US2657021A - Apparatus for the mechanical production of acoustic vibrations for use in emulsification, dispersion or like processes - Google Patents

Apparatus for the mechanical production of acoustic vibrations for use in emulsification, dispersion or like processes Download PDF

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US2657021A
US2657021A US298978A US29897852A US2657021A US 2657021 A US2657021 A US 2657021A US 298978 A US298978 A US 298978A US 29897852 A US29897852 A US 29897852A US 2657021 A US2657021 A US 2657021A
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jet
blade
outlet
liquid
emulsification
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US298978A
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Eric C Cottell
John E Goodman
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/08Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J19/10Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing sonic or ultrasonic vibrations
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F31/00Mixers with shaking, oscillating, or vibrating mechanisms
    • B01F31/80Mixing by means of high-frequency vibrations above one kHz, e.g. ultrasonic vibrations
    • B01F31/81Mixing by means of high-frequency vibrations above one kHz, e.g. ultrasonic vibrations by vibrations generated inside a mixing device not coming from an external drive, e.g. by the flow of material causing a knife to vibrate or by vibrating nozzles
    • GPHYSICS
    • G10MUSICAL INSTRUMENTS; ACOUSTICS
    • G10KSOUND-PRODUCING DEVICES; METHODS OR DEVICES FOR PROTECTING AGAINST, OR FOR DAMPING, NOISE OR OTHER ACOUSTIC WAVES IN GENERAL; ACOUSTICS NOT OTHERWISE PROVIDED FOR
    • G10K7/00Sirens
    • G10K7/005Ultrasonic sirens
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S116/00Signals and indicators
    • Y10S116/19Wave generator with resonating element

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • Engineering & Computer Science (AREA)
  • Acoustics & Sound (AREA)
  • Multimedia (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • Organic Chemistry (AREA)
  • Physical Water Treatments (AREA)

Description

2,657,021 OF ACOUSTIC DISPERSION CHANI IN LIK ed J W L Amm T m Ewm LWW. a T m E CE c w .E U EH w RF 0 s O NH AA RR m 3 w v 5A 9 1 7 2 .L c O E PROCESSES uly 15, 1952 OR Fil Patented Oct. 27, 1953 APPARATUS FOR THE MECHANICAL PRO- DUCTION OF ACOUSTIC VIBRATION S FOR USE IN EMULSIFICATION, DISPERSION OR LIKE PROCESSES Eric C. Cottell, Ilkley, and John E. Goodman, Stanks, Leeds, England Application July 15, 1952, Serial No. 298,978 In Great Britain February 22, 1951 Claims. 1
This invention relates to apparatus for the mechanical production of acoustic vibrations generally in the ultrasonic range in a manner suitable particularly for use in the emulsification or homogenisation of oil and water and suspensions of solid matter in liquids and like purposes.
The apparatus makes use of the known principle of mechanical production of ultrasonic or like acoustic vibrations which is used in a liquid whistle and which consists essentially in causing a jet of liquid to impinge on a vibratory member so as to produce high frequency vibrations, but applies this principle in a practical arrangement capable of being put to numerous industrial uses and particularly in a readily portable form.
According to the invention the apparatus consist in a jet-form structure to which liquid can be supplied under pressure and having one or more restricted outlets or nozzles which direct the liquid stream against a blade or like vibrator so as to produce acoustic vibrations generally in the ultrasonic range, the jet-form structure and vibrator being mounted so as to be readily introduced into or close to the medium to be treated.
Preferably a blade or other form of vibrator is mounted on the jet-form structure which in turn is mounted on the end of the fluid supply pipe or in a frame or on arms and such pipe, frame or arms can be adapted for fixing upon a vessel which is to contain the medium to be treated or can be swung into and out of working position as desired.
In order that the invention may be clearly understood and readily carried into eifect the same will now be more fully described with reference to and by the aid of the accompanying drawings, wherein:
Figures 1 and 2 are respectively an elevation and plan of one form of portable apparatus according to the invention shown mounted on the side of a mixing pan.
Figure 3 is an elevation mainly in section of the body of the jet-form structure.
Figure 4 is an elevation of a bell-like nose piece forming the outer end of the jet-form structure.
Figure 5 is a plan of the body shown in Figure 3.
Figure 6 is a transverse section taken on the line A-A in Figure 5 showing the detail of the jet-form outlet.
In the illustrated embodiment of the invention a rotary pump l and electric motor 2 are 2 mounted as a unit in a casing from which depend suction and delivery pipes 3, 4. The lower end of the delivery pipe 4 has connected to it the jet-form structure which may be moulded in a suitable synthetic material or cast in suitable metal.
This jet-form structure is shown as consisting of a body in halves 5, 6 with an outer covering 1, or alternatively the two halves can be bolted together, the body being connected at the inner end by a union 8 to the delivery pipe 4 and having an internal passage 9 which is circular at its inner end and gradually flattens out in smooth contours towards the outer end where it forms a slit like outlet l0. This outlet I0 may vary somewhat in shape, but as illustrated its section is represented by the intersection of two circles of the same radius which radius is such that a straight line joining the two points of intersection is in the ratio of 50:1 relative to the height of the rightangular upright drawn from the centre of such line to the circumference of one circle. With the dimensions w and t indicated in Figure 6, the diameter of each circle would be represented by In any event the shape of outlet will be designed with the object of producing a jet of liquid best adapted to co-operate with the vibratory blade.
The blade H is preferably made of spring steel of the shape illustrated with a hollow ground edge on which the liquid jet impinges. This blade is clamped by narrow strips and screws I2 to two arms l3 formed with or secured to the body half 6, so that the blade is free to vibrate at its own frequency without support along its sharpened edge.
A resonant bell or nose piece I i can be screwed onto the threaded ends of the body halves to surround the blade and its mounting, and this bell has its internal bore reduced to form an open circular end It of a diameter approximately equivalent to the length of the jet-form outlet I0. By this means the eiiect of the vibration may be amplified and a cavity maintained in the bell by the ejector eifect of the liquid passing at high speed across the blade and through the bell. This may maintain the velocity of the jet across the blade at a faster rate than if it were immersed in the liquid without the bell attached, owing to the inertia of the liquid itself slowing down the jet when it is not passing through the bell.
The casing of the motor 2 is shown with a swivel bracket [6 by which the whole apparatus can be pivotally mounted on the side of a pan or like vessel I1 to contain the liquid to be treated and this bracket can include readily detachable clamping means to enable the apparatus to be moved at will. The apparatus can be counterbalanced by suitable means (not shown) so as to be readily lowered into the vessel. Alternatively the apparatus would be arranged for suspending above the vessel and lowering into it.
It is intended generally to operate the apparatus with the outlet and blade below the liquid level in the vessel, though it may operate just above the surface with the suction pipe 3 dipping below.
When operating with the apparatus the mixture is drawn into the pump and then expelled through the jet-form outlet at a pressure (say) of from 130 to 300 lbs., per square inch, impinging on the blade and deflecting it. The elasticity of the blade itself restores it to its normal position and it is again deflected in the opposite direction. This cycle continues at very high speed and ultrasonic oscillation results. Cavitation at the blade tip causes violent agitation of the liquid and consequent emulsification or such like due to very high pressures realised on the collapse of the cavities.
The pump can be provided with a by-pass to vary its capacity and, therefore, the pressure and intensity of the oscillations produced.
As an alternative a thick blade of concave wedge or other shape may be mounted on a torsion bar which would allow the blade to vibrate although too thick to oscillate due to its own elasticity. In such case there would be less likelihood of the blade breaking through fatigue.
It is believed that an apparatus according to the invention will be of more simple and compact construction than any at present employed in industry, and may have an extensive application in the pharmaceutical, cosmetic, textile, food. mineral preparation, brewing, oil, engineering and other industries.
Practical tests indicate that the apparatus will absorb only a small fraction of the power needed by equivalent emulsifiers of conventional types and its efficiency will enable less emulsifying agent to be used and produce a very finely divided suspension.
We claim:
1. Apparatus for producing emulsification or homogenisation of oil and water and suspensions of solid matter in liquids and like purposes by mechanically produced acoustic vibrations in or near the ultrasonic range, comprising in combination a jet-form structure having at least one restricted outlet or nozzle, a blade-like vibrator element having at least a portion thereof supported for vibratory movement and located with its thin edge in line with said outlet, means for passing the liquid to be treated under pressure through said jet-form structure and against the thin edge of said vibrator element so as to produce the acoustic vibrations, and means for introducing said jet-form structure and vibrator element into or close to the medium to be treated.
2. Apparatus for producing emulsification or homogenisation of oil and water and suspensions of solid matter in liquids and like purposes by mechanically produced acoustic vibrations in or near the ultrasonic range, comprising in combination a jet-form structure having at least one restricted outlet or nozzle, a blade-like vibrator element having at least a portion thereof capable of vibratory movement and mountedonsaid structure with its thin edge in line with said outlet, means for passing the liquid to be treated under pressure through a delivery pipe on which said structure is mounted and through said structure and against the thin edge of said vibrator element so as to produce the acoustic vibrations, and means for supporting said delivery pipe, jet-form structure and vibrator element in connection with a vessel which is to contain the medium to be treated so as to be capable of readily being moved into and out of working position.
3. Apparatus as called for in claim 2, including a jet-form structure having an internal passage which changes by smooth contours from a substantially circular inlet at the inner end to a slit-like outlet at the outer end, and a vibratory blade located substantially in the plane of said slit-like outlet so as to receive the jet of liquid against its free edge.
4. Apparatus as called for in claim 2, including a jet-form structure having an internal passage which changes by smooth contours from a substantially circular inlet at the inner end to a slit-like outlet at the outer end, and a vibratory blade located substantially in the plane of said slit-like outlet sov as to receive the jet of liquid against its free edge and a resonant bell or nose piece applied to the outer end ,of said jet-form structure and surrounding said blade and its mounting and having a circular opening in its outer end of a diameter approximately equivalent to the length of the jet-form outlet.
5. Apparatus for producing emuls fi n Qr homogenisation of oil and water and suspensions of solid matter in liquids and like purposes by mechanically produced acoustic vibrations in or near the ultrasonic range comprising in combination an electric motor and a pump driven thereby mounted as a unit, a suction pipe and a delivery pipe connected to and supported from said pump, a jet-form structure mounted on the outer end of said delivery pipe and having an internal passage which changes by smooth con-.- tours from a substantially circular inlet at the inner end to a slit-like outlet at the outer end, a thin vibratory blade clamped by its thicker edge to two arms projectin forwards from said jet-form structure and located with its sharpened edge opposite and parallel to said slit-like outlet so as to be vibrated by the liquid jet impinging on it, a resonant bell or nose piece applied to the outer end of said jet-form structure and surrounding said blade and its mounting and having a circular opening in its outer end of a diameter approximately equivalent to the length of said slit-like outlet, and disengageable means for supporting the complete apparatus in connection with a vessel to contain the liquid to be treated with the suction pipe dipping into said liquid and for enabling said apparatus to be lowered into and raised out of working position.
ERIC C. COTTELL. JOHN E. GOODMAN.
References Cited in the file of this patent UNITED STATES PATENTS 7 Number Name Date 1,445,427 Werner Feb. 13, 1923 1,678,225 Kincade July 24, 1928 2,005,800 OBoyle "June 25, 1935
US298978A 1951-02-22 1952-07-15 Apparatus for the mechanical production of acoustic vibrations for use in emulsification, dispersion or like processes Expired - Lifetime US2657021A (en)

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Cited By (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2713998A (en) * 1953-05-18 1955-07-26 Eicken Henri Means for emulsifying sizing and the like products
US2968584A (en) * 1956-10-31 1961-01-17 Corning Glass Works Glass tube cleaning
US3111278A (en) * 1960-10-04 1963-11-19 Nathan H Buschman Comminuting machine
US3123305A (en) * 1964-03-03 Hydrodynamic vibrative atomizer
US3169013A (en) * 1963-01-14 1965-02-09 John P B Jones Sonic emulsifying and homogenization apparatus
US3176964A (en) * 1961-01-05 1965-04-06 Sonic Eng Corp Method and apparatus for producing acoustic vibrations in fluids
US3211577A (en) * 1962-10-23 1965-10-12 Gen Electric Process for coating ferrous material with magnesium oxide
US3285579A (en) * 1963-05-09 1966-11-15 Guerin Robert Devices for homogenizing a mixture by ultra-sound vibrations
US3398944A (en) * 1966-01-28 1968-08-27 Macrosonics Corp Metallurgical processing apparatus
US3408050A (en) * 1966-01-13 1968-10-29 Sonic Eng Corp Apparatus for mixing fluids
DE1296439B (en) * 1965-08-27 1969-05-29 Sonic Eng Corp Device for generating sound vibrations in a flowing liquid
US3658302A (en) * 1968-12-31 1972-04-25 Louis Duthion Feed unit for a fuel burner
US3677525A (en) * 1969-12-31 1972-07-18 Sonic Dev Corp Pressure wave atomizing apparatus
US3687369A (en) * 1970-10-12 1972-08-29 North American Car Corp Cleaning apparatus

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1445427A (en) * 1922-02-11 1923-02-13 Ernest E Werner Method of producing emulsions
US1678225A (en) * 1926-10-28 1928-07-24 Jerry W Kincade Agitator for chemically purifying oil
US2005800A (en) * 1934-07-14 1935-06-25 Hugh Wright Mixing apparatus

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1445427A (en) * 1922-02-11 1923-02-13 Ernest E Werner Method of producing emulsions
US1678225A (en) * 1926-10-28 1928-07-24 Jerry W Kincade Agitator for chemically purifying oil
US2005800A (en) * 1934-07-14 1935-06-25 Hugh Wright Mixing apparatus

Cited By (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3123305A (en) * 1964-03-03 Hydrodynamic vibrative atomizer
US2713998A (en) * 1953-05-18 1955-07-26 Eicken Henri Means for emulsifying sizing and the like products
US2968584A (en) * 1956-10-31 1961-01-17 Corning Glass Works Glass tube cleaning
US3111278A (en) * 1960-10-04 1963-11-19 Nathan H Buschman Comminuting machine
US3176964A (en) * 1961-01-05 1965-04-06 Sonic Eng Corp Method and apparatus for producing acoustic vibrations in fluids
US3211577A (en) * 1962-10-23 1965-10-12 Gen Electric Process for coating ferrous material with magnesium oxide
US3169013A (en) * 1963-01-14 1965-02-09 John P B Jones Sonic emulsifying and homogenization apparatus
US3285579A (en) * 1963-05-09 1966-11-15 Guerin Robert Devices for homogenizing a mixture by ultra-sound vibrations
DE1296439B (en) * 1965-08-27 1969-05-29 Sonic Eng Corp Device for generating sound vibrations in a flowing liquid
US3408050A (en) * 1966-01-13 1968-10-29 Sonic Eng Corp Apparatus for mixing fluids
US3398944A (en) * 1966-01-28 1968-08-27 Macrosonics Corp Metallurgical processing apparatus
US3658302A (en) * 1968-12-31 1972-04-25 Louis Duthion Feed unit for a fuel burner
US3677525A (en) * 1969-12-31 1972-07-18 Sonic Dev Corp Pressure wave atomizing apparatus
US3687369A (en) * 1970-10-12 1972-08-29 North American Car Corp Cleaning apparatus

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