US165189A - Improvement in the manufacture of gas - Google Patents

Improvement in the manufacture of gas Download PDF

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US165189A
US165189A US165189DA US165189A US 165189 A US165189 A US 165189A US 165189D A US165189D A US 165189DA US 165189 A US165189 A US 165189A
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gas
retort
manufacture
pipe
improvement
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    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10JPRODUCTION OF PRODUCER GAS, WATER-GAS, SYNTHESIS GAS FROM SOLID CARBONACEOUS MATERIAL, OR MIXTURES CONTAINING THESE GASES; CARBURETTING AIR OR OTHER GASES
    • C10J3/00Production of combustible gases containing carbon monoxide from solid carbonaceous fuels

Definitions

  • Fig. 2 is a top view of the perforated or grated bottom of the vertical retort shown in Fig. l.
  • My invention relates to the manufacture of illuminating-gas; and consists in superheatin g an admixture of hydrocarbon vapors and steam or aqueous vapors, and then passing the same through an incandescent mass of mixed carbonaceous and decomposing material contained within a closed chamber.
  • A indicates a vertical retort, of brick or other suitable refractory material, surrounded by an iron jacket or casing, B, between which and the brick-work is a small intermediate space, b, which may be filled with broken brick, or similar material commonly employed in Iilling in, where allowance is to be made for expansion and contraction in structures.
  • the bottom of vertical chamber A is grated or reticulated to permit the upward passage of air from pit a, into which it is forced through pipe C.
  • D D are doors or man-holes, one above and the other below the grated bottom or diaphragm al and a2 are a series of holes made through the walls of the retort for the introduction of a rod or poker to loosen up the contents of the retort when necessary.
  • the holes a2 are closed by a cap or :other suitable means.
  • E is the exit-pipe for gas to be used for heating or illuminating
  • F a similar-pipev :forconducting oif waste gases
  • G being a bell or other closed hopper for filling the chamber with carbonaceons and other material.
  • I proceed as follows: The valve in wastepipe F being opened and Jthat in E closed, a fire is started on the perforated or grated diaphragm and the chamber filled with' coal, anthrapite coal, or breeze, and a niixture oftle sziwwitli'"ci'der or" slag containing carbonaceous matter and iron.
  • the blast is admitted through pipe C, and the waste gases, carbonio acid, nitrogen, die., conducted oif by pipe F and utilized.
  • valves in pipe F and C are closed by shutting on" the blast, the valve in pipe E, leading to the Wadshers, exhaust-pum andgsuowmeten is o M r 1-lew,an steam and hlfdrocarbonsware'ditted into pipe s, whence, after becoming admixed and superheated, they are discharged into the incandescent material contained in the retort, where decomposition and recomposition takes place. ⁇
  • the iron by its presence with the carbonaceous material in the retort at the time the superheated admixture of steam and hydrocarbon is passed through, facilitates the decomposition and recomposition of the several gases and vapors, adding to the speed and certainty of the process.
  • the temperature of the mass in the retort will be reduced belov.' the working point, and as soon as this is discovered the steam is shut off, the valve leading to the gasometer closed, and those in the blast and waste-gas pipe opened, which will soon bring up the contents of the retort to the required temperature, after which the several steps above described may be repeated.
  • the gas produced as above may, subsequent to its production, be carbureted by passing it through or over gasoline or other light petroleum products.
  • the gas, subsequent or prior to this, may be purified from sulphuretl ed hydrogen by passing it through oxide of iron, and the carbonic-acid gas by washing through caustic soda or lime.

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Combustion & Propulsion (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Manufacture And Refinement Of Metals (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
  • Carbon And Carbon Compounds (AREA)

Description

4H. w c. TwEnnLE.
VManufacturas ofas.
Patented July 6,1875.
No. |6-5,\a9.
UNITED STATES PATENT CEEIGE.
`HERBERTVV. C. TWEDDLE, OF PITTSBURG, PENNSYLVANIA.
IMPROVEMENT IN THE MANuFAcTuRE oF GAS.
,Specification forming part of Letters Patent No. 165.189, dated July 6, 1875 application tiled l March 5, 1875.
To all whom it may concern Be it known that l, HERBERT W. U. TWED- DLE, of Pittsburg, in the county of Allegheny and State ofPennsylvaniamave invented a new and useful Improvement in Manufacture of Gas; and I do hereby declare the following to be a full, clear, and exact description thereof', reference being had to the accompanying drawing forming part of this specification, in Which- Figure 1 is a View of apparatus which may be employed in carrying out my invention. Fig. 2 is a top view of the perforated or grated bottom of the vertical retort shown in Fig. l.
Like letters refer to like parts wherever they occur.
My invention relates to the manufacture of illuminating-gas; and consists in superheatin g an admixture of hydrocarbon vapors and steam or aqueous vapors, and then passing the same through an incandescent mass of mixed carbonaceous and decomposing material contained within a closed chamber.
I will first describe the apparatus that may be employed, referring therefor to the accompanying drawing, and then specify the method of using the devices.
In the drawing, A indicates a vertical retort, of brick or other suitable refractory material, surrounded by an iron jacket or casing, B, between which and the brick-work is a small intermediate space, b, which may be filled with broken brick, or similar material commonly employed in Iilling in, where allowance is to be made for expansion and contraction in structures. The bottom of vertical chamber A is grated or reticulated to permit the upward passage of air from pit a, into which it is forced through pipe C. D D are doors or man-holes, one above and the other below the grated bottom or diaphragm al and a2 are a series of holes made through the walls of the retort for the introduction of a rod or poker to loosen up the contents of the retort when necessary. The holes a2 are closed by a cap or :other suitable means. Arranged within the brick-work is a steam-pipe, s, perforated at different points to admit steam to the interior ofthe retort, and connecting at one or more points with branch pipes o, which is used for introducing a hydrocarbon, so that steam and hydrocarbon may be forced into the vertical chamber at a point above the diaphragm. E is the exit-pipe for gas to be used for heating or illuminating, and F a similar-pipev :forconducting oif waste gases, G being a bell or other closed hopper for filling the chamber with carbonaceons and other material. The several pipes C, E, F, and o 'are provided with suitable valves, as shown at c, e, f, and o. h h are sight-holes for examining the state of the retort.
Having an apparatus of the class described, I proceed as follows: The valve in wastepipe F being opened and Jthat in E closed, a fire is started on the perforated or grated diaphragm and the chamber filled with' coal, anthrapite coal, or breeze, and a niixture oftle sziwwitli'"ci'der or" slag containing carbonaceous matter and iron. The blast is admitted through pipe C, and the waste gases, carbonio acid, nitrogen, die., conducted oif by pipe F and utilized. As soon as the mass withinthe chamber has been raised to the desired temperature, the valves in pipe F and C are closed by shutting on" the blast, the valve in pipe E, leading to the Wadshers, exhaust-pum andgsuowmeten is o M r 1-lew,an steam and hlfdrocarbonsware'ditted into pipe s, whence, after becoming admixed and superheated, they are discharged into the incandescent material contained in the retort, where decomposition and recomposition takes place.`
The iron, by its presence with the carbonaceous material in the retort at the time the superheated admixture of steam and hydrocarbon is passed through, facilitates the decomposition and recomposition of the several gases and vapors, adding to the speed and certainty of the process. After this operation has been conducted for a time, the temperature of the mass in the retort will be reduced belov.' the working point, and as soon as this is discovered the steam is shut off, the valve leading to the gasometer closed, and those in the blast and waste-gas pipe opened, which will soon bring up the contents of the retort to the required temperature, after which the several steps above described may be repeated.
It may at times be advantageous to admit steam for a short time after the-air-blast has been cut on, and before the valve in the wastegas pipe has been closed, so as to insure the freedom ofthe retort from waste gases before the Valve leading to the gasometer is opened. During the working ofthe retort a slight vacuum is kept up by means of a pump or other' means.
The gas produced as above may, subsequent to its production, be carbureted by passing it through or over gasoline or other light petroleum products. The gas, subsequent or prior to this, may be purified from sulphuretl ed hydrogen by passing it through oxide of iron, and the carbonic-acid gas by washing through caustic soda or lime.
By this process one ton (two thousand two hundred and forty pounds) of hard coal or coke will produce about one hundred and iifty-ve thousand/feet of heating-gas 5 added to which two and a half to three gallons of gasoline of high quality will produce a gas of sixteen-candle power.
Having thus described my invention, what I claim, and desire to secure by Letters Patent, is-
As an improvement in the manufacture of illuminating-gas, the process herein described, viz., superheatin g anV admixture of hydrocarbon vapor and steam, and then passing the salne through an incandescent mass of mixed carbonaceous and decomposing material contained within a closed chamber, substantially as specified.
In testimony whereof I, the said HERBERT W. C. TWEDDLE, have hereunto set my hand. Y HERBERT WV. C. TWEDDLE.
Witnesses:
F. W. RITTER, Jr., T. B. KERR.
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