US2506326A - Article of tungsten and wrought copper joined by cast copper - Google Patents

Article of tungsten and wrought copper joined by cast copper Download PDF

Info

Publication number
US2506326A
US2506326A US722795A US72279547A US2506326A US 2506326 A US2506326 A US 2506326A US 722795 A US722795 A US 722795A US 72279547 A US72279547 A US 72279547A US 2506326 A US2506326 A US 2506326A
Authority
US
United States
Prior art keywords
copper
tungsten
joined
target
wrought
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
US722795A
Inventor
Roy L Adams
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
General Electric Co
Original Assignee
General Electric Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by General Electric Co filed Critical General Electric Co
Priority to US722795A priority Critical patent/US2506326A/en
Priority to GB4034/48A priority patent/GB648607A/en
Application granted granted Critical
Publication of US2506326A publication Critical patent/US2506326A/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Images

Classifications

    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J35/00X-ray tubes
    • H01J35/02Details
    • H01J35/04Electrodes ; Mutual position thereof; Constructional adaptations therefor
    • H01J35/08Anodes; Anti cathodes
    • H01J35/12Cooling non-rotary anodes
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00Stock material or miscellaneous articles
    • Y10T428/12All metal or with adjacent metals
    • Y10T428/12493Composite; i.e., plural, adjacent, spatially distinct metal components [e.g., layers, joint, etc.]
    • Y10T428/12771Transition metal-base component
    • Y10T428/12806Refractory [Group IVB, VB, or VIB] metal-base component
    • Y10T428/12826Group VIB metal-base component
    • Y10T428/1284W-base component
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00Stock material or miscellaneous articles
    • Y10T428/12All metal or with adjacent metals
    • Y10T428/12493Composite; i.e., plural, adjacent, spatially distinct metal components [e.g., layers, joint, etc.]
    • Y10T428/12771Transition metal-base component
    • Y10T428/12861Group VIII or IB metal-base component
    • Y10T428/12903Cu-base component
    • Y10T428/1291Next to Co-, Cu-, or Ni-base component

Definitions

  • the present invention comprises composite metal bodies consisting of tungsten and copper parts joined in good heat-conducting relation and thereby being adapted for use as targets in X-ray devices.
  • Target electrodes or targets as heretofore fabricated have consisted of a charge-receiving plate of tungsten imbedded in a backing plate of copper which functioned as a means for carrying away the heat which was generated by the impingement of high velocity electrons on the tungsten plate during the functioning of an X-ray tube containing such target electrode.
  • a plate of tungsten backed with copper has constituted both a discharge-receiving electrode and a wall-member in the evacuated envelope in which the electron discharge for producing X-rays was caused to operate. It was found that leakage of gas occurred from the exterior into the evacuated interior of such devices, which interfered with their proper functioning and in many cases caused complete failure.
  • the copper backing for the X-ray target consisted of copper solidified from fusion in the process of fabrication by casting copper against th target metal.
  • the entry of gas into the evacuated space appears to be due to slow molecular diffusion of gas (e. g. components of air) along the very slightly open grain boundaries characteristic of interdendritic shrinkage which occurs in some degree in all forms of cast or resolidified fused metal, the gas thereupon diffusing around the tungsten target into the evacuated space.
  • gas e. g. components of air
  • composite metal articles are constructed of tungsten joined to a body of wrought copper by an intermediate layer of fused copper (that is, copper resolidifled from fusion) which functions as a cementing layer uniting the tungsten or other target metal and wrought copper in good heat-conducting relation.
  • Fig. l is a side elevation of a high voltage X-ray outfit embodying my invention
  • Figs. 2, 3 and 4 are sectional views of different stages of target fabrication
  • Fig. 5 is a sectional view of a complete target.
  • Leakage of gas into the evacuated space within an X-ray apparatus has been found to be particularly troublesome in high voltage, high pow- 2 ered X-ray devices, such as shown for example in Fig. l, and described in detail in Charlton and Westendorp, U. S. Patent 2,144,524, patented January 17, 1939.
  • an extension tube i is provided leading from the main X-ray chamber 2.
  • a source of cathode rays (electrons) as for example, an incandescent filament (not shown in the drawing) is provided in the main chamber.
  • a beam of electrons which may be suitably focussed by well understood means, is directed upon the end wall 3 of the X-ray apparatus. The impact of the electrons on the target generates X-rays which pass through the target and are radiated to the exterior. It is important, therefore, that the target and backing plate should be as thin as practicable.
  • an elongated mass of wrought copper t which is dense and impervious to molecular diffusion of gas, is placed as shown in Fig. 2 into end-abutting relation to a plate 5 of tungsten, tantalum or other chosen refractory metal in a shallow graphite holder 6.
  • Encircling the mold is the primary winding '5 of an induction heater.
  • This winding when supplied with alternating current of suitable frequency (e. g. about 1,000 to 2,000 eye/sec.) induces sufiicient energy into the graphite holder and its contents to cause fusion of a thin layer 8 (Fig. 3) of the copper mass 4 which is immediately adjacent the tungsten disk.
  • the heating apparatus and its contents are surrounded during the fusion step with a reducing gas, such as hydrogen or a mixture of hydrogen and nitrogen.
  • a reducing gas such as hydrogen or a mixture of hydrogen and nitrogen.
  • the molten copper wets the tungsten and becomes intimately united therewith upon cooling.
  • the fusion does not extend an appreciable distance away from the tungsten disk, due to the good heat conductivity of the mass of copper i extending away from the heating zone.
  • the mass of copper with its attached plate of tungsten is removed from the induction heater and allowed to cool.
  • the plate of refractory metal and a desired portion 4' of the mass of copper to which the refractory metal has become joined is out off from the main mass 4 by any convenient mechanical means.
  • the final product is a plate of refractory metal backed by a plate 4 of wrought copper, which is joined to the refractory metal by a thin layer 8 of copper which has been fused and thereupon resolidified. As shown in Fig. 5 it is applied by welding or otherwise to the end of extension tube l which ordinarily consists oi copper.

Landscapes

  • X-Ray Techniques (AREA)
  • Analysing Materials By The Use Of Radiation (AREA)

Description

y 1950 R. L. ADAMS 2,506,326
ARTICLE OF TUNGSTEN AND WRO T COPPER JOINED CAST COP R Filed J 18, 1947 Fig.1
Fig.5.
Fig.2, l WC W6 MOSFERE F152. 4. 5
Inventor: Roy L. Adams,
by -z (MW His/Attorney.
Patented May 2, 1950 Roy L. Adams, Schenectady, N. Y., assignor to General Electric Company, a corporation of New York Application January 18, 1947, Serial No. 22,795
1 Claim.
The present invention comprises composite metal bodies consisting of tungsten and copper parts joined in good heat-conducting relation and thereby being adapted for use as targets in X-ray devices.
Target electrodes or targets as heretofore fabricated have consisted of a charge-receiving plate of tungsten imbedded in a backing plate of copper which functioned as a means for carrying away the heat which was generated by the impingement of high velocity electrons on the tungsten plate during the functioning of an X-ray tube containing such target electrode.
In some forms of high-poWered X-ray devices a plate of tungsten backed with copper has constituted both a discharge-receiving electrode and a wall-member in the evacuated envelope in which the electron discharge for producing X-rays was caused to operate. It was found that leakage of gas occurred from the exterior into the evacuated interior of such devices, which interfered with their proper functioning and in many cases caused complete failure.
In these devices the copper backing for the X-ray target consisted of copper solidified from fusion in the process of fabrication by casting copper against th target metal. The entry of gas into the evacuated space appears to be due to slow molecular diffusion of gas (e. g. components of air) along the very slightly open grain boundaries characteristic of interdendritic shrinkage which occurs in some degree in all forms of cast or resolidified fused metal, the gas thereupon diffusing around the tungsten target into the evacuated space.
As a consequence of my present invention I have provided an improved composite body of tungsten andcopper through which such diffusion of gas can not occur. In accordance with my invention composite metal articles are constructed of tungsten joined to a body of wrought copper by an intermediate layer of fused copper (that is, copper resolidifled from fusion) which functions as a cementing layer uniting the tungsten or other target metal and wrought copper in good heat-conducting relation.
My invention is illustrated by the accompanying drawing in which Fig. l is a side elevation of a high voltage X-ray outfit embodying my invention; Figs. 2, 3 and 4 are sectional views of different stages of target fabrication Fig. 5 is a sectional view of a complete target.
Leakage of gas into the evacuated space within an X-ray apparatus has been found to be particularly troublesome in high voltage, high pow- 2 ered X-ray devices, such as shown for example in Fig. l, and described in detail in Charlton and Westendorp, U. S. Patent 2,144,524, patented January 17, 1939. In such apparatus an extension tube i is provided leading from the main X-ray chamber 2. A source of cathode rays (electrons) as for example, an incandescent filament (not shown in the drawing) is provided in the main chamber. A beam of electrons which may be suitably focussed by well understood means, is directed upon the end wall 3 of the X-ray apparatus. The impact of the electrons on the target generates X-rays which pass through the target and are radiated to the exterior. It is important, therefore, that the target and backing plate should be as thin as practicable.
When copper is joined to a plate of tungsten, or other refractory metal, by casting fused copper against the plate of refractory metal, the crystallization shrinkage of the solidified copper causes the trouble heretofore noted. Wrought copper on the other hand is non-pervious to gas.
In carrying out my invention an elongated mass of wrought copper t, which is dense and impervious to molecular diffusion of gas, is placed as shown in Fig. 2 into end-abutting relation to a plate 5 of tungsten, tantalum or other chosen refractory metal in a shallow graphite holder 6. Encircling the mold is the primary winding '5 of an induction heater. This winding when supplied with alternating current of suitable frequency (e. g. about 1,000 to 2,000 eye/sec.) induces sufiicient energy into the graphite holder and its contents to cause fusion of a thin layer 8 (Fig. 3) of the copper mass 4 which is immediately adjacent the tungsten disk. Preferably the heating apparatus and its contents are surrounded during the fusion step with a reducing gas, such as hydrogen or a mixture of hydrogen and nitrogen. Under these conditions the molten copper wets the tungsten and becomes intimately united therewith upon cooling. The fusion, however, does not extend an appreciable distance away from the tungsten disk, due to the good heat conductivity of the mass of copper i extending away from the heating zone. The mass of copper with its attached plate of tungsten is removed from the induction heater and allowed to cool.
As indicated in Fig. 4, the plate of refractory metal and a desired portion 4' of the mass of copper to which the refractory metal has become joined is out off from the main mass 4 by any convenient mechanical means. The final product is a plate of refractory metal backed by a plate 4 of wrought copper, which is joined to the refractory metal by a thin layer 8 of copper which has been fused and thereupon resolidified. As shown in Fig. 5 it is applied by welding or otherwise to the end of extension tube l which ordinarily consists oi copper.
When a composite plate thus constructed is used as a target member in an evacuated X-ray device as shown in Fig. 1, slow entry of gas from the atmosphere into the evacuated interior of the X-ray tube through the composite target doesnot occur.
What I claim as new and desire to secure by Letters Patent of the United States is:
An X-ray device comprising an evacuated envelope and an X-ray target,v Said target con- REFERENCES CITED The following references are of record in the file of this patent:
UNITED STATES PATENTS Number Name Date 2*,013311 Hummel Sept. 3, 1935 15 2,019,599- Driggs Nov. 5, 1935 2,116,387 Briggs et a1. May 3, 1938
US722795A 1947-01-18 1947-01-18 Article of tungsten and wrought copper joined by cast copper Expired - Lifetime US2506326A (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
US722795A US2506326A (en) 1947-01-18 1947-01-18 Article of tungsten and wrought copper joined by cast copper
GB4034/48A GB648607A (en) 1947-01-18 1948-02-11 Improvements relating to target electrodes for x-ray devices

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US722795A US2506326A (en) 1947-01-18 1947-01-18 Article of tungsten and wrought copper joined by cast copper

Publications (1)

Publication Number Publication Date
US2506326A true US2506326A (en) 1950-05-02

Family

ID=24903412

Family Applications (1)

Application Number Title Priority Date Filing Date
US722795A Expired - Lifetime US2506326A (en) 1947-01-18 1947-01-18 Article of tungsten and wrought copper joined by cast copper

Country Status (2)

Country Link
US (1) US2506326A (en)
GB (1) GB648607A (en)

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2846753A (en) * 1951-09-28 1958-08-12 Gen Electric Method of making thin metal sections vacuum tight
US3066402A (en) * 1956-11-29 1962-12-04 Ingels Glenn Rex Method of and product for hard facing
US3180023A (en) * 1961-02-02 1965-04-27 Kaiser Aluminium Chem Corp Method of joining an electrically conductive metal to a refractory hard metal
US3245143A (en) * 1961-09-25 1966-04-12 Csf Method of producing a vacuum-tight joint of relatively thin parts
US3455663A (en) * 1966-03-24 1969-07-15 Mallory & Co Inc P R Composite metal joint and a copper-silver,titanium brazing alloy
EP0034768A2 (en) * 1980-02-12 1981-09-02 Kabushiki Kaisha Toshiba Method for manufacturing an anode of an X-ray tube
US20040046004A1 (en) * 2001-01-31 2004-03-11 Barnes John James Metallurgically bonded layered article having a curved surface

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2013411A (en) * 1932-06-04 1935-09-03 Westinghouse Lamp Co Pluro-metallic rod
US2019599A (en) * 1932-02-06 1935-11-05 Westinghouse Lamp Co Process for producing clad metals
US2116387A (en) * 1934-10-30 1938-05-03 Westinghouse Electric & Mfg Co Means and method of constructing x-ray anodes

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2019599A (en) * 1932-02-06 1935-11-05 Westinghouse Lamp Co Process for producing clad metals
US2013411A (en) * 1932-06-04 1935-09-03 Westinghouse Lamp Co Pluro-metallic rod
US2116387A (en) * 1934-10-30 1938-05-03 Westinghouse Electric & Mfg Co Means and method of constructing x-ray anodes

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2846753A (en) * 1951-09-28 1958-08-12 Gen Electric Method of making thin metal sections vacuum tight
US3066402A (en) * 1956-11-29 1962-12-04 Ingels Glenn Rex Method of and product for hard facing
US3180023A (en) * 1961-02-02 1965-04-27 Kaiser Aluminium Chem Corp Method of joining an electrically conductive metal to a refractory hard metal
US3245143A (en) * 1961-09-25 1966-04-12 Csf Method of producing a vacuum-tight joint of relatively thin parts
US3455663A (en) * 1966-03-24 1969-07-15 Mallory & Co Inc P R Composite metal joint and a copper-silver,titanium brazing alloy
EP0034768A2 (en) * 1980-02-12 1981-09-02 Kabushiki Kaisha Toshiba Method for manufacturing an anode of an X-ray tube
EP0034768B1 (en) * 1980-02-12 1984-11-14 Kabushiki Kaisha Toshiba Method for manufacturing an anode of an x-ray tube
US20040046004A1 (en) * 2001-01-31 2004-03-11 Barnes John James Metallurgically bonded layered article having a curved surface
US6955288B2 (en) * 2001-01-31 2005-10-18 E. I. Du Pont De Nemours And Company Metallurgically bonded layered article having a curved surface

Also Published As

Publication number Publication date
GB648607A (en) 1951-01-10

Similar Documents

Publication Publication Date Title
US3734480A (en) Lamellar crucible for induction melting titanium
US2506326A (en) Article of tungsten and wrought copper joined by cast copper
US3539859A (en) X-ray generator tube with graphite rotating anode
US2327586A (en) X-ray tube
US3347772A (en) Rf sputtering apparatus including a capacitive lead-in for an rf potential
US3281174A (en) Art of sealing quartz to metal
US2506327A (en) Article of tungsten and wrought copper joined by sintered copper
US3436584A (en) Electron emission source with sharply defined emitting area
US1893380A (en) Soldering apparatus
US3842305A (en) X-ray tube anode target
GB1430723A (en) Mass for a high-temperature-resistant emission electrode and process for the production of said mass
US1897586A (en) Gaseous electric discharge device
US2112718A (en) Electric discharge device
US1953813A (en) X-ray tube
US2900281A (en) Method of bonding metal borides to graphite
US1733744A (en) Composite x-ray target
US2379397A (en) Anode structure
US3037142A (en) X-ray generator tubes
US2167515A (en) Electronic discharge tube
US2435273A (en) Method of coating with tungsten carbide
US2903611A (en) X-ray tube comprising a cast copper anode sealed with a copper-silver electric alloy
US1625427A (en) Target for X-ray tubes
US2210131A (en) Electric discharge vessel
US1267888A (en) Incandescent-cathode device.
US1253156A (en) Roentgen-ray device.