US159451A - Joseph w - Google Patents
Joseph w Download PDFInfo
- Publication number
- US159451A US159451A US159451DA US159451A US 159451 A US159451 A US 159451A US 159451D A US159451D A US 159451DA US 159451 A US159451 A US 159451A
- Authority
- US
- United States
- Prior art keywords
- cylinder
- pipe
- steam
- liquor
- joseph
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 239000000126 substance Substances 0.000 description 18
- 239000012535 impurity Substances 0.000 description 8
- 239000001760 fusel oil Substances 0.000 description 6
- 239000000463 material Substances 0.000 description 6
- 238000000034 method Methods 0.000 description 4
- 238000000746 purification Methods 0.000 description 4
- 229920002472 Starch Polymers 0.000 description 2
- 241000009298 Trigla lyra Species 0.000 description 2
- 239000011358 absorbing material Substances 0.000 description 2
- 239000003610 charcoal Substances 0.000 description 2
- 238000005352 clarification Methods 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 230000002939 deleterious Effects 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 239000003921 oil Substances 0.000 description 2
- 230000001706 oxygenating Effects 0.000 description 2
- 235000015096 spirit Nutrition 0.000 description 2
- 235000019698 starch Nutrition 0.000 description 2
- 239000008107 starch Substances 0.000 description 2
- 235000020357 syrup Nutrition 0.000 description 2
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/30—Processes for preparing, regenerating, or reactivating
- B01J20/34—Regenerating or reactivating
- B01J20/345—Regenerating or reactivating using a particular desorbing compound or mixture
- B01J20/3458—Regenerating or reactivating using a particular desorbing compound or mixture in the gas phase
- B01J20/3466—Regenerating or reactivating using a particular desorbing compound or mixture in the gas phase with steam
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/30—Processes for preparing, regenerating, or reactivating
- B01J20/34—Regenerating or reactivating
- B01J20/345—Regenerating or reactivating using a particular desorbing compound or mixture
- B01J20/3475—Regenerating or reactivating using a particular desorbing compound or mixture in the liquid phase
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2220/00—Aspects relating to sorbent materials
- B01J2220/50—Aspects relating to the use of sorbent or filter aid materials
- B01J2220/58—Use in a single column
Definitions
- This invention consists in an improved mode or process of purifying and renewing the packing or absorbln g material without removing the same from the cylinder, all substantiallyr as I will now proceed to describe.
- A is the cylinder in which the liquors are treated.
- B is the pump by which the liquors are forced into the cylinder.
- O is the supply-pipe through which the liquor is forced.
- D is the feed-pipe through which the liquor is drawn by the pump B.
- E is the waste-pipe through which the surplus liquor is allowed to escape into the receptacle from whence it was drawn.
- F represents a safetyvalve in the supply-pipe C
- Gr is a pressurea b c d ef represent the screens with which the cylinder is provided.
- g is a check-valve in the supply-pipe C.
- k is the separate airpump.
- m is the steam-pipe connecting the same with 4 the boiler, and is provided with a cock, w1.
- n is the pipe for conducting air or steam into the cylinder. I? is the superheater connected with the pipe n. 1" is a pipe connecting the steam-pipe m with the pipe n.
- s is the pressure-gage; t, safety-valve.
- c is the charging-screw in the cylinder.
- y is the double or T-shaped discharge-pipe at the bottom of the cylinder, each branch of which is provided with a cock, .r2 x3.
Landscapes
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Distillation Of Fermentation Liquor, Processing Of Alcohols, Vinegar And Beer (AREA)
Description
gage in the same.
UNITED STATES JOSEPH W. REFORD, OF NEW YORK, N. Y.,AASSIGNOR OF ONE-HALF HIS RIGHT TO WILLIAM WATT, JR., OF SAME PLAGE.
IMPROVEMENT IN THE PURIFICATION 0F FILTERING AND OXYGENATING SUBSTANCES WHILEWITHIN THE RECTlFYlNG-CYLINDER.
Specification forming part of Letters Patent No. 159,451, dated February 2, 1875; application led September 25, 1874.
same parts.
This invention consists in an improved mode or process of purifying and renewing the packing or absorbln g material without removing the same from the cylinder, all substantiallyr as I will now proceed to describe.
In the drawings, A is the cylinder in which the liquors are treated. B is the pump by which the liquors are forced into the cylinder. O is the supply-pipe through which the liquor is forced. D is the feed-pipe through which the liquor is drawn by the pump B. E is the waste-pipe through which the surplus liquor is allowed to escape into the receptacle from whence it was drawn. F represents a safetyvalve in the supply-pipe C, and Gr is a pressurea b c d ef represent the screens with which the cylinder is provided. g is a check-valve in the supply-pipe C.
In my improvements k is the separate airpump. m is the steam-pipe connecting the same with 4 the boiler, and is provided with a cock, w1. n is the pipe for conducting air or steam into the cylinder. I? is the superheater connected with the pipe n. 1" is a pipe connecting the steam-pipe m with the pipe n. s is the pressure-gage; t, safety-valve. c is the charging-screw in the cylinder. y is the double or T-shaped discharge-pipe at the bottom of the cylinder, each branch of which is provided with a cock, .r2 x3.
'Io enable those skilled in the art to fully understand and use my invention, I will proceed to describe its operation.
After the packing has been -used until it becomes foul, Iforce all of the liquor out ofthe cylinder, by means of a jet of steam introduced through the pipe m and the pipes r and n, rst closing the cocks mi and x4 and opening x5. I then remove the charging-screw o in the cylinder, and introduce certain chemicals in a liquid form-which may be sugar and starch-which unite with and take up the fusel-oil and other impurities left by the liquor in its passage through JEhe several different clarifying substances. 'lhese impurities are then, with the chemicals, expelled from the cylinder by ordinary steam pressure through the pipe y into a separate receptacle from that into which the rectified liquor is discharged, the cock x2 in the discharge-pi pe being rst closed and m3 opened for the purpose. By this means the fusel-oil and other impure substances extracted from the liquor are saved, and may be utilized for other purposes. I then open the cocks .nl and m4 and closest5 inthe piper, and introduce into the cylinder, through the pipes m and n, a jet of steam, which passes through the superheater l?, and is thereby raised to 3000 Farenheit, more or less, as is found necessary. This steam in its passage through the cylinder thoroughly carbonizes and renews the clarifying material without the necessity of its removal from the cylinder, and the apparatus is again ready to continue the rectifying operation, thus economizing much time and material.V
I have mentioned as chemicals, to be introduced at the charging screw o, sugar and starch, but any other substances which will readily combine with and carry off the fuseloil and other impurities, withoutl leaving any deleterious residuum or destroying the character of the packing, may be used. These chemicals are adapted to the purification of the packing, after spirits have been clarified. Other suitable substances may be used after the clarification of sirups or oils. The vsuperheater P may be heated with either charcoal or gas, and is only intended to be used during the cleaning process.
PATENT GEEIGE.
whereby the grosser and valuable deposits are removed, and by them introducing superheated steam into the top of the cylinder, and forcing it through the packing or absorbing material, whereby the finer impurities are removed, substantially as described, and for the purpose specified.
JOSEPH WM. REFORD.
Witnesses:
WM. WATT, Jr., W. W. SMITH.
Publications (1)
| Publication Number | Publication Date |
|---|---|
| US159451A true US159451A (en) | 1875-02-02 |
Family
ID=2228861
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US159451D Expired - Lifetime US159451A (en) | Joseph w |
Country Status (1)
| Country | Link |
|---|---|
| US (1) | US159451A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3528657A (en) * | 1967-09-21 | 1970-09-15 | Richard Quelch | Suspension seat toy and juvenile rest furniture |
-
0
- US US159451D patent/US159451A/en not_active Expired - Lifetime
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3528657A (en) * | 1967-09-21 | 1970-09-15 | Richard Quelch | Suspension seat toy and juvenile rest furniture |
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