US20040005237A1 - Post-delubrication peening for forged powder metal components - Google Patents

Post-delubrication peening for forged powder metal components Download PDF

Info

Publication number
US20040005237A1
US20040005237A1 US10/367,641 US36764103A US2004005237A1 US 20040005237 A1 US20040005237 A1 US 20040005237A1 US 36764103 A US36764103 A US 36764103A US 2004005237 A1 US2004005237 A1 US 2004005237A1
Authority
US
United States
Prior art keywords
preform
powder metal
component
delubrication
peening
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Abandoned
Application number
US10/367,641
Inventor
Fuping Liu
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Priority to US10/367,641 priority Critical patent/US20040005237A1/en
Assigned to JPMORGAN CHASE BANK, AS COLLATERAL AGENT reassignment JPMORGAN CHASE BANK, AS COLLATERAL AGENT SECURITY INTEREST (SEE DOCUMENT FOR DETAILS). Assignors: METALDYNE CORPORATION
Publication of US20040005237A1 publication Critical patent/US20040005237A1/en
Assigned to METALDYNE CORPORATION reassignment METALDYNE CORPORATION TERMINATION AND RELEASE OF SECURITY INTEREST IN PATENT RIGHTS Assignors: JPMORGAN CHASE BANK, N.A., AS COLLATERAL AGENT
Abandoned legal-status Critical Current

Links

Images

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F3/00Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
    • B22F3/10Sintering only
    • B22F3/1017Multiple heating or additional steps
    • B22F3/1021Removal of binder or filler
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F3/00Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
    • B22F3/12Both compacting and sintering
    • B22F3/16Both compacting and sintering in successive or repeated steps
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F3/00Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
    • B22F3/17Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces by forging
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F2998/00Supplementary information concerning processes or compositions relating to powder metallurgy
    • B22F2998/10Processes characterised by the sequence of their steps

Definitions

  • This invention relates to shot peening a powder metal component and, in particular, to shot peening the powder metal forged component following delubrication but prior to sintering the powder metal component.
  • the powder metal is molded to a desired configuration then sintered to retain the configuration of the component and finally forged to its final configuration.
  • decarburization and oxide penetration occurs between sintering and forging.
  • the hot part After exiting from the sintering furnace, the hot part is exposed to the air and the moisture created by lubricant/coolant spraying prior to forging, the part has interconnected pores throughout. Oxygen and moisture penetrates the surface through these interconnected pores leading to decarburization and oxide penetration.
  • post-forging shot peening removes the oxide on the surface of the component, the oxide entrapped in the channels and pores below the surface remain.
  • the present invention overcomes the disadvantages of the prior known processes for manufacturing powder metal components by shot peening the preform after delubing and prior to sintering to create a densified outer layer to reduce decarburization, oxide penetration and surface porosity on the finished components.
  • the process of the present invention begins by molding powder metal material into a preform configuration.
  • the preform is passed through a delubrication furnace to extract or decompose lubricant found in the preform. This delubrication creates an interconnected porosity. Passing the preform through a shot peening operation closes a majority of the surface pores creating a densified layer with increased ductility and enhanced resistance to cracking.
  • PDP post-delubrication shot peening
  • the component is sintered and then forged into its final configuration.
  • the post-delubrication shot peening eliminates oxide in pores and between particles allowing the forging to be more effective in closing pores and establishing inter-particle bonding.
  • FIG. 1 is a flow chart of a prior art process for forming powder metal components
  • FIG. 2 is a flow chart for the process of the present invention
  • FIG. 3 is an optical micrograph showing the porosity of a preformed powder metal component
  • FIG. 4 is an optical micrograph showing the decarburization of a typical and a component manufacture with the present process.
  • FIGS. 1 and 2 there are shown flow charts for the prior known process 100 of forming a powder metal component and the new process 10 of the present invention.
  • the process 10 can be used in the manufacture of a variety of powder metal components particularly where the strength and reliability of the component is critical.
  • the present process was developed in connection with the manufacture of connecting rods for vehicle engines.
  • the prior known process of sintering and forging powder metal components resulted in oxides trapped in the channels and pores of the preformed powder metal component which can cause fatigue and stress cracks in the component.
  • the process of the present invention begins with compaction or molding 12 of powder metal material into a preform configuration.
  • the molding process 12 utilizes a lubricant to facilitate the molding process.
  • the next step involves delubrication 14 of the perform.
  • delubing 14 is accomplished by passing the perform through a furnace which preheats the component to 1200° F.-1800° F. in an atmosphere which includes H 2 and N 2 .
  • the delubed perform component is subjected to shot peening 16 which creates a densified outer layer within which interconnected pores are eliminated on the component.
  • This Post-Delubrication Peening (PDP) eliminates oxides in pores and between particles throughout an outer layer of the component. Since approximately 60% of component failures are caused by crack initiations within 0.20 mm of the surface, PDP increases the fatigue life of the end product. With PDP, applicant has successfully manufactured powder metal components with improved surface conditions. Furthermore, the densified layer resulting from the PDP 16 increases ductility and enhances resistance to cracking during forging.
  • post-delubrication peening 16 is carried out with a shot speed of less than 100 m/second with a shot hardness of 47-51 Re.
  • the component is sintered 18 and then forged 20 to form the powder metal component. Additional steps such as removal of flash or additional machining may also be applied to the component. In one example, the component is sintered in a furnace less than 2450° F. for less than 60 minutes.

Abstract

A process of forming powder metal components which minimizes decarburization and oxidation of the component prior to final forging. The process begins by molding powder metal material into a preform configuration. The preform is delubricated to extract lubricant found in the pores of the preform. Passing the preform through a shot peening operation closes a majority of the surface pores creating a densified layer within which interconnected pores are eliminated. Following post-delubrication peening (PDP), the component is sintered and then forged into its final configuration.

Description

    CROSS-REFERENCE TO RELATED APPLICATIONS
  • This application claims priority from U.S. Provisional Application No. 60/219,516 filed on Jul. 20, 2000, and is a continuation of U.S. patent application Ser. No. 09/653,889, filed Sep. 1, 2000.[0001]
  • BACKGROUND OF THE INVENTION
  • I. Field of the Invention [0002]
  • This invention relates to shot peening a powder metal component and, in particular, to shot peening the powder metal forged component following delubrication but prior to sintering the powder metal component. [0003]
  • II. Description of the Prior Art [0004]
  • In the currently utilized method of forming powder metal components, the powder metal is molded to a desired configuration then sintered to retain the configuration of the component and finally forged to its final configuration. However, it has been determined that decarburization and oxide penetration occurs between sintering and forging. After exiting from the sintering furnace, the hot part is exposed to the air and the moisture created by lubricant/coolant spraying prior to forging, the part has interconnected pores throughout. Oxygen and moisture penetrates the surface through these interconnected pores leading to decarburization and oxide penetration. Once the surface and pores are oxidized between sintering and forging, it is difficult to close the pores by forging resulting in a weakened component. Although post-forging shot peening removes the oxide on the surface of the component, the oxide entrapped in the channels and pores below the surface remain. [0005]
  • SUMMARY OF THE PRESENT INVENTION
  • The present invention overcomes the disadvantages of the prior known processes for manufacturing powder metal components by shot peening the preform after delubing and prior to sintering to create a densified outer layer to reduce decarburization, oxide penetration and surface porosity on the finished components. [0006]
  • The process of the present invention begins by molding powder metal material into a preform configuration. The preform is passed through a delubrication furnace to extract or decompose lubricant found in the preform. This delubrication creates an interconnected porosity. Passing the preform through a shot peening operation closes a majority of the surface pores creating a densified layer with increased ductility and enhanced resistance to cracking. Following post-delubrication shot peening (hereinafter “PDP”), the component is sintered and then forged into its final configuration. The post-delubrication shot peening eliminates oxide in pores and between particles allowing the forging to be more effective in closing pores and establishing inter-particle bonding. [0007]
  • Other objects, features and advantages of the invention will be apparent from the following detailed description taken in connection with the following drawings.[0008]
  • BRIEF DESCRIPTION OF THE DRAWING
  • The present invention will be more fully understood by reference to the following detailed description of a preferred embodiment of the present invention when read in conjunction with the accompanying drawing, in which like reference characters refer to like parts throughout the views and in which: [0009]
  • FIG. 1 is a flow chart of a prior art process for forming powder metal components; [0010]
  • FIG. 2 is a flow chart for the process of the present invention; [0011]
  • FIG. 3 is an optical micrograph showing the porosity of a preformed powder metal component; and [0012]
  • FIG. 4 is an optical micrograph showing the decarburization of a typical and a component manufacture with the present process.[0013]
  • DETAILED DESCRIPTION OF A PREFERRED EMBODIMENT OF THE PRESENT INVENTION
  • Referring first to FIGS. 1 and 2, there are shown flow charts for the prior known process [0014] 100 of forming a powder metal component and the new process 10 of the present invention. The process 10 can be used in the manufacture of a variety of powder metal components particularly where the strength and reliability of the component is critical. The present process was developed in connection with the manufacture of connecting rods for vehicle engines. The prior known process of sintering and forging powder metal components resulted in oxides trapped in the channels and pores of the preformed powder metal component which can cause fatigue and stress cracks in the component.
  • The process of the present invention begins with compaction or molding [0015] 12 of powder metal material into a preform configuration. The molding process 12 utilizes a lubricant to facilitate the molding process. The next step involves delubrication 14 of the perform. In a preferred embodiment of the process, delubing 14 is accomplished by passing the perform through a furnace which preheats the component to 1200° F.-1800° F. in an atmosphere which includes H2 and N2.
  • In a variation from the prior known processes, the delubed perform component is subjected to shot peening [0016] 16 which creates a densified outer layer within which interconnected pores are eliminated on the component. This Post-Delubrication Peening (PDP) eliminates oxides in pores and between particles throughout an outer layer of the component. Since approximately 60% of component failures are caused by crack initiations within 0.20 mm of the surface, PDP increases the fatigue life of the end product. With PDP, applicant has successfully manufactured powder metal components with improved surface conditions. Furthermore, the densified layer resulting from the PDP 16 increases ductility and enhances resistance to cracking during forging. In a preferred embodiment of the process, post-delubrication peening 16 is carried out with a shot speed of less than 100 m/second with a shot hardness of 47-51 Re.
  • Following the PDP step [0017] 16, the component is sintered 18 and then forged 20 to form the powder metal component. Additional steps such as removal of flash or additional machining may also be applied to the component. In one example, the component is sintered in a furnace less than 2450° F. for less than 60 minutes.
  • The concept of PDP was inspired by analysis of powder metal connecting rods which showed fatigue cracks just below the surface of the component. An optical micrograph of the component in FIG. 3 shows that porosity morphology is affected by oxidation. FIG. 4 depicts the reduction of decarburization achieved by PDP on the surface of the connecting rod. Accordingly, it has been found that post-delubrication peening reduces oxides and decarburization by over 70% creating a surface condition better than that of the prior known process. The densified surface layer achieved by PDP enhances powder metal component performance whether forging is applied as a secondary operation or not. [0018]
  • The foregoing detailed description has been given for clearness of understanding only and no unnecessary limitations should be understood therefrom as some modifications will be obvious to those skilled in the art without departing from the scope and spirit of the appended claims. [0019]

Claims (9)

What is claimed is:
1. A process for the manufacture of powder metal components comprising the steps of:
molding a powder metal material into a preform configuration;
delubricating said powder metal preform;
subjecting said powder metal preform to shot peening to density an outer layer of said preform;
sintering said shot peened preform; and
forging said sintered preform.
2. The process as defined in claim 1 wherein said powder metal preform is subjected to a shot speed of less than 100 meters per second.
3. The process as defined in claim 1 wherein said powder metal preform is delubricated at a temperature between 1200° F. and 1800° F. in an atmosphere which includes N2 and H2.
4. A process for the manufacture of powder metal components comprising the steps of:
molding a powder metal material into a preform configuration; subjecting said preform to a process for densifying the surface of said preform;
sintering said preform; and forging said preform.
5. The process of claim 4 wherein said surface densification process comprises shot peening.
6. The process of claim 5 wherein the shot hardness is between 47 to 51 Re.
7. The process as defined in claim 5 wherein said powder metal preform is subjected to a shot speed of less than 100 meters per second.
8. The process as defined in claim 4 wherein said sintering of said preform is preformed in a furnace less than 2,450° F.
9. The process as defined in claim 8 wherein said perform is sintered in said furnace for less than 60 minutes.
US10/367,641 2000-07-20 2003-02-14 Post-delubrication peening for forged powder metal components Abandoned US20040005237A1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
US10/367,641 US20040005237A1 (en) 2000-07-20 2003-02-14 Post-delubrication peening for forged powder metal components

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US21951600P 2000-07-20 2000-07-20
US65388900A 2000-09-01 2000-09-01
US10/367,641 US20040005237A1 (en) 2000-07-20 2003-02-14 Post-delubrication peening for forged powder metal components

Related Parent Applications (1)

Application Number Title Priority Date Filing Date
US65388900A Continuation 2000-07-20 2000-09-01

Publications (1)

Publication Number Publication Date
US20040005237A1 true US20040005237A1 (en) 2004-01-08

Family

ID=30002728

Family Applications (1)

Application Number Title Priority Date Filing Date
US10/367,641 Abandoned US20040005237A1 (en) 2000-07-20 2003-02-14 Post-delubrication peening for forged powder metal components

Country Status (1)

Country Link
US (1) US20040005237A1 (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2011142813A1 (en) 2010-05-12 2011-11-17 Cellectis Sa Dynamic mixing and electroporation chamber and system
CN102421554A (en) * 2009-05-04 2012-04-18 Gkn烧结金属股份有限公司 Adhesive joining for powder metal components
GB2519190A (en) * 2012-02-24 2015-04-15 Charles Malcolm Ward-Close Processing of metal or alloy objects
CN111421137A (en) * 2020-06-09 2020-07-17 宁波海特技术转移有限公司 Electric heating forging and sintering integrated method for powder sintered part blank

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3779747A (en) * 1972-09-05 1973-12-18 Gleason Works Process for heating and sintering ferrous powder metal compacts
US3795129A (en) * 1971-10-07 1974-03-05 S Goto Method of forging sintered articles of high density
US6171546B1 (en) * 1996-06-14 2001-01-09 Högan{umlaut over (a)}s AB Powder metallurgical body with compacted surface

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3795129A (en) * 1971-10-07 1974-03-05 S Goto Method of forging sintered articles of high density
US3779747A (en) * 1972-09-05 1973-12-18 Gleason Works Process for heating and sintering ferrous powder metal compacts
US6171546B1 (en) * 1996-06-14 2001-01-09 Högan{umlaut over (a)}s AB Powder metallurgical body with compacted surface

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102421554A (en) * 2009-05-04 2012-04-18 Gkn烧结金属股份有限公司 Adhesive joining for powder metal components
US20120132160A1 (en) * 2009-05-04 2012-05-31 Gerald Michael Malen Adhesive joining for powder metal components
US8857390B2 (en) * 2009-05-04 2014-10-14 Gkn Sinter Metals, Llc Adhesive joining for powder metal components
WO2011142813A1 (en) 2010-05-12 2011-11-17 Cellectis Sa Dynamic mixing and electroporation chamber and system
GB2519190A (en) * 2012-02-24 2015-04-15 Charles Malcolm Ward-Close Processing of metal or alloy objects
GB2519190B (en) * 2012-02-24 2016-07-27 Malcolm Ward-Close Charles Processing of metal or alloy objects
CN111421137A (en) * 2020-06-09 2020-07-17 宁波海特技术转移有限公司 Electric heating forging and sintering integrated method for powder sintered part blank

Similar Documents

Publication Publication Date Title
US7416696B2 (en) Powder metal materials and parts and methods of making the same
US5878323A (en) Process for producing split type mechanical part
KR100405910B1 (en) Process for the preparation of a powder metallurgical component and compacted component of metal powder
JP3774625B2 (en) Method for forging sintered parts
US20040005237A1 (en) Post-delubrication peening for forged powder metal components
JP3389590B2 (en) Manufacturing method of connecting rod
JP3499370B2 (en) Sintering cold forging method
DE102015216321A1 (en) Method for producing a piston
US6537487B1 (en) Method of manufacturing form tools for forming threaded fasteners
JPH11117002A (en) Compact raw material of metallic powder and its production
US5997605A (en) Method of producing mating parts
US11719138B2 (en) Sintered alloy valve guide and method of producing sintered alloy valve guide
JPS59155660A (en) Hollow cam shaft and manufacture thereof
JPH0610284B2 (en) Sintered member manufacturing method
JP3835103B2 (en) Sintered alloy and method of hardening the same
JPH0623403B2 (en) Manufacturing method of sintered forged joint
JP3871825B2 (en) Recompression molded body of metallic powder molding material, sintered body obtained from the recompression molded body, and production method thereof
JP2002235865A (en) Solenoid core of solenoid valve and its manufacturing method
JP2001294904A (en) Method for producing iron sintered parts
JPH08143910A (en) Production of sintered forged product
KR102541042B1 (en) Die casting using sintered material and die casting product manufactured therefrom
JP2000063908A (en) Sintered forged part and production thereof
JP3763796B2 (en) Manufacturing method of sintered member with inner hole with excellent coaxiality accuracy
JPS5993803A (en) Composite sintering and forging method
JP3003257B2 (en) Manufacturing method of alloy members

Legal Events

Date Code Title Description
AS Assignment

Owner name: JPMORGAN CHASE BANK, AS COLLATERAL AGENT, NEW YORK

Free format text: SECURITY INTEREST;ASSIGNOR:METALDYNE CORPORATION;REEL/FRAME:014836/0307

Effective date: 20001128

STCB Information on status: application discontinuation

Free format text: ABANDONED -- FAILURE TO RESPOND TO AN OFFICE ACTION

AS Assignment

Owner name: METALDYNE CORPORATION, MICHIGAN

Free format text: TERMINATION AND RELEASE OF SECURITY INTEREST IN PATENT RIGHTS;ASSIGNOR:JPMORGAN CHASE BANK, N.A., AS COLLATERAL AGENT;REEL/FRAME:018861/0489

Effective date: 20070111