UA96281C2 - Method for producing sulfonamides and intermediates - Google Patents

Method for producing sulfonamides and intermediates

Info

Publication number
UA96281C2
UA96281C2 UAA200808447A UAA200808447A UA96281C2 UA 96281 C2 UA96281 C2 UA 96281C2 UA A200808447 A UAA200808447 A UA A200808447A UA A200808447 A UAA200808447 A UA A200808447A UA 96281 C2 UA96281 C2 UA 96281C2
Authority
UA
Ukraine
Prior art keywords
formula
equivalents
base
intermediates
nitro
Prior art date
Application number
UAA200808447A
Other languages
Russian (ru)
Ukrainian (uk)
Inventor
Томас Шмідт
Йоахім Гебхардт
Сандра Льор
Міхаель Кайль
Ян Хендрік Веверс
Міхаель Рак
Гуідо Майєр
Аксель Плешке
Original Assignee
Басф Се
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Басф Се filed Critical Басф Се
Publication of UA96281C2 publication Critical patent/UA96281C2/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/02—Preparation of esters of nitric acid
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/02—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
    • B01J31/0234—Nitrogen-, phosphorus-, arsenic- or antimony-containing compounds
    • B01J31/0255—Phosphorus containing compounds
    • B01J31/0257—Phosphorus acids or phosphorus acid esters
    • B01J31/0262—Phosphorus acids or phosphorus acid esters comprising phosphinous acid (-ester) groups (R2P(OR')) or the isomeric phosphine oxide groups (R3P=O), i.e. R= C, R'= C, H
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/02—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
    • B01J31/0234—Nitrogen-, phosphorus-, arsenic- or antimony-containing compounds
    • B01J31/0255—Phosphorus containing compounds
    • B01J31/0267—Phosphines or phosphonium compounds, i.e. phosphorus bonded to at least one carbon atom, including e.g. sp2-hybridised phosphorus compounds such as phosphabenzene, the other atoms bonded to phosphorus being either carbon or hydrogen
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
    • C07C303/34—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of amides of sulfuric acids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2531/00—Additional information regarding catalytic systems classified in B01J31/00
    • B01J2531/90—Catalytic systems characterized by the solvent or solvent system used
    • B01J2531/96—Water
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2531/00—Additional information regarding catalytic systems classified in B01J31/00
    • B01J2531/90—Catalytic systems characterized by the solvent or solvent system used
    • B01J2531/98—Phase-transfer catalysis in a mixed solvent system containing at least 2 immiscible solvents or solvent phases
    • B01J2531/985—Phase-transfer catalysis in a mixed solvent system containing at least 2 immiscible solvents or solvent phases in a water / organic solvent system
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/02—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
    • B01J31/0272—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides containing elements other than those covered by B01J31/0201 - B01J31/0255

Abstract

The invention relates to methods for producing sulfonamides of formula I, wherein the variables have the designations cited in the description, by reacting m-nitro-benzoic acid chlorides of formula II with aminosulfons of formula III, under the influence of B equivalents of base IV. Said method is characterised in that, during step a) the aminosulfon of formula III is reacted with B1 equivalents of base IV, and during step b), the reaction mixture resulting from step a) is reacted with m-nitro-benzoic acid chlorides of formula II and B2 equivalents of base IV; B, B1 and B2 having the designations cited in the description. EMBED ISISServer , (I)
UAA200808447A 2005-12-01 2006-11-23 Method for producing sulfonamides and intermediates UA96281C2 (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE200510057681 DE102005057681A1 (en) 2005-12-01 2005-12-01 Preparation of fluorinated m-nitro-benzoic acid chloride compound, useful to prepare sulfonamide compound, comprises reacting a fluorinated m-nitro-benzoic acid compound with a chlorinating agent in the presence of a phosphine derivative

Publications (1)

Publication Number Publication Date
UA96281C2 true UA96281C2 (en) 2011-10-25

Family

ID=38047613

Family Applications (3)

Application Number Title Priority Date Filing Date
UAA200808447A UA96281C2 (en) 2005-12-01 2006-11-23 Method for producing sulfonamides and intermediates
UAA201111380A UA107567C2 (en) 2005-12-01 2006-11-23 Method for producing fluorinated m-nitrobenzoic acid chlorides
UAA201101802A UA98291C2 (en) 2005-12-01 2006-11-23 Methods for producing sulfonamides

Family Applications After (2)

Application Number Title Priority Date Filing Date
UAA201111380A UA107567C2 (en) 2005-12-01 2006-11-23 Method for producing fluorinated m-nitrobenzoic acid chlorides
UAA201101802A UA98291C2 (en) 2005-12-01 2006-11-23 Methods for producing sulfonamides

Country Status (5)

Country Link
CN (1) CN101351443B (en)
AR (2) AR096111A2 (en)
DE (1) DE102005057681A1 (en)
UA (3) UA96281C2 (en)
ZA (1) ZA200805691B (en)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104610100B (en) * 2015-01-09 2016-09-14 华东理工大学 A kind of nitrogen chlorine type chlorination reagent
CN108218709A (en) * 2016-12-14 2018-06-29 江苏联化科技有限公司 The separation method of the fluoro- benzoic acid nitration products of the chloro- 4- of 2-

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5238908A (en) * 1989-08-31 1993-08-24 Rohm And Haas Company Herbicidal glutaramic acids and derivatives
CN100368392C (en) * 2002-10-30 2008-02-13 巴斯福股份公司 Bifunctional phenyliso(thio)cyanates, processes and intermediates products for their preparation

Also Published As

Publication number Publication date
DE102005057681A1 (en) 2007-06-06
UA98291C2 (en) 2012-04-25
ZA200805691B (en) 2009-11-25
AR096112A2 (en) 2015-12-09
CN101351443A (en) 2009-01-21
UA107567C2 (en) 2015-01-26
CN101351443B (en) 2012-11-28
AR096111A2 (en) 2015-12-09

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