30 of the stand. By rotating collar 32 in the appropriate direction, the anvil 20 may be uncoupled from the stand 31 or may be brought into tight fitting relation therewith.
The circular rear face of the rear flange portion 34 of stand 31 is seated against the forwardmost of two axially aligned cylindrical shoes 35 and 36. The'rearmost shoe 36 is seated in turn against the cylindrical end face 37 of a hydraulic piston 38. Each of the shoes 35 and 36 has a slight diametral taper. Therefore, by relatively rotating the shoes 35 and 36, it is possible to make slight angular adjustment between the central axis of the piston 38 and the center line of action of the assembly comprised of stand 31 and anvil 20.
When suitable angular-adjustment has so been obtained, the stand 31, shoes 35, 36 and piston 38 are clamped together by a sleeve 39 having an inwardly projecting annular lip 40 which fits over and engages the rear flange 34 of the stand 31. When flange 34 has been so engaged by lip 40, the sleeve 39 is secured to the front end of the piston 38 by screws 41 which are distributed at angular intervals around the sleeve, and which axially extend through apertures (not shown) in the sleeve to be received in threaded holes (not shown) in the piston. By rotating these screws 41 in the direction appropriate to draw sleeve 39 towards piston 38, a tight fitting assembly may be obtained of stand 31, shoes 35, 36 and the piston.
The hydraulic piston 38 comprises a larger diameter forward portion 45, a smaller diameter rearward portion 46, and a bearing ring 47 which is an integral part of the piston, and which is of greater diameter than either the forward portion 45, or the rearward portion 46. The piston 38 'is received within a cylinder 48 formed in a cylinder block 49 of circular cross section. The forward portion 45 of the piston is encircled by an annular packing ring 50 disposed in an annular recess 51 which radially enlarges the forward end of the cylinder, and which provides an annular shoulder 52 at right angles to the cylinder axis. The p-acking. ring-50 is'forced against the shoulder 52 by a gland 53 having a sleeve portion 54 which is inserted into recess 51 to bear against the packing ring. The gland 53 also has a radially projecting, annular flange 54a seated against the forward surface of cylinder block 49. The gland is secured to the cylinder block 44 by screws (not shown) passing through flange 54a to be received in threaded holes in the cylinder block.
The rearward portion 46 of the piston 38 is encircled by a bushing 55 and by an annular packing ring 56 which is interposed between the bushing and the bearing ring 47. A circular plate 57 is disposed to the rear of piston portion 46, and is secured thereto by axially extending screws (not shown). The periphery of plate 57 axially registers with the bushing 55. Accordingly, when the screws which attach plate 57 to piston portion 46 are turned to draw the plate towards the piston portion, the plate 57 will press against the bushing 55 to thereby squeeze the packing ring 56 between the bushing and the bearing ring 47. As will be evident, the plate 57, bushing 55 and packing ring 56 will travel with the piston 38.
The rear end of the cylinder 48 is characterized by a circular hub 60 which extends axially into the cylinder, and which is of smaller radius than the cylinder. An expandible diaphragm 61 of Buna rubber or the like is stretched over the front of the hub with the margins of the diaphragm being folded back over the axially extending, peripheral surface of the hub to lie flat against such peripheral surface. The diaphragm 61 is clamped in. place by an annular ring 62 which is inserted into the annular space between the hub and the cylinder wall, and which is thereafter drawn towards the rear end of the cylinder by the turning of screws (not shown) which pass axially through the ring 62 to be received in threaded apertures (not shown) in the cylinder block 49. The drawing of the ring, as described, towards the rear end of the cylinder will cause the periphery of the diaphragm 61 to be tightly clamped between the hub 60 and the ring 62 to thereby form a fluid tight space between the diaphragm and the hub.
For the purpose of inducing forward travel of the piston 38, hydraulic fluid under pressure is inrodued into the space between the front end surface of the hub 60 and the expandible diaphragm 61 by a conduit 70 passing through the cylinder block 49 and hub 60. The presence of the diaphragm precludes the leakage of hydraulic fluid which would otherwise occur if the high pressure fluid were permitted to flow freely into contact with the rear end of piston and thereby be subject to extrusion out of the ram unit through the clearance space between the piston and the cy'inder.
Under the pressure of the fluid, the diaphragm 61 expands to displace forwardly the piston 38, and to thereby cause the piston to exert pressure through, the anvil 20 on the pyrophillite block 11 and on the object 16 encased thereby. After the object 10 has been compressed in this manner for a desired time interval, the piston 38 is returned to its normal rearward position by injecting air into the space between bearing ring 47 and stationary packing ring 50 by way of a conduit 71 which runs diagonally from the front surface of cylinder block 49 to the said space.
As shown in Fig. 2, the entire ram unit 12 is supported in place by having the cylinder block 49 received within a cylindrical well 74 formed in the reinforced central portion of a crosshead 82. The cylinder block 49 has at its forward end a radially projecting flange portion 75' which is received within an annular recess 76a radially enlarging the front end of well 74 and providing an an nular shoulder 76 against which the flange 75 bears. The cylinder block 49 is secured to crosshead 82 by screws (not shown) which pass throughrpertures (not shown) in flange 74 to be received in threaded holes in the cylinder block. If desired, the cylinder block 49 and the crosshead 82 may beformed. from one unitary.
piece, in which case the well 74, flange 75, recess 76a and shoulder 76 are eliminated.
For the purpose of permitting hydraulic connections to be made to the ram unit 12 and of otherwise permitting convenient access to the rear end of the ram unit, the central reinforced portion of the crosshead 82 has formed therein a cylindrical bore 77 which is concentric with but of smaller radial size than the cylindrical well 74.
As shown in Fig. 1, the ram units 13-17 are each mounted in the same way as ram unit 12. In the embodiment shown in Fig. 1, each crosshead is disposed to have its major extent lie transverse to the center line of action of the associated ram unit, and to have such line of action pass approximately or, preferably, exactly through the geometric center of the major extent of the crosshead. Moreover, each crosshead has margins which are each parallel to and adjacent to a margin of an adjacent crosshead, and the crossheads are each marginally connected to adjacent crossheads to form a polyhedral frame enclosing the ram units and supporting the ram units in substantially predetermined spaced position relative to each other.
We have found that this arrangement of the frame and pressure generating units has distinct advantages. The frame is completely self-supporting and high pressures are not exerted against any bad or other foundation support. The frame may also be constructed with a minimum number of major or heavy components. Furthermore, when the frame is cubical in form, the ram units are balanced in pairs and directly oppose each other. Such arrangement facilitates an optimum alignment and balance of forces on the central object and reduces the angular moments which during operation tend to deform the frame and cause misalignment of the pressure generating units.
In some applications of the invention, it might be desired that all acting ram units lie in a common plane as do the shown units 12-15. In that case, there would be no ram units and crossheads corresponding to the units 16, 17 and the crossheads 86, 87. The frame formed of the marginally connected crossheads would then be closed in the two dimensions in which the acting ram units lie and would be open in the third dimension.
In the polyhedral frame shown in Fig. 1, the six crossheads 82-87 lie in the surfaces of a cube and each of the crossheads might, if desired, be of square configuration, in which case the frame would he cubical in form. In practice, however, it is preferable to cut away the corners of each crosshead to shape each such crosshead in the form of a cross and produce a frame with a configuration substantially like that shown in Fig. 1. The cruciform configuration of the crossheads 82-87 provides openings for convenient access to the interior of the apparatus and also reduces the overall weight of the frame, while retaining the required mechanical strength.
We have discovered that important advantages in operation are secured by empfoying an articulated frame. Such a frame is produced by having the crossheads connected through joints which offer relatively low resistance to angular movement between adjacent crossheads and permit self-alignment of the frame under the stresses deveoped in operation. For example, hinges may be employed to connect each crosshead to its contiguous crossheads. As shown in Fig. 1, the hinges may be comprised of a set of clevises 89, 90, 91 projecting from the left-hand margin of crosshead 85 and interleaved with a second set of clevises 92, 93, 94 projecting from the right-hand margin of crosshead 82 to provide a continuous central bore through both sets of clevises and a hinge pin 95 which passes through such central bore, to join the crossheads 82 and 85. Similar hinges may be employed, as shown in Fig. 1, to connect each crosshead with each of the four other crossheads which are adjacent thereto. The frame formed of the crossheads may be easily disassembled and reassembled by the simple procedure of driving the hinge pins out of and back into the bores provided by the interleaved sets of clevises. No turning or other manipulation of connecting elements is required.
If desired, the hinge pin 95 may be constructed to be expandible by using as a pin the combination (Fig. 6) of an outer cylindrical collet 99 having: a conically tapered bore 99a and an inner mandrel 100 fitted into bore 99a at one end of the collet, and having a conical taper matching that of the bore. The collet is split at one end by one or more axially running slots 9% extending from one end of the collet. The collet may be substan.ia.ly uniformly expanded in diameter by driving the mandrel into the bore of the collet, and play between the hinge pin and the clevises may thereby be eliminated.
In the described hinge pin and clevis swingable connection, a tension or compression forceacting thereon from one of the connected crossheads will be distributed among the clevises on that crosshead, to be divided into separate smaller stresses which are aliquot fractions of the tension or compression force, and which act in shear against a corresponding number of cross sections of the hinge pin. The total holding strength of the hinge is thus equal to the sum of the holding strengths of the individual cross sections thereof which are subjected to shearing stress. A total holding strength is thereby provided which is several times greater than the holding strength which would be provided if an equal cross sectional area of the pin or other connector were subjected to a stress acting in tension. The hinge pin and clevis arrangement thereby provides the required holding strength with the minimum of bulk and weight. Also, disassembly and reassembly of the frame is facilitated.
Figs. 3 and 4 illustrate some of the forces and moments acting in the Fig. 1 embodiment and show schematically some principal elements involved in the production of such moments and forces, namely crossheads 82-85, connectors 95-98 for joining the crossheads together into a frame, ram units 12 and 15, and the central cubic block 11 of pyrophillite. In both figures the point x marks the center of cubic block 11, the rams 12 and 15 act upon the block 11 with forces represented by the arrows P and the same ram units 12 and 15 simultaneously react upon their respective crossheads 83 and with forces represented by the arrows F In both figures, the dotted line a-a through the center point x is the line with which the center lines of action of the rams 12 and 15 will coincide when such ram units are aligned to act with maximum elficiency upon the block 11.
Fig. 3 represents (with much exaggeration) a situation in which the frame is not quite true so that the crossheads as, 84 are not, as desired, exactly at right angles to the crossheads 83, 85, but, instead, are inclined at an angle to the last named crossheads. In this situation, if it be assumed that the center line of action of each of ram units 12 and 15 is a line which forwardly passes through the center of the square face of block 11 which is presented thereto, and which rearwardly passes through the center point of the associated crosshead, it will be seen from Fig. 3 that the rams 12 and 15 will act upon the block 11 with respective forces F which do not pass through the center point x, and are not in alignment with each other. Because of this misalignment of the forces F there will be a substantial loss in the amount of super-high pressure which the apparatus can effectively exert upon the pyrophillite block 11. If the connector elements -98 are such as to provide rigid connections between the crossheads 82-85, there is no convenient way by which this misalignment of the forces F can be overcome.
Furthermore, in the situation shown in Fig. 3, the rams 12 and 15 will exert on crossheads 83, 85 reactive forces F which are not at right angles to the crossheads. Because of this lack of right angle relation, the force F on'the crosshead 83 will have a component f in line with the lie of crosshead 83 and directed away from the crosshead 82. Also, the force F, on crosshead 85 will have a component f in line with the crosshead 85 and directed towards crosshead 82. These two components f will act as a moment of force. If the connector elements 95-98 are of such character as to rigidly connect together the crossheads 82-85, the mentioned moment of force will be communicated to both of crossheads 82 and 84, and will set up substantial stresses thereon. Such stresses might be so great as to cause intolerable deformation or mechanical failure of the frame.
Such obstacles to satisfactory operation are substantially eliminated when the connector elements 95, 98 are such as to connect together in swingable relation the crossheads 82-85. The problem of stresses set up by the aforementioned moments of force is eliminated because the moments of force cannot be communicated to the crossheads 82. 84 through the hinges. Also, the misalignment of the forces P on cube 11 will be eliminated or substantially reduced because the articulated frame formed by crossheads 82-85 and the hinges 95-98 will respond automatically to the forces exerted on the frame to bring the forces F into better alignment. This is so for the following reasons.
When the ram units 12 and 15 exert the shown reactive forces F, outwardly upon, respectively, the crossheads 83 and 35, the component of each force P, which is at right angles to the lie of the crosshead subjected thereto is a component which will always be many times greater than the component which is in line with the lie of the crosshead. Consequently, the reactive forces F will tend to spread apart the crossheads 83, 85 by the maximum possible amount. Because the elements 95-93 are hinge connectors rather than rigid connectors, the reactive forces P, will actually be effective to cause an increase in the spacing of crossheads 83, 85, in the situation represented by Fig. 3. However, by so increasing the spacing between the last named crossheads, the mentioned reactive forces will cause the entire frame formed of'all the crossheads and all the hinge connectors to change in configuration from the parallelogram shown in Fig. 3 to the perfect square which is shown in Fig. 4. Since the center line of action of each of the rams 12 and 15 passes through the center of the face presented thereto by cube 11 and through the center of the associated crosshead, as shown in Fig. 4, the effect of the described realignment of the frame will be to bring the center lines of action of both of ram units 12 and 15 approximately or exactly to that ideal alignment condition where such center lines of action are both in coincidence with the line aa through the center point x of the cube 11.
Such realignment of the articulated frame of hinge connectors and crossheads into a square can be stated in terms of a general principle which we have discovered. That principle is that an articulated polyhedral frame will respond to forces originating from within, and directed outwardly against the face members of the frame along center lines of action approximately at right angles to the face members and through the centers thereof, to adjust itself in configuration to conform as closely as possible to an ideal geometric polyhedron after which the frame is modeled. The greater the forces exerted outwardly upon the face members of the articulated polyhedral frame, the truer will be the actual configuration of the frame to the theoretical configuration of the ideal polyhedron. it is thereby practical to obtain with such an articulated frame a more accurate and reliable alignment in operation of the pressure generating units of super-high pressure apparatus than if a rigid frame Were employed to mount such pressure generating units.
Returning to a consideration of Fig. 4, it will be seen that the crosshead 85 is urged outwardly by a reactive force F from the ram unit 15. This outward g -sass;
urging of the mentioned reactive force F, is counteracted by restraining forces 7, exerted by the crossheads 82 and 84 (among others) through the connector elements and 98 on the crosshead 85. Since in Pig. 4 the crossheads 82 and 84- are at right angles to the crosshead 85, the restraining forces 7,- will also act at right angles to the crosshead 85 and, hence, will have no component which is in line with the lie of crosshead 85. The situation where the restraining crossheads are at right angles to the restrained crosshead, and where, accordingly, the restraining forces 1, act at right angles to the restrained crosshead is particularly advantageous because the restraining crossheads need provide less strength in tension than if the restraining forces acted at other than right angles to the restrained crosshead. However, even where the frame is, for example, tetrahedral so that the restraining forces act at other than right angles to a given crosshead to be restrained, the connectfon in hinged relation of the crossheads provides a substantial advantage. The fact that the frame is self truing as described and tends to conform to the configuration of the ideal polyhedron after which the frame is modeled, serves to produce a close to perfect balance of the components of the restraining forces which act in the plane of each crosshead. If it happens, as a transient matter, that the balance is not quite perfect, the frame willautomatically realign itself to produce a perfect balance, and the restraining forces cannot set up any moments of force which will produce cumulative stresses on the frame.
In Fig. 5 there is shown another embodiment in which the frame is in the form of a tetrahedron. In this embodiment, the pyrophillite block (not shown) is in the form of a tetrahedron, and the four triangular faces of the tetrahedral block are acted upon by four ram units 161-104 whose center lines of action pass through the said four faces at right angles thereto and through the centers thereof to intersect at a common point marking the center of the pyrophillite block. The front faces of the anvils of the ram units are in the shape of equilateral triangles of smaller size than the registering equilateral triangular faces of the tetrahedral pyrophillite block. The mountings for the four ram units 1014M are provided by four crosshead plates -108. Each crosshead plate is disposed to have the plane of its major extent perpendicular to the center line of action of the associated ram unit, and to have such line of action pass through the center of the crosshead. Moreover, each crosshead is connected to every other crosshead by a plurality of hinge means disposed at the margins of the crossheads. The crossheads 105-108 are thus joined in swingable relation to form an articulated tetrahedral frame.
As will be noted, the crossheads HTS-1% are not of the triangular configuration which would conform to the corresponding triangular faces of a perfect geometric tetrahedron. The configuration of the crossheads is that of the triangular faces of a geometric tetrahedron when such triangular faces have been modified by having the vertex portions thereof cut away. Such crossheads permit convenient access through the frame to the interior of the apparatus, and permit a reduction in weight while maintaining the required mechanical strength. With respect to the details of the ram units and of the hinges, the Fig. 5 embodiment is similar to the embodiment shown in Figs. 1 and 2. v
The frame may also be in the form of an octahedron. For eXample eight of the quasi-triangular crossheads shown in Fig. 5 may be joined into an octahedral frame in which each crosshead centrally supports one of eight ram units. With the ram units in octahedral disposition, the front faces of the anvils would be in the shape of equilateral triangles and would press on a central pyrophillite block formed in the shape of a regular octahedron. Such octahedral disposition of the ram units would be similar to the cubic disposition shown in Fig. 1 in that the ram units would be balanced in pairs. Moreover, for a given total pressure area provided by the anvils, the octahedral disposition, like the cubic disposition, permits a greater volume of material in the pyrophillite block than could be provided in the tetra hedral arrangement shown in Fig. 5.
It will be understood that the above-described embodiments are exemplary only and that the invention set forth herein comprehends embodiments differing in form and/or detail from the above-described embodiments. Hence, the invention is not to be considered as limited save as is consonant with the scope of the following claims.
We claim:
1. In apparatus having a plurality of pressure generating units adapted to exert pressures on a centrally located object, a polyhedral arrangement of crossheads, each crosshead supporting one of said pressure generating units, said crossheads forming an articulated selfaligning polyhedral frame supporting said pressure generating units in mutually spaced relation.
2. Apparatus as in claim 1 with the pressure generating units so arranged that the direction of all generated pressures pass through the geometric center of the apparatus.
3. Apparatus as in claim 1 with the pressure generating units so arranged that all generated pressures remain in static equilibrium.
4. Apparatus as in claim 1 wherein the polyhedral frame has the configuration of a regular polyhedron.
5. Apparatus as in claim 1 wherein the articulation and selfaligning of the frame is obtained by means of hinged connections between the crossheads.
6. Apparatus for applying high pressure to an object comprising a plurality of pressure generating units and crossheads, each pressure generating unit being centrally mounted on one of said crossheads to project inwardly toward said object and each crosshead being connected through movable joints with adjacent crossheads to form an articulated frame enclosing and supporting said pressure generating units.
7. In apparatus having a plurality of pressure generating units disposed about a central object and adapted to exert pressure on said object, the combination therewith comprising, a plurality of crossheads each mounting one of said units to project inwardly towards said object, each crosshead being disposed in relation to its associated pressure generating unit to have the major extent of the crosshead lie transverse to the center line of action of the unit and to have such line of action intersect the crosshead at a central location in the major extent thereof, and each crosshead haying margins which are each contiguous to a margin of an adjacent crosshead, the said crosshead being each connected with adjacent crossheads at such contiguous margins to form a frame enclosing said pressure generating units and supporting said units in mutually spaced relation.
8. In apparatus having a plurality of pressure generating units disposed about a centrally located object and adapted to exert on said object a plurality of pressure producing forces, the combination therewith comprising, a plurality of crossheads each mounting one of said units to project inwardly from such crosshead towards said object, each crosshead being disposed in relation to its associated pressure generating unit to have the major extent of the crosshead lie transverse to the center line of action of the unit and to have such line of action intersect the crosshead at a central location in the major extent thereof, the said crossheads being each yieldably connected through joints with adjacent crossheads to form an articulated frame supporting said pressure generating units in mutually spaced relation.
9. Apparatus as in claim 8 wherein said crossheads are connected by hinges.
10. Apparatus as in claim 8 wherein said crossheads are connected by hinges each comprised of a set of clevises extending outward from one of two adjacent crossheads interleaved with a set of clevises extending outward from the other of said two crossheads to form a central bore through both sets of clevises, and a hinge pin traversing said central bore and connecting in swingable relation said two sets of clevises.
11. Apparatus as in claim 10 wherein said hinge pin is a combination comprising, an outer cylindrical member which is split at one end and which has a conically tapered bore extending axially into said pin from said one end and diminishing in diameter with progress away from said end, and an inner cylindrical member having a conically tapered portion which matches the taper of said bore and which is received therein, the said inner member being adapted to selectively adjust the effective diameter of said outer member by adjustment in axial position of said inner member relative to said outer member.
12. Apparatus for applying high pressure at a central region thereof to a test body comprised of an object to be compressed and a casing therefor of pressure-transmitting material, said apparatus comprising, a plurality of at least three units of which each is operative to generate pressure on said object, and of which each is comprised at least of an anvil having a smaller front face than rear face, the anvils of said units being disposed with their front faces towards and rear faces away from said region and being distributed about said region to enclose it in at least two dimensions excepting for gaps left between each anvil and the ones adjacent thereto to permit movement of said anvils relative to and towards the center of said region, and a plurality of crossheads of which each has a central portion backing a respective one of said units, and of which each crosshead is connected with adjacent crossheads to form a frame enclosing and supporting said pressure generating units.
13. Apparatus for applying high pressure at a central region thereof to a test body comprised of an object to be compressed and a casing therefor of pressure-transmitting material, said apparatus comprising, a plurality of at least three units of which each is operative to generate pressure on said object, and of which each is comprised at least of an anvil having a smaller front face than rear face, the anvils of said units being disposed with their front faces towards and rear faces away from said region and being distributed about said region to enclose it in at least two dimensions excepting for gaps left between each anvil and the ones adjacent thereto to permit movement of said anvils relative to and towards the center of said region, and a plurality of crossheads of which each has a central portion backing a respective one of said units, and of which each crosshead is connected through movable joints with adjacent crossheads to form an articulated frame enclosing and supporting said pressure generating units.
References Cited in the file of this patent UNITED STATES PATENTS 689,567 Secor Dec. 24, 1901 935,809 Parkhurst Oct. 5, 1909 945,992 Stevens Ian. 11, 1910 1,536,035 Twardowsky Apr. 28, 1925 1,750,432 Rollman Mar. 11, 1930 1,755,723 Bloss et a1. Apr. 22, 1930 2,410,581 Hess Nov. 5, 1946 2,894,281 Provse et al July 14, 1959 2,918,699 Hall Dec. 29, 1959
US804546A 1959-04-06 1959-04-06 Super-high pressure apparatus Expired - Lifetime US2968837A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
US804546A US2968837A (en) 1959-04-06 1959-04-06 Super-high pressure apparatus

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US804546A US2968837A (en) 1959-04-06 1959-04-06 Super-high pressure apparatus

Publications (1)

Publication Number Publication Date
US2968837A true US2968837A (en) 1961-01-24

Family

ID=25189230

Family Applications (1)

Application Number Title Priority Date Filing Date
US804546A Expired - Lifetime US2968837A (en) 1959-04-06 1959-04-06 Super-high pressure apparatus

Country Status (1)

Country Link
US (1) US2968837A (en)

Cited By (27)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3088168A (en) * 1959-08-13 1963-05-07 Edward C Lloyd Multiple-anvil high pressure apparatus
US3093862A (en) * 1961-05-24 1963-06-18 Barogenics Inc Compact hydrostatic pressure apparatus
US3096544A (en) * 1960-06-17 1963-07-09 Asea Ab High pressure vessel with punch
US3118177A (en) * 1960-06-20 1964-01-21 Asea Ab Autoclave
US3134139A (en) * 1961-02-28 1964-05-26 Gen Electric High pressure apparatus
US3159876A (en) * 1962-05-23 1964-12-08 Research Corp High pressure press
US3179979A (en) * 1962-09-25 1965-04-27 Gen Electric High pressure die
US3182353A (en) * 1963-01-29 1965-05-11 Research Corp Guide means for high pressure press
US3328838A (en) * 1963-12-30 1967-07-04 Barogenics Inc High pressure methods and apparatus
US3346922A (en) * 1964-03-31 1967-10-17 Barogenics Inc Press structures
US3418922A (en) * 1967-01-03 1968-12-31 Barogenics Inc Load-bearing frame structure
US3418923A (en) * 1967-01-03 1968-12-31 Barogenics Inc Compact frame structures
US3989795A (en) * 1973-08-13 1976-11-02 Iowa State University Research Foundation, Inc. Method of compressing ceramic refractory bodies
US4414028A (en) * 1979-04-11 1983-11-08 Inoue-Japax Research Incorporated Method of and apparatus for sintering a mass of particles with a powdery mold
US4766808A (en) * 1986-04-04 1988-08-30 Uniflex-Hydraulic Gmbh Radial press with v-shaped press jaws
US20070009626A1 (en) * 2005-07-06 2007-01-11 David Hall Strain matched threads for a high pressure high temperature press apparatus
US20070122512A1 (en) * 2005-07-06 2007-05-31 Hall David R Strain Matched Threads for a High Pressure High Temperature Press Apparatus
US20080193581A1 (en) * 2007-02-12 2008-08-14 Hall David R Anvil for a HPHT Apparatus
US20080241293A1 (en) * 2007-03-27 2008-10-02 Hall David R Radial Compression Element for a HTHP Cartridge
US7467937B1 (en) 2007-11-29 2008-12-23 Hall David R Preloaded threads for a high-temperature high-pressure press
US7513764B1 (en) 2008-09-30 2009-04-07 Hall David R High pressure press
US20110104318A1 (en) * 2009-10-29 2011-05-05 Hall David R High Pressure, High Temperature Back-Up with a Circumferential Relief
CN103691364A (en) * 2013-12-18 2014-04-02 桂林桂冶重工股份有限公司 Cubic hydraulic machine
US8739697B1 (en) 2009-10-29 2014-06-03 Us Synthetic Corporation High pressure press with tensioning assembly and related methods
US20150047518A1 (en) * 2012-03-30 2015-02-19 Element Six Limited Press assembly and coupling mechanism for same
US20220152966A1 (en) * 2017-09-28 2022-05-19 Us Synthetic Corporation Multi-anvil high pressure press and related methods
US11534999B1 (en) 2009-10-29 2022-12-27 Us Synthetic Corporation Reinforced press base, strengthening ring, and method of reinforcing a press base

Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US689567A (en) * 1900-09-11 1901-12-24 Gen Power Company Engine-frame.
US935809A (en) * 1907-06-28 1909-10-05 Edward B Parkhurst Engine or motor.
US945992A (en) * 1909-03-18 1910-01-11 Gen Electric Diaphragm-motor.
US1536035A (en) * 1923-08-13 1925-04-28 Twardowsky John Diaphragm-actuated mechanism
US1750432A (en) * 1925-11-16 1930-03-11 Ohio Cultivator Co Press
US1755723A (en) * 1929-06-07 1930-04-22 Internat Derrick & Equipment C Self-aligning pitman bearing
US2410581A (en) * 1943-09-13 1946-11-05 American Steel Foundries Hydraulic press
US2894281A (en) * 1955-05-05 1959-07-14 Bar Products Company Molding press
US2918699A (en) * 1958-04-28 1959-12-29 Research Corp High pressure press

Patent Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US689567A (en) * 1900-09-11 1901-12-24 Gen Power Company Engine-frame.
US935809A (en) * 1907-06-28 1909-10-05 Edward B Parkhurst Engine or motor.
US945992A (en) * 1909-03-18 1910-01-11 Gen Electric Diaphragm-motor.
US1536035A (en) * 1923-08-13 1925-04-28 Twardowsky John Diaphragm-actuated mechanism
US1750432A (en) * 1925-11-16 1930-03-11 Ohio Cultivator Co Press
US1755723A (en) * 1929-06-07 1930-04-22 Internat Derrick & Equipment C Self-aligning pitman bearing
US2410581A (en) * 1943-09-13 1946-11-05 American Steel Foundries Hydraulic press
US2894281A (en) * 1955-05-05 1959-07-14 Bar Products Company Molding press
US2918699A (en) * 1958-04-28 1959-12-29 Research Corp High pressure press

Cited By (46)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3088168A (en) * 1959-08-13 1963-05-07 Edward C Lloyd Multiple-anvil high pressure apparatus
US3096544A (en) * 1960-06-17 1963-07-09 Asea Ab High pressure vessel with punch
US3118177A (en) * 1960-06-20 1964-01-21 Asea Ab Autoclave
US3134139A (en) * 1961-02-28 1964-05-26 Gen Electric High pressure apparatus
US3093862A (en) * 1961-05-24 1963-06-18 Barogenics Inc Compact hydrostatic pressure apparatus
US3159876A (en) * 1962-05-23 1964-12-08 Research Corp High pressure press
US3179979A (en) * 1962-09-25 1965-04-27 Gen Electric High pressure die
US3182353A (en) * 1963-01-29 1965-05-11 Research Corp Guide means for high pressure press
US3328838A (en) * 1963-12-30 1967-07-04 Barogenics Inc High pressure methods and apparatus
US3346922A (en) * 1964-03-31 1967-10-17 Barogenics Inc Press structures
US3418922A (en) * 1967-01-03 1968-12-31 Barogenics Inc Load-bearing frame structure
US3418923A (en) * 1967-01-03 1968-12-31 Barogenics Inc Compact frame structures
US3989795A (en) * 1973-08-13 1976-11-02 Iowa State University Research Foundation, Inc. Method of compressing ceramic refractory bodies
US4414028A (en) * 1979-04-11 1983-11-08 Inoue-Japax Research Incorporated Method of and apparatus for sintering a mass of particles with a powdery mold
US4766808A (en) * 1986-04-04 1988-08-30 Uniflex-Hydraulic Gmbh Radial press with v-shaped press jaws
US20070009626A1 (en) * 2005-07-06 2007-01-11 David Hall Strain matched threads for a high pressure high temperature press apparatus
US7186104B2 (en) * 2005-07-06 2007-03-06 Hall David R Strain matched threads for a high pressure high temperature press apparatus
US20070122512A1 (en) * 2005-07-06 2007-05-31 Hall David R Strain Matched Threads for a High Pressure High Temperature Press Apparatus
US7354262B2 (en) * 2005-07-06 2008-04-08 Hall David R Strain matched threads for a high pressure high temperature press apparatus
US20080193581A1 (en) * 2007-02-12 2008-08-14 Hall David R Anvil for a HPHT Apparatus
US7569249B2 (en) 2007-02-12 2009-08-04 Hall David R Anvil for a HPHT apparatus
US7497675B2 (en) 2007-02-12 2009-03-03 Hall David R Piston for a HPHT apparatus
US7481639B2 (en) 2007-02-12 2009-01-27 Hall David R Back-up for a HPHT apparatus
US7467936B2 (en) 2007-03-27 2008-12-23 Hall David R Radial compression element for a HTHP cartridge
US20080241293A1 (en) * 2007-03-27 2008-10-02 Hall David R Radial Compression Element for a HTHP Cartridge
US7467937B1 (en) 2007-11-29 2008-12-23 Hall David R Preloaded threads for a high-temperature high-pressure press
US7513764B1 (en) 2008-09-30 2009-04-07 Hall David R High pressure press
US7517203B1 (en) 2008-09-30 2009-04-14 Hall David R High pressure press
US7540732B1 (en) 2008-09-30 2009-06-02 Hall David R High pressure press
US8857328B1 (en) 2009-10-29 2014-10-14 Us Synthetic Corporation High pressure press and method of making the same
US10195700B1 (en) * 2009-10-29 2019-02-05 Us Synthetic Corporation High pressure press with tensioning assembly and related methods
US11878485B1 (en) 2009-10-29 2024-01-23 Us Synthetic Corporation Reinforced press base, strengthening ring, and method of reinforcing a press base
US8739697B1 (en) 2009-10-29 2014-06-03 Us Synthetic Corporation High pressure press with tensioning assembly and related methods
US8850971B1 (en) 2009-10-29 2014-10-07 Us Synthetic Corporation Reinforced press base, strengthening ring, and method of reinforcing a press base
US20110104318A1 (en) * 2009-10-29 2011-05-05 Hall David R High Pressure, High Temperature Back-Up with a Circumferential Relief
US8910568B1 (en) 2009-10-29 2014-12-16 Us Synthetic Corporation Reinforced press base, piston cavity sleeve, and method of reinforcing a press base
US11858230B1 (en) 2009-10-29 2024-01-02 Us Synthetic Corporation High pressure press and method of making the same
US10150270B1 (en) 2009-10-29 2018-12-11 Us Synthetic Corporation High pressure press and method of making the same
US8066500B2 (en) 2009-10-29 2011-11-29 Hall David R High pressure, high temperature back-up with a circumferential relief
US10220586B1 (en) 2009-10-29 2019-03-05 Us Synthetic Corporation Reinforced press base, strengthening ring, and method of reinforcing a press base
US10414113B1 (en) 2009-10-29 2019-09-17 Us Synthetic Corporation Reinforced press base, piston cavity sleeve, and method of reinforcing a press base
US11534999B1 (en) 2009-10-29 2022-12-27 Us Synthetic Corporation Reinforced press base, strengthening ring, and method of reinforcing a press base
US11524473B1 (en) 2009-10-29 2022-12-13 Us Synthetic Corporation Reinforced press base, piston cavity sleeve, and method of reinforcing a press base
US20150047518A1 (en) * 2012-03-30 2015-02-19 Element Six Limited Press assembly and coupling mechanism for same
CN103691364A (en) * 2013-12-18 2014-04-02 桂林桂冶重工股份有限公司 Cubic hydraulic machine
US20220152966A1 (en) * 2017-09-28 2022-05-19 Us Synthetic Corporation Multi-anvil high pressure press and related methods

Similar Documents

Publication Publication Date Title
US2968837A (en) Super-high pressure apparatus
US2958900A (en) Pellet mill die assembly
US3150413A (en) High pressure presses and components thereof
US3350905A (en) Liquid pressure bulge forming apparatus
US3458217A (en) Tubular coupling having low profile band segments with means for preventing relative rotation
US4351153A (en) Hydraulic control device
US7150617B1 (en) Multiple position press
US4021181A (en) Tie rod connection for die closing unit of injection molding machine
GB1186239A (en) Mounting Pin Assembly.
US3278993A (en) Apparatus subjected to large tonnage loads and/or high pressures
US3934423A (en) Power cylinder construction
US3323731A (en) Grinding apparatus primarily for lignocellulose containing material
US2940779A (en) Balanced face flange
GB1487219A (en) Bolted joints
JPH0363112A (en) Center mechanism of tire vulcanizer
US3683754A (en) Hydraulic cylinder
US3182353A (en) Guide means for high pressure press
US3091804A (en) Hydrostatic press for an elongated object
WO2007110736A2 (en) Radial press for joining high pressure hydraulic pipes
US4029400A (en) Pressure balanced cooled mirror with axially movable transfer tube assemblies
US3219370A (en) Flanged joint
US3674403A (en) High-pressure apparatus
GB1390012A (en) Bolt tightening apparatus
JPS5872748A (en) Method and device for incorporating torsional vibration attenuator or torsional elastic coupling
US3328838A (en) High pressure methods and apparatus