US1529919A - Pulp-bleaching method and apparatus - Google Patents

Pulp-bleaching method and apparatus Download PDF

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US1529919A
US1529919A US541463A US54146322A US1529919A US 1529919 A US1529919 A US 1529919A US 541463 A US541463 A US 541463A US 54146322 A US54146322 A US 54146322A US 1529919 A US1529919 A US 1529919A
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pulp
bleaching
main
air
uptake
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US541463A
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August F Richter
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Stebbins Engineering and Manufacturing Co
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Stebbins Engineering and Manufacturing Co
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    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21CPRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C9/00After-treatment of cellulose pulp, e.g. of wood pulp, or cotton linters ; Treatment of dilute or dewatered pulp or process improvement taking place after obtaining the raw cellulosic material and not provided for elsewhere
    • D21C9/10Bleaching ; Apparatus therefor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/50Circulation mixers, e.g. wherein at least part of the mixture is discharged from and reintroduced into a receptacle

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  • This invention is designed to provide a simple and eicient method and apparatus for carrying out the pulp-bleaching method disclosed" in Heiskan'en Patent No. 1,27*?,- 926, dated Sept. 3, 1918, and the speclal object of the invention is to so construct the apparatus as to reduce to a minimum the consumption of steam, bleach and power, as more fully hereinafter set forth.
  • FIG. 1 is a view partly in side elevation and partly in vertical section, taken on the line 1--1 of Fig. 2;
  • Fig. 2 is a miniature plan view of a series of units of my apparatus
  • Fig. 3 is a detail vertical sectional view through the air ring or nozzle.
  • 5 designates the main tank of each unit and 6 two supplemental conduits or receptacles arranged at opposite sides of the main receptacle, all three receptacles being circular in crosssection.
  • the supplemental receptacles 6 are much smaller in diameter than the main receptacle and they serve to convey 'the pulp and bleach to the upper end of the main receptacle and empty the same thereinto, the upper ends of these uptakes 6 entering the main receptacle at opposite sides through openings therein, these openings being located at or near the upper end of the main receptacle.
  • the bottom of the main tank is tapered downwardly to a throat 7 leading into a short horizontal conduit 8 which forms a part of the uptakes 6, each end of this conduit being connected to the adjacent lower end of one of the uptakes by a curved upwardly-tapering conduit 9.
  • Extending through stuliing-boxes 10 in the walls of the curved conduits 9 is a shaft 11 mounted in suitable bearings 12 and driven by Suitable fast and loose pulleys 13.
  • Axed. to the shaft 11 is a air of screw-impellers 14 which fit the conduit 8 and are arranged at opposite sides .of the throat 7.
  • impellers are arranged to oppose each other, so as to impel the pul outwardly in opposite directions from t e throat 7, so that in the operation of the apparatus these screw-impellers will draw equal amounts of pulp down through throat 7 and for-ce it outwardly and upwardly into the uptakes, thereby delivering it back into 'the main receptacle at the upper ends thereof.
  • This arrangement of opposed impellers and two uptakes enables me to move the pulp without end-thrust on the impeller shaft, since the two impellers balance each other so far as end-thrust is concerned.
  • the main receptacles are located side by side, as shown in Fig. 2, and are connected by overflow tubes or troughs 15, in each of which works a screw 16, these screws all being fastened to a common shaft 17 driven by any suitable power mechanism.
  • the pulp is kept in constant circulation in each unit (a unit being composed of a main ⁇ .tank and two supplemental uptakes) and at the same time a quantity of the pulp equal to the quantity fed into the first tank is carried over into the next adjacent tank.
  • the screws or Ipropellers 16 ensure a constant and uniform feed of the pulp from unit to unit and enables me to handlethick pulp.
  • Each of the curved conduits 9 is connected to the vertical part of the uptake .ASSIGNOR TO STEBBINS ENGL by means of an air-ring 18 which is hol-y low and is adapted to be connected to a compressed-air supply through an inlet 19.
  • the interior of the ring 18. is connected to a supplemental air channel 20 by means of air-holes 21, associated with each of -which is a needle-valve 22 by which the amount of air entering-the hole' 21 is regulated.
  • the annular channel 20 is connected to the interior of the uptake by upwardlyinclined nozzle-passages 23, whereby one or more upwardly-directed'compressed-air currentsv is directed into the upgoing mass of pulp.
  • liquor of the bleach comes in contact with cellulose or pulp is greatly aided by this aeration, thereby speeding up the bleaching action.
  • an apparatus for bleaching pulp a main-tank, a pair of conduits arranged at- 'opposite sides of the' main tank having their upper ends discharging into the main tank, a horizontal conduit arranged across the lower, open end of the main tank and arranged to discharge into the lower ends ofthe conduits, and a shaft extending horizontally through said horizontal conduit and provided with a pair of. opposed propellers arranged at opposite sides of said open end of the main tank, for the purpose set forth.
  • a. pulp-bleaching apparatus em bodying an uptake for conveying the pulp upwardly, means for propelling the pulp, and means for introducing a bleaching-accelerating fluid under pressure into said uptake, this latter means embodying a plurality of nozzles arranged around the uptake and directed upwardly to thereby introduce theizid into the mass of pulp in the form of aplurality of upwardly-directed streams, for the purpose set forth;
  • tank-units each comprising a mam vtank and a palr of supplemental or uptake.

Description

March 17, 1925. 1,529,919
A. F. RICHTER PULP BLEAGHING METHOD AND APPARATUS Filed March 6, 1922 Patented Mar. 17, 1925.
AUGUST F. RICHTER, OF WATERTOWN, NEW YORK, NEERING AND MANUFACTURING COMPANY, OF
PORATION OF NEW YORK. A
WATERTOWN, NEW YORK, A COR- PULP-BLEACHING METHOD AND APPARATUS.A
Application tiled March 6, 1922. Serial No. 541,463.
To all whom it may concern. y Be it known that I, AUGUST F. RICHTER, a citizen of the United States of America, and a resident of Watertown, county .of Jefferson, and State of New York, have 1nvented certain new and useful Improvements in Pulp-Bleaching Methods and Apparatus, of which the following is a full and clear specification. Y
This invention is designed to provide a simple and eicient method and apparatus for carrying out the pulp-bleaching method disclosed" in Heiskan'en Patent No. 1,27*?,- 926, dated Sept. 3, 1918, and the speclal object of the invention is to so construct the apparatus as to reduce to a minimum the consumption of steam, bleach and power, as more fully hereinafter set forth.
It will be understood, however, that this invention is not exclusively confined to the carrying out of the method disclosed in the aforesaid patent.
In the drawing- Fig. 1 is a view partly in side elevation and partly in vertical section, taken on the line 1--1 of Fig. 2;
Fig. 2 is a miniature plan view of a series of units of my apparatus; i
Fig. 3 is a detail vertical sectional view through the air ring or nozzle.
Referring to the drawing, 5 designates the main tank of each unit and 6 two supplemental conduits or receptacles arranged at opposite sides of the main receptacle, all three receptacles being circular in crosssection. The supplemental receptacles 6 are much smaller in diameter than the main receptacle and they serve to convey 'the pulp and bleach to the upper end of the main receptacle and empty the same thereinto, the upper ends of these uptakes 6 entering the main receptacle at opposite sides through openings therein, these openings being located at or near the upper end of the main receptacle.
The bottom of the main tank is tapered downwardly to a throat 7 leading into a short horizontal conduit 8 which forms a part of the uptakes 6, each end of this conduit being connected to the adjacent lower end of one of the uptakes by a curved upwardly-tapering conduit 9. Extending through stuliing-boxes 10 in the walls of the curved conduits 9 is a shaft 11 mounted in suitable bearings 12 and driven by Suitable fast and loose pulleys 13. Axed. to the shaft 11 is a air of screw-impellers 14 which fit the conduit 8 and are arranged at opposite sides .of the throat 7. These impellers are arranged to oppose each other, so as to impel the pul outwardly in opposite directions from t e throat 7, so that in the operation of the apparatus these screw-impellers will draw equal amounts of pulp down through throat 7 and for-ce it outwardly and upwardly into the uptakes, thereby delivering it back into 'the main receptacle at the upper ends thereof. This arrangement of opposed impellers and two uptakes enables me to move the pulp without end-thrust on the impeller shaft, since the two impellers balance each other so far as end-thrust is concerned. This overcomes anobjection found to exist in the apparatus shown in the Heiskanen patent, since in the Heiskanen structure there was liability that the end-thrust on the impeller would unstepthe shaft. In this way, I am enabled to work unusually thick pulp, i. e., pulp having a very high percentage of fiber to water, thereby greatly economizing in steam, power and bleach.
The main receptacles are located side by side, as shown in Fig. 2, and are connected by overflow tubes or troughs 15, in each of which works a screw 16, these screws all being fastened to a common shaft 17 driven by any suitable power mechanism. As in the Heiskanen method, the pulp is kept in constant circulation in each unit (a unit being composed of a main\.tank and two supplemental uptakes) and at the same time a quantity of the pulp equal to the quantity fed into the first tank is carried over into the next adjacent tank. The screws or Ipropellers 16 ensure a constant and uniform feed of the pulp from unit to unit and enables me to handlethick pulp. It is 0bvious that if on'e unit contains a little more than the next one, the discharge-screw thereof will immediately correct the situation by carrying a little more over into the next unit, thereby ensuring substantially the same level of pulp in all the main receptacles to thus ensure a uniform distribution throughout the system.
Each of the curved conduits 9 is connected to the vertical part of the uptake .ASSIGNOR TO STEBBINS ENGL by means of an air-ring 18 which is hol-y low and is adapted to be connected to a compressed-air supply through an inlet 19. The interior of the ring 18. is connected to a supplemental air channel 20 by means of air-holes 21, associated with each of -which is a needle-valve 22 by which the amount of air entering-the hole' 21 is regulated. The annular channel 20 is connected to the interior of the uptake by upwardlyinclined nozzle-passages 23, whereby one or more upwardly-directed'compressed-air currentsv is directed into the upgoing mass of pulp. These upwardly-flowing air currents tend to lift the stock and thus Iassist the impellers greatly in keeping it .moving This air 'also cuts down friction by giving the stock a sort of air cushion to travel on and "thus enables me to move the heaviest stock at a .minimum consumption of power. And, furthermore, the chemical reaction that takes place when the calcium chloride may be employed.
liquor of the bleach comes in contact with cellulose or pulp is greatly aided by this aeration, thereby speeding up the bleaching action.
It will be understood, of course, that any other fluid, such as oxygen, chlorine gas or any other liquid or gas which will assist in moving as well as bleaching the stock I do not desire to be understood as limiting myself to the precise details of construction and arrangement shown, as variamade 4without departingv from the spirit and scope of my invention andimprovements. I therefore reserve -the' right to. all such variations and modifications as properly fall within the scope of my' invention and imrovements and as set forth. in` the terms of the following claims.
f What I claim is:
1. ln an apparatus for bleaching pulp, a main-tank, a pair of conduits arranged at- 'opposite sides of the' main tank having their upper ends discharging into the main tank, a horizontal conduit arranged across the lower, open end of the main tank and arranged to discharge into the lower ends ofthe conduits, and a shaft extending horizontally through said horizontal conduit and provided with a pair of. opposed propellers arranged at opposite sides of said open end of the main tank, for the purpose set forth.
2. In a. pulp-bleaching apparatus em bodying an uptake for conveying the pulp upwardly, means for propelling the pulp, and means for introducing a bleaching-accelerating fluid under pressure into said uptake, this latter means embodying a plurality of nozzles arranged around the uptake and directed upwardly to thereby introduce the luid into the mass of pulp in the form of aplurality of upwardly-directed streams, for the purpose set forth;
3. In an apparatus for bleaching pulp, a
'series of tank-units,I each comprising a mam vtank and a palr of supplemental or uptake.
sure into said uptake at the lower endthereof,.said latter means embodying a nozzle extending only to the interior surface of the uptake so that the Huid will 1ubricate and thus reduce the friction of the Iupgoing pulp. tions and modifications therefrom may be 5. The method herein described ofY bleaching pulp consisting lin maintaining-an upgoing continuously-moving` mass. ofpulp l 'andhwater and bleaching agent,'and contin-` uously introducing under pressure .into'the' lower end of said upgoing column of pulp "a bleaching accelerating fluid, this fluid being delivered at a point between thejpulp and the enclosing wall of the uptake, for the purpose set forth.
6. The method herein described of bleaching paper pulp consisting in injecting under pressure a plurality of jets of bleachl ing-accelerating fluid directly into a mass of mixed pulp and bleaching liquor to thereby not only agitate the mass to thus intimately mix the bleaching-accelerating uid with the pulp and the bleaching liquor, but also to assist in moving the same.
ln testimony whereof l hereunto aiiix my signature. v
AUGUST F. RICHTER.
US541463A 1922-03-06 1922-03-06 Pulp-bleaching method and apparatus Expired - Lifetime US1529919A (en)

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2492047A (en) * 1946-03-30 1949-12-20 Du Pont Bleaching wood pulp
US3053067A (en) * 1957-08-21 1962-09-11 Sunds Verkst Er Aktiebolag Towers for treating stock, substantially for the continuous bleaching of cellulose pulp or for the storing of such pulp
US3660225A (en) * 1968-07-11 1972-05-02 South African Pulp Paper Delignification and bleaching of cellulose pulp layers with oxygen gas
DE2523191A1 (en) * 1974-06-14 1975-12-18 Mo Och Domsjoe Ab METHOD FOR DELIGNICIFYING LIGNOCELLULOSIC MATERIAL
US3963561A (en) * 1973-08-27 1976-06-15 Kamyr Aktiebolag Recirculation of unconsumed oxygen pulp bleaching gas
US10201787B2 (en) * 2010-07-15 2019-02-12 Curium Us Llc Slurry dispenser for radioisotope production

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2492047A (en) * 1946-03-30 1949-12-20 Du Pont Bleaching wood pulp
US3053067A (en) * 1957-08-21 1962-09-11 Sunds Verkst Er Aktiebolag Towers for treating stock, substantially for the continuous bleaching of cellulose pulp or for the storing of such pulp
US3660225A (en) * 1968-07-11 1972-05-02 South African Pulp Paper Delignification and bleaching of cellulose pulp layers with oxygen gas
US3963561A (en) * 1973-08-27 1976-06-15 Kamyr Aktiebolag Recirculation of unconsumed oxygen pulp bleaching gas
DE2523191A1 (en) * 1974-06-14 1975-12-18 Mo Och Domsjoe Ab METHOD FOR DELIGNICIFYING LIGNOCELLULOSIC MATERIAL
US10201787B2 (en) * 2010-07-15 2019-02-12 Curium Us Llc Slurry dispenser for radioisotope production

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