US130336A - Improvement in spirit-stills - Google Patents

Improvement in spirit-stills Download PDF

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US130336A
US130336A US130336DA US130336A US 130336 A US130336 A US 130336A US 130336D A US130336D A US 130336DA US 130336 A US130336 A US 130336A
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chamber
spirit
pipe
stills
chambers
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14Fractional distillation or use of a fractionation or rectification column

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  • This invention relates to apparatus for distilling alcoholic liquids by a process of redistillation, whereby the vapor rising from one distillation is condensed and afterward returned for distillation over again, to separate the more highly volatile particles from those which are less so.
  • the improvements consist, first, in a novel construction of the still, with 'one or more spirit-chambers having curved bottoms to facilitate drawing ofi from said chambers.
  • the improvements also comprise a novel arrangement of a scroll or fence, edge uppermost, within each or certain of the spiritchambers, said scroll commencing at a point near the center of the chamber, and traversin g in an equal or unequal manner the bottom of the spirit-chamber, for the purpose of cansing a circulation of the spirits to be distilled.
  • the improvements likewise include the application of a drop-pipe to the spirit-chambers, arranged to convey the impurities from an upper chamber to the center of the chamber beneath it, said pipe being so constructed as to prevent the vapors from the lower chamber passing up it to the chamber above.
  • a novel feature also consists in a combination, with each or any of the spirit-chambers, of a thermometer, arranged and constructed to connect with the center of the chamber, for the purpose of indicating the temperature of the latter at its center, where the heat is the greatest, to dictate the necessary regulation of heat required.
  • the improvements furthermore comprise a system of separate condensers for the separate spirit chambers; likewise a novel and advantageous construction of the condensers, the same preferably being made of an inner and outer'sheet-metal case, the inner one of which is composed of pockets fitted with reversely-arranged return strips or blocks f i lation of the vapors to be condensed in a serpentine manner through the pockets, while the cooling liquid enters between the pockets and spaces, separating them from the outer case, thus obtaining a very efficient condensing-surface.
  • Figure 1 represents a mainly sectional vertical view ofa still with the improvements applied to it;
  • Fig. 2 a horizontal section through one of the condensers at the line a: m;
  • Fig. 3 a sectional v.plan of one of the spirit-chambers.
  • the still illustrated in the drawing only shows three spirit-chambers, arranged one above the other, and a corresponding number and arrangement of condensers, but any greater number of both may be used.
  • the lower condenser of the series may be cooled by the beer or wash in its way to the spirit chamber or boiler, while the other condensers may either be cooled by the beer or by water.
  • A, B, and 0 represent three condensers, arrangedas described.
  • These condensers are each made up of an outer sheetmetal case and inner shell or case, the latter being formed of sheet-metal pockets b b, disposed vertically in parallel courses at a suitable distance apart, and communicating, top and bottom, at the same side or end, by cross-chambers c d, with the pipes by which the vapor is passed to, andreturned, when condensed, from the con denser.
  • the pipe 1 is immersed at its delivery-end in a tube or receiver, m, containing spirits or water, and arranged to form a liquid trap on the bottom of the chamber F to prevent back pressure or escape of the vapors generated within said chamber.
  • the condensed products of the chamber F are returned, by a siphonic drop-pipe, G, to a similar fluid-trap in the lower boiler D for redistillation, while the volatile matter in said chamber F passes, by a pipe, It, to the second condenser B, from whence the product of condensation and vapor passes, by a pipe, I, to the next upper spirit-chamber H, that is of like construction with the chamber F, and is similarly provided with a scroll or 'fence, steam-coil, siphonic drop-pipe G for returningimpurities orunevaporated matter back to the center of-the spiritchamber below it, and an escape-pipe for the vapor to the next condenser 0, from whence the process may be continued as before, or where it may terminate.
  • vchamber is. a separate still, heated by a separate heater, and provided with a separate condenser, but operating successively upon higher distillations, and returning unevaporated matter for redistillation, whereby a high-proof spirit may be obtained in a most economical and perfect manner.
  • each one is provided with an outside thermometer, I, the tube 8 of which is arranged to project into the central portion of the chamber, where the heat is greatest, especially'when the spirit to be distilled has its travel over the bottom of the chamber extended, as is here the case, by the scroll or fence.
  • thermometer I having its tube 8 extending into the central portion of said chamber, substantially as and for the purpose described.
  • a condenser composed of an outer case or shell, A, and inner case, consisting of a series of pockets, 1) b, and reversely-arranged return-strips e e, having cross-connecting tubes or passages c d and inlets and outlets It I, all arranged for operation substantially as shown and described.

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Description

J. c. THOMPSON.
Improvement in Spirit-Stills.
' N0. 130,336. Patented Aug 6,1872.
Fay-2.
jtngsses;
UNITED STATES PATENT QFFICE.
JOHN C. THOMPSON, OF BROOKLYN, NEW YORK.
IMPROVEMENT IN SPIRIT-STILLS.
Specification forming part of Letters Patent No. 130,336, dated August 6, 1872.
To all whom it may concern Be it known that I, J OHN G. THOMPSON, of Brooklyn, in the county of Kings and State of New York, have invented certain new and useful Improvements in Stills, of which the following is a full, clear, and exact description, reference being had to the accompanying drawing forming part of this specification.
This invention relates to apparatus for distilling alcoholic liquids by a process of redistillation, whereby the vapor rising from one distillation is condensed and afterward returned for distillation over again, to separate the more highly volatile particles from those which are less so. The improvements consist, first, in a novel construction of the still, with 'one or more spirit-chambers having curved bottoms to facilitate drawing ofi from said chambers. The improvements also comprise a novel arrangement of a scroll or fence, edge uppermost, within each or certain of the spiritchambers, said scroll commencing at a point near the center of the chamber, and traversin g in an equal or unequal manner the bottom of the spirit-chamber, for the purpose of cansing a circulation of the spirits to be distilled. The improvements likewise include the application of a drop-pipe to the spirit-chambers, arranged to convey the impurities from an upper chamber to the center of the chamber beneath it, said pipe being so constructed as to prevent the vapors from the lower chamber passing up it to the chamber above. A novel feature also consists in a combination, with each or any of the spirit-chambers, of a thermometer, arranged and constructed to connect with the center of the chamber, for the purpose of indicating the temperature of the latter at its center, where the heat is the greatest, to dictate the necessary regulation of heat required. The improvements furthermore comprise a system of separate condensers for the separate spirit chambers; likewise a novel and advantageous construction of the condensers, the same preferably being made of an inner and outer'sheet-metal case, the inner one of which is composed of pockets fitted with reversely-arranged return strips or blocks f i lation of the vapors to be condensed in a serpentine manner through the pockets, while the cooling liquid enters between the pockets and spaces, separating them from the outer case, thus obtaining a very efficient condensing-surface.
Having thus specified the object and nature of the invention, its description will be pro ceeded with in reference to the accompanying drawing. I
Figure 1 represents a mainly sectional vertical view ofa still with the improvements applied to it; Fig. 2, a horizontal section through one of the condensers at the line a: m; and Fig. 3, a sectional v.plan of one of the spirit-chambers.
Similar letters of reference indicate corresponding parts throughout the several figures.
The still illustrated in the drawing only shows three spirit-chambers, arranged one above the other, and a corresponding number and arrangement of condensers, but any greater number of both may be used. The lower condenser of the series may be cooled by the beer or wash in its way to the spirit chamber or boiler, while the other condensers may either be cooled by the beer or by water. A, B, and 0 represent three condensers, arrangedas described. These condensers are each made up of an outer sheetmetal case and inner shell or case, the latter being formed of sheet-metal pockets b b, disposed vertically in parallel courses at a suitable distance apart, and communicating, top and bottom, at the same side or end, by cross-chambers c d, with the pipes by which the vapor is passed to, andreturned, when condensed, from the con denser. These pockets are fitted with a series of reversely-disposed metal strips or blocks, 0 e, secured by rivets passing through them and the pockets, and of an elongated-U description, entering one within the other so as to form return-strips to establish a serpentine course or channel, f, for the vapor or liquid, while the spaces 9 between the pockets 1) b and the spaces separating them from the outer case contain the cooling liquid. This forms an easily made and very efficient condenser. The beer or mash to be distilled enters the lower condenser A by the pipe h, and, circulating as k, to the condenser A, .from whence the condensed product or spirits passes, by a pipe,
I, to a spirit-chamber, F, arranged above the boiler D, and constructed with a curved bottom, which may either be convex or concave on its upper surface, accordingly as the pipe Z is arranged to deliver at the center or periphery of the chamber. I The object of thus curvspirit-chamber F is also fitted with an open scroll or fence, M, having its edge uppermost, said scroll commencing at a point near the center of the chamber and traversing in a regular or irregular manner the bottom of said chamber, whereby an extended circulation of the spirits over the bottom of the chamber and about the steam-coil is produced, thus expediting evaporation. The pipe 1 is immersed at its delivery-end in a tube or receiver, m, containing spirits or water, and arranged to form a liquid trap on the bottom of the chamber F to prevent back pressure or escape of the vapors generated within said chamber. The condensed products of the chamber F are returned, by a siphonic drop-pipe, G, to a similar fluid-trap in the lower boiler D for redistillation, while the volatile matter in said chamber F passes, by a pipe, It, to the second condenser B, from whence the product of condensation and vapor passes, by a pipe, I, to the next upper spirit-chamber H, that is of like construction with the chamber F, and is similarly provided with a scroll or 'fence, steam-coil, siphonic drop-pipe G for returningimpurities orunevaporated matter back to the center of-the spiritchamber below it, and an escape-pipe for the vapor to the next condenser 0, from whence the process may be continued as before, or where it may terminate. The siphonic droppipes connecting each spirit-chamber with the one below it prevent any passage of vapor from the one chamber to the other; and each;
vchamber is. a separate still, heated by a separate heater, and provided with a separate condenser, but operating successively upon higher distillations, and returning unevaporated matter for redistillation, whereby a high-proof spirit may be obtained in a most economical and perfect manner. To regulate the temperature of the several spirit-chambers each one is provided with an outside thermometer, I, the tube 8 of which is arranged to project into the central portion of the chamber, where the heat is greatest, especially'when the spirit to be distilled has its travel over the bottom of the chamber extended, as is here the case, by the scroll or fence.
What is here claimed, and desired to be sccured by Letters Patent, is-- V 1. In a still having one or more spirit-chamhere, the curved or convex bottoms, in combination with the open scroll or fence M, substantially as specified, for the purpose set forth.
2. The connection of an upper with a lower spirit-chamber by a siphon-shaped drop-pipe, G, arranged to convey the impurities from the upper spirit-chamber to the center of the one beneath it, essentially as specified.
3. The arrangement in the spirit-chamber of the thermometer I, having its tube 8 extending into the central portion of said chamber, substantially as and for the purpose described.
4. In a still composed of a series of spiritchambers for successive operations, as described, the application of a separate con-- denser to each chamber, essentially as specified.
5. A condenser composed of an outer case or shell, A, and inner case, consisting of a series of pockets, 1) b, and reversely-arranged return-strips e e, having cross-connecting tubes or passages c d and inlets and outlets It I, all arranged for operation substantially as shown and described. v
JOHN C. THOMPSON.
Witnesses:
FRED. HAYNES, lt. IE. RABEAU.
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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2837469A (en) * 1949-10-07 1958-06-03 Heraeus Gmbh W C Distilling apparatus for the production of pure water

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2837469A (en) * 1949-10-07 1958-06-03 Heraeus Gmbh W C Distilling apparatus for the production of pure water

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