US2504522A - Quartz-to-metal seal - Google Patents

Quartz-to-metal seal Download PDF

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Publication number
US2504522A
US2504522A US41250A US4125048A US2504522A US 2504522 A US2504522 A US 2504522A US 41250 A US41250 A US 41250A US 4125048 A US4125048 A US 4125048A US 2504522 A US2504522 A US 2504522A
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United States
Prior art keywords
thimble
quartz
rod
tube
wall
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Expired - Lifetime
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US41250A
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Greiner Alfred
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General Electric Co
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General Electric Co
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Priority to US41250A priority Critical patent/US2504522A/en
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Publication of US2504522A publication Critical patent/US2504522A/en
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    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J5/00Details relating to vessels or to leading-in conductors common to two or more basic types of discharge tubes or lamps
    • H01J5/32Seals for leading-in conductors
    • H01J5/40End-disc seals, e.g. flat header
    • H01J5/42End-disc seals, e.g. flat header using intermediate part
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J2893/00Discharge tubes and lamps
    • H01J2893/0033Vacuum connection techniques applicable to discharge tubes and lamps
    • H01J2893/0034Lamp bases

Definitions

  • This invention relates to quartz-to-metal seals for high pressure discharge devices, such as high pressure mercury vapor discharge lamps.
  • the lamp stem comprises a tube l of vitreous material, such as quartz, through which extends a thick conductor rod 2, of tungsten, for example, having an electrode of refractory metal 3 which may be of tungsten mounted on its inner end.
  • the tube I is provided with a flare at its inner end (not shown) for fusion with the walls of an opening in a spherical quartz envelope to close the opening and support the electrode 3 in proper position therein.
  • the quartz envelope may have another stem of similar structure provided with a cooperating electrode all as disclosed in the aforesaid co-pending application.
  • the rod 2 In order to conduct large currents to the lamp, which may have a current consumption of kilowatts and higher, the rod 2 must be of substantial thickness. It is well known that fused joints between the metal rod and quartz which will be gas-tight over a temperature range of hundreds of degrees centigrade cannot be made when the metal conductor is thick enough to In the stem struc-- ture shown in the drawing, and in the similar structure disclosed in the co-lpending application, the quartz stem tube 2 is not fused, therefore, to the conductor rod.
  • a thimble of metal 4, such as molybdenum, is hermetically united around the rod I, by a brazed platinum joint, for example, and a thin feathered sealing edge 5 on the thimble is embedded in the wall of the quartz tube 2 which is hermetically 2 fused therewith to constitute the seal between the rod i and the tube 2.
  • a spacer having a cylindrical part around the rod and engaging the rod and the end wall of the thimble, and having also a disc-like flange at its end toward the open end of the thimble is provided between the rod and the inner wall of the thimble to keep these parts in alignment during manufacture of the seal and also to close off the inside of the thimble above its sealing edge portion.
  • the quartz is fused only to the inner and outer surfaces of the said sealing edge portion and not to the inner surface of the thicker portions of the thimble which avoids cracking of the seal.
  • this portion of the cylindrical thimble wall is supported against such forces by a spacer including a cylindrical part 6 engaging the said cylindrical thimble wall and the end wall 1 of the thimble and a disc part 8 engaging the rod I and constituting an inwardly extending annular flange.
  • the spacer 6, 8 thus serves to align the rod i and the thimble 4, prevents the plastic quartz going into the thimble beyond the sealing edge portion 5 during fabrication of the stem and, in addition, supports the portion of the thimble wall between the feathered sealing edge portion 5 and the end wall 1 against forces tending to bow it inward.
  • the stem structure disclosed herein is thus capable of withstanding even higher pressures than that disclosed and claimed in the co-pending application.
  • a thin molybdenum foil 9 is wrapped around the rod and the outer surface of the thimble back from the sealing edge to prevent the quartz tube 2 sticking thereto during fabrication of the stem.
  • a high pressure resistantstem comprising a high softening point vitreous stem tube, a refractory metal conductor rod extending through said 2,sos,s22
  • a refractory metal thimble wholly within said tube, hermetically united to and around said rodand having a relatively thin cylindrical wall tapering to a sealing edge and with its said edge embedded in the wall of said tube to hermetically seal of! the space between the tube and the outside of the thimble from the space in the thimble, a refractory metal spacer member within the thimble and around the rod and having a cylindrical part engaging the inner surface of the cylindrical thimble wall to strengthen the said wall against forces tending to collapse it and having also an inwardly extending annular flange disposed around the rod and adjacent the inner end of the sealing edge to mechanically close the annular space between the rod and the thimble and limit the flow of plastic vitreous material into the thimble in the fabrication of the stem.
  • a stem for high pressure mercury vapor discharge lamp having a quartz envelope, a quartz stem tube, a thick tungsten rod extending through said tube, a molybdenum thimble wholly within said tube, hermetically united to and around said rod and having a relatively thin cylindrical wall tapering to a sealing edge and with its said edge embedded in the wall of said tube to hermetically seal oil the space between the tube and the outside of the thimble from the 4 space inthe thimble, a molybdenum spacer member within the thimble and around the rod and having a cylindrical part engaging the inner surface of the cylindrical thimble wall to strengthen the said wall against forces tending to collapse it and having also an inwardly extending annular flange disposed around the rod and adjacent the inner end of the sealing edge to mechanically close the annular space between the rod and the thimble and limit the flow of plastic vitreous material into the thimble in the fabrication of the stem.

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  • Vessels And Coating Films For Discharge Lamps (AREA)

Description

April 18, 1950 A. GREINER 2,504,522
QUARTZ-TO-METAL SEAL Filed July 29, 1948 hverw tor: AkFred Greiner, b5 W(-//%m- His A+=lrow-neg conduct such heavy currents.
Patented Apr. 18, 1950 QUARTZ-TO-METAL SEAL Alfred Greiner, Cleveland Heights, Ohio, aa-
signer to General Electric Company,
tion of New York Application July 29, 1948, Serial No. 41,250
2 Claims.
This invention relates to quartz-to-metal seals for high pressure discharge devices, such as high pressure mercury vapor discharge lamps.
In my co-pending application Serial No. 24,523, filed May 1, 1948, which application is assigned to the assignee of the present application, a quartz-to-metal seal in the form of a stem comprising a conductor and a thimble hermetically united around the conductor and having a feathered sealing edge embedded in and making a fused hermetic joint with the wall of the stem tube is disclosed and claimed. The principal object of my invention is to provide an improved seal of this type also in the form of a stem and capable of withstanding even higher vapor pressures. Further objects and advantages of the invention will appear from the following description of a species thereof and from the accompanying drawing in the single figure of which a seal in the form of a stem embodying the invention is shown in an elevational, partly sectional fragmentary view.
Referring to the drawing, the lamp stem comprises a tube l of vitreous material, such as quartz, through which extends a thick conductor rod 2, of tungsten, for example, having an electrode of refractory metal 3 which may be of tungsten mounted on its inner end. The tube I is provided with a flare at its inner end (not shown) for fusion with the walls of an opening in a spherical quartz envelope to close the opening and support the electrode 3 in proper position therein. The quartz envelope may have another stem of similar structure provided with a cooperating electrode all as disclosed in the aforesaid co-pending application.
In order to conduct large currents to the lamp, which may have a current consumption of kilowatts and higher, the rod 2 must be of substantial thickness. It is well known that fused joints between the metal rod and quartz which will be gas-tight over a temperature range of hundreds of degrees centigrade cannot be made when the metal conductor is thick enough to In the stem struc-- ture shown in the drawing, and in the similar structure disclosed in the co-lpending application, the quartz stem tube 2 is not fused, therefore, to the conductor rod. Instead, a thimble of metal 4, such as molybdenum, is hermetically united around the rod I, by a brazed platinum joint, for example, and a thin feathered sealing edge 5 on the thimble is embedded in the wall of the quartz tube 2 which is hermetically 2 fused therewith to constitute the seal between the rod i and the tube 2.
In the aforesaid co-pending application a spacer having a cylindrical part around the rod and engaging the rod and the end wall of the thimble, and having also a disc-like flange at its end toward the open end of the thimble is provided between the rod and the inner wall of the thimble to keep these parts in alignment during manufacture of the seal and also to close off the inside of the thimble above its sealing edge portion. Thus, during manufacture the quartz is fused only to the inner and outer surfaces of the said sealing edge portion and not to the inner surface of the thicker portions of the thimble which avoids cracking of the seal.
While such seals successfully withstand temperature changes of hundreds of degrees centigrade and pressures of the order of many atmospheres, such as the mercury VBJDOI pressure in high pressure quartz arc lamps, the part of the cylindrical thimble wall between feathered sealing edge portion and the end wall of the thimble is unsupported against the force of the pressure in the lamp during operation tending to bow it inward.
In the stern shown in the drawing, this portion of the cylindrical thimble wall is supported against such forces by a spacer including a cylindrical part 6 engaging the said cylindrical thimble wall and the end wall 1 of the thimble and a disc part 8 engaging the rod I and constituting an inwardly extending annular flange. The spacer 6, 8 thus serves to align the rod i and the thimble 4, prevents the plastic quartz going into the thimble beyond the sealing edge portion 5 during fabrication of the stem and, in addition, supports the portion of the thimble wall between the feathered sealing edge portion 5 and the end wall 1 against forces tending to bow it inward. The stem structure disclosed herein is thus capable of withstanding even higher pressures than that disclosed and claimed in the co-pending application.
A thin molybdenum foil 9 is wrapped around the rod and the outer surface of the thimble back from the sealing edge to prevent the quartz tube 2 sticking thereto during fabrication of the stem.
What we claim as new and desire to secure by Letters Patent of the United States is:
1. In a high pressure resistantstem comprisinga high softening point vitreous stem tube, a refractory metal conductor rod extending through said 2,sos,s22
tube, a refractory metal thimble wholly within said tube, hermetically united to and around said rodand having a relatively thin cylindrical wall tapering to a sealing edge and with its said edge embedded in the wall of said tube to hermetically seal of! the space between the tube and the outside of the thimble from the space in the thimble, a refractory metal spacer member within the thimble and around the rod and having a cylindrical part engaging the inner surface of the cylindrical thimble wall to strengthen the said wall against forces tending to collapse it and having also an inwardly extending annular flange disposed around the rod and adjacent the inner end of the sealing edge to mechanically close the annular space between the rod and the thimble and limit the flow of plastic vitreous material into the thimble in the fabrication of the stem.
2. In a stem for high pressure mercury vapor discharge lamp having a quartz envelope, a quartz stem tube, a thick tungsten rod extending through said tube, a molybdenum thimble wholly within said tube, hermetically united to and around said rod and having a relatively thin cylindrical wall tapering to a sealing edge and with its said edge embedded in the wall of said tube to hermetically seal oil the space between the tube and the outside of the thimble from the 4 space inthe thimble, a molybdenum spacer member within the thimble and around the rod and having a cylindrical part engaging the inner surface of the cylindrical thimble wall to strengthen the said wall against forces tending to collapse it and having also an inwardly extending annular flange disposed around the rod and adjacent the inner end of the sealing edge to mechanically close the annular space between the rod and the thimble and limit the flow of plastic vitreous material into the thimble in the fabrication of the stem.
ALFRED GREINER.
REFERENCES CITED The following references are of record in the file of this patent:
UNITED STATES PATENTS
US41250A 1948-07-29 1948-07-29 Quartz-to-metal seal Expired - Lifetime US2504522A (en)

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Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2583388A (en) * 1947-05-01 1952-01-22 Gen Electric Conducting seal for high-pressure lamps
US2716584A (en) * 1953-12-16 1955-08-30 Westinghouse Electric Corp Double hermetic seal for gaseous discharge lamps
US3213184A (en) * 1962-12-11 1965-10-19 Gen Electric Metal to ceramic sealing structure
US3320352A (en) * 1964-09-29 1967-05-16 Gen Electric Quartz-to-metal seal
US3340025A (en) * 1964-05-04 1967-09-05 Philips Corp Refractory metal-to-ceramic seal
US3386158A (en) * 1966-03-28 1968-06-04 Alfred E. Milch Method of forming a refractory metal-to-ceramic seal
US3386159A (en) * 1964-05-04 1968-06-04 Philips Corp Method of forming a refractory metal-to-ceramic seal
US3435180A (en) * 1967-08-03 1969-03-25 Gen Electric Method of making a molybdenum-tungsten thimble seal
US3487536A (en) * 1966-02-24 1970-01-06 Teledyne Inc Method of forming a high temperature ceramic-to-metal seal
US3571487A (en) * 1967-11-30 1971-03-16 Patent Treuhand Ges Fuer Elektrische Gluehlampen Mbh Vitreous silica-to-metal seal
US4788885A (en) * 1985-02-02 1988-12-06 Robert Bosch Gmbh Housing consisting of at least two parts

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1159335A (en) * 1913-03-06 1915-11-02 Arthur A Noyes Seal for vacuum apparatus.
US1716140A (en) * 1923-09-28 1929-06-04 Westinghouse Electric & Mfg Co Method of making gas-tight seals between glass and metal
DE598214C (en) * 1930-11-23 1934-06-07 Siemens & Halske Akt Ges Process for the production of a ring-shaped or cap-shaped seal of metal in glass or quartz
US2409360A (en) * 1942-04-03 1946-10-15 Gen Electric Seal structure for electric lamps and similar devices
US2409361A (en) * 1942-04-03 1946-10-15 Gen Electric Seal for electric lamps and similar devices

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1159335A (en) * 1913-03-06 1915-11-02 Arthur A Noyes Seal for vacuum apparatus.
US1716140A (en) * 1923-09-28 1929-06-04 Westinghouse Electric & Mfg Co Method of making gas-tight seals between glass and metal
DE598214C (en) * 1930-11-23 1934-06-07 Siemens & Halske Akt Ges Process for the production of a ring-shaped or cap-shaped seal of metal in glass or quartz
US2409360A (en) * 1942-04-03 1946-10-15 Gen Electric Seal structure for electric lamps and similar devices
US2409361A (en) * 1942-04-03 1946-10-15 Gen Electric Seal for electric lamps and similar devices

Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2583388A (en) * 1947-05-01 1952-01-22 Gen Electric Conducting seal for high-pressure lamps
US2716584A (en) * 1953-12-16 1955-08-30 Westinghouse Electric Corp Double hermetic seal for gaseous discharge lamps
US3213184A (en) * 1962-12-11 1965-10-19 Gen Electric Metal to ceramic sealing structure
US3340025A (en) * 1964-05-04 1967-09-05 Philips Corp Refractory metal-to-ceramic seal
US3386159A (en) * 1964-05-04 1968-06-04 Philips Corp Method of forming a refractory metal-to-ceramic seal
US3320352A (en) * 1964-09-29 1967-05-16 Gen Electric Quartz-to-metal seal
US3487536A (en) * 1966-02-24 1970-01-06 Teledyne Inc Method of forming a high temperature ceramic-to-metal seal
US3386158A (en) * 1966-03-28 1968-06-04 Alfred E. Milch Method of forming a refractory metal-to-ceramic seal
US3435180A (en) * 1967-08-03 1969-03-25 Gen Electric Method of making a molybdenum-tungsten thimble seal
US3571487A (en) * 1967-11-30 1971-03-16 Patent Treuhand Ges Fuer Elektrische Gluehlampen Mbh Vitreous silica-to-metal seal
US4788885A (en) * 1985-02-02 1988-12-06 Robert Bosch Gmbh Housing consisting of at least two parts

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