US2268323A - Fastening - Google Patents
Fastening Download PDFInfo
- Publication number
- US2268323A US2268323A US401882A US40188241A US2268323A US 2268323 A US2268323 A US 2268323A US 401882 A US401882 A US 401882A US 40188241 A US40188241 A US 40188241A US 2268323 A US2268323 A US 2268323A
- Authority
- US
- United States
- Prior art keywords
- fastening
- fastenings
- solution
- withdrawal
- monoammonium phosphate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
- C23C22/05—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
- C23C22/06—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6
- C23C22/07—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing phosphates
- C23C22/08—Orthophosphates
Definitions
- Our invention consists of a treatment of ferrous metal fastenings that greatly increases the resistance to withdrawal of the metal fastenings from wood. This improvement-in -resistance to withdrawal is obtained by the simultaneous etching and coating of the surface in such a way that a finely roughened surface is produced. This surface permits a better contact between the fastening and the wood than is possible with plain, cement coated, or grossly roughened surfaces.
- An object of our invention is the production of a fastening by the use of a water solution of monoammonium phosphate.
- the method herein described possesses the advantage of being extremely simple, as no subsequent treatment is necessary after rinsing with water.
- concentration and temperature of the monoammonium phosphate solution employed and the time of exposure of the fastening to the solution may be varied widely to produce fastenings having the desired surface characteristics.
- the fastening to be treated is immersed for substantially seven hours in a substantially ten percent aqueous solution of monoamminum phosphate at room temperature. It is then withdrawn, rinsed with water, and air-dried.
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- Chemical & Material Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Chemical Treatment Of Metals (AREA)
Description
Patented Dec. 30, 1941 FASTENING Theodore J. Martin and Arthur Van Kleeck, Madison, Wis., dedicated to the free use of the People of the United States of America No Drawing. Application July 10, 1941, Serial No. 401,882
(Granted under the act of March 3, 1883, as amended April 30, 1928; 370 O. G. 757) 2 Claims.
This application is made under the act of March 3, 1883, as amended by the act of April 30, 1928, and the invention herein described and claimed, if patented, may be manufactured and used by or for the Govermnent of the United States of America for governmental purposes, without the payment to us of any royalty thereon.
We hereby dedicate the invention herein described, ii patented, to the free use of the people of the United States of America.
Our invention consists of a treatment of ferrous metal fastenings that greatly increases the resistance to withdrawal of the metal fastenings from wood. This improvement-in -resistance to withdrawal is obtained by the simultaneous etching and coating of the surface in such a way that a finely roughened surface is produced. This surface permits a better contact between the fastening and the wood than is possible with plain, cement coated, or grossly roughened surfaces.
An object of our invention is the production of a fastening by the use of a water solution of monoammonium phosphate.
We have found from tests recently made on nails treated with monoammonium phosphate solution that their resistance to withdrawal is considerably greater than that of bright nails.
The principal advantage of our product over those heretofore patented is its simplicity in manufacture. After withdrawal of the nails from the treating solution, a water rinse and air-drying is all that is necessary to produce our product, as compared with an hours exposure to a humidity of 80 per cent at 100 C. in a wellknown patented process.
The mechanism of the process that we prefer to employ in obtaining our product is:
(1) The fastening is subjected to the action of a water solution of ammonium phosphate;
(2) The fastening is withdrawn from the solution, rinsed in water and dried.
The method herein described possesses the advantage of being extremely simple, as no subsequent treatment is necessary after rinsing with water.
We have also found that by the use of monoammonium phosphate our ferrous metal fastenings are resistant to corrosion.
We have also found that the concentration and temperature of the monoammonium phosphate solution employed and the time of exposure of the fastening to the solution may be varied widely to produce fastenings having the desired surface characteristics.
The following is a preferred example of a treatment which has given excellent results for a ferrous metal fastening:
The fastening to be treated is immersed for substantially seven hours in a substantially ten percent aqueous solution of monoamminum phosphate at room temperature. It is then withdrawn, rinsed with water, and air-dried.
A number of tests made on wire nails, treated as above described gave decidedly higher values for resistance to withdrawal than were obtained where similar fastenings having plain, cement .coated or grossly roughened surfaces obtained by sandblasting or treatment with phosphate preparations other than monoammonium phosphate.
Having thus described our invention, what we claim for Letters Patent is:
l. The method of producing increased withdrawal resistance to metal fastenings consisting in treating said fastenings with a chemical solution containing as its essential active ingredient monoammonium phosphate.
2. The process of treating metal fastenings for producing increased withdrawal resistance, which comprises subjecting said fastenings to the action of a bath containing monoammonium phosphate.
thence washing and drying.
THEODORE J. MARTIN. ARTHUR VAN KLEECK.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US401882A US2268323A (en) | 1941-07-10 | 1941-07-10 | Fastening |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US401882A US2268323A (en) | 1941-07-10 | 1941-07-10 | Fastening |
Publications (1)
Publication Number | Publication Date |
---|---|
US2268323A true US2268323A (en) | 1941-12-30 |
Family
ID=23589627
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US401882A Expired - Lifetime US2268323A (en) | 1941-07-10 | 1941-07-10 | Fastening |
Country Status (1)
Country | Link |
---|---|
US (1) | US2268323A (en) |
Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2609308A (en) * | 1947-11-22 | 1952-09-02 | Parker Rust Proof Co | Method and material for producing coatings on metal |
US2702768A (en) * | 1948-07-23 | 1955-02-22 | Parker Rust Proof Co | Ferrous surface coating process using alkali metal phosphates and hydroxylamines |
US2769737A (en) * | 1952-03-26 | 1956-11-06 | Parker Rust Proof Co | Amine phosphate coating solutions and method of coating |
US2811473A (en) * | 1953-12-07 | 1957-10-29 | United States Steel Corp | Composition and method for increasing surface resistivity of silicon steel |
US3020122A (en) * | 1959-05-28 | 1962-02-06 | Colgate Palmolive Co | Inhibiting rusting of aerosol type containers |
US3178319A (en) * | 1958-06-05 | 1965-04-13 | Geraldine D Henricks | Phosphate coating compositions and methods of making and using the same |
US3450576A (en) * | 1965-10-20 | 1969-06-17 | Atomic Energy Commission | Inhibition of uranium metal corrosion |
-
1941
- 1941-07-10 US US401882A patent/US2268323A/en not_active Expired - Lifetime
Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2609308A (en) * | 1947-11-22 | 1952-09-02 | Parker Rust Proof Co | Method and material for producing coatings on metal |
US2702768A (en) * | 1948-07-23 | 1955-02-22 | Parker Rust Proof Co | Ferrous surface coating process using alkali metal phosphates and hydroxylamines |
US2769737A (en) * | 1952-03-26 | 1956-11-06 | Parker Rust Proof Co | Amine phosphate coating solutions and method of coating |
US2811473A (en) * | 1953-12-07 | 1957-10-29 | United States Steel Corp | Composition and method for increasing surface resistivity of silicon steel |
US3178319A (en) * | 1958-06-05 | 1965-04-13 | Geraldine D Henricks | Phosphate coating compositions and methods of making and using the same |
US3020122A (en) * | 1959-05-28 | 1962-02-06 | Colgate Palmolive Co | Inhibiting rusting of aerosol type containers |
US3450576A (en) * | 1965-10-20 | 1969-06-17 | Atomic Energy Commission | Inhibition of uranium metal corrosion |
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