TWI496545B - A process that minimizes the activity of raw materials - Google Patents

Description

A process for making the activity of raw materials extremely frozen

The invention provides a raw material active cryopreservation process, in particular a process for improving the life of an active ingredient contained in a raw material (food or cosmetic), which can make the active material extremely cold.

According to the variety of food and cosmetics, for example, in addition to general food rations, there are also foods that generally have a skin-beautifying or nutritional health effect, while for the latter, most of the ingredients have so-called skin-beautifying or For the active ingredients that are beneficial to the body, in order to be able to effectively preserve the active ingredients for a long time, all manufacturers have studied the way of long-term preservation. Similarly, cosmetics also have so-called active ingredients, and for preservation, the same long-term preservation is studied. The way.

In general, there is no special way of preservation, and it is usually not effective for long time placement. When it is sold to consumers, it has already deteriorated. Therefore, in order to improve this situation, the problem and the problem are solved, that is, the inventor and the inventor of the present invention. The relevant manufacturers in this industry are eager to study the direction of improvement.

Therefore, the inventors of the present invention have collected the relevant materials in view of the above-mentioned deficiencies, and have designed and improved such raw materials (food or by continuous trial and modification) through multi-party evaluation and consideration, and with years of experience accumulated in the industry. A patent for the life of an active ingredient contained in a cosmetic product.

The main object of the present invention is to pass the process of controlling the freezing time and temperature to freeze the raw material which is originally in the form of powder into a state of freezing (solidification), and to quickly dissolve after adding a normal temperature liquid.

In order to achieve the above object, the process of the present invention is as follows: first, at least one raw material containing the active ingredient is vacuum freeze-dried in a closed space of -40 degrees for 2 hours; and then the temperature is changed to -30 degrees to carry out the raw material. test; If the raw materials meet the freezing conditions, then adjust the temperature to -20 degrees for 3 hours; after 3 hours, adjust the temperature to -15 degrees for 24 hours; after 24 hours, adjust the temperature to - 10 degrees ice stored for 20 hours; after 20 hours, the temperature was adjusted to 0 degrees for 15 hours; after 15 hours, the temperature was adjusted to 10 degrees for 6 hours; finally, after 6 hours, the temperature was adjusted to 25 The ice is stored for 6 hours; thereby, the raw material is subjected to the effect of freezing (solidification) after the above freezing process, and the active ingredient contained in the raw material is effectively stored for a long period of time, so that only the user wants to use it in the future. After adding a normal temperature liquid, the raw material can be dissolved instantaneously, and the active ingredient still has the advantage.

By the above technique, it is possible to break through the problem of the inability to effectively store the active ingredient for a long time in the conventional use, and to achieve the practical progress of the present invention as the above advantages.

In order to achieve the above objects and effects, the technical means and the structure of the present invention will be described in detail with reference to the preferred embodiments of the present invention.

Referring to the first embodiment, which is a flow chart of a preferred embodiment of the present invention, it can be clearly seen from the drawings that the main process steps of the present invention are as follows: (a) at least one material containing the active ingredient at -42 degrees Vacuum freeze-drying in a confined space of -38 degrees for 2 hours; (b) storage of the raw material in a confined space at a temperature of -32 to -28 degrees; (c) storage of the raw material at a temperature of -22 to -18 degrees 3 hours in a confined space; (d) change the temperature in the confined space to -17 degrees to -13 degrees, and store the material in this temperature environment for 24 hours; (e) change the temperature in the confined space to -12 Degree to -8 degrees, so that the raw materials are stored in this temperature environment for 20 hours; (f) change the temperature in the confined space to -2 degrees to 2 degrees, so that the raw materials are warmed Store in an environment for 15 hours; (g) change the temperature in the confined space to 8 degrees to 12 degrees, and store the material in this temperature environment for 6 hours; and (h) change the temperature in the confined space to 23 degrees to At 27 degrees, the raw materials were stored in this temperature environment for 6 hours to form a frozen state of the raw materials.

Thereby, the raw material is subjected to the effect of freezing (solidification) after the above-mentioned freezing process, and the raw material is dried to become loose and porous, and the user needs to add the normal temperature liquid in the future to make the raw material dissolve completely instantaneously and quickly, and Active ingredients (eg, proteins or microorganisms) still exist.

In the pre-operation before step (a), the steps are as follows: (a1) taking a powdery raw material; (a2) subjecting the raw material to ultra-micron pulverization; (a3) taking a solvent and mixing with the original raw material The raw material is formed by (a4), and the raw material mixed with the solvent is filled in a can; (a5) is freeze-dried, and the oxidizable substance can be protected by the raw material in the case of freeze-drying.

Therefore, the raw material of the step (a) can also be loaded from the tank and then subjected to steps (a) to (h).

Further, the temperature of the step (a) is preferably -40 degrees, the temperature of the step (b) is preferably -30 degrees, and the temperature of the step (c) is preferably -20 degrees, (d) The optimum temperature is -15 degrees, the optimum temperature of step (e) is -10 degrees, the optimum temperature of step (f) is 0 degrees, and the optimum temperature of step (g) is 10 degrees, ( h) The optimum temperature for the step is 25 degrees.

In particular, the time for the raw material to be stored in step (b) is based on the physical properties of the raw material itself. If the frozen condition is not met after the test, step (c) will not be carried out. If the freezing condition is met, the step (c) is not used. Waiting for the scheduled time.

Therefore, the key to the process of improving the activity of the raw material in the present invention is to improve the conventional use:

1. Through the process technology of controlling the freezing time and temperature, the original raw material which is originally in the form of powder is frozen into a state of frozen crystal (solidification), and after adding the normal temperature liquid The advantage of rapid dissolution.

Second, since the drying is carried out in a frozen state, the volume is almost constant and the original structure is maintained.

3. After drying, the material is loose and porous, so it can be completely dissolved quickly after adding water.

4. Since it is carried out under vacuum, there is very little oxygen, so oxidizable substances can be protected.

5. Freezing and sublimation drying can eliminate 95%-99% of water, so that the raw materials can be preserved for a long time without deterioration, achieve secondary protection, and safe without preservatives, in a completely sterilized state.

However, the above description is only for the preferred embodiment of the present invention, and thus the scope of the present invention is not limited thereto, so that the simple modification and equivalent structural changes that are made by using the specification and the contents of the present invention should be the same. It is included in the scope of the patent of the present invention and is combined with Chen Ming.

In summary, the invention can effectively achieve the efficacy and purpose of the process for rapidly freezing the raw material. Therefore, the invention is an invention with excellent practicability, and is an application for conforming to the invention patent.提出 Submit an application in accordance with the law, and hope that the trial committee will grant the invention as soon as possible to protect the inventor's hard work. If there is any doubt in the trial committee, please do not hesitate to give instructions, the inventor will try his best to cooperate and feel polite.

The first figure is a flow chart of a preferred embodiment of the invention.

Claims (10)

A process for extremely freezing the activity of a raw material, wherein the process steps are as follows: (a) vacuum-drying at least one raw material containing the active ingredient in a closed space of -42 degrees to -38 degrees for 2 hours; (b) The raw materials are stored in a closed space at a temperature of -32 to -28 degrees; (c) the raw materials are stored in a closed space at a temperature of -22 to -18 degrees for 3 hours; (d) the temperature in the closed space is changed to - 17 degrees to -13 degrees, the raw materials are stored in this temperature environment for 24 hours; (e) the temperature in the closed space is changed to -12 degrees to -8 degrees, so that the raw materials are stored in this temperature environment for 20 hours; Change the temperature in the confined space to -2 degrees to 2 degrees, and store the material in this temperature environment for 15 hours; (g) change the temperature in the confined space to 8 to 12 degrees to make the material at this temperature environment It is stored for 6 hours; and (h) the temperature in the closed space is changed to 23 degrees to 27 degrees, and the raw materials are stored in this temperature environment for 6 hours to form a frozen state of the raw materials. A process as described in claim 1, wherein the temperature of the step (a) is preferably -40 degrees. A process as described in claim 1, wherein the temperature of the raw material is extremely frozen, wherein the temperature of the step (b) is preferably -30 degrees. A process as described in claim 1, wherein the temperature of the step (c) is optimally -20 degrees. A process as described in claim 1, wherein the temperature of the step (d) is -15 degrees. A process as described in claim 1, wherein the temperature of the step (e) is optimally -10 degrees. A process as described in claim 1, wherein the temperature of the step (f) is 0 degree. A process as described in claim 1 of the patent application, which can completely freeze the activity of the raw material, The optimum temperature of step (g) is 10 degrees. A process as described in claim 1, wherein the temperature of the step (h) is 25 degrees. For example, in the process of claim 1, the raw material can be absolutely frozen, and further comprises a raw material, which is obtained by super-micron pulverizing the raw material, then taking a solvent for mixing, and then filling. The raw material.