UA108882C2 - METHOD FOR GROWING OF CUPRUM(I)PENTATIOPHOSPHATE(V) BROMIDE Cu6PS5Br MONOCRYSTALS BY DIRECTIONAL CRYSTALLIZATION FROM SMELT - Google Patents

METHOD FOR GROWING OF CUPRUM(I)PENTATIOPHOSPHATE(V) BROMIDE Cu6PS5Br MONOCRYSTALS BY DIRECTIONAL CRYSTALLIZATION FROM SMELT

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Publication number
UA108882C2
UA108882C2 UAA201213996A UAA201213996A UA108882C2 UA 108882 C2 UA108882 C2 UA 108882C2 UA A201213996 A UAA201213996 A UA A201213996A UA A201213996 A UAA201213996 A UA A201213996A UA 108882 C2 UA108882 C2 UA 108882C2
Authority
UA
Ukraine
Prior art keywords
monocrystals
smelt
growing
cu6ps5br
cuprum
Prior art date
Application number
UAA201213996A
Other languages
Russian (ru)
Ukrainian (uk)
Inventor
Артем Ігорович Погодін
Олександр Павлович Кохан
Андрій Михайлович Соломон
Ігор Петрович Студеняк
Original Assignee
Державний Вищий Навчальний Заклад "Ужгородський Національний Університет"
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Державний Вищий Навчальний Заклад "Ужгородський Національний Університет" filed Critical Державний Вищий Навчальний Заклад "Ужгородський Національний Університет"
Priority to UAA201213996A priority Critical patent/UA108882C2/en
Publication of UA108882C2 publication Critical patent/UA108882C2/en

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Abstract

The invention relates to inorganic chemistry and inorganic material science. A method for growing of cuprum(I)pentatiphosphate (V) bromide Cu6PS5Br monocrystals by directional crystallization from smelt comprises the step heating of vacuum-treated quarts ampoules containing starting components cooper, phosphorus, sulfur and pre-synthesized CuBr in the required stoichiometric ratio. The heating is carried out to maximal temperature and smelt is kept at this temperature during 24 hours with further growing of monocrystals, wherein maximal temperature of synthesis is 1330 K, and monocrystals are grown with rate of 3 mm/day in ampoules with the conical end. The proposed method is intuitive, fast and allows to produce monocrystalls of large sizes.
UAA201213996A 2012-12-10 2012-12-10 METHOD FOR GROWING OF CUPRUM(I)PENTATIOPHOSPHATE(V) BROMIDE Cu6PS5Br MONOCRYSTALS BY DIRECTIONAL CRYSTALLIZATION FROM SMELT UA108882C2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
UAA201213996A UA108882C2 (en) 2012-12-10 2012-12-10 METHOD FOR GROWING OF CUPRUM(I)PENTATIOPHOSPHATE(V) BROMIDE Cu6PS5Br MONOCRYSTALS BY DIRECTIONAL CRYSTALLIZATION FROM SMELT

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
UAA201213996A UA108882C2 (en) 2012-12-10 2012-12-10 METHOD FOR GROWING OF CUPRUM(I)PENTATIOPHOSPHATE(V) BROMIDE Cu6PS5Br MONOCRYSTALS BY DIRECTIONAL CRYSTALLIZATION FROM SMELT

Publications (1)

Publication Number Publication Date
UA108882C2 true UA108882C2 (en) 2015-06-25

Family

ID=53675778

Family Applications (1)

Application Number Title Priority Date Filing Date
UAA201213996A UA108882C2 (en) 2012-12-10 2012-12-10 METHOD FOR GROWING OF CUPRUM(I)PENTATIOPHOSPHATE(V) BROMIDE Cu6PS5Br MONOCRYSTALS BY DIRECTIONAL CRYSTALLIZATION FROM SMELT

Country Status (1)

Country Link
UA (1) UA108882C2 (en)

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