US1740227A - Cellulose precipitating agent - Google Patents
Cellulose precipitating agent Download PDFInfo
- Publication number
- US1740227A US1740227A US132900A US13290026A US1740227A US 1740227 A US1740227 A US 1740227A US 132900 A US132900 A US 132900A US 13290026 A US13290026 A US 13290026A US 1740227 A US1740227 A US 1740227A
- Authority
- US
- United States
- Prior art keywords
- methanol
- cellulose
- threads
- precipitating agent
- manufacture
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 229920002678 cellulose Polymers 0.000 title description 12
- 239000001913 cellulose Substances 0.000 title description 12
- 230000001376 precipitating effect Effects 0.000 title description 10
- 239000003795 chemical substances by application Substances 0.000 title description 2
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 51
- 239000000243 solution Substances 0.000 description 14
- 238000004519 manufacturing process Methods 0.000 description 9
- 229920002955 Art silk Polymers 0.000 description 7
- 239000007864 aqueous solution Substances 0.000 description 6
- 229920000297 Rayon Polymers 0.000 description 5
- 229910017053 inorganic salt Inorganic materials 0.000 description 3
- 238000001556 precipitation Methods 0.000 description 3
- TWRXJAOTZQYOKJ-UHFFFAOYSA-L Magnesium chloride Chemical compound [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 description 2
- CSNNHWWHGAXBCP-UHFFFAOYSA-L Magnesium sulfate Chemical compound [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 description 2
- 150000007522 mineralic acids Chemical class 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000002253 acid Substances 0.000 description 1
- 230000015271 coagulation Effects 0.000 description 1
- 238000005345 coagulation Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000002657 fibrous material Substances 0.000 description 1
- 229910001629 magnesium chloride Inorganic materials 0.000 description 1
- 229910052943 magnesium sulfate Inorganic materials 0.000 description 1
- 235000019341 magnesium sulphate Nutrition 0.000 description 1
- AFCCDDWKHLHPDF-UHFFFAOYSA-M metam-sodium Chemical compound [Na+].CNC([S-])=S AFCCDDWKHLHPDF-UHFFFAOYSA-M 0.000 description 1
- 125000001570 methylene group Chemical group [H]C([H])([*:1])[*:2] 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 239000004627 regenerated cellulose Substances 0.000 description 1
- 239000012266 salt solution Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F2/00—Monocomponent artificial filaments or the like of cellulose or cellulose derivatives; Manufacture thereof
- D01F2/06—Monocomponent artificial filaments or the like of cellulose or cellulose derivatives; Manufacture thereof from viscose
- D01F2/08—Composition of the spinning solution or the bath
Definitions
- This invention has reference to improvements in the precipitation of cellulose from its solutions by means of which a very strong and superior grade of an artificial fibrous material may be produced.
- aqueous or acidified aqueous salt solutions have been employed as a rule.
- a precipitating bath in which the Water is replaced by methanol presents great advantages over the precipitating baths heretofore known.
- aprecipitating bath consisting of a solution of magnesium chloride or magnesium-sulphate in methanol and an inorganic acid is particularly suitable. It is also possible within the scope of this invention to employ a mixture of methanol and aninorganic acid or merely a solution of an inorganic salt in methanol.
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Artificial Filaments (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE1740227X | 1925-09-01 |
Publications (1)
Publication Number | Publication Date |
---|---|
US1740227A true US1740227A (en) | 1929-12-17 |
Family
ID=7741328
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US132900A Expired - Lifetime US1740227A (en) | 1925-09-01 | 1926-08-31 | Cellulose precipitating agent |
Country Status (4)
Country | Link |
---|---|
US (1) | US1740227A (enrdf_load_stackoverflow) |
BE (1) | BE335964A (enrdf_load_stackoverflow) |
FR (1) | FR620612A (enrdf_load_stackoverflow) |
NL (1) | NL21229C (enrdf_load_stackoverflow) |
-
0
- BE BE335964D patent/BE335964A/xx unknown
- NL NL21229D patent/NL21229C/xx active
-
1926
- 1926-08-25 FR FR620612D patent/FR620612A/fr not_active Expired
- 1926-08-31 US US132900A patent/US1740227A/en not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
FR620612A (fr) | 1927-04-26 |
BE335964A (enrdf_load_stackoverflow) | |
NL21229C (enrdf_load_stackoverflow) |
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