TWI287086B - Method and system for producing stress corrosion cracking - Google Patents

Method and system for producing stress corrosion cracking Download PDF

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Publication number
TWI287086B
TWI287086B TW94137931A TW94137931A TWI287086B TW I287086 B TWI287086 B TW I287086B TW 94137931 A TW94137931 A TW 94137931A TW 94137931 A TW94137931 A TW 94137931A TW I287086 B TWI287086 B TW I287086B
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Taiwan
Prior art keywords
tube
stress corrosion
temperature
pipe
cracks
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TW94137931A
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Chinese (zh)
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TW200716961A (en
Inventor
Ming-Sheng Yu
Hsui-Pei Hsu
Yam-Hui Wu
Yun-Hwa Hwang
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Inst Of Nuclear Energy Res Ato
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Priority to TW94137931A priority Critical patent/TWI287086B/en
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Publication of TWI287086B publication Critical patent/TWI287086B/en

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Abstract

A method and system for producing stress corrosion cracking (SCC) is disclosed, that the method is employed to cause the inner wall of a tube sample to generate stress corrosion cracks while applying a pressure difference and a temperature difference between the inner and outer walls of the tube sample. The system of the invention comprises: a tube, having an enclosed space formed therein for receiving a solution; and a heating apparatus, capable of heating the tube continuously until the outer wall of the pipe reaches a specific operating temperature; wherein the inner wall of the pipe is subjecting to a specific operating pressure while the outer wall of the pipe is maintaining at the specific operating temperature by the heating apparatus. The present invention can accelerate stress corrosion cracks to be generated on a specific tube by means of manual simulation, so that the evaluation of crack depth on the inner wall of a tube through the testing of tube samples with stress corrosion cracking, which is made out of the specific tube, can be improved on both inspection reliability and accuracy.

Description

Ί287086 九、發明說明·· 【發明所屬之技術領域】 本發明係有關一種用於製作應力腐蝕裂縫之方法及系 統’特別是有關於一種利用Inconel 600管件試樣内外兩 侧之溫度差及壓力差,於該管件試樣之内管壁表面上製作 出裂縫之方法及系統。 【先前技術】 目前核電廠為了維護蒸汽產生器運轉上的安全,都 執?有關蒸汽產生H管絲化、劣化監測、塞管與修補以 及哥限評估的工作,因此如何精確量測裂縫型態及 , 並獲得裂縫在不同裂縫深度的成長速率,實為組件劣=管 理成功與㈣重要目素,透職有應力腐料縫(s corrosi°ncradang,取)之管件試樣所提供的檢洌坪估 和驗證的功能,將有助於内总辟到产町柷州。平估 度與精確度。 B壁裂縫深度檢測評估的可靠 /習知放電加工技術所製作的刻痕,於昧 往往不夠精確,故依據此必 卞怙衣縫尺寸時 曲線,容易降低檢測評估的可^檢’所建立的裂縫校準 必要透過人工模擬的方式來與精確度,所以的確有 件試樣,以建立正確的出具有應力腐蝕裂縫的管 有鑑於此,本發明扭山 _ 方法及系統,透過本發明 料製作應力錢裂縫之 可以在模擬蒸汽產生器之1nconel 600管件試樣 Μ的糸統中,作為測試和評估管件一 1287086 次側應力腐蝕裂縫成長行為的觀察和探討,並可用於量 . 測、紀錄和計算各階段裂縫長度與深度的各自成長率。 【發明内容】 - 本發明的主要目的是在一管件試樣之内管壁上製作出 ,· 應力腐蝕裂缝以模擬蒸汽產生器中管束内壁上所產生之裂 * 縫。 本發明的次要目的是利用管件試樣内不同深度裂縫的 _ 檢測,得到一應力腐蝕裂縫非破壞檢測之校準曲線。 為達到上述目的,本發明提出一種用於製作應力腐蝕 裂縫之方法,該方法可於一管件之内管壁表面上製作出軸 向和圓周向兩種裂縫。首先放置一第一反應溶液於該管件 之内部;接著密封該管件以使該管件之内部為一第一封閉 空間;最後加熱該管件以使該管件之外管壁溫度維持於一 第一操作溫度,其中於該第一操作溫度下,該管件之内部 係對應維持於一第一操作壓力。 響 該方法更包括將該管件放置於一箱體之内部,並對該 管件施加一軸向應力,然後加熱該箱體以使該箱體之内部 溫度維持於一第二操作溫度,其中該箱體之内部為一第二 封閉空間並具有一第二反應溶液,此時於該第二操作溫度 * 下,該箝體之内部係對應維持於一第二操作壓力。 . 為達上述目的,本發明另提出一種用於製作應力腐蝕 裂縫之系統,該系統包括一管件及一加熱裝置,該管件係 具有一第一封閉空間以容置一第一反應溶液;該加熱裝置 係用以持續對該管件進行加熱直到該管件之外管壁溫度維 7 1287086 k 持於-第-操作溫度,在該第—操作溫度下,該管件之内 A 部係對應維持於一第一操作壓力。 該加熱裝置更包括—溫度控制器及一溫度感測器,該 =控:器係用以控制該管件之外管壁溫度維持於該第一 ㈣溫度,該溫度感測器制明量該管件之外管壁溫度。 : 較佳地,該管件係與-第-通氣管組合後而構成該第 .該第一通氣管上係設置有 = 二::該管件之兩端開口則分别焊接-端塞,其中: 於上&開口之端塞開設有―通孔以供 管:’此外,該管件與該加熱裝置間另設置有接該 覆蓋於該管件之外側,該伴護元 7G件 . 保產70件可為一不銹鋼管。 較佳地,該管件之材質為Inconel 600鋥入厶 一操作溫度約為35(rc,該第一操作麼力約為鎳=’该第 第一反應溶液為H雜,頭力該 權之Ν_溶液並依據該議 積=為,量濃度 之CU2〇。 饮骽積另添加300克/升 為達上述目的,本發明又提出—種用制 裂縫之系統,該系統包括_f件、―、氣作應力腐餘 及一加熱裝置,該管件係具有一第— —固定裝置以 一反應溶液;該箱體係具有-第二封閉二容置一第 f 一第二反應溶液;該固定裝置係用二以置該管件 官件施加-軸向應力;該加熱裝置係用以::官件並對該 ^熱直到該管件之外管壁溫度維持二-Ϊ、、讀該箱體進 2於該第-操作溫度下,該及操作溫度’ 對應維持於-第一操倾力及一第^=之内部係分別 8 1287086 該加熱裝置更包括一溫度控制器及一溫度感測器,該 溫度控制器係用以控制該管件之外管壁之溫度雉持二該^ 一操作溫度;該溫度感測器係用以測量該第二反應溶=之 溫度,其中該第二反應溶液之溫度係與該管件之外乾辟、、西 度相同。 該固定裝置更包括一固定架及一鎖固元件,該固定架 係用以固定該管件;該鎖固元件係用於抵緊該管件以二= 管件施加一軸向應力。 ^ 較佳地,該官件係與一第一通氣管組合後而構成誃 一封閉空間,該箱體係與一第二通氣管組合後而構成ς 二封閉空間,該第一通氣管上係設置有一第一洩壓裝^, 該第二通氣管上係設置有—第二祕裝置及_壓力計 於該管件之兩端開明分簡接—端塞,位於上端開 端塞係開設有-通孔以供該第—通氣管連接該管件。^ 較佳地’該管件之材質為I— 6GG鎳合金,該第 一据 、、玛洛么 2 Π Π . u ΊΊ 287086 IX. OBJECTS OF THE INVENTION · TECHNICAL FIELD OF THE INVENTION The present invention relates to a method and system for producing stress corrosion cracks, particularly relating to a temperature difference and a pressure difference between the inner and outer sides of a sample of an Inconel 600 tube. A method and system for making a crack on the surface of a tube wall of the tube sample. [Prior Art] At present, nuclear power plants are responsible for maintaining the safety of steam generators. Regarding the work of steam generation of H-tube filamentization, deterioration monitoring, plugging and repairing, and evaluation of the Ge, how to accurately measure the crack pattern and obtain the growth rate of the crack at different crack depths, it is a component inferior = successful management With (4) important objectives, the function of inspection and verification provided by the pipe specimens with the stress-corrosion joints (s corrosi°ncradang, taken) will help the inner general to the production town of Zhangzhou. Flatness and accuracy. The scoring made by the reliable/known electrical discharge machining technology for the detection and evaluation of the depth of the B-wall crack is often not accurate enough. Therefore, according to the curve of the seam size, it is easy to reduce the testability of the test. Crack calibration must be done by manual simulation and accuracy, so there is indeed a sample to establish the correct tube with stress corrosion cracks. In view of this, the twisted mountain method and system of the present invention, the stress is produced by the material of the present invention. The money crack can be used in the simulation of the 1nconel 600 tube specimen of the steam generator, as a test and evaluation of the growth behavior of the tube 1278068 secondary stress corrosion crack growth, and can be used for measurement, recording and calculation. The respective growth rates of crack length and depth at each stage. SUMMARY OF THE INVENTION - The main object of the present invention is to produce a stress corrosion crack on a pipe wall of a pipe sample to simulate a crack formed on the inner wall of the pipe bundle in the steam generator. The secondary object of the present invention is to obtain a calibration curve for non-destructive detection of stress corrosion cracks by utilizing the _ detection of cracks at different depths in the pipe sample. In order to achieve the above object, the present invention provides a method for producing a stress corrosion crack which can produce both axial and circumferential cracks on the inner wall surface of a pipe. First placing a first reaction solution inside the tube; then sealing the tube to make the inside of the tube a first closed space; finally heating the tube to maintain the temperature of the tube outside the tube at a first operating temperature The inner portion of the tube is maintained at a first operating pressure at the first operating temperature. The method further comprises placing the tube inside a box and applying an axial stress to the tube, and then heating the box to maintain the internal temperature of the box at a second operating temperature, wherein the box The inside of the body is a second closed space and has a second reaction solution. At this second operating temperature*, the internal portion of the caliper body is correspondingly maintained at a second operating pressure. In order to achieve the above object, the present invention further provides a system for producing a stress corrosion crack, the system comprising a tube member and a heating device, the tube member having a first closed space for accommodating a first reaction solution; the heating The device is configured to continuously heat the pipe until the pipe wall temperature dimension of the pipe is 7 1287086 k is maintained at the -first operating temperature, and at the first operating temperature, the A portion of the pipe is maintained correspondingly An operating pressure. The heating device further includes a temperature controller and a temperature sensor, wherein the control device is configured to control the temperature of the pipe wall outside the pipe to be maintained at the first (four) temperature, and the temperature sensor defines the pipe fitting Outside the wall temperature. Preferably, the tubular member is combined with the first-ventilating tube to form the first. The first venting tube is provided with a second: the two ends of the tubular member are respectively welded-end plug, wherein: The end of the upper & opening is provided with a through hole for the tube: 'In addition, the tube and the heating device are additionally provided to cover the outer side of the tube, the auxiliary element 7G. The production of 70 pieces can be It is a stainless steel tube. Preferably, the material of the tube is Inconel 600, and the operating temperature is about 35 (rc, the first operation is about nickel = 'the first reaction solution is H-heter, the head force is the right) _ solution and according to the convergence =, the concentration of CU2 〇. Drinking sputum added another 300 g / liter for the above purpose, the present invention also proposes a system for cracking, the system includes _f pieces, , the gas is used as a stress corrosion and a heating device, the pipe has a first-fixing device as a reaction solution; the tank system has a second closed two-capacity-f-second reaction solution; the fixing device is Applying an axial force to the tubular member; the heating device is used for: the official member and the heat until the temperature of the tube wall is maintained two-Ϊ, and the casing is read into At the first operating temperature, the operating temperature 'corresponds to the first operating force and the first internal frequency are respectively 8 1287086. The heating device further comprises a temperature controller and a temperature sensor, the temperature The controller is configured to control the temperature of the pipe wall outside the pipe to maintain the operating temperature; The temperature sensor is configured to measure the temperature of the second reaction solution, wherein the temperature of the second reaction solution is the same as that of the tube, and the fixture further includes a fixing frame and a lock. a fixing member for fixing the tubular member; the locking member is for abutting the tubular member to apply an axial stress to the tubular member. ^ Preferably, the official member is combined with a first venting tube Thereafter, a closed space is formed, and the box system is combined with a second vent pipe to form a second closed space. The first vent pipe is provided with a first pressure relief device, and the second vent pipe is provided on the second vent pipe. Yes - the second secret device and the _ pressure gauge open at each end of the pipe member are connected to the terminal plug, and the upper end open end is provided with a through hole for the first vent pipe to connect the pipe member. ^ Preferably The material of the pipe is I-6GG nickel alloy, the first data, Marlow 2 Π Π. u Ί

9 1287086 【實施方式】 為使貝審查委員能對本發明之特徵、目的及功能有 7步的認知與瞭解,茲配合圖式詳細說明如後: 3青多"考圖—,m /-έ. β 圖—係顯示本發明用於製作應力腐蝕裂 =之方法之實施步驟圖。首先放置—第—反應溶液於一管 ’此為步驟sl〇1 ;接著密封該管件以使該管件之 二二1 —封閉空間’此為步驟S1G2;最後加熱該管件 驟之外管壁溫度維持於一第一操作溫度,此為步 雉中於該第—操作溫度下,該管件之内部係對應 維持於一第—操作壓力。 之内部溫度雉持於 放置右一笛 第一麵作溫度,其中該箱體之内部係 可透過故在加熱該箱體之同時’該管件 第二摔作八吸收熱量而達到升溫之效果,於該 壓力。、/皿又下,該相體之内部係對應維持於一第二操作 ^參考圖二,管件21G的底端開口及頂端分別焊 2端塞211與212’其+端塞211與端塞212之二= 二2\!,質相同’在端塞212上另開設有一通孔213 从八、氣官214穿插而過並與端塞213緊密結合, ^ 21〇與通氣管214於組合後係形成一封閉空間215。' 二总210内係放置有一反應溶液216以利於在管件的 b壁上製作出應力腐蝕裂縫,其中管件21〇之材質為 10 12870869 1287086 [Embodiment] In order to enable the Beck Review Committee to have a 7-step understanding and understanding of the features, purposes and functions of the present invention, it is described in detail with the following figures: 3 青多"考图—, m /-έ . Fig. - shows a step-by-step diagram of the method of the present invention for producing stress corrosion cracking. First, the first-reaction solution is placed in a tube 'this step sl 〇 1; then the tube is sealed so that the tube is in the second enclosure - the closed space' is the step S1G2; finally, the temperature of the tube wall is maintained outside the tube At a first operating temperature, in the step, at the first operating temperature, the internal portion of the tube is maintained at a first operating pressure. The internal temperature is maintained at the temperature of the first side of the right flute, wherein the interior of the box is permeable, so that while the tank is being heated, the second member of the tube is absorbing eight heat to achieve the effect of warming up. The pressure. The inner portion of the phase body is maintained in a second operation. Referring to FIG. 2, the bottom end opening and the top end of the tube member 21G are respectively welded to the end plugs 211 and 212', and the + end plugs 211 and the end plugs 212. The second one is two 2\!, the same quality'. Another through hole 213 is formed in the end plug 212. The air member 214 is inserted through and tightly coupled with the end plug 213, and the 21 〇 and the vent tube 214 are combined. A closed space 215 is formed. There is a reaction solution 216 placed in the second total 210 to facilitate the formation of stress corrosion cracks on the b wall of the pipe. The material of the pipe 21 is 10 1287086.

In:el 600鎳合金’反應溶液216為一強驗溶液,該強 .驗洛液可由重1百分率濃度4〇%之隨^溶液以及細克/ 升之CuW所組成’ cU2〇係按照Na〇fj溶液之體積之比例來 添加。 • 在通氣管214上則設置有一壓力計217及一洩壓裝置 • 218壓力计217係用以測量管件21 〇之内部壓力;、戈壓梦 .置218係用於快速釋放管件210之内部以 210内邛壓力過大時而造成管件2ι〇爆裂,其中泡壓裝置 籲218可為-破裂片,當壓力過大時,該破裂片會無法承受 而自動裂開,藉此可降低管件21〇的内部壓力。 加熱裝置220則用來持續對管件21〇進行加熱直到管 件210之外官壁溫度維持於一第一操作溫度(約為 C )’由於官件210之内部體積不變,因此管件21〇之内部 壓力會隨著官内溫度的上升而增大,在該第一操作溫度 下,官件210之内部壓力會對應維持於一第一操作壓力(約 1200psi),由於管件210之外管壁溫度會略高於内管壁溫 _度’再加上管件210之内部壓力會高於其外部壓力(常壓 為14.7psi),因此在管件210之内管壁會承受應力而產生 軸向裂縫。 此外,加熱裝置220與管件110間另設置有一保護元 件219以隔離管件210和加熱裝置220,其中保護元件219 可為一不銹鋼管,以避免穿透裂縫生成而導致洩漏之強鹼 溶液破壞加熱裝置220,而加熱裝置220可為圓柱狀外型 以容置管件210。加熱裝置220包括有一溫度控制器(未 圖式)以及一溫度感測器222,該溫度控制器用來控制管 1287086 件210之外管壁溫度維持於 你 器222用來測量管件21〇之 刼作▲度;該溫度感測 222可為-熱電偶。最後再:壁溫度,其中溫度感測器 離保護襄置230内,以防止統放置於—適當的隔 出而危害到操作人員。 谷液216於操作時不慎喷 請參考圖三,管件31〇的 接有端塞311與端塞312夷=~口及頂端開口分別焊 與管㈣〇之材質相同,其中端塞夷3 9與端塞312之材質係 以供一通氣管314穿插㈣通孔313 營侔ή η盘、s 碥塞3緊途、結合,此時 总 /、通軋g 314於組合後係形成一封閉空間315。 官=310内係放置有-反應溶液316以利於在管件則的 内官壁上製作出圓周向應力腐蝕裂縫,其中管件31〇之材 質為Inconel 600鎳合金,反應溶液316為_強鹼溶液, 該強鹼溶液可由重量百分率濃度40%之NaOH溶液以及300 克/升之CmO所組成,CiM)係按照NaOH溶液之體積之比例 來添加。此外通氣管314上設置有一洩壓裝置317,用於 • 快速釋放管件310之内部壓力,以避免管件310内部壓力 過大時而造成管件310爆裂,洩壓裝置317可為一破裂片。 固定裝置320係用以固定管件310並對管件310施加 一軸向應力,其中固定裝置320可為一固定架(如圖四所 示)用於固定管件310,另外再搭配鎖固元件321與322, 鎖固元件321與322可為螺栓,其中鎖固元件321與322 係分別透過端塞311與312鎖固於固定裝置320上,並可 提供一軸向力量給警件310。 箱體330係與通氣管331於組合後係形成一封閉空間 !287〇86 抑2’箱體330内部具有一反應液體333,其中反應液體3 可為一去離子水,箱體330可為一抗高溫及抗高壓之33 鋼槽。通氣管331上設置有一壓力計334及一茂壓不錢 335,壓力計334係用以測量箱體330之内部壓力;、冷^置 置335係用於快速釋放箱體330之内部壓力,以避务f襄 330内部壓力過大時而造成箱體330爆裂,其中洩壓=體 335可為一破裂片,當壓力過大時,該破裂片會無法广, 而自動裂開,藉此來降低箱體330的内部壓力。“承交 加熱裝置340係設置於箱體330之外側,加熱裝置 包括有一溫度控制器(未圖式)以及一溫度感測器"3』4,0 該’里度控制為用以控制管件31〇之外管壁溫度維持於哕 一操作溫度(約為3〇〇。〇);溫度感測器342用於蜊旦= 溶液333之溫度,其中溫度感測器332可為一熱電μ 、s加熱裝置340開始加熱直到反應溶液333的溫度等 第t操ί溫度(約為3〇rc)’由於箱體330内部體積 祕變’因此箱體330之内部壓力會隨著箱内溫度的上升而 增大,在該第二操作溫度下,箱體33〇之内部壓力廡 333 、,皿又上升,官件31〇内之溫度亦會跟著上昇,由於管 310的内部體積不變’故在該第一操作溫度下,管件⑽ ΐSit 111應維持於一第一操作壓力(約4〇〇PS1), ^ ;要承受有一軸向應力,再加上内外兩側的 ^因此官“⑺之时壁會將產生 斤述本發明提出一種用於在Inconel 600管件 13 1287086 出:腐蝕裂縫之方法及系統,此方法可加速製作 ^具ΐ㈣或圓周向應力腐#裂縫之管件試樣,透過此 夠模_真實管束中之裂縫,其所獲得的裂縫可作 偏ίϊί㈣驗證之用,破實有提昇内管壁裂縫檢測評 估的可靠度與精確度。 之限:工,僅為本發明之較佳實施例,當不能以 之均等變化及=圍。即Α凡依本發明申請專利範圍所做 離本發明之精將不失本發明之要義所在,亦不脫 狀況。 中和乾圍,故都應視為本發明的進—步實施 【圖式簡單說明] 圖一係顯示 施步驟圖。 本發明用於製作應力腐蝕裂縫之方法之實 縫之系統之第一較 缝之系統之第二較In:el 600 nickel alloy 'reaction solution 216 is a strong solution, the strength. The test solution can be composed of a 1% concentration of 4% by weight of the solution and a fine gram / liter of CuW 'cU2 〇 according to Na〇 The ratio of the volume of the fj solution is added. • A venting tube 214 is provided with a pressure gauge 217 and a pressure relief device. • The 218 pressure gauge 217 is used to measure the internal pressure of the tubular member 21; and the 218 is used to quickly release the interior of the tubular member 210. When the pressure in the inner pressure of 210 is too large, the pipe member 2 〇 ruptures, and the damper device 218 can be a rupture piece. When the pressure is too large, the rupture piece can be unbearably and automatically cracked, thereby reducing the inside of the pipe member 21〇. pressure. The heating device 220 is used to continuously heat the pipe member 21〇 until the temperature of the official wall outside the pipe member 210 is maintained at a first operating temperature (about C)', since the internal volume of the official member 210 is constant, the inside of the tubular member 21 is The pressure will increase with the increase of the internal temperature. At the first operating temperature, the internal pressure of the official member 210 will be maintained at a first operating pressure (about 1200 psi), due to the temperature of the tube wall outside the tube 210. Slightly higher than the inner tube wall temperature _ degree 'and the internal pressure of the tube 210 will be higher than its external pressure (normal pressure is 14.7 psi), so the tube wall will be subjected to stress within the tube 210 to generate axial cracks. In addition, a protection element 219 is further disposed between the heating device 220 and the tube member 110 to isolate the tube member 210 and the heating device 220, wherein the protection member 219 can be a stainless steel tube to prevent the strong alkali solution from leaking and causing leakage to damage the heating device. 220, and the heating device 220 may have a cylindrical shape to accommodate the tubular member 210. The heating device 220 includes a temperature controller (not shown) and a temperature sensor 222 for controlling the temperature of the tube wall outside the tube 1280068 210 to be maintained by the device 222 for measuring the tube 21 ▲ degree; the temperature sensing 222 can be a thermocouple. Finally, the wall temperature, in which the temperature sensor is placed inside the protective device 230, prevents the system from being placed in the proper isolation and jeopardizing the operator. In case of accidental spraying, the liquid 216 is sprayed. Please refer to Figure 3. The end of the tube 31 接 is connected with the end plug 311 and the end plug 312. The opening and the top opening are respectively welded to the same material as the tube (4), and the end plug is 3 9 The material of the end plug 312 is used for inserting a vent pipe 314 (4) through hole 313. The y disk and the s dam 3 are tightly combined, and the total/pass rolling g 314 is combined to form a closed space 315. . The official solution 310 has a reaction solution 316 to facilitate the formation of a circumferential stress corrosion crack on the inner wall of the pipe member, wherein the pipe member 31 is made of Inconel 600 nickel alloy, and the reaction solution 316 is a strong alkali solution. The strong base solution may be composed of a 40% by weight NaOH solution and 300 g/L of CmO, and CiM) is added in proportion to the volume of the NaOH solution. In addition, a venting device 317 is disposed on the vent tube 314 for quickly releasing the internal pressure of the tube member 310 to prevent the tube member 310 from bursting when the internal pressure of the tube member 310 is excessively large. The pressure releasing device 317 can be a rupture piece. The fixing device 320 is used for fixing the pipe member 310 and applying an axial stress to the pipe member 310. The fixing device 320 can be a fixing frame (as shown in FIG. 4) for fixing the pipe member 310, and further matching the locking members 321 and 322. The locking elements 321 and 322 can be bolts, wherein the locking elements 321 and 322 are respectively fixed to the fixing device 320 through the end plugs 311 and 312, and can provide an axial force to the warning member 310. The box body 330 and the vent tube 331 are combined to form a closed space! 287 〇 86 2 2 ′ inside the box 330 has a reaction liquid 333, wherein the reaction liquid 3 can be a deionized water, the tank 330 can be a 33 steel tanks resistant to high temperatures and high pressures. The ventilator 331 is provided with a pressure gauge 334 and a pressureless 335. The pressure gauge 334 is used to measure the internal pressure of the tank 330. The cold 335 is used to quickly release the internal pressure of the tank 330 to avoid the internal pressure. When the internal pressure of the f襄330 is too large, the box 330 is bursting, wherein the pressure relief body 335 can be a rupture piece. When the pressure is too large, the rupture piece can not be widened and automatically cracked, thereby lowering the box 330. Internal pressure. "The receiving heating device 340 is disposed on the outer side of the casing 330. The heating device includes a temperature controller (not shown) and a temperature sensor "3』4,0. The 'Rid control is used to control the pipe fittings. The wall temperature outside 31〇 is maintained at the first operating temperature (about 3 〇〇. 〇); the temperature sensor 342 is used for the temperature of the solution 333, wherein the temperature sensor 332 can be a thermoelectric μ, The heating device 340 starts heating until the temperature of the reaction solution 333 is equal to the temperature (about 3 〇 rc) 'because the internal volume of the tank 330 is secreted', so the internal pressure of the tank 330 rises with the temperature inside the tank. Increasingly, at the second operating temperature, the internal pressure 庑 333 of the casing 33 、, the dish rises again, and the temperature inside the official member 31 亦 also rises, because the internal volume of the tube 310 does not change. At the first operating temperature, the pipe (10) ΐSit 111 should be maintained at a first operating pressure (about 4 〇〇 PS1), ^; to withstand an axial stress, plus the inner and outer sides of the ^ so the official "(7) The wall will produce the pounds described herein. The present invention is proposed for use in the Inconel 600 pipe fittings 13 1287086 Out: Corrosion crack method and system, this method can accelerate the fabrication of pipe specimens with ΐ(4) or circumferential stress corrosion# cracks, through which the cracks in the tangible tube bundle can be verified by the cracks. For the purpose of use, the reliability and accuracy of the crack detection and evaluation of the inner wall are improved. Limitations: Work, only the preferred embodiment of the present invention, when it is not possible to vary equally and =. That is, the essence of the present invention is not limited to the scope of the present invention. Neutralization and dry circumference should be regarded as the further implementation of the present invention. [Simple description of the drawing] Figure 1 shows the step diagram. The second comparison of the first seam system of the system for producing a solid seam of the method for producing stress corrosion cracks

圖二為本發明用於製作應力腐蝕裂 佳實施例不意圖。 圖二為本發明用於製作應力腐蝕裂 佳實施例不意圖。 圖四為圖三中之固定架之示意圖。 【主要元件符號說明】 210〜管件 211〜端塞 212〜端塞 14 1287086Figure 2 is a schematic view of a preferred embodiment of the present invention for making stress corrosion cracking. Figure 2 is a schematic view of a preferred embodiment of the present invention for making stress corrosion cracking. Figure 4 is a schematic view of the fixing frame in Figure 3. [Main component symbol description] 210~pipe fitting 211~end plug 212~end plug 14 1287086

213〜通孔 214〜 <通氣管 215〜 封閉空間 216〜反應溶液 217〜壓力計 218〜 …;戈壓裝置 219- '保護元件 220〜 '加熱裝置 222〜 '溫度感測器 230〜 隔離保護裝置 310〜 …管件 311〜 端塞 312〜 端塞 313〜 通孔 314〜 通氣管 315〜 封閉空間 316〜反應溶液 317〜 洩壓裝置 320〜 固定裝置 321、 322〜鎖固元件 330〜 箱體 331〜 通氣管 332〜 封閉空間 1287086 333〜反應溶液 / 334〜壓力計 . 335〜洩壓裝置 340〜加熱裝置 • 342〜溫度感測器213~ through hole 214~ < vent pipe 215~ closed space 216~ reaction solution 217~pressure gauge 218~...; pressure device 219-'protection element 220~' heating device 222~'temperature sensor 230~ isolation protection Device 310~...tube 311~end plug 312~end plug 313~ through hole 314~ vent pipe 315~closed space 316~reaction solution 317~ pressure relief device 320~ fixed device 321, 322~locking element 330~ box 331 ~ vent pipe 332 ~ closed space 1287086 333 ~ reaction solution / 334 ~ pressure gauge. 335 ~ pressure relief device 340 ~ heating device • 342 ~ temperature sensor

Claims (1)

!287〇86 十、申請專利範圍: 1. -種用於製作應力腐_縫之法^ =面上製作出裂縫,該方法【二;:驟1件 置反應溶液於該管件之内部; 密:該管件以使該管件之内部二 閉 L該管之外管壁溫度維々、及 應維持於-第一操作壓力。 牛之内部係對 之 2. ::請專利範圍第(項所 於 3方=中該方法更包括對咖裂縫 之 = = 之用:製作應力腐:裂縫 該箱體之内部係為—第-秦置該'件於一箱體之内部, 4·如申請專利範圍二 :、門 方法,其中該方法^所述之用於製作應力腐蝕裂縫之 溫度維持於一第’一 4σ匕括加熱該箱體以使該箱體之内部 箱體之内料於該第二操作溫度下,該 5. 如申請專利範圍第3頊、、第二操作壓力。 方法,其中該箱 、所述之用於製作應力腐蝕裂縫之 6. -種用於製:二:内部具有-第二反應溶液。 -管件,其係:有4裂縫之系統’包括: 液;以及 弟—封閉空間以容置一第一反應溶 外管壁溫度續對該管件進行加熱直到該管件之 一第一操作溫度,其中於該第一操 17 ^87086 作溫度下,該官件之内部係對應維持於一第一操作壓 - 力。 ' 7·如申晴專利範圍第6項所述之用於製作應力腐餘裂縫之 系統’其巾該管件係與—第—通氣f組合後而構成該第 。 一封閉空間。 8·如/申明專利範圍第6項所述之用於製作應力腐餘裂縫之 系統,其中該管件與該加熱裝置間設置有一保護元件覆 盘於該管件之外側。 春9.如中請專利範圍第6項所述之用於製作應力腐㈣縫之 系統,其中該加熱裝置更包括一溫度控制器,用以控制 該管件之外管壁溫度維持於該第一操作溫度。 10·如申請專利範圍第6項所述之用於製作應力腐蝕裂縫 之系統,其中該加熱裝置更包括一溫度感測器,用以測 量該管件之外管壁溫度。 11·如申請專利範圍第7項所述之用於製作應力腐蝕裂縫 之系統,其中該第一通氣管上係設置有一洩壓裝置。 12·如申請專利範圍第7項所述之用於製作應力腐蝕裂縫 之系統’其中該第一通氣管上係設置有一壓力計。 13·却申請專利範圍7項所述之用於製作應力腐蝕裂縫之 .系統,其中該管件之兩端開口分別焊接一端塞,位於上 裢開口之端塞係開設有一通孔以供該第一通氣管連接 該管件。 14·如申請專利範圍第8項所述之用於製作應力腐蝕裂縫 之系統,其中該保護元件為一不銹鋼管。 18 1287086 專::圍第6項所述之用於製作應力腐蝕裂縫 二!該管件之材質為1_鎳合金。 之李έΙ H圍第6項所述之用於製作應力腐餘裂縫 :該第一反應溶液為-強驗溶液。 之系二::罈第16項所述之用於製作應力腐蝕裂縫 40^ Na〇H a如申請專利範圍第Γ=加綱克/升之⑽。 19::統’其中該第-二=^應_裂縫 ;專:=第6項所述之用於製作 ”統’其中該第—操作壓力為測㈣。 .一,用於製作應力腐餘縫之系統,包括: ^件其係具有—第—封閉空間以容置-第-反應溶 1定裝iW定該管件並對該管件施加—轴向應 一 二封閉空間以容置該管件及一第 作:度下,該管件及該箱體之内;;別對工, 一第—操作壓力及-第二操作壓力。應維持於 轉第通碧錢而構成該 19 1287086 第一封閉空間。 . 22.如申請專利範圍第20項所述之用於製作應力腐蝕裂縫 之系統,其中該箱體係與一第二通氣管組合後而構成該 第二封閉空間。 - 23.如申請專利範圍第20項所述之用於製作應力腐蝕裂缝 ; 之系統,其中該加熱裝置更包括一溫度控制器,用以控 制該管件之外管壁之溫度維持於該第一操作溫度。 24. 如申請專利範圍第20項所述之用於製作應力腐蝕裂縫 _ 之系統,其中該加熱裝置更包括一溫度感測器,用以測 量該第二反應溶液之溫度。 25. 如申請專利範圍第21項所述之用於製作應力腐蝕裂縫 之系統,其中該第一通氣管上係設置有一第一洩壓裝 置。 26. 如申請專利範圍21項所述之用於製作應力腐蝕裂缝之 系統,其中該管件之兩端開口分別焊接一端塞,位於上 端開口之端塞係開設有一通孔以供該第一通氣管連接 • 該管件。 27. 如申請專利範圍第22項所述之用於製作應力腐蝕裂縫 之系統,其中該第二通氣管上係設置有一第二洩壓裝 置。 28. 如申請專利範圍第22項所述之用於製作應力腐蝕裂縫 : 之系統,其中該第二通氣管上係設置有一壓力計。 29. 如申請專利範圍第20項所述之用於製作應力腐蝕裂縫 之系統,其中該固定裝置更包括一固定架用以固定該管 20 1287086 件。 . 30.如申請專利範圍第20項所述之用於製作應力腐蝕裂縫 之系統,其中該固定裝置更包括一鎖固元件用於抵緊該 管件以對該管件施加一轴向應力。 • 31.如申請專利範圍第20項所述之用於製作應力腐蝕裂縫 ; 之系統,其中該管件之材質為Inconel 600鎳合金。 32.如申請專利範圍第20項所述之用於製作應力腐蝕裂缝 之系統,其中該第一反應溶液為一強鹼溶液。 • 33.如申請專利範圍第32項所述之用於製作應力腐蝕裂缝 之系統,其中該強鹼溶液為重量濃度40%之NaOH溶液 且依據該NaOH溶液體積另添加300克/升之Cu2〇。 34. 如申請專利範圍第20項所述之用於製作應力腐蝕裂縫 之系統,其中該第二反應溶液為一去離子水。 35. 如申請專利範圍第20項所述之用於製作應力腐蝕裂縫 之系統,其中該第一操作溫度為30(TC。 36. 如申請專利範圍第20項所述之用於製作應力腐蝕裂縫 • 之系統,其中該第一操作壓力為400psi。 37. 如申請專利範圍第20項所述之用於製作應力腐蝕裂縫 之系統,其中該第二j喿作壓力為1250psi。 38. 如申請專利範圍第20項所述之用於製作應力腐蝕裂縫 ' 之系統,其中該箱體為一抗高溫及抗高壓之不銹鋼槽。 21!287〇86 X. The scope of application for patents: 1. - The method used to make stress rust _ seam method ^ = crack on the surface, the method [2;: 1 piece of reaction solution in the inside of the pipe; The tube is such that the inside of the tube is closed, the temperature of the tube wall outside the tube is maintained, and should be maintained at a first operating pressure. The internal part of the cow is 2. The scope of the patent is required (the item is in the 3 party = the method is more included in the crack of the coffee = =: the production of stress rot: the internal part of the box is - - Qin placed the 'piece inside a box, 4 · as claimed in the scope of the second:, the door method, wherein the method described in the method for the production of stress corrosion cracks maintained at a 'four σ 匕 heating The casing is such that the inner casing of the casing is filled with the second operating temperature, as in the third aspect of the patent application, the second operating pressure. The method, wherein the tank is used for 6. Produce stress corrosion cracks - - for the production of: 2: internal - second reaction solution - pipe fittings, its system: system with 4 cracks 'including: liquid; and brother - closed space to accommodate a first Reacting the outer wall temperature continues to heat the tube until a first operating temperature of the tube, wherein the internal portion of the official member is maintained at a first operating pressure at the temperature of the first operation 17 ^ 87086 - Force. '7·For the production as described in item 6 of the Shenqing patent scope The system of the residual cracks is formed by combining the pipe fittings with the first-ventilation f. A closed space. 8. The use of the stress-corrosion cracks as described in Item 6 of the claim patent. a system, wherein a protective element is disposed on the outer side of the tube between the tube and the heating device. Spring 9. The system for making a stress rot (four) seam according to item 6 of the patent application, wherein the heating device Furthermore, a temperature controller is provided for controlling the temperature of the tube wall outside the tube to be maintained at the first operating temperature. 10. The system for producing stress corrosion cracks according to claim 6 of the patent application, wherein the heating device Furthermore, a temperature sensor is provided for measuring the temperature of the pipe wall outside the pipe. 11. The system for producing stress corrosion cracks according to claim 7, wherein the first vent pipe is provided with a A pressure relief device. 12. A system for producing stress corrosion cracks as described in claim 7 wherein a pressure gauge is provided on the first vent tube. The system for producing stress corrosion cracks, wherein the ends of the tube are respectively welded with one end plug, and the end plug of the upper jaw opening is provided with a through hole for the first vent tube to connect the tube. The system for producing stress corrosion cracks according to Item 8 of the patent scope, wherein the protection component is a stainless steel tube. 18 1287086 Special:: The material for stress corrosion cracking described in Item 6! It is a nickel alloy. It is used to make stress corrosion cracks as described in Item 6 of the H.: The first reaction solution is a strong solution. The system is as described in Item 16: Produce stress corrosion cracks 40^ Na〇H a as in the scope of patent application Γ = plus gram / liter (10). 19:: The system of the first-two = ^ should be _ crack; special: = the sixth item is used to make the "system" where the first - operating pressure is measured (four). First, used to make stress residual a seaming system comprising: a member having a first-enclosed space for accommodating - a first reaction 1 fixing iW to define the tubular member and applying the axial member to the tubular member to accommodate the tubular member and a first work: the degree, the pipe and the inside of the box;; do not work, a first - operating pressure and - the second operating pressure. Should be maintained in the transfer of the money and constitute the 19 1287086 first closed space 22. The system for making a stress corrosion crack according to claim 20, wherein the tank system is combined with a second vent tube to form the second closed space. The system for producing a stress corrosion crack according to Item 20, wherein the heating device further comprises a temperature controller for controlling the temperature of the pipe wall outside the pipe to be maintained at the first operating temperature. For the production of stress corrosion cracks as described in item 20 of the patent scope _ The system, wherein the heating device further comprises a temperature sensor for measuring the temperature of the second reaction solution. 25. The system for producing stress corrosion cracks according to claim 21, wherein the A venting tube is provided with a first pressure relief device. 26. The system for making stress corrosion cracks according to claim 21, wherein the ends of the tube are respectively welded with one end plug at the end of the upper end opening. The plug system has a through hole for the first vent pipe to connect to the pipe. 27. The system for making a stress corrosion crack according to claim 22, wherein the second vent pipe is provided with a first 2. A pressure relief device. 28. A system for making a stress corrosion crack as described in claim 22, wherein the second vent tube is provided with a pressure gauge. 29. As claimed in claim 20 The system for producing a stress corrosion crack, wherein the fixing device further comprises a fixing frame for fixing the tube 12 1287086. 30. As claimed in claim 20 A system for making a stress corrosion crack, wherein the fixture further includes a locking element for abutting the tube to apply an axial stress to the tube. 31. As described in claim 20 A system for producing a stress corrosion crack; the material of the tube is Inconel 600 nickel alloy. The system for producing stress corrosion cracks according to claim 20, wherein the first reaction solution is a A system for producing stress corrosion cracks as described in claim 32, wherein the strong alkali solution is a 40% by weight NaOH solution and an additional 300 g is added according to the volume of the NaOH solution. Li Cu2〇. 34. The system for making a stress corrosion crack according to claim 20, wherein the second reaction solution is a deionized water. 35. The system for making stress corrosion cracks according to claim 20, wherein the first operating temperature is 30 (TC. 36. used to make stress corrosion cracks as described in claim 20 • The system wherein the first operating pressure is 400 psi 37. The system for making a stress corrosion crack as described in claim 20, wherein the second pressure is 1250 psi. The system for producing stress corrosion cracks according to item 20, wherein the tank is a stainless steel tank resistant to high temperature and high pressure.
TW94137931A 2005-10-28 2005-10-28 Method and system for producing stress corrosion cracking TWI287086B (en)

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