US27A - Composition op paints - Google Patents
Composition op paints Download PDFInfo
- Publication number
- US27A US27A US27DA US27A US 27 A US27 A US 27A US 27D A US27D A US 27DA US 27 A US27 A US 27A
- Authority
- US
- United States
- Prior art keywords
- lead
- carbonate
- paints
- add
- water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 239000003973 paint Substances 0.000 title description 4
- 239000000203 mixture Substances 0.000 title description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 12
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 10
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 6
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 6
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 6
- 238000009835 boiling Methods 0.000 description 6
- QDOXWKRWXJOMAK-UHFFFAOYSA-N dichromium trioxide Chemical compound O=[Cr]O[Cr]=O QDOXWKRWXJOMAK-UHFFFAOYSA-N 0.000 description 6
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 5
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 4
- 229910052802 copper Inorganic materials 0.000 description 4
- 239000010949 copper Substances 0.000 description 4
- MOUPNEIJQCETIW-UHFFFAOYSA-N lead chromate Chemical compound [Pb+2].[O-][Cr]([O-])(=O)=O MOUPNEIJQCETIW-UHFFFAOYSA-N 0.000 description 4
- 239000013049 sediment Substances 0.000 description 4
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 3
- 239000002253 acid Substances 0.000 description 3
- 229910052742 iron Inorganic materials 0.000 description 3
- DCYOBGZUOMKFPA-UHFFFAOYSA-N iron(2+);iron(3+);octadecacyanide Chemical compound [Fe+2].[Fe+2].[Fe+2].[Fe+3].[Fe+3].[Fe+3].[Fe+3].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-] DCYOBGZUOMKFPA-UHFFFAOYSA-N 0.000 description 3
- 229910017604 nitric acid Inorganic materials 0.000 description 3
- 229960003351 prussian blue Drugs 0.000 description 3
- 239000013225 prussian blue Substances 0.000 description 3
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 2
- 238000013019 agitation Methods 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- PSFDQSOCUJVVGF-UHFFFAOYSA-N harman Chemical compound C12=CC=CC=C2NC2=C1C=CN=C2C PSFDQSOCUJVVGF-UHFFFAOYSA-N 0.000 description 2
- 229940072033 potash Drugs 0.000 description 2
- 235000015320 potassium carbonate Nutrition 0.000 description 2
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Substances [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 2
- 235000019614 sour taste Nutrition 0.000 description 2
- 229910052717 sulfur Inorganic materials 0.000 description 2
- 239000011593 sulfur Substances 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- XFXPMWWXUTWYJX-UHFFFAOYSA-N Cyanide Chemical compound N#[C-] XFXPMWWXUTWYJX-UHFFFAOYSA-N 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- ZCDOYSPFYFSLEW-UHFFFAOYSA-N chromate(2-) Chemical compound [O-][Cr]([O-])(=O)=O ZCDOYSPFYFSLEW-UHFFFAOYSA-N 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- XMXNVYPJWBTAHN-UHFFFAOYSA-N potassium chromate Chemical compound [K+].[K+].[O-][Cr]([O-])(=O)=O XMXNVYPJWBTAHN-UHFFFAOYSA-N 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/14—Compounds of lead
- C09C1/20—Lead chromate
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/22—Compounds of iron
- C09C1/26—Iron blues
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/60—Optical properties, e.g. expressed in CIELAB-values
Definitions
- my invention consists in using-1st flowers of sulfur, sulfuric acid, and carbonate of lead in forming Prussianblue. 2d in using nitric acid, and carbonate of lead to form chrome yellow. 3d in the further use of flowers of sulfur to form chrome green, 4th in the formation of a metallic green from sulfate of copper, and carbonate of lead.
- the sulfur prevents the green fro-m discharging the blue when exposed to the atmosphere. the formation of a metallic green-from sulfate of copper, and carbonate of lead.
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Paints Or Removers (AREA)
Description
UNITED STATES PATENT OFFICE.
HARMAN HIBBARD, OF DARIEN, NEW YORK.
coivirosrrrou or PAINTS.
Specification of Letters Patent No. 27, dated September 20, 18 36.
To all whom it may concern:
Be it known that I, HARMAN HIBBARD, of Darien, in the county of Genesee and State of New York, have invented a new and useful Improvement in the Art of Manufacturing Paints; and I do hereby declare that the followingis a full and exact description.
The nature of my invention consists in using-1st flowers of sulfur, sulfuric acid, and carbonate of lead in forming Prussianblue. 2d in using nitric acid, and carbonate of lead to form chrome yellow. 3d in the further use of flowers of sulfur to form chrome green, 4th in the formation of a metallic green from sulfate of copper, and carbonate of lead.
To enable others skilled in the art to make and use my invention, I will proceed to describe the process by which these paints may be prepared.
To make Prussian blue, dissolve 16 lbs. sulfate of iron in as small a quantity of boiling water as possible, dissolve 1 lb. of prussiate of potash in 1 pint of boiling water after being finely pulverized, and add to the sulfate of iron add 1 lb. of carbonate of lead and 1} lb. of flowers of sulfur previouly ground together in water, then add sulfuric acid till effervescence ceases, the sediment should be left with an excess, of acid possessing a sour taste, the whole should be tho-roughly blended together, and then left to dry.
To make chrome yellow, to 16 lbs. carbonate of lead finely ground in water, and put into a tub containing 16 gallons of boiling water add 1 lb. chromate of potash (previously dissolved in 3 gallons of boiling water) to the solution of potash add 8,-oz. nitric acid, and add this mixture to the tub containingthe carbonate of lead, taking care to keep up agitation for some minutes then leave, and the lead will fall, decant the water, and dry the sediment.
To make chrome-green, to 1, lb. Prussian blue add 2, lbs. of chrome yellow, and 1 lb. flowers of. sulfur, the-whole should bemoistened with water and finely pulverized together, a suflicient quantity of sulfuric acid should be added to leave a sour taste if the effervescenceceases, the sediment should then be dried without washing.
To form a metallic green, dissolve 1, lb. sulfate of copper in 3 gallons of boiling water, and add 1, lb. carbonate of lead, previously pulverized in 1, pint of hot-water,
then put into 3 gallons of boiling water,
pour the solution lead intothe solution of copper slowly, and at the same time keep up a constant agitation, it may then be left to subside, pour off the water, and dry the sediment.
hat I claim as my invention, and desire rating the composition with oxygen which forms the blue,I use the carbonate of lead to precipitate the iron, to discharge the'superfluous acid, and to assist in forming a body to the paint.
2. In the use of nitric acid, and carbonate of lead in preparing chrome yellow, the acid discharges the carbon contained in the lead and causes the chromate, and lead to unite.
3. In the further use of the flowers of sulfur in preparing chrome green, the sulfur prevents the green fro-m discharging the blue when exposed to the atmosphere. the formation of a metallic green-from sulfate of copper, and carbonate of lead.
I-IARMAN HIBBARD.
Witnesses:
BARNEY E. SEAVER, ISAIAH RANO.
Publications (1)
| Publication Number | Publication Date |
|---|---|
| US27A true US27A (en) | 1836-09-20 |
Family
ID=2060305
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US27D Expired - Lifetime US27A (en) | Composition op paints |
Country Status (1)
| Country | Link |
|---|---|
| US (1) | US27A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4831345A (en) * | 1988-06-17 | 1989-05-16 | The United States Of America As Represented By The Secretary Of The Navy | Stripline power divider |
| RU2291707C2 (en) * | 2000-12-12 | 2007-01-20 | Канека Корпорейшн | Compositions for prophylaxis or relief of multiple risk factor syndromes |
| DE102016102341B4 (en) | 2015-02-13 | 2024-04-18 | Avaya Inc. | System and method for topic-based disconnection in instant messaging |
-
0
- US US27D patent/US27A/en not_active Expired - Lifetime
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4831345A (en) * | 1988-06-17 | 1989-05-16 | The United States Of America As Represented By The Secretary Of The Navy | Stripline power divider |
| RU2291707C2 (en) * | 2000-12-12 | 2007-01-20 | Канека Корпорейшн | Compositions for prophylaxis or relief of multiple risk factor syndromes |
| DE102016102341B4 (en) | 2015-02-13 | 2024-04-18 | Avaya Inc. | System and method for topic-based disconnection in instant messaging |
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