US2315405A - Means for treating textiles - Google Patents
Means for treating textiles Download PDFInfo
- Publication number
- US2315405A US2315405A US305960A US30596039A US2315405A US 2315405 A US2315405 A US 2315405A US 305960 A US305960 A US 305960A US 30596039 A US30596039 A US 30596039A US 2315405 A US2315405 A US 2315405A
- Authority
- US
- United States
- Prior art keywords
- kilograms
- kilogram
- mixture
- parts
- acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 239000004753 textile Substances 0.000 title description 13
- 239000000203 mixture Substances 0.000 description 23
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 15
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 14
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 12
- 239000002253 acid Substances 0.000 description 11
- 239000000417 fungicide Substances 0.000 description 9
- 150000002148 esters Chemical class 0.000 description 8
- MONCZSPIFIQNAX-UHFFFAOYSA-N 1-chloro-4-[2,2,2-trichloro-1-(4-chlorophenyl)ethyl]benzene;dimethoxy-(4-nitrophenoxy)-sulfanylidene-$l^{5}-phosphane Chemical compound COP(=S)(OC)OC1=CC=C([N+]([O-])=O)C=C1.C1=CC(Cl)=CC=C1C(C(Cl)(Cl)Cl)C1=CC=C(Cl)C=C1 MONCZSPIFIQNAX-UHFFFAOYSA-N 0.000 description 7
- RLSSMJSEOOYNOY-UHFFFAOYSA-N m-cresol Chemical compound CC1=CC=CC(O)=C1 RLSSMJSEOOYNOY-UHFFFAOYSA-N 0.000 description 7
- 229940100630 metacresol Drugs 0.000 description 7
- 239000000080 wetting agent Substances 0.000 description 7
- 239000002725 coal tar dye Substances 0.000 description 6
- 239000000835 fiber Substances 0.000 description 6
- 230000000855 fungicidal effect Effects 0.000 description 6
- 239000000443 aerosol Substances 0.000 description 5
- 238000011282 treatment Methods 0.000 description 5
- DBEFONQGRSUFQO-UHFFFAOYSA-N 3-(2-Methylpropanoyloxy)-8-(2-methylbutanoyloxy)-9,10-epoxy-p-mentha-1,3,5-triene Chemical compound C=1C=C(C)C=C(OC(=O)C(C)C)C=1C1(COC(=O)C(C)CC)CO1 DBEFONQGRSUFQO-UHFFFAOYSA-N 0.000 description 4
- 125000001931 aliphatic group Chemical group 0.000 description 4
- 125000003118 aryl group Chemical group 0.000 description 4
- 239000003513 alkali Substances 0.000 description 3
- 239000007864 aqueous solution Substances 0.000 description 3
- 239000004359 castor oil Substances 0.000 description 3
- 235000019438 castor oil Nutrition 0.000 description 3
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 description 3
- 239000003921 oil Substances 0.000 description 3
- 235000019198 oils Nutrition 0.000 description 3
- FJKROLUGYXJWQN-UHFFFAOYSA-N 4-hydroxybenzoic acid Chemical compound OC(=O)C1=CC=C(O)C=C1 FJKROLUGYXJWQN-UHFFFAOYSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 239000004902 Softening Agent Substances 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 239000004744 fabric Substances 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 150000002989 phenols Chemical class 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 238000005507 spraying Methods 0.000 description 2
- MGSRCZKZVOBKFT-UHFFFAOYSA-N thymol Chemical compound CC(C)C1=CC=C(C)C=C1O MGSRCZKZVOBKFT-UHFFFAOYSA-N 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 238000009736 wetting Methods 0.000 description 2
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical class OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 244000178870 Lavandula angustifolia Species 0.000 description 1
- 235000010663 Lavandula angustifolia Nutrition 0.000 description 1
- 239000005844 Thymol Substances 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- RGCKGOZRHPZPFP-UHFFFAOYSA-N alizarin Chemical compound C1=CC=C2C(=O)C3=C(O)C(O)=CC=C3C(=O)C2=C1 RGCKGOZRHPZPFP-UHFFFAOYSA-N 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- 238000004040 coloring Methods 0.000 description 1
- 239000007859 condensation product Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- -1 for instance Substances 0.000 description 1
- 239000003230 hygroscopic agent Substances 0.000 description 1
- 238000009940 knitting Methods 0.000 description 1
- 239000001102 lavandula vera Substances 0.000 description 1
- 235000018219 lavender Nutrition 0.000 description 1
- 239000000314 lubricant Substances 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- PSZYNBSKGUBXEH-UHFFFAOYSA-N naphthalene-1-sulfonic acid Chemical compound C1=CC=C2C(S(=O)(=O)O)=CC=CC2=C1 PSZYNBSKGUBXEH-UHFFFAOYSA-N 0.000 description 1
- 235000019645 odor Nutrition 0.000 description 1
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 238000009987 spinning Methods 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 229960000790 thymol Drugs 0.000 description 1
- 235000015112 vegetable and seed oil Nutrition 0.000 description 1
- 239000008158 vegetable oil Substances 0.000 description 1
- 238000009941 weaving Methods 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/244—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus
- D06M13/248—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus with compounds containing sulfur
- D06M13/256—Sulfonated compounds esters thereof, e.g. sultones
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S516/00—Colloid systems and wetting agents; subcombinations thereof; processes of
- Y10S516/01—Wetting, emulsifying, dispersing, or stabilizing agents
- Y10S516/03—Organic sulfoxy compound containing
- Y10S516/04—Protein or carboxylic compound containing
Definitions
- This invention relates to means for treating textiles and refers more particularly to a wetting or spraying composition which is applied to textile yarns or fabrics in order to make them more amenable to further treatments.
- the objects of the present invention may be realized, broadly, through'the use of a mixture containing as its main component parts a wetting agent or similar penetrant harmless to all textiles, and an acid and/or an alkali fungicide having wetting properties, along with a lubricant and a dye, and with the further possible addition of staying-in agents, solvents, aromatics and softening agents.
- sulfonated esters of aliphatic dibasic acids particularly in the form of their alzoic acid, chlorinated phenol and parachlor metacresol.
- An acid fungicide such as parachlor metacresol, or analkali fungicide, such as a parahydr xyb nzoic acid ester, may be mixed separately with the wettingagent, or; a single mixture nated castor oil, was found to be a suitable lubri,-,
- the general Treatment of the yarn is considerably improved if a staying-in agent, i. e. a suitable hygroscopic agent, such as any glycerine derivative, for instance, sorban," which is a sugar derivative or ethylene glycol, is added to the mixture.
- a staying-in agent i. e. a suitable hygroscopic agent, such as any glycerine derivative, for instance, sorban
- glycerine derivative for instance, sorban
- the wetting agents and the fungicides are used in conjunction withan alcohol, as
- solvent for instance, methylalcohol
- An amino condensation product may be added as a softening agent to the mixture to soften the fibers and improve their appearance and feeling.
- the ingredients of the mixture may be used in different proportions. From 10 to parts by weight of a sulfonated ester of an aliphatic dibasic acid may be used in conjunction with 30 to parts by weight of butyl alcohol to constitute the wetting agent. From 1 to 15 parts by weight of an acid fungicide and/or an alkali fungicide,
- an ester of hydroxybenzoic acid may be mixed with the stated amounts of the wetting agent.
- This mixture may receive from 10 to 70 parts by 10 kilograms of a 25% concentration of an ester of a sulphonated bi-carboxylic acid sold on the market under the registered trade-name "Aerosol O T Clear in butyl alcohol are mixed with 9 kilograms of methyl alcohol. 0.25 kilogram of parachlor metacresol, 0.25 kilogram of oil 1nd 0.025 kilogram of a thymol derivative are added to the mixture, along with 0.005 kilogram of a coal tar dye and 0.06 kilogram of an aromatic.
- the mixture may be preserved in 50 to 150 liter containers for long periods of time. From. 1% to 10% of the mixture are used in an aqueous solution for spraying the yarn for a few. seconds. The percentage of the mixture in water depends ;o a great extent upon the quality and texture 3f the textile fibers and the subsequent use to v which they are intended.
- Example 2 7 kilograms of a 25% concentration of the said Aerosol O '1 Clear are mixed with.2.5 kilograms of a 50% concentration of Aerosol T Clear in butyl alcohol and are added to 10 kilograms of methy alcohol. 3 kilograms of ethylene glycol, 0.25 kilogram of parachlor metacresol, 0.2 kilogram of oil and 0.06 kilogram of a thymol derivative are added to the mixture, in addition to 0.005 kilogram of a coal tar dye and 0.06 kilogram of an aromatic.
- the mixture is sprayed upon a textile yarn in in aqueous solution of 1 to 5%.
- Example 3 g 14 kilograms of a 50% concentration of Aerosol O T Clear in butyl alcohol are mixed with 11 kilograms of methyl alcohol and 7 kilograms of ethylene glycol, 5 kilograms of sulphonated castor oil, 2.2 kilograms of a thymol :lerivative, 0.04 kilogram of an aromatic (lavender) and 0.008 kilogram of a coal tar dye are added to the mixture.
- the mixture is used in an aqueous solution of 1% to 10%.
- Example 5 kilograms of sodium alkyl naphthalene sulphonate are mixed with 12 kilograms of ethylene glycol, 10 kilograms of methyl alcohol, 6 kilograms of sulphonated castor oil, 2 kilograms of parachlor metacresol, 0.4 kilograms of an ester of hr'droxybenzoic" acid and chlorinated phenol and 0.01 kilogram of a coal tar dye. The mixture is dissolved for use in 99% to 90% of water.
- Example 6 7.2 kilograms of a concentration of Aerosol O T Clear in butyl alcohol are mixed with 6 kilograms of methyl alcohol, and 0.15 kilogram of parachlor metacresol, 0.004 kilogram of a coal tar dye, 0.15 kilogram of Turkey-red oil, 0.3 kilogram of a thymol derivative and 0.02 kilogram of a natural or synthetic aromatic are added to the mixture, the final mixture being used in anaqueous solution of 1% to 10%.
- Example 7 composition or proportions, as the same may be modified in various particulars or be applied in many varied relations without departclaimed inven ing from the spirit or scope of the tion.
- a composition for the preliminary treatment of textile fibers comprising, in combination, 10 to 75 parts by weight of a sulfonated ester of an aliphatic dibasic acid, to 150 parts by weight of butyl alcohol and l to 15 parts by weight of a fungicide of the class consisting of parachlormetacresol and parahydroxybenzoic acid esters.
- a composition for the preliminary treatment of textile fibers comprising, in combination 10 to parts by weight of a sulfonated ester of an aliphatic dibasic acid, 30 to parts by weight of butyl alcohol, 1 to 15 parts by weight of parachlor metacresol and from 1 to 40 parts by weight of a sulphonated vegetable oil.
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Description
- Patented Mar. 30, 1943 FFHCE 2,315,405 MEANS FOR, TREATING TEXTILES Charles F. Dulken, Arlington, N. J.
No Drawing. Application November 24, 1939,
/ Serial No. 305,960
2 Claims. (Cl. 252-81) This invention relates to means for treating textiles and refers more particularly to a wetting or spraying composition which is applied to textile yarns or fabrics in order to make them more amenable to further treatments.
It was found most desirable to spray or moisten textile fabrics and, particularly, textile yarns prior to the weaving, spinning, twisting, doubling or knitting operations with asolution containing ingredients which adhere to the fibers of the yarn and which have the effect of removing kinks out of the yarn, increasing its strength and flexibility and protecting it from excessive drying, mildew and molding. This preliminary treatment of the yarn serves, consequently, the purpose of preparing the yarn for further operations and improving those qualities of yarn which are most usefulin the course of these operations. It is among the principal objects of the present invention to provide a composition which is most suitable fo may contain both acid and alkali fungicides in commonly used in the textile industry, or sulphothis purpose and-through the used which the best possible results may be attained.
Other objects of the present invention will become apparent in the course of the following Specification.
The objects of the present invention may be realized, broadly, through'the use of a mixture containing as its main component parts a wetting agent or similar penetrant harmless to all textiles, and an acid and/or an alkali fungicide having wetting properties, along with a lubricant and a dye, and with the further possible addition of staying-in agents, solvents, aromatics and softening agents. 1
As the wetting agent, it was found advantageous to employ sulfonated esters of aliphatic dibasic acids, particularly in the form of their alzoic acid, chlorinated phenol and parachlor metacresol. An acid fungicide. such as parachlor metacresol, or analkali fungicide, such as a parahydr xyb nzoic acid ester, may be mixed separately with the wettingagent, or; a single mixture nated castor oil, was found to be a suitable lubri,-,
cant, which mixes easilywith the above described wetting agents and fungicides and facilitates their action.
A In many instances, the general Treatment of the yarn is considerably improved if a staying-in agent, i. e. a suitable hygroscopic agent, such as any glycerine derivative, for instance, sorban," which is a sugar derivative or ethylene glycol, is added to the mixture.
It isadvantageous, although not necessary, to add a suitable dye, such as a coal tar dye, to the mixture in order to remove any original coloring remaining in the yarn.
Preferably, the wetting agents and the fungicides are used in conjunction withan alcohol, as
solvent, for instance, methylalcohol.
An amino condensation product may be added as a softening agent to the mixture to soften the fibers and improve their appearance and feeling.
It is also advisable to use aromatics in order not to leave any unpleasant odors in the textile fibers.
The ingredients of the mixture may be used in different proportions. From 10 to parts by weight of a sulfonated ester of an aliphatic dibasic acid may be used in conjunction with 30 to parts by weight of butyl alcohol to constitute the wetting agent. From 1 to 15 parts by weight of an acid fungicide and/or an alkali fungicide,
such as parachlormetacresol, a thymol derivative,
Or an ester of hydroxybenzoic acid may be mixed with the stated amounts of the wetting agent.
This mixture may receive from 10 to 70 parts by 10 kilograms of a 25% concentration of an ester of a sulphonated bi-carboxylic acid sold on the market under the registered trade-name "Aerosol O T Clear in butyl alcohol are mixed with 9 kilograms of methyl alcohol. 0.25 kilogram of parachlor metacresol, 0.25 kilogram of oil 1nd 0.025 kilogram of a thymol derivative are added to the mixture, along with 0.005 kilogram of a coal tar dye and 0.06 kilogram of an aromatic.
The mixture may be preserved in 50 to 150 liter containers for long periods of time. From. 1% to 10% of the mixture are used in an aqueous solution for spraying the yarn for a few. seconds. The percentage of the mixture in water depends ;o a great extent upon the quality and texture 3f the textile fibers and the subsequent use to v which they are intended.
Example 2 7 kilograms of a 25% concentration of the said Aerosol O '1 Clear are mixed with.2.5 kilograms of a 50% concentration of Aerosol T Clear in butyl alcohol and are added to 10 kilograms of methy alcohol. 3 kilograms of ethylene glycol, 0.25 kilogram of parachlor metacresol, 0.2 kilogram of oil and 0.06 kilogram of a thymol derivative are added to the mixture, in addition to 0.005 kilogram of a coal tar dye and 0.06 kilogram of an aromatic.
The mixture is sprayed upon a textile yarn in in aqueous solution of 1 to 5%.
Example 3 g 14 kilograms of a 50% concentration of Aerosol O T Clear in butyl alcohol are mixed with 11 kilograms of methyl alcohol and 7 kilograms of ethylene glycol, 5 kilograms of sulphonated castor oil, 2.2 kilograms of a thymol :lerivative, 0.04 kilogram of an aromatic (lavender) and 0.008 kilogram of a coal tar dye are added to the mixture.
The mixture is used in an aqueous solution of 1% to 10%.
Example 5 kilograms of sodium alkyl naphthalene sulphonate are mixed with 12 kilograms of ethylene glycol, 10 kilograms of methyl alcohol, 6 kilograms of sulphonated castor oil, 2 kilograms of parachlor metacresol, 0.4 kilograms of an ester of hr'droxybenzoic" acid and chlorinated phenol and 0.01 kilogram of a coal tar dye. The mixture is dissolved for use in 99% to 90% of water.
Example 6 7.2 kilograms of a concentration of Aerosol O T Clear in butyl alcohol are mixed with 6 kilograms of methyl alcohol, and 0.15 kilogram of parachlor metacresol, 0.004 kilogram of a coal tar dye, 0.15 kilogram of Turkey-red oil, 0.3 kilogram of a thymol derivative and 0.02 kilogram of a natural or synthetic aromatic are added to the mixture, the final mixture being used in anaqueous solution of 1% to 10%.
Example 7 example, composition or proportions, as the same may be modified in various particulars or be applied in many varied relations without departclaimed inven ing from the spirit or scope of the tion.
What is claimed is:
1. A composition for the preliminary treatment of textile fibers, comprising, in combination, 10 to 75 parts by weight of a sulfonated ester of an aliphatic dibasic acid, to 150 parts by weight of butyl alcohol and l to 15 parts by weight of a fungicide of the class consisting of parachlormetacresol and parahydroxybenzoic acid esters.
2. A composition for the preliminary treatment of textile fibers, comprising, in combination 10 to parts by weight of a sulfonated ester of an aliphatic dibasic acid, 30 to parts by weight of butyl alcohol, 1 to 15 parts by weight of parachlor metacresol and from 1 to 40 parts by weight of a sulphonated vegetable oil.
CHARLES F. DULKEN.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US305960A US2315405A (en) | 1939-11-24 | 1939-11-24 | Means for treating textiles |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US305960A US2315405A (en) | 1939-11-24 | 1939-11-24 | Means for treating textiles |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| US2315405A true US2315405A (en) | 1943-03-30 |
Family
ID=23183114
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US305960A Expired - Lifetime US2315405A (en) | 1939-11-24 | 1939-11-24 | Means for treating textiles |
Country Status (1)
| Country | Link |
|---|---|
| US (1) | US2315405A (en) |
-
1939
- 1939-11-24 US US305960A patent/US2315405A/en not_active Expired - Lifetime
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