US1222967A - Method of preparing adhesive coatings and applying them to fabrics without the use of solvents. - Google Patents

Method of preparing adhesive coatings and applying them to fabrics without the use of solvents. Download PDF

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US1222967A
US1222967A US8456716A US8456716A US1222967A US 1222967 A US1222967 A US 1222967A US 8456716 A US8456716 A US 8456716A US 8456716 A US8456716 A US 8456716A US 1222967 A US1222967 A US 1222967A
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fabrics
mixture
applying
solvents
adhesive coatings
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US8456716A
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James Meade
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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09JADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J7/00Adhesives in the form of films or foils
    • C09J7/20Adhesives in the form of films or foils characterised by their carriers
    • C09J7/21Paper; Textile fabrics
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09JADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J7/00Adhesives in the form of films or foils
    • C09J7/30Adhesives in the form of films or foils characterised by the adhesive composition
    • C09J7/35Heat-activated

Definitions

  • Fig. 2 is an enlarged View of a portion thereof.
  • an adhesive solid I may employ guttapercha, pontianac, balata, and various other gumsor resins which possess the property of becoming plastic and adhesive under .the influence of heat. It is to be understood that when hereinafter gums or gummy solids are referred to, it is intended toembrace all suitable inspissated vegetable juices, and the like. With this solid, to permit it to be brought to the proper state of plasticity and to be highly adhesive whenheated and again cooled, I mix with it a suflicient amount, say 10%, of a wax, or wax-like substance, which may be mineral, animal or vegetable. Of these I prefer paraflin, bees wax or carnauba. The term wax-like substance is to be considered to comprehend all waxes and substances which resemble them in character.
  • the correct proportions of the gums and Waxes are first reduced to a proper state of division and mixed in a preliminary way by being ground together in a mill indicated at A.
  • This mill may consist of a pair of differentially driven rolls 10, 10, preferably hollow and heated by steam-pipes 11 to a temperature at which both the gum and wax are somewhat softened.
  • the temperature at which the substances named become plastic is from 170 to 180 Fahrenheit.
  • From the receptacle 12 of the mill the mixture, now in the condition of a thick paste or dough, is transferred to a tank 13 containing a liquid, preferably water, heated by a steampipe 14: to a temperature of about 200 F. While the mass is still more softened there- 'by, it remains in a condition in which it may be handled.
  • the coating mix" ture is placed as required in-the hopper 15 of a mixer B, where it is advanced by a C, at the rear of the gage-knife 21.
  • This knife has a hollow support 22 to which is connected a steam-pipe 23, Steam enters I the coating in the properly plastic condition until it is fully spread. In its movement through the machine it is then dried in the customary manner by steam-pipes 24L and received as the completed goods upon a winding roll 25.
  • the adhesive come under the influence of a degree of heat great enough to so harden it that it loses its flexibility, this being approximately 220 F.
  • steps is in the best condition to receive the treatment which is being given, which will be free from stickiness until heated for a purpose of final utilization, and which when thus heated and applied will be highly adhesive.
  • the method of applying adhesive coatings to fabrics which consists in mixing a gummy solid and a Wax-like solid at a temperature at which the solids become plastic, and spreading the'mixture upon the fabric under the influence of a higher temperature.
  • the method of preparing adhesive coatings which consists in grinding together and mixing a gum and a wax at a temperature at least that at which the mixture becomes plastic, immersing the mixture in a liquid heated to a higher temperature, and tempering the mixture at a still higher temperature.

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Footwear And Its Accessory, Manufacturing Method And Apparatuses (AREA)
  • Application Of Or Painting With Fluid Materials (AREA)
  • Adhesive Tapes (AREA)

Description

Patented Apr. 17, 1917.
XXNI away,
I. MEADE.
METHOD OF PREPARING ADHESIVE COATINGS AND APPLYING THEM TO FABRICS WITHOUT I THE USE OF SOLVENTS.
APPLICATION FILED MAR. 16, 1916- I m U MIL "Ill".
JAMES MEAIDE, OF STO UGI-ITON, MASSACHUSETTS.
METHOD OF PREPARING ADHESIVE COATINGS AND APPLYING THEM TO FABRICS .WITHOU'I. THE USE OF SOLVENTS.
ful Method of Preparing Adhesive Coatings andApplying Them to Fabrics Without'the Use 'of Solvents, ofwhich the following is a specification.
In the preparation of adhesively coated fabrics, such as duck which with a layer of a sticky substance applied to one face is commonly used for the well known gem insoles for Goodyear welt shoes, the usual practice is to first treat a solid adhesive, say
gutta-percha, with a solvent, as naphtha. This makes a solution of such a consistency that it may be readily distributed uniformly over the fabric by means of a spreader. This procedure, however, has several objectionable-features. To get the solution into condition for spreading requires nearly twenty-four hours. The solvent is so highly volatile that it is necessary to have the solution quite thin to permit it to remain sufiiciently fluid throughout the spreading operation. This causes it to run when first applied, and only a shallow coating can successfully be given the fabric. Consequently, to obtain the necessary depth of adhesive, several coatings are spread one upon another adding greatly to the time and expense of production. When the solution-c'oatedfabric is utilized for such workas insoles, it is the .usual practice to cut it, many layers at a. I time, with heated dies.
These when they come in contact with the adhesive dry.out the solvent and cause the edges of the cut insoles to stick together, often requiring that they be picked laboriously apart. There is also the general objection to the employment of volatile solvents that the fumes are liable to become ignited, as by sparks from motors driving the machinery in which the dissolved adhesive is operated upon, causing explosions and fires. By my method, I eliminate the solvent and apply to the fabric in a single brief series of operations as thick a coating as is desired, giving an inexpensive product which may conveniently be handled without danger of sticking when being cut to form.
In Figure 1 of the accompanying drawing an organization is illustrated by which my improved method maybe carried out, while Specification of Letters Patent.
Patented Apr. 17, 191%.
Application filed March 16, 1916. Serial No. 84,567;
Fig. 2 is an enlarged View of a portion thereof.
As an adhesive solid I may employ guttapercha, pontianac, balata, and various other gumsor resins which possess the property of becoming plastic and adhesive under .the influence of heat. It is to be understood that when hereinafter gums or gummy solids are referred to, it is intended toembrace all suitable inspissated vegetable juices, and the like. With this solid, to permit it to be brought to the proper state of plasticity and to be highly adhesive whenheated and again cooled, I mix with it a suflicient amount, say 10%, of a wax, or wax-like substance, which may be mineral, animal or vegetable. Of these I prefer paraflin, bees wax or carnauba. The term wax-like substance is to be considered to comprehend all waxes and substances which resemble them in character.
The correct proportions of the gums and Waxes are first reduced to a proper state of division and mixed in a preliminary way by being ground together in a mill indicated at A., This mill may consist of a pair of differentially driven rolls 10, 10, preferably hollow and heated by steam-pipes 11 to a temperature at which both the gum and wax are somewhat softened. The temperature at which the substances named become plastic is from 170 to 180 Fahrenheit. From the receptacle 12 of the mill the mixture, now in the condition of a thick paste or dough, is transferred to a tank 13 containing a liquid, preferably water, heated by a steampipe 14: to a temperature of about 200 F. While the mass is still more softened there- 'by, it remains in a condition in which it may be handled. From the tank the coating mix" ture is placed as required in-the hopper 15 of a mixer B, where it is advanced by a C, at the rear of the gage-knife 21. This knife has a hollow support 22 to which is connected a steam-pipe 23, Steam enters I the coating in the properly plastic condition until it is fully spread. In its movement through the machine it is then dried in the customary manner by steam-pipes 24L and received as the completed goods upon a winding roll 25. During no step in the process does the adhesive come under the influence of a degree of heat great enough to so harden it that it loses its flexibility, this being approximately 220 F.
By this method I obtain, with little expenditure of time, a mixture which at. all
steps is in the best condition to receive the treatment which is being given, which will be free from stickiness until heated for a purpose of final utilization, and which when thus heated and applied will be highly adhesive.
1 claim:
1. The method of applying adhesive coatings to fabrics which consists in mixing a gummy solid and a Wax-like solid at a temperature at which the solids become plastic, and spreading the'mixture upon the fabric under the influence of a higher temperature.
2. The method of applying adhesive coatings to fabrics which consists in grinding together and mixing a gum anda wax at a temperature at least that at which the mixture becomes plastic, tempering this mixture at a higher temperature, and spreading the mixture upon the fabric under the influence of a still higher temperature.
3. The method of applying adhesive coatnaaaeer ings to fabrics which consists in grinding together and mixing a gum and a wax at a temperature of approximately 170 F, tempering this mixture at approximately 210 F., and spreading the mixture upon the fabric under the influence of a temperature of approximately from 212 to 215 F.
4. The method of preparing adhesive coatings which consists in grinding together and mixing a gum anda wax at a temperature at least that at which the mixture becomes plastic, immersing the mixture in a liquid heated tora higher temperature, and tempering the mixture.
5. The method of preparing adhesive coatings which consists in grinding together and mixing a gum and a wax at a temperature at least that at which the mixture becomes plastic, immersing the mixture in a liquid heated to a higher temperature, and tempering the mixture at a still higher temperature.
6. The method of applying adhesive coatings-tq fabrics which consists in grinding together and mixing a gum and a wax at a temperature of approximately 17 0 F, immersing the mixture in a liquid heated approximately to 200 F., tempering the mixture at a temperature of approximately 210 F, and spreading the mixture upon the fabric under the influence of a temperature of from 212 to 215 F.
Signed at Stoughton, in the county of Norfolk and State of Massachusetts, this 13th day of March, 1916.
JAMES MEADE.
US8456716A 1916-03-16 1916-03-16 Method of preparing adhesive coatings and applying them to fabrics without the use of solvents. Expired - Lifetime US1222967A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2846492A (en) * 1956-02-15 1958-08-05 Vanderbilt Co R T Adhesives containing chlorinated natural rubber, hypochlorinated natural rubber and wax
US3073303A (en) * 1960-03-14 1963-01-15 Kendall & Co Perforated adhesive tapes

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2846492A (en) * 1956-02-15 1958-08-05 Vanderbilt Co R T Adhesives containing chlorinated natural rubber, hypochlorinated natural rubber and wax
US3073303A (en) * 1960-03-14 1963-01-15 Kendall & Co Perforated adhesive tapes

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