US2339870A - Pipette - Google Patents

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Publication number
US2339870A
US2339870A US385973A US38597341A US2339870A US 2339870 A US2339870 A US 2339870A US 385973 A US385973 A US 385973A US 38597341 A US38597341 A US 38597341A US 2339870 A US2339870 A US 2339870A
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United States
Prior art keywords
bulb
tube
suction
interconnecting
shaft
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Expired - Lifetime
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US385973A
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Waddy T Mathis
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Clay Adams Inc
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Clay Adams Inc
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Priority to US385973A priority Critical patent/US2339870A/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01LCHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
    • B01L3/00Containers or dishes for laboratory use, e.g. laboratory glassware; Droppers
    • B01L3/02Burettes; Pipettes
    • B01L3/021Pipettes, i.e. with only one conduit for withdrawing and redistributing liquids
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01LCHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
    • B01L3/00Containers or dishes for laboratory use, e.g. laboratory glassware; Droppers
    • B01L3/02Burettes; Pipettes
    • B01L3/021Pipettes, i.e. with only one conduit for withdrawing and redistributing liquids
    • B01L3/0213Accessories for glass pipettes; Gun-type pipettes, e.g. safety devices, pumps

Definitions

  • This invention relates generally to pipettes and similar laboratory apparatus. More particularly my invention relates to the type of pipettes used for transferring or collecting measured quantities or fluids.
  • the principal object of my invention is to provide a novel device for use with pipettes and similar laboratory apparatus by means of which a predetermined constant quantity or quantities of fluid may be automatically drawn into the pipette and in which such constant quantity of fluid may be altered and regulated, in accordance with desired requirements.
  • FIG. 1 is a front elevational view, partly in sectionyof a pipette and automatic measuring device constructed in accordance with my invention
  • Fig. 2 is a side elevational view of a portion thereof.
  • Fig. 3 is a; vertical sectional view of a portion of the apparatus shown in Fig. 1, and illustrating astepinthe use thereof.
  • I For creating a suction, in order to draw fluid into the tube I U, I employ a collapsible rubber bulb I2 'of any suitable standard construction having a bottom aperture I2a communicating with the hollow interior thereof.
  • the said bulb I2 is connected to the tube ID by means of a nipple l5 having a tapered projecting portion l5a frictionally received and held in the aperture [2a and having an opening l5 provided with a resilient lining member I! into which there is frictionally received, the upper end of the tube I 0.
  • the said frame 22 comprises a wall 22b integral with the bottom wall 22a and extending upwardly therefrom in the form of a loop.
  • the said loop substantially follows the contour of the outer surface of the bulb and .is of such size as to snugly accommodate the said bulb I2 therein, when in non-collapsed condition, to form a housing therefor.
  • the wall 221) is provided with a through aperture 25 into which there is slidably mounted a shaft member 26.
  • a portion of the Wall 221) surrounding the aperture 25 may be provided with an extension 2'! to form a better bearing surface for the shaft 26.
  • an enlarged head 28 At one end of the shaft 26 and disposed between the inner surface wall 22b and the bulb is an enlarged head 28, so constructed and arranged that when the shaft 26 is slidably moved inwardly in the direction of the arrow A, the bulb [2, held in position by the frame 22, will be collapsed. Upon release of the shaft 26, the normal resilience of the bulb l2 will slidably restore the shaft 26 to its original position as in Fig. l of the drawing and at the same time a suction will be created to automatically draw fluid into the tube I ii.
  • a suitable finger piece 30 may be provided at the opposite end of the shaft 26 from that of the enlarged head 28 to facilitate the sliding movement of the shaft 26.
  • a portion of the shaft 26 is provided with threads 3
  • the second nut 33 serves as a locknut to prevent displacement of the nut 32 from its selected position.
  • the volume of fluid drawn into the tube may be regulated as desired.
  • an open frame or housing such as shown at 22, provides for unrestricted access to the bulb l2, for drawing into the tube [0, or expelling therefrom, an amount of fluid which differs from the amount controlled by the setting of the adjustable nuts 32, 33, without disturbing the setting of the nuts.
  • said last named means comprising a unitary openlooped frame for said bulb and a compressor unit mounted on said frame, said compressor unit comprising a rod slidably supported in said frame and having an enlarged head portion adapted to engage said bulb and to compress the same upon sliding movement of said rod.
  • a compressor unit mounted on said frame, said compressor unit comprising a rod slidably supported in said frame and having an enlarged head portion adapted to engage said bulb and to compress the same upon sliding movement of said rod and a finger piece on said rod to facilitate the sliding movement thereof.
  • a tube a suction bulb
  • a member for interconnecting said bulb with said tube whereby a suction may be created in said tube upon compressing and releasing said bulb
  • said member having a recess at one end for the reception of said tube and a projection at the other end for mounting said bulb
  • means supported by said interconnecting member for causing said bulb to be compressed
  • said last named means comprising a housing for said bulb, a compressor unit mounted on said housing, said compressor unit comprising a rod slidably supported in said housing and an abutment member on said rod to limit the amount of sliding movement thereof to provide a constant amount of compression of said bulb.
  • the said locking means comprises a nutthreadedly mounted on said rod.
  • a removable tube and a pre-assembled compressor unit
  • said compressor unit comprising a suction bulb, a member for interconnecting said bulb with said tube, whereby a suction may be created in said tube by the compressing and releasing of said bulb
  • said interconnecting member having a recess at one end for the reception of said removable tube and a projection at the other end for mounting said bulb, and means supported by said interconnecting member for causing said bulb to be compressed.
  • a removable tube and a pre-assembled compressor unit said compressor unit comprising a suction bulb, a memher for interconnecting said bulb with said tube, whereby a suction may be created in said tube by the compressing and releasing of said bulb, said interconnecting member having a recess at one end for the reception of said removable tube and a projection at the other end for mounting said bulb, and means supported by said interconnecting member for causing said bulb to be compressed, said last named means including means for limiting the amount of compression of said bulb so that a constant predetermined quantity of fluid may be drawn into said tube.

Description

Jan.25, 1944. w, T MA HS 7 2,339,870
PIPETTE Filed March 51, 1941 m! a!!! a!!! MIL- INVENTOR M400) 7? MAT/#8 BEA. ow V ATTORNEY Patented Jan. 25, 1944 'PIPETTE Waddy T. Mathis, Hamden, Conn., assignor to Clay Adams Co. Inc., New York, N. Y.,-a-co1'- poration of New York Application March 31, 1941, Serial No. 385,973
12 Claims.
This invention relates generally to pipettes and similar laboratory apparatus. More particularly my invention relates to the type of pipettes used for transferring or collecting measured quantities or fluids.
" The principal object of my invention is to provide a novel device for use with pipettes and similar laboratory apparatus by means of which a predetermined constant quantity or quantities of fluid may be automatically drawn into the pipette and in which such constant quantity of fluid may be altered and regulated, in accordance with desired requirements.
Other objects of my'invention will in part be obvious and in part hereinafter pointed out.
In the accompanying drawing Fig. 1 is a front elevational view, partly in sectionyof a pipette and automatic measuring device constructed in accordance with my invention;
Fig. 2 is a side elevational view of a portion thereof; and
Fig. 3 is a; vertical sectional view of a portion of the apparatus shown in Fig. 1, and illustrating astepinthe use thereof.
Referring now in detail to the drawing I have shown a pipette or tube ID of the type customarily employed in laboratory work for transferring and collecting fluids and provided with suitable graduations II for measuring quantities of fluid drawn into the tube l0.
For creating a suction, in order to draw fluid into the tube I U, I employ a collapsible rubber bulb I2 'of any suitable standard construction having a bottom aperture I2a communicating with the hollow interior thereof. The said bulb I2 is connected to the tube ID by means of a nipple l5 having a tapered projecting portion l5a frictionally received and held in the aperture [2a and having an opening l5 provided with a resilient lining member I! into which there is frictionally received, the upper end of the tube I 0. An aperture 18 in the nipple l5 communieating-with opening l6 and with the hollow interior of the bulb l2, completes the air passage- 20 designed to threadedly receive thereon the threaded aperture 2[ in the bottom wall 22a of a frame 22'. The said frame 22 comprises a wall 22b integral with the bottom wall 22a and extending upwardly therefrom in the form of a loop. The said loop substantially follows the contour of the outer surface of the bulb and .is of such size as to snugly accommodate the said bulb I2 therein, when in non-collapsed condition, to form a housing therefor.
The wall 221) is provided with a through aperture 25 into which there is slidably mounted a shaft member 26. A portion of the Wall 221) surrounding the aperture 25 may be provided with an extension 2'! to form a better bearing surface for the shaft 26.
At one end of the shaft 26 and disposed between the inner surface wall 22b and the bulb is an enlarged head 28, so constructed and arranged that when the shaft 26 is slidably moved inwardly in the direction of the arrow A, the bulb [2, held in position by the frame 22, will be collapsed. Upon release of the shaft 26, the normal resilience of the bulb l2 will slidably restore the shaft 26 to its original position as in Fig. l of the drawing and at the same time a suction will be created to automatically draw fluid into the tube I ii. A suitable finger piece 30 may be provided at the opposite end of the shaft 26 from that of the enlarged head 28 to facilitate the sliding movement of the shaft 26.
In accordance with my invention I have provided the following means whereby a predetermined and constant amount of fluid may be automatically drawn into the tube Ill and expelled therefrom, each time the shaft 26 is slidably moved to collapse and to release the bulb l2.
A portion of the shaft 26 is provided with threads 3| On which there is threadedly received a pair of nuts 32 and 33. It is therefore seen that the shaft 26 may be slidably moved in the direction of the arrow A only until the nut 32 strikes the wall portion 21. In other words, the length of the stroke of the shaft 26 is controlled by the position of the nut 32 on the shaft 26. The second nut 33 serves as a locknut to prevent displacement of the nut 32 from its selected position.
It is also noted that once the position of the nut 32 on the shaft has been selected in accord ance with the amount of fluid it is desired to drawinto the tube Iii, repeated constant quantities of fluid may be quickly and automatically collected in the tube in, by merely pressing the fmger piece 30, to first slidably move the shaft 26 from the position shown in Fig. 1 to the position shown in Fig. 3 with the nut 32 in abutting relationship with the wall portion 27, and then releasing said finger piece, to permit the bulb to expand to its normal size.
In view of the fact that the nuts 32 and 33 are threadedly received on the shaft 26 the volume of fluid drawn into the tube may be regulated as desired.
It should be noted that the use of an open frame or housing, such as shown at 22, provides for unrestricted access to the bulb l2, for drawing into the tube [0, or expelling therefrom, an amount of fluid which differs from the amount controlled by the setting of the adjustable nuts 32, 33, without disturbing the setting of the nuts.
It will thus be seen that there is provided a device in which the several objects of this invention are achieved, and which is well adapted to meet the conditions of practical use.
As various possible embodiments might be made of the above invention, and as various changes might be made in the embodiment above set forth, it is to be understood that all matter herein set forth or shown in the accompanying drawing is to be interpreted as illustrative and not in a limiting sense.
Having described my invention, I claim as new and desire to secure by Letters Patent:
1. In a laboratory apparatus of the class described, the combination of a tube, a suction bulb, a member for interconnecting said bulb with said tube whereby a suction may be created in said tube upon compressing and releasing said bulb and means supported by said interconnecting member for causing said bulb to be compressed, said last named means comprising a unitary open looped frame for said bulb and a compressor unit mounted on said frame.
2. In a laboratory apparatus of the class described, the combination of a tube, a suction bulb, a member for interconnecting said bulb with said tube whereby a suction may be created in said tube upon compressing and releasing said bulb and means supported by said interconnecting member for causing said bulb to be compressed, said last named means comprising a frame partially enclosing said bulb and a compressor unit mounted on said frame, said compressor unit comprising a rod slidably supported in said frame, said partially enclosing frame permitting direct hand compression of the bulb, without disturbing the compressor unit.
3. In a laboratory apparatus of the class described, the combination of a tube, a suction bulb, a member for interconnecting said bulb with said tube whereby a suction may be created in said tube upon compressing and releasing said bulb and means supported by said interconnecting member for causing said bulb to be compressed,
said last named means comprising a unitary openlooped frame for said bulb and a compressor unit mounted on said frame, said compressor unit comprising a rod slidably supported in said frame and having an enlarged head portion adapted to engage said bulb and to compress the same upon sliding movement of said rod.
4. In a laboratory apparatus of the class described, the combination of a tube, a suction bulb, a member for interconnecting said bulb with said tube whereby a suction may be created in said tube upon compressing and releasing said bulb, said member having a recess at one end for the reception of said tube and a projection at the other end for mounting said bulb, means supported by said interconnecting member for causing said bulb to be compressed, said last named means comprising a unitary open looped frame.
for said bulb, a compressor unit mounted on said frame, said compressor unit comprising a rod slidably supported in said frame and having an enlarged head portion adapted to engage said bulb and to compress the same upon sliding movement of said rod and a finger piece on said rod to facilitate the sliding movement thereof.
5. In a laboratory apparatus of the class described, the combination of a tube, a suction bulb, a member for interconnecting said bulb with said tube whereby a suction may be created in said tube upon compressing and releasing said bulb, said member having a recess at one end for the reception of said tube and a projection at the other end for mounting said bulb, means supported by said interconnecting member for causing said bulb to be compressed, said last named means comprising a housing for said bulb, a compressor unit mounted on said housing, said compressor unit comprising a rod slidably supported in said housing and an abutment member on said rod to limit the amount of sliding movement thereof to provide a constant amount of compression of said bulb.
6. In a laboratory apparatus of the class described, the combination of a tube, a rubber suction bulb, a member for interconnecting said bulb with said tube whereby a suction may be created in said tube upon compressing and releasing said bulb, means supported by said interconnecting member for causing said bulb to be compressed, said last named means comprising a housing for said bulb and a compressor. unit mounted on said housing, said compressor unit comprising a rod slidably supported in said 7. In a laboratory apparatus ofthe class described, the combination of a tube, a rubber sucttion bulb, a member for interconnecting said bulb with said tube whereby a suction may be created in said tube upon compressing and. re-
leasing said bulb, means supported by said interconnecting member'for causing said bulb to ill 9. In a laboratory apparatus of the class de-' scribed, the combination according to claim 7 in which said abutment member comprises a nut.
threadedly mounted on said rod and in'which the said locking means comprises a nutthreadedly mounted on said rod. 10. In a laboratory apparatus of the class described, the combination according to claim 6, in which the housing only partially encloses the bulb, for direct hand manipulation of the bulb; without disturbing the setting of the adjustable abutment member of the compressor unit.
l1.'In a laboratory apparatus of the class do scribed, the combination of a removable tube and a pre-assembled compressor unit, said compressor unit comprising a suction bulb, a member for interconnecting said bulb with said tube, whereby a suction may be created in said tube by the compressing and releasing of said bulb, said interconnecting member having a recess at one end for the reception of said removable tube and a projection at the other end for mounting said bulb, and means supported by said interconnecting member for causing said bulb to be compressed.
12. In a laboratory apparatus of the class described, the combination of a removable tube and a pre-assembled compressor unit, said compressor unit comprising a suction bulb, a memher for interconnecting said bulb with said tube, whereby a suction may be created in said tube by the compressing and releasing of said bulb, said interconnecting member having a recess at one end for the reception of said removable tube and a projection at the other end for mounting said bulb, and means supported by said interconnecting member for causing said bulb to be compressed, said last named means including means for limiting the amount of compression of said bulb so that a constant predetermined quantity of fluid may be drawn into said tube.
WADDY T. MATHIS.
US385973A 1941-03-31 1941-03-31 Pipette Expired - Lifetime US2339870A (en)

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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2428577A (en) * 1945-09-06 1947-10-07 Waddy T Mathis Liquid-measuring dispenser
US2431192A (en) * 1944-09-14 1947-11-18 Charles E Munson Dispensing device
US2661741A (en) * 1949-09-02 1953-12-08 Hermac International Ltd Fountain syringe bag
US2751081A (en) * 1954-02-12 1956-06-19 Motte Charles V B La Water demineralizer
US3349937A (en) * 1961-08-31 1967-10-31 Cooke Engineering Company Titration apparatus
US3684408A (en) * 1970-07-29 1972-08-15 Electro Nucleonics Peristaltic metering and dispensing pump
US10814320B2 (en) * 2016-08-08 2020-10-27 Nalge Nunc International Corporation Capillary transfer pipettes and related methods

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2431192A (en) * 1944-09-14 1947-11-18 Charles E Munson Dispensing device
US2428577A (en) * 1945-09-06 1947-10-07 Waddy T Mathis Liquid-measuring dispenser
US2661741A (en) * 1949-09-02 1953-12-08 Hermac International Ltd Fountain syringe bag
US2751081A (en) * 1954-02-12 1956-06-19 Motte Charles V B La Water demineralizer
US3349937A (en) * 1961-08-31 1967-10-31 Cooke Engineering Company Titration apparatus
US3684408A (en) * 1970-07-29 1972-08-15 Electro Nucleonics Peristaltic metering and dispensing pump
US10814320B2 (en) * 2016-08-08 2020-10-27 Nalge Nunc International Corporation Capillary transfer pipettes and related methods

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