US2721952A - Grid structure and the process of making - Google Patents

Grid structure and the process of making Download PDF

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US2721952A
US2721952A US287705A US28770552A US2721952A US 2721952 A US2721952 A US 2721952A US 287705 A US287705 A US 287705A US 28770552 A US28770552 A US 28770552A US 2721952 A US2721952 A US 2721952A
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grid
ring
disc
members
blank
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US287705A
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David E Kenyon
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Sperry Corp
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Sperry Rand Corp
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    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J19/00Details of vacuum tubes of the types covered by group H01J21/00
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J2893/00Discharge tubes and lamps
    • H01J2893/0001Electrodes and electrode systems suitable for discharge tubes or lamps
    • H01J2893/0012Constructional arrangements
    • H01J2893/0019Chemical composition and manufacture
    • H01J2893/0022Manufacture
    • H01J2893/0024Planar grids
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S428/00Stock material or miscellaneous articles
    • Y10S428/922Static electricity metal bleed-off metallic stock
    • Y10S428/9265Special properties
    • Y10S428/929Electrical contact feature
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S428/00Stock material or miscellaneous articles
    • Y10S428/922Static electricity metal bleed-off metallic stock
    • Y10S428/9335Product by special process
    • Y10S428/939Molten or fused coating
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T29/00Metal working
    • Y10T29/49Method of mechanical manufacture
    • Y10T29/49616Structural member making
    • Y10T29/4962Grille making
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T29/00Metal working
    • Y10T29/49Method of mechanical manufacture
    • Y10T29/49826Assembling or joining
    • Y10T29/49888Subsequently coating

Definitions

  • the present invention relates to minute grid electrodes for extremely high frequency electron tubes such as microwave klystrons and triodes, for example.
  • This application is a continuation-in-part of application Serial No. 155,432, filed April 12, 1950, now abandoned, by the same inventor, and assigned to the same assignee.
  • the present invention is concerned with grids of a much fined order of size, viz, of the order of onertenth inch diameter and smaller. Grids of such small size are required in klystrons, for instance, operating at wavelengths of the order of one centimeter (frequencies of the. order of 30,000 megacycles per second). In grids of this order of size, the vane. elements are so fine as to be, hardly visible to the naked eye, strongly militating against, attempts at, jig assembly of individual grid pieces.
  • minutev grids possessing the aforementioned attributes of a good electrode are produced by winding a pair of unlike metal strips.v into a, spiraloid form, bonding. the strips together into a rigid disc, cutting from sectors thereof, a plurality of discs each having a diameter which is a fraction of the diameter of the original rigid disc, mounting each of these discs in a conformal ring, bonding the disc and ring together, and removing, by etch n the material of one ofthe two original metal strips, to leave thin corre spondingly curved arcuate vanes of the desired material.
  • Each vane element extends across the interior of the grid' ring, free from any bent tabs, and is bonded directly at its. transverse end surfaces to the'inner surface of the E An object. of the present invention, therefore, is to ICC tion, has relatively high mechanical stability and ruggedness, and very low electron interception.
  • Still another object of the invention is to provide a workable process for fabricating grids of the abovementioned type.
  • Fig. l is an enlarged plan view of a disc structure comprised of interleaved spiraloid members, formed according to the present invention at an early stage of fabrication of the grid;
  • Fig. 2 is a vertical sectional view taken along lines 2-2 of Fig. 1;
  • Fig. 3 shows a sector cut from the structure of Fig. lon the lines 33 thereof, and indicates where a circular portion is derived therefrom;
  • Fig. 4 is a plan view of a circular section of Fig. 3 after a grinding operation
  • Fig. 5 is a plan view of the structure of Fig. 4 supported in a mounting means;
  • Fig. 6 is a plan view of a completed grid structure according to the present invention.
  • Fig. 7 is a vertical section of Fig. 6 taken along lines 77 thereof;
  • Fig. 8. is a perspective view of a form of apparatus suitable for use in carrying out a part of the method of the instant invention.
  • Fig. 9 is an elevational view, partly in longitudinal sec,- tion, of the apparatus of Fig. 8.
  • Fig. 10 is a cross sectional view of the structure of Fig. 9 taken along lines 10-10 thereof.
  • disc 16 is shown, whichis formed by winding two ribbon-like members 17 and 18 together to prov de a fiat disc structure comprised of spiraloid. or convoluted interleaved members.
  • Members 17 and 13 are constituted of continuous strips of. ribbon of different metals, ribbon 17 being of iron, for example, and ribbon 18 being of tungsten, molybdenum, or other suitable grid material.
  • ribbon 17 being of iron, for example
  • ribbon 18 being of tungsten, molybdenum, or other suitable grid material.
  • adjacent portions of members 17' and 18 may be joined together by brazing with a suitable brazing material such as copper, cupro-nickel or manganese.
  • the upper and lower faces 20 and 25, respectlvely, of the disc 16 may be ground to a finished or desired grid thickness or axial depth, such as indicated at 30. instead of grinding to a finished dimension at this stage, the faces 20 and 25 may be ground merely to insure that each face is perfectly fiat and planar.
  • the ground surfaces preferably are immediately provided with a protective plating, such as chromium.
  • the plated disc is then heated, if desired, in wet hydrogen at low heat, approximately 800 C., in order to oxidize the chromium.
  • the disc 16 after grinding and plating, is cut into sectors, one of which is shown in Fig. 3, by employing an abrasive wheel or other suitable cutting apparatus- It has been found that as many as 10 usable sectors may be cut from a single disc such as 16, depending upon its perfection and size.
  • the sector such as shown in Fig. 3, is then mounted between two collinear pins (not shown) which frictionally support the sector at the faces thereof. are synchronously rotated, thereby rotating the sector.
  • a grinding mechanism (not shown) is employed to. edge grind the rotating sector until a disc is formed as is Both pins shown in Fig. 4. During this operation care should be taken to insure that the oxidized chromium surface is not damaged by abrasion.
  • the resulting grid blank 21 has both faces protected by oxidized chromium, with the edge a bright, ground surface.
  • the grid blank 21 is surrounded by'a tightly fitting ring 22 and apertured disc 23.
  • Ring 22 may be composed for instance, of gold, copper or nickel.
  • Apertured disc 23 is comprised of iron, steel, or other suitable material.
  • the assembly is brazed at a temperature suitable for fusing the ring 22 to the periphery of grid blank 21 without destroying the ring.
  • ring 22 is of copper, it is preferable to employ a very thin layer of gold solder between the periphery of grid blank 21 and the ring 22 preparatory for the brazing operation.
  • the gold solder which is a gold alloy, has a lower melting point than the copper.
  • ring 22 is of nickel, copper powder is utilized to braze the ring 22 to the grid blank 21. In lieu of copper powder, the inner surface of the ring of nickel could be copper plated. The oxidized chromium plating prevents any of the brazing material from flowing onto either face of the grid blank 21.
  • the assembly is preferably fired in a hydrogen atmosphere, as with a hydrogen bell jar (not shown).
  • a hydrogen atmosphere is found beneficial to insure that the molten metal wets the end surfaces of the members comprising the grid blank 21, particularly the transverse or cross-cut ends of members 18. If such a procedure is not followed when dealing with extremely closely spaced surfaces, such as the cylindrical outer surface of grid blank 21 and the cylindrical inner surface of the ring 22, the surface tension of the molten metal customarily prevents it from flowing sufliciently to form a suitable bond.
  • the oxidized chromium coating protects the faces of the grid blank 21 and prevents the molten brazing material from wetting either face of the grid blank 21.
  • the faces of the assembly comprising grid blank 21, ring 22, and apertured disc 23 may be ground to a finished grid thickness, if the grinding process described in referring to dimension 30 in Fig. 2 was not carried out.
  • the apertured disc 23 is removed from the rest of the structure. This can be done by a cutting operation, after which the ring 22 is polished to remove any peripheral burrs that may exist after the cutting.
  • the structure is then etched in a suitable bath of hydrochloric or sulphuric acid, for example, to remove the iron vane elements. If hydrochloric acid is employed for etching, it will also remove any chromium on the faces of grid blank 21, if the face grinding process supra was not undertaken.
  • the structure may also be electro-etched in a bath of sodium hydroxide, if desired, to remove burrs which remain after any of the face grinding processes.
  • the apertured disc 23 from the grid blank 21 and ring 22 may be removed by the same etching process as is employed to remove the iron vanes.
  • the structure may also be etched in a bath of ammonium hydroxide and hydrogen peroxide to remove any remnants of the copper brazing material which may exist on the faces of the grid blank 21 and ring 22.
  • Grids of the above-described type are capable of fabrication in extremely small sizes. Examples of the minute dimensions of a few of the highly successful grids. Of 1 .1%
  • grid 24 comprises curved vanes 18 which form a section of a flat spiraloid structure.
  • Each vane has its transverse or crosscut ends supported by ring member 22. There is uniform spacing between vanes.
  • Each of the vanes 18 has a width greatly in excess of its thickness, with the width dimension of each vane oriented in a direction parallel to the axis of the ring 22. Accordingly, the orientation of the vanes 18 is such as to provide ample mechanical rigidity and strength for the minute size thereof, and at the same time provide a grid structure 24 which presents a minimum electron beam intercepting area.
  • the thickness of the vanes 18 may be reduced by a suitable etching fluid, such as by treating the grid 24 with molten potassium nitrate.
  • a suitable etching fluid such as by treating the grid 24 with molten potassium nitrate.
  • care must be taken to ensure that the structure of the vanes 18 is not impaired. If the action is permitted to progress too far the vanes 18 may neck down at a point and break. It has been found possible and practical to reduce the vanes 18 to one-half their original thickness.
  • jig 28, suitable for use in fabricating the disc 16 of Fig. 1 has a body portion 29 with a reduced-diameter continuation 31.
  • the continuation 31 is formed with an internally-threaded portion 32 for cooperation with screw 33.
  • the screw 33 together with washer 34 and continuation 31 is effective for maintaining the cap 36 of the jig 28 rigid against axial movement relative to the body portion 29.
  • Between the body portion 29 and the cap 36 is a circular slotted washer 37, the slot 40 of which is provided for receiving the end 19 of the iron ribbon 17 in order to secure it during the winding operation.
  • washer 37 is shown as circular it is obvious that the periphery thereof could have an oval shape, or even substantially flat portions.
  • an enlarged washer 38 On one side of the slotted washer 37 is positioned an enlarged washer 38, the diameter of which is preferably greater than that of body portion 29 to facilitate the removal of the disc 16 from the jig 28.
  • a disc 39 of suitable brazing material such as copper, cupro-nickel, or
  • the end 19 of the iron ribbon 17 may be inserted into the slotted portion 40 of washer 37, with the tungsten ribbon 18 resting beneath the iron ribbon 17. If desired, the end 19 of ribbon 17 may be initially bent to cooperate with the slot 40 in order to facilitate the start of the winding operation.
  • the ribbons 17 and 18 may be wound together: Aiterthe space bctweem the enlarged'washer38 and disc 33 is filled with the altegnate, interleaved layers of ironand;tungstemribbonsHand 1'8, the'free end-of one 017- bothof the ribbons 1 7 and 18- may be wrapped around or-pinched over'arotatable securing member 41, whichmember-41 is: rotatable about an axis disposedfiat' right-angles to thelongitudinal axis-of the 28: Stop pin 42 limits the swing of the securingmember-ll, toprevent 'themember '41 from rotating therebeyond.
  • thefdisc39melts to solidly braze together the iron and tungsten ribbons'17 and- 18; At'the sameg time, the heat'involved in thejfusing operation iseflective for removing stresses from the iron and-tungsten;1 ibbonslT'and- 18, After the formation of the sol-idly brazed disc11'6,,it'm%y'be removedfrom the jig 28 by disengaging the cap'36-I The enlarged washer 38 facilitates this operation.
  • the removal of! stresses and-the: joining tosether of the ribbon membersl' ns- .18. may be effected in separate operations.
  • the disc.39j which. constitutes thebrazing, material, maybe omitted. from thejig. 28. .After. thewin'ding operation, the ribbons. 17 and. 18. may. be subjectedinitial-ly to high temperature.
  • a small. piece of coppen may. be placed prior to-the application of. heatat the-end fthe iron ribbon 17. most remote from. the center. of the spiral configuration. Such apiece of. copper, after.
  • the assembly may be fired with a suitable brazing material to solidly braze together the iron and tungsten ribbons 17 and 18.
  • the ribbons 17 and 18 of the disc 16 may be brazed or joined together in a somewhat different manner by employing, for instance, a copper-plated iron ribbon in place of the previously mentioned iron ribbon 17.
  • Disc 39 may then be omitted.
  • the copper plating melts, acting as a brazing flux to join together the spiraloid members 17 and 18.
  • the resulting structure may not be as solid as that provided by the other techniques discussed herein.
  • An electron permeable grid structure comprising a ring member having an inner diameter of less than approximately 0.1 inch, a plurality of spaced curved vane elements mounted within said ring member, said van elements being curved in the same direction within a plane containing said ring member, said plane being perpendicular to the axis of said ring member, the width dimension of each vane element extending in a direction substantially parallel to the axis of said ring member, the transverse ends of said vane elements directly abutting the inner surface of said ring member and being bonded thereto.
  • An electron permeable grid structure comprising a ring member having an inner diameter of less than approximately 0.1 inch, a plurality of arcuate vane elements mounted within said ring member, said vane elements being uniformly spaced and curved in the same direction within a plane containing said ring member, said plane being perpendicular to the axis of said ring member, each of said vane elements having substantially the same crosssectional area with the longer dimension of each crosssectional area extending in a direction substantially parallel to the axis of said ring member, the transverse ends .6 of said vane elements directly abutting the inner-surface of said ring member andbeing bonded thereto,
  • An electron permeable grid structure comprising a,
  • ring member having an, inner; diameter of less than proximately 0.1 inch, a plurality off spaced curved vane elements mounted within said ring membersaid vane elements being curved in thesame direction within a planecontaining said ring member, said plane being perpendicular to the axis of-i'said' ring member, each, Qfisaidvane elementshaving substantially the same cross sectional area with-thelong er dimension of each .c1;osssectional area extending in a direction substantially par,- allel to the axis of saidi'ring member, the transverse ends of said vane elements abutting the inner surface, of'said ring member andbeingbonded' thereto, the corresponding narrow edges of said vane, elements having polished coplanar surfaces. 7 p
  • a grid structure comprising a plurality offspaeedp curved metallic ribbon,elements,mountediedgewise within a supporting'member, saidsupporting member having i e d e v su faces e m x m m nea stanc bet'weenany two points on said inner surface of said sup; porting member being'l'ess thanapproximately 0.1 inch, said ribbon elements being curvediin the same direction within aplane containing said supporting-member, each of said ribbonelements having substantially the same cross-sectional area with their transverse ends directly abutting-and: joining A the inner-surface of: said supporting member;
  • i In. electrompermeable. apparatus having an: axis, a circularly-shaped mounting ring symmetrically disposed about said axis, said ring having an inner diameter of less than approximately 0.1 inch, and a plurality of spaced metallic vanes having cross-cut ends directly abutted and supported by said ring, each of said vanes being relatively Wide compared to the thickness thereof with the wide dimension oriented in a direction parallel to said axis, whereby a relatively small cross-sectional area is presented to an electron beam aligned with said axis, said vanes forming a section of a fiat spiraloid structure.
  • a method of forming an electron discharge tube grid structure comprising the steps of ,forming a disc comprised of interleaving spiraloid ribbon members of different metals, brazing said members together to rigidity said disc, cutting a grid blank from a sector of said disc, mounting said grid blank in a mounting ring, and removing elements of one of said metals which constitute part of said grid blank.
  • an electron discharge tube grid structure comprising the steps of winding iron and tungsten ribbons to form a disc structure comprised of interleaving spiraloid members, brazing together said ribbons to rigidity said disc, grinding both faces of said disc to transform said disc to a desired thickness, plating said ground faces, cutting a sector from said plated disc, edgegrinding said sector into a circular grid blank, mounting and brazing said grid blank in a mounting ring, grinding said mounted grid blank to a finished thickness, and chemically removing the plating and iron from said grid blank to form tungsten vanes supported in said mounting ring.
  • a method of fabricating a grid for electron discharge devices comprising the steps of forming a disc-like structure having arcuate members of desired grid material separated by arcuate members of material different from said desired grid material, bonding said arcuate members together to consolidate said disc-like structure, removing a section from said disc-like structure to form a suitable grid blank of desired grid configuration having arcuate laminated elements of said members, bonding a supporting means to said grid blank to support the arcuate elements of said desired grid material, and removing from said grid blank, elements of said material different from said desired grid material to form a rigid grid structure having spaced arcuate grid elements mounted in said supporting means.
  • a method of forming a grid structure for electron discharge tubes comprising the steps of winding tight interleaving spiraloid members from ribbons of dissimilar materials, one of said materials being of the desired grid material and the other of said materials being a temporary material to be subsequently removed, the spiraloid members of said desired material being separated by the spiraloid members of said other material, bonding said spiraloid members of said ribbons together to form a rigid disc-like structure, cutting from a sector of said disc-like structure, a grid blank comprising arcuate laminations of ribbons of said dissimilar materials bonded together, bonding the ends of said arcuate laminations to a supporting means, and removing said temporary material present in said grid blank to reduce said blank to a set of spaced arcuate ribbon portions mounted in said supporting means.
  • a method of forming a grid structure for electron discharge tubes comprising the steps of winding first and second chemically dissimilar metallic ribbons into a disclike structure comprised of interleaving spiraloid mem bers, the spiraloid member of said first metallic ribbon being separated by the spiraloid member of said second metallic ribbon, brazing said spiraloid members to form a rigid structure, cutting a sector from said structure to form a grid blank of desired configuration and size, mounting and brazing said grid blank to a supporting frame, and etching the mounted section to remove portions of said second chemically dissimilar metallic ribbon present therein.
  • a method of fabricating a grid for electron discharge devices comprising the steps of winding at least two elongated members of dissimilar materials into a substantially flat structure having tight interleaving convoluted members, one of said materials being of desired grid material and the other of said materials being a temporary material to be subsequently removed, the members of desired material being separated by members of said other material, bonding said convoluted members to consolidate said substantially flat structure, removing a section from said structure to form a grid blank of desired configuration, said grid blank being comprised of laminated elements of said members, bonding the ends of the elements of desired grid material to a grid supporting means, and removing the elements of said other material present in said grid blank to reduce said blank to a set of spaced elements of desired grid material mounted in said supporting means.

Description

Oct. 25, 1955 D. E. KENYON 2,721,952
GRID STRUCTURE AND THE PROCESS OF MAKING Filed May 14, 1952 ATTORNEY United States Patent GRID STRUCTURE AND THE PROCESS OF MAKING David E. Kenyon, Huntington, N. Y., assignor to Sperry Rand Corporation, a corporation of Delaware Application May 14, 1052 Serial No. 287,705
11 Claims. (Cl. 313-348) The present invention relates to minute grid electrodes for extremely high frequency electron tubes such as microwave klystrons and triodes, for example. This application is a continuation-in-part of application Serial No. 155,432, filed April 12, 1950, now abandoned, by the same inventor, and assigned to the same assignee.
It is customary to design grids for klystrons and related microwave tubes in such a way as toprovide for minimum electron interception, maximum mechanical stability, and relative insensitivity to high operating temperatures. For klystron tubes operating in the range of frequency of 3000 to 6000 megacycles, a variety of grid designs have been successfully used, prominent among which are vane type grids. These usually comprise cantilever-type vanes attached to the cylindrical interior surface of a grid mountingring and projecting inwardly part way toward the center thereof. In one. prior grid construction suitable for grids of the order of one-half inch in diameter, for use in microwave tubes operating in. frequency ranges such as set forth above, grids have been jig-assembled with arched. vanes extending across the grid ring interior. Each vane. is attached: at both ends to the ring interior surface by solder junctions of bent tabs at the. vane ends.
The present invention is concerned with grids of a much fined order of size, viz, of the order of onertenth inch diameter and smaller. Grids of such small size are required in klystrons, for instance, operating at wavelengths of the order of one centimeter (frequencies of the. order of 30,000 megacycles per second). In grids of this order of size, the vane. elements are so fine as to be, hardly visible to the naked eye, strongly militating against, attempts at, jig assembly of individual grid pieces.
In accordance with the present invention, minutev grids possessing the aforementioned attributes of a good electrode are produced by winding a pair of unlike metal strips.v into a, spiraloid form, bonding. the strips together into a rigid disc, cutting from sectors thereof, a plurality of discs each having a diameter which is a fraction of the diameter of the original rigid disc, mounting each of these discs in a conformal ring, bonding the disc and ring together, and removing, by etch n the material of one ofthe two original metal strips, to leave thin corre spondingly curved arcuate vanes of the desired material. Each vane element extends across the interior of the grid' ring, free from any bent tabs, and is bonded directly at its. transverse end surfaces to the'inner surface of the E An object. of the present invention, therefore, is to ICC tion, has relatively high mechanical stability and ruggedness, and very low electron interception.
Still another object of the invention is to provide a workable process for fabricating grids of the abovementioned type.
Other objects and advantages of this invention will become apparent from the following specification, taken in connection with the accompanying drawings wherein the invention is embodied in concrete form.
in the drawings,
Fig. l is an enlarged plan view of a disc structure comprised of interleaved spiraloid members, formed according to the present invention at an early stage of fabrication of the grid;
Fig. 2 is a vertical sectional view taken along lines 2-2 of Fig. 1;
Fig. 3 shows a sector cut from the structure of Fig. lon the lines 33 thereof, and indicates where a circular portion is derived therefrom;
Fig. 4 is a plan view of a circular section of Fig. 3 after a grinding operation;
Fig. 5 is a plan view of the structure of Fig. 4 supported in a mounting means;
Fig. 6 is a plan view of a completed grid structure according to the present invention;
Fig. 7 is a vertical section of Fig. 6 taken along lines 77 thereof;
Fig. 8. is a perspective view of a form of apparatus suitable for use in carrying out a part of the method of the instant invention;
Fig. 9 is an elevational view, partly in longitudinal sec,- tion, of the apparatus of Fig. 8; and
Fig. 10 is a cross sectional view of the structure of Fig. 9 taken along lines 10-10 thereof.
Referring to Figs. 1 and 2, disc 16 is shown, whichis formed by winding two ribbon- like members 17 and 18 together to prov de a fiat disc structure comprised of spiraloid. or convoluted interleaved members. Members 17 and 13 are constituted of continuous strips of. ribbon of different metals, ribbon 17 being of iron, for example, and ribbon 18 being of tungsten, molybdenum, or other suitable grid material. In order to provide a mechanically rigid discv 16, adjacent portions of members 17' and 18 may be joined together by brazing with a suitable brazing material such as copper, cupro-nickel or manganese.
Referring to. Fig. 2, the upper and lower faces 20 and 25, respectlvely, of the disc 16 may be ground to a finished or desired grid thickness or axial depth, such as indicated at 30. instead of grinding to a finished dimension at this stage, the faces 20 and 25 may be ground merely to insure that each face is perfectly fiat and planar. The ground surfaces preferably are immediately provided with a protective plating, such as chromium. The plated disc is then heated, if desired, in wet hydrogen at low heat, approximately 800 C., in order to oxidize the chromium.
The disc 16, after grinding and plating, is cut into sectors, one of which is shown in Fig. 3, by employing an abrasive wheel or other suitable cutting apparatus- It has been found that as many as 10 usable sectors may be cut from a single disc such as 16, depending upon its perfection and size.
The sector, such as shown in Fig. 3, is then mounted between two collinear pins (not shown) which frictionally support the sector at the faces thereof. are synchronously rotated, thereby rotating the sector. A grinding mechanism (not shown) is employed to. edge grind the rotating sector until a disc is formed as is Both pins shown in Fig. 4. During this operation care should be taken to insure that the oxidized chromium surface is not damaged by abrasion. The resulting grid blank 21 has both faces protected by oxidized chromium, with the edge a bright, ground surface.
Referring to Fig. 5, the grid blank 21 is surrounded by'a tightly fitting ring 22 and apertured disc 23. Ring 22 may be composed for instance, of gold, copper or nickel. Apertured disc 23 is comprised of iron, steel, or other suitable material.
If a gold ring is employed, the assembly is brazed at a temperature suitable for fusing the ring 22 to the periphery of grid blank 21 without destroying the ring. If ring 22 is of copper, it is preferable to employ a very thin layer of gold solder between the periphery of grid blank 21 and the ring 22 preparatory for the brazing operation. The gold solder, which is a gold alloy, has a lower melting point than the copper. If ring 22 is of nickel, copper powder is utilized to braze the ring 22 to the grid blank 21. In lieu of copper powder, the inner surface of the ring of nickel could be copper plated. The oxidized chromium plating prevents any of the brazing material from flowing onto either face of the grid blank 21.
During the above-described mounting operation of grid blank 21, the assembly is preferably fired in a hydrogen atmosphere, as with a hydrogen bell jar (not shown). The use of a hydrogen atmosphere is found beneficial to insure that the molten metal wets the end surfaces of the members comprising the grid blank 21, particularly the transverse or cross-cut ends of members 18. If such a procedure is not followed when dealing with extremely closely spaced surfaces, such as the cylindrical outer surface of grid blank 21 and the cylindrical inner surface of the ring 22, the surface tension of the molten metal customarily prevents it from flowing sufliciently to form a suitable bond. The oxidized chromium coating protects the faces of the grid blank 21 and prevents the molten brazing material from wetting either face of the grid blank 21.
After brazing ring 22 to the periphery of grid blank 21, the faces of the assembly comprising grid blank 21, ring 22, and apertured disc 23 may be ground to a finished grid thickness, if the grinding process described in referring to dimension 30 in Fig. 2 was not carried out.
After the mounting and grinding operations above, the apertured disc 23 is removed from the rest of the structure. This can be done by a cutting operation, after which the ring 22 is polished to remove any peripheral burrs that may exist after the cutting. The structure is then etched in a suitable bath of hydrochloric or sulphuric acid, for example, to remove the iron vane elements. If hydrochloric acid is employed for etching, it will also remove any chromium on the faces of grid blank 21, if the face grinding process supra was not undertaken. The structure may also be electro-etched in a bath of sodium hydroxide, if desired, to remove burrs which remain after any of the face grinding processes.
Instead of cutting the apertured disc 23 from the grid blank 21 and ring 22, it may be removed by the same etching process as is employed to remove the iron vanes. In the case where a nickel grid ring is employed the structure may also be etched in a bath of ammonium hydroxide and hydrogen peroxide to remove any remnants of the copper brazing material which may exist on the faces of the grid blank 21 and ring 22.
The result of the foregoing procedure is an electronpermeable structure or grid 24, as shown in Fig. 6, which has a plurality of arcuate members or vanes 18, the transverse or cross-cut ends of which abut and are supported by a mounting means, such as ring 22.
Grids of the above-described type are capable of fabrication in extremely small sizes. Examples of the minute dimensions of a few of the highly successful grids. Of 1 .1%
present invention made according to the novel method disclosed herein are set forth below:
0. D. I. D. Axial vane Vane Grid Grid Depth spacing Thick- Ring, Ring, of Gr1d, inch ness, inch inch inch inch This method allows independent control of any and all of the above dimensions.
Referring to Fig. 6, it will be noted that grid 24 comprises curved vanes 18 which form a section of a flat spiraloid structure. Each vane has its transverse or crosscut ends supported by ring member 22. There is uniform spacing between vanes. Each of the vanes 18 has a width greatly in excess of its thickness, with the width dimension of each vane oriented in a direction parallel to the axis of the ring 22. Accordingly, the orientation of the vanes 18 is such as to provide ample mechanical rigidity and strength for the minute size thereof, and at the same time provide a grid structure 24 which presents a minimum electron beam intercepting area.
If desired, the thickness of the vanes 18 may be reduced by a suitable etching fluid, such as by treating the grid 24 with molten potassium nitrate. However, the action with this treatment is quite rapid. In such operations designed to reduce the thickness of the vanes 18, care must be taken to ensure that the structure of the vanes 18 is not impaired. If the action is permitted to progress too far the vanes 18 may neck down at a point and break. It has been found possible and practical to reduce the vanes 18 to one-half their original thickness.
Referring to Figs. 8 through 10, jig 28, suitable for use in fabricating the disc 16 of Fig. 1, has a body portion 29 with a reduced-diameter continuation 31. The continuation 31 is formed with an internally-threaded portion 32 for cooperation with screw 33. The screw 33 together with washer 34 and continuation 31 is effective for maintaining the cap 36 of the jig 28 rigid against axial movement relative to the body portion 29. Between the body portion 29 and the cap 36 is a circular slotted washer 37, the slot 40 of which is provided for receiving the end 19 of the iron ribbon 17 in order to secure it during the winding operation. Although washer 37 is shown as circular it is obvious that the periphery thereof could have an oval shape, or even substantially flat portions. On one side of the slotted washer 37 is positioned an enlarged washer 38, the diameter of which is preferably greater than that of body portion 29 to facilitate the removal of the disc 16 from the jig 28. On the other side of the slotted washer 37 is placed a disc 39 of suitable brazing material, such as copper, cupro-nickel, or
manganese.
The end 19 of the iron ribbon 17 may be inserted into the slotted portion 40 of washer 37, with the tungsten ribbon 18 resting beneath the iron ribbon 17. If desired, the end 19 of ribbon 17 may be initially bent to cooperate with the slot 40 in order to facilitate the start of the winding operation. By rotating the jig 28 about its longitudinal axis, the ribbons 17 and 18 may be wound together: Aiterthe space bctweem the enlarged'washer38 and disc 33 is filled with the altegnate, interleaved layers of ironand;tungstemribbonsHand 1'8, the'free end-of one 017- bothof the ribbons 1 7 and 18- may be wrapped around or-pinched over'arotatable securing member 41, whichmember-41 is: rotatable about an axis disposedfiat' right-angles to thelongitudinal axis-of the 28: Stop pin 42 limits the swing of the securingmember-ll, toprevent 'themember '41 from rotating therebeyond.
While the ribbon-members 1-7 and'181are mounted, on the jig 28; as shown mostclearly in Fig. 1,0, the assembly maybe-fired in a hydrogen atmosphere by use of a 'h-ydrogen'belljar. During'stich a process, thefdisc39melts to solidly braze together the iron and tungsten ribbons'17 and- 18; At'the sameg time, the heat'involved in thejfusing operation iseflective for removing stresses from the iron and-tungsten;1 ibbonslT'and- 18, After the formation of the sol-idly brazed disc11'6,,it'm%y'be removedfrom the jig 28 by disengaging the cap'36-I The enlarged washer 38 facilitates this operation.
If desired, the removal of! stresses and-the: joining tosether of the ribbon membersl' ns- .18. ma be effected in separate operations. Under such circumstances, the disc.39j, which. constitutes thebrazing, material, maybe omitted. from thejig. 28. .After. thewin'ding operation, the ribbons. 17 and. 18. may. be subjectedinitial-ly to high temperature. A small. piece of coppenmay. be placed prior to-the application of. heatat the-end fthe iron ribbon 17. most remote from. the center. of the spiral configuration. Such apiece of. copper, after. melting and subsequent solidification, is efiective for holding together the spiral of iron and tungsten ribbons 17 and 18, thereby facilitating its removal from the jig 28. Subsequently, the assembly may be fired with a suitable brazing material to solidly braze together the iron and tungsten ribbons 17 and 18.
The ribbons 17 and 18 of the disc 16 may be brazed or joined together in a somewhat different manner by employing, for instance, a copper-plated iron ribbon in place of the previously mentioned iron ribbon 17. Disc 39 may then be omitted. During the firing operation, the copper plating melts, acting as a brazing flux to join together the spiraloid members 17 and 18. However, the resulting structure may not be as solid as that provided by the other techniques discussed herein.
Since many changes could be made in the above construction and many apparently widely different embodiments of this invention could be made without departing from the scope thereof, it is intended that all matter contained in the above description or shown in the accompanying drawings shall be interpreted as illustrative and not in a limiting sense.
What is claimed is:
1. An electron permeable grid structure comprising a ring member having an inner diameter of less than approximately 0.1 inch, a plurality of spaced curved vane elements mounted within said ring member, said van elements being curved in the same direction within a plane containing said ring member, said plane being perpendicular to the axis of said ring member, the width dimension of each vane element extending in a direction substantially parallel to the axis of said ring member, the transverse ends of said vane elements directly abutting the inner surface of said ring member and being bonded thereto.
2. An electron permeable grid structure comprising a ring member having an inner diameter of less than approximately 0.1 inch, a plurality of arcuate vane elements mounted within said ring member, said vane elements being uniformly spaced and curved in the same direction within a plane containing said ring member, said plane being perpendicular to the axis of said ring member, each of said vane elements having substantially the same crosssectional area with the longer dimension of each crosssectional area extending in a direction substantially parallel to the axis of said ring member, the transverse ends .6 of said vane elements directly abutting the inner-surface of said ring member andbeing bonded thereto,
3; An electron permeable grid; structure comprising a,
ring member having an, inner; diameter of less than proximately 0.1 inch, a plurality off spaced curved vane elements mounted within said ring membersaid vane elements being curved in thesame direction within a planecontaining said ring member, said plane being perpendicular to the axis of-i'said' ring member, each, Qfisaidvane elementshaving substantially the same cross sectional area with-thelong er dimension of each .c1;osssectional area extending in a direction substantially par,- allel to the axis of saidi'ring member, the transverse ends of said vane elements abutting the inner surface, of'said ring member andbeingbonded' thereto, the corresponding narrow edges of said vane, elements having polished coplanar surfaces. 7 p
t; A grid structure comprising a plurality offspaeedp curved metallic ribbon,elements,mountediedgewise within a supporting'member, saidsupporting member having i e d e v su faces e m x m m nea stanc bet'weenany two points on said inner surface of said sup; porting member being'l'ess thanapproximately 0.1 inch, said ribbon elements being curvediin the same direction within aplane containing said supporting-member, each of said ribbonelements having substantially the same cross-sectional area with their transverse ends directly abutting-and: joining A the inner-surface of: said supporting member;
i In. electrompermeable. apparatus. having an: axis, a circularly-shaped mounting ring symmetrically disposed about said axis, said ring having an inner diameter of less than approximately 0.1 inch, and a plurality of spaced metallic vanes having cross-cut ends directly abutted and supported by said ring, each of said vanes being relatively Wide compared to the thickness thereof with the wide dimension oriented in a direction parallel to said axis, whereby a relatively small cross-sectional area is presented to an electron beam aligned with said axis, said vanes forming a section of a fiat spiraloid structure.
6. A method of forming an electron discharge tube grid structure comprising the steps of ,forming a disc comprised of interleaving spiraloid ribbon members of different metals, brazing said members together to rigidity said disc, cutting a grid blank from a sector of said disc, mounting said grid blank in a mounting ring, and removing elements of one of said metals which constitute part of said grid blank.
7. The method of forming an electron discharge tube grid structure comprising the steps of winding iron and tungsten ribbons to form a disc structure comprised of interleaving spiraloid members, brazing together said ribbons to rigidity said disc, grinding both faces of said disc to transform said disc to a desired thickness, plating said ground faces, cutting a sector from said plated disc, edgegrinding said sector into a circular grid blank, mounting and brazing said grid blank in a mounting ring, grinding said mounted grid blank to a finished thickness, and chemically removing the plating and iron from said grid blank to form tungsten vanes supported in said mounting ring.
8. A method of fabricating a grid for electron discharge devices comprising the steps of forming a disc-like structure having arcuate members of desired grid material separated by arcuate members of material different from said desired grid material, bonding said arcuate members together to consolidate said disc-like structure, removing a section from said disc-like structure to form a suitable grid blank of desired grid configuration having arcuate laminated elements of said members, bonding a supporting means to said grid blank to support the arcuate elements of said desired grid material, and removing from said grid blank, elements of said material different from said desired grid material to form a rigid grid structure having spaced arcuate grid elements mounted in said supporting means.
9. A method of forming a grid structure for electron discharge tubes, comprising the steps of winding tight interleaving spiraloid members from ribbons of dissimilar materials, one of said materials being of the desired grid material and the other of said materials being a temporary material to be subsequently removed, the spiraloid members of said desired material being separated by the spiraloid members of said other material, bonding said spiraloid members of said ribbons together to form a rigid disc-like structure, cutting from a sector of said disc-like structure, a grid blank comprising arcuate laminations of ribbons of said dissimilar materials bonded together, bonding the ends of said arcuate laminations to a supporting means, and removing said temporary material present in said grid blank to reduce said blank to a set of spaced arcuate ribbon portions mounted in said supporting means.
10. A method of forming a grid structure for electron discharge tubes, comprising the steps of winding first and second chemically dissimilar metallic ribbons into a disclike structure comprised of interleaving spiraloid mem bers, the spiraloid member of said first metallic ribbon being separated by the spiraloid member of said second metallic ribbon, brazing said spiraloid members to form a rigid structure, cutting a sector from said structure to form a grid blank of desired configuration and size, mounting and brazing said grid blank to a supporting frame, and etching the mounted section to remove portions of said second chemically dissimilar metallic ribbon present therein.
11. A method of fabricating a grid for electron discharge devices, comprising the steps of winding at least two elongated members of dissimilar materials into a substantially flat structure having tight interleaving convoluted members, one of said materials being of desired grid material and the other of said materials being a temporary material to be subsequently removed, the members of desired material being separated by members of said other material, bonding said convoluted members to consolidate said substantially flat structure, removing a section from said structure to form a grid blank of desired configuration, said grid blank being comprised of laminated elements of said members, bonding the ends of the elements of desired grid material to a grid supporting means, and removing the elements of said other material present in said grid blank to reduce said blank to a set of spaced elements of desired grid material mounted in said supporting means.
References Cited in the file of this patent UNITED STATES PATENTS 2,157,050 Bilger et al May 2, 1939 2,169,937 Wempe Aug. 15, 1939 2,203,315 Vivie June 4, 1940 2,261,154 Hansen et al Nov. 4, 1941 2,296,885 Vance Sept. 29 1942 2,499,977 Scott Mar. 7, 1950 2,515,267 Salisbury July 18, 1950
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Cited By (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2921363A (en) * 1955-06-30 1960-01-19 Bell Telephone Labor Inc Fabrication of grid structures for electron discharge devices
US2988667A (en) * 1957-08-20 1961-06-13 Eitel Mccullough Inc Grid structure and method of making the same
US3123900A (en) * 1964-03-10 Method of manufacture of a flow element or pulsation dampener
US3164740A (en) * 1960-04-29 1965-01-05 Rca Corp Electron tube grids and method of making the same
US3186884A (en) * 1960-05-02 1965-06-01 Philips Corp Method of manufacturing grid plates
US3215512A (en) * 1961-06-09 1965-11-02 Texas Instruments Inc Composite refractory articles
DE1216439B (en) * 1962-01-11 1966-05-12 Hitachi Ltd Process for the production of extremely small grids with flat strut-like bars for electrical discharge vessels
US3275428A (en) * 1963-05-21 1966-09-27 American Optical Corp Method of making honeycomb structure
US3294504A (en) * 1962-03-06 1966-12-27 Mosaic Fabrications Inc Method of making fiber bundles
US3319318A (en) * 1964-02-24 1967-05-16 Stanford Research Inst Thin gas tight window assembly
US3371407A (en) * 1964-02-21 1968-03-05 Power Jets Res & Dev Ltd Method of producing a composite metallic material billet
US3491429A (en) * 1967-08-31 1970-01-27 Us Time Corp The Method of construction of a rate gyroscope
US3650718A (en) * 1969-11-14 1972-03-21 Westinghouse Electric Corp Fusion method for spaced conductive element window
US4184350A (en) * 1978-06-26 1980-01-22 Sun Chemical Corporation High-production method and apparatus for making spiral convolution electrical heating coils
US4969265A (en) * 1988-09-06 1990-11-13 Calsonic Corporation Method of producing metal support for exhaust gas catalyst

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2157050A (en) * 1937-08-20 1939-05-02 Cuno Eng Corp Igniter coil manufacture
US2169937A (en) * 1937-02-15 1939-08-15 Wempe Bernhard Method of producing perforated metal sheets
US2203315A (en) * 1937-03-30 1940-06-04 Rca Corp Apparatus for manufacturing condenser electrodes
US2261154A (en) * 1939-07-22 1941-11-04 Univ Leland Stanford Junior Grid structure for high frequency apparatus
US2296885A (en) * 1941-06-28 1942-09-29 Bell Telephone Labor Inc Electron discharge device
US2499977A (en) * 1943-11-03 1950-03-07 Gen Electric Method of forming grid-like structures
US2515267A (en) * 1947-04-10 1950-07-18 Sperry Corp Grid structure and method of fabrication

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2169937A (en) * 1937-02-15 1939-08-15 Wempe Bernhard Method of producing perforated metal sheets
US2203315A (en) * 1937-03-30 1940-06-04 Rca Corp Apparatus for manufacturing condenser electrodes
US2157050A (en) * 1937-08-20 1939-05-02 Cuno Eng Corp Igniter coil manufacture
US2261154A (en) * 1939-07-22 1941-11-04 Univ Leland Stanford Junior Grid structure for high frequency apparatus
US2296885A (en) * 1941-06-28 1942-09-29 Bell Telephone Labor Inc Electron discharge device
US2499977A (en) * 1943-11-03 1950-03-07 Gen Electric Method of forming grid-like structures
US2515267A (en) * 1947-04-10 1950-07-18 Sperry Corp Grid structure and method of fabrication

Cited By (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3123900A (en) * 1964-03-10 Method of manufacture of a flow element or pulsation dampener
US2921363A (en) * 1955-06-30 1960-01-19 Bell Telephone Labor Inc Fabrication of grid structures for electron discharge devices
US2988667A (en) * 1957-08-20 1961-06-13 Eitel Mccullough Inc Grid structure and method of making the same
US3164740A (en) * 1960-04-29 1965-01-05 Rca Corp Electron tube grids and method of making the same
US3186884A (en) * 1960-05-02 1965-06-01 Philips Corp Method of manufacturing grid plates
US3215512A (en) * 1961-06-09 1965-11-02 Texas Instruments Inc Composite refractory articles
DE1216439B (en) * 1962-01-11 1966-05-12 Hitachi Ltd Process for the production of extremely small grids with flat strut-like bars for electrical discharge vessels
US3294504A (en) * 1962-03-06 1966-12-27 Mosaic Fabrications Inc Method of making fiber bundles
US3275428A (en) * 1963-05-21 1966-09-27 American Optical Corp Method of making honeycomb structure
US3371407A (en) * 1964-02-21 1968-03-05 Power Jets Res & Dev Ltd Method of producing a composite metallic material billet
US3319318A (en) * 1964-02-24 1967-05-16 Stanford Research Inst Thin gas tight window assembly
US3491429A (en) * 1967-08-31 1970-01-27 Us Time Corp The Method of construction of a rate gyroscope
US3650718A (en) * 1969-11-14 1972-03-21 Westinghouse Electric Corp Fusion method for spaced conductive element window
US4184350A (en) * 1978-06-26 1980-01-22 Sun Chemical Corporation High-production method and apparatus for making spiral convolution electrical heating coils
US4969265A (en) * 1988-09-06 1990-11-13 Calsonic Corporation Method of producing metal support for exhaust gas catalyst

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