US2459759A - N-monochlorocyclohexylamine - Google Patents

N-monochlorocyclohexylamine Download PDF

Info

Publication number
US2459759A
US2459759A US695051A US69505146A US2459759A US 2459759 A US2459759 A US 2459759A US 695051 A US695051 A US 695051A US 69505146 A US69505146 A US 69505146A US 2459759 A US2459759 A US 2459759A
Authority
US
United States
Prior art keywords
monochlorocyclohexylamine
per cent
alliger
glen
cyclohexylamine
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
US695051A
Inventor
Alliger Glen
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Bridgestone Firestone Inc
Original Assignee
Firestone Tire and Rubber Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Firestone Tire and Rubber Co filed Critical Firestone Tire and Rubber Co
Priority to US695051A priority Critical patent/US2459759A/en
Application granted granted Critical
Publication of US2459759A publication Critical patent/US2459759A/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C06—EXPLOSIVES; MATCHES
    • C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
    • C06B43/00—Compositions characterised by explosive or thermic constituents not provided for in groups C06B25/00 - C06B41/00

Definitions

  • the compound is prepared by adding one mol of sodium hypochlorite to 1.16 mols of cyclohexylamine. When no excess of cyclohexylamine was used, some dichlorocyclohexylamine was formed. The reaction-takes place according to the following equation:

Description

Patented Jan. 18, 1949 UNITED STATES PATENT OFFICE N-MONOCHLOROCYCLOHEXYLAMINE Glen Alliger, Cuyahoga Falls, Ohio, assignor to The Firestone Tire & Rubber Company, Akron, Ohio, a corporation of Ohio No Drawing; Application September 5, 1946, Serial No. 695,051
1 Claim. 1
The subject of this invention is N -monochloro-= cyclohexylamine, a new chemical compound v which is useful as an intermediate as, for example, in reactions with mercaptides having the formula RrSNa in which R may be any of the 5 usual mercaptide groups, such as an alkyl group, benzothiazyl, thiocarbamyl, etc.
The compound is prepared by adding one mol of sodium hypochlorite to 1.16 mols of cyclohexylamine. When no excess of cyclohexylamine was used, some dichlorocyclohexylamine was formed. The reaction-takes place according to the following equation:
, 2 Analysis for CsHmNCl:
Calc.: 01, 25.53 per cent Found: Cl, 26.93 per cent The usual strong oxidizing properties of N- chloroamines were exhibited by this compound; e. g., it liberated iodine from potassium iodide.
What I claim is:
N -monochlorocyclohexylamine.
GLEN ALLIGER.
REFERENCES CITED The following references are of record in the file of this patent:
UNITED STATES PATENTS Number Name Date 2,333,468 Cooper Nov. 2, 1943 FOREIGN PATENTS Number Country Date 586,351 Germany Oct. 20, 1933 Certificate of Correction Patent No. 2,459,759. January 18, 1949.
GLEN ALLIGER It is hereby certified that error appears in the printed specification of the above numbered patent requiring correction as follows:
Column 2, line 2, for 25.53 per cent read 26.53 per cent;
and that the said Letters Patent should be read with this correction therein that the same may conform to the record of the case in the Patent Ofiice.
Signed and sealed this 16th day of August, A. D. 1949.
THOMAS F. MURPHY, 7 Assistant Oommz'ssi oner of Patents.
US695051A 1946-09-05 1946-09-05 N-monochlorocyclohexylamine Expired - Lifetime US2459759A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
US695051A US2459759A (en) 1946-09-05 1946-09-05 N-monochlorocyclohexylamine

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US695051A US2459759A (en) 1946-09-05 1946-09-05 N-monochlorocyclohexylamine

Publications (1)

Publication Number Publication Date
US2459759A true US2459759A (en) 1949-01-18

Family

ID=24791355

Family Applications (1)

Application Number Title Priority Date Filing Date
US695051A Expired - Lifetime US2459759A (en) 1946-09-05 1946-09-05 N-monochlorocyclohexylamine

Country Status (1)

Country Link
US (1) US2459759A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2894028A (en) * 1956-10-12 1959-07-07 Grace W R & Co Cyclohexylideneimino compounds
US3112650A (en) * 1960-06-01 1963-12-03 Ralph M Nester Pressure measuring device
US3904686A (en) * 1973-09-24 1975-09-09 Universal Oil Prod Co Preparation of thiocarbamyl sulfenamides

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE586351C (en) * 1932-04-09 1933-10-20 I G Farbenindustrie Akt Ges Process for the preparation of sulfenamides twice substituted on nitrogen
US2333468A (en) * 1940-11-06 1943-11-02 Monsanto Chemicals Vulcanizing rubber and product obtained thereby

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE586351C (en) * 1932-04-09 1933-10-20 I G Farbenindustrie Akt Ges Process for the preparation of sulfenamides twice substituted on nitrogen
US2333468A (en) * 1940-11-06 1943-11-02 Monsanto Chemicals Vulcanizing rubber and product obtained thereby

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2894028A (en) * 1956-10-12 1959-07-07 Grace W R & Co Cyclohexylideneimino compounds
US3112650A (en) * 1960-06-01 1963-12-03 Ralph M Nester Pressure measuring device
US3904686A (en) * 1973-09-24 1975-09-09 Universal Oil Prod Co Preparation of thiocarbamyl sulfenamides

Similar Documents

Publication Publication Date Title
GB1009005A (en) Defoaming and surface active compositions
US2459759A (en) N-monochlorocyclohexylamine
US2588899A (en) Stabilized compositions containing high molecular weight halogenated materials
US3624029A (en) Halogen-containing polymeric rubber compositions having improved scorch resistance
US2321306A (en) Accelerator of vulcanization
GB950626A (en) Process for the manufacture of carbon bodies
US2985632A (en) Gr-s cured with dicamyl peroxide and sulfur
US2824845A (en) Episulfide compounds and stabilized polymer compositions containing same
GB800168A (en) Hydrocarbontin isodithiocarbamates
US2261024A (en) Vulcanization accelerator
US2342545A (en) Vulcanization of rubber
US2158021A (en) Vulcanization of rubber
US3532693A (en) 2-morpholinosulfinylbenzothiazoles
US2560032A (en) N,n'-piperazino bis-sulfenamides
US2158022A (en) Vulcanization of rubber
US2404585A (en) Latex activator
US2174674A (en) Plasticized composition
US2441032A (en) Acyl thiocarbamo sulfenamides as new chemicals
US2381059A (en) Synthetic rubber composition
US3816475A (en) Color stabilizer for maleic anhydride
US1440961A (en) Process for vulcanizing rubber and products obtained thereby
US3066146A (en) N-(2-benzothiazolylthio) maleimide
US2193626A (en) Manufacture of thiazole derivatives
US2960495A (en) Polymers containing polysulfide and spirobi (meta-dioxane) groups
US3645968A (en) Silicone elastomers containing iron compounds as stabilizers