TW531638B - An error evaluation technique for incident angle in a rotating element ellipsometer using quartz crystal - Google Patents
An error evaluation technique for incident angle in a rotating element ellipsometer using quartz crystal Download PDFInfo
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- TW531638B TW531638B TW89101857A TW89101857A TW531638B TW 531638 B TW531638 B TW 531638B TW 89101857 A TW89101857 A TW 89101857A TW 89101857 A TW89101857 A TW 89101857A TW 531638 B TW531638 B TW 531638B
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531638531638
五、發明說明(l) 本發明係在一轉動式橢圓偏光儀的樣品座上加一可 旋轉的平台以放置異向單軸石英(uniaxial quartz crystal)以量測轉動式橢圓偏光儀因轉動而產生之入射 角偏差(圖一),一般被認知為轉動式橢圓偏光儀寄生誤差 (parasitic error) 〇 > 轉動式橢圓偏光儀由於無須補波片已廣為應用在光 譜的量測上。但由於有轉動元件,除非光學元件的平面 均無斜角,否則必產生光束的移動,故而造成入射角的寄 生誤差,此誤差早在1 974年揭露於Zeidler J.R. et’al· Appl· Opt· 13,1938。除了使用造價昂貴的光學 元件,本發明利用一異向單軸石英量測並評估偏光儀中的 寄生誤差’藉以消除橢圓偏光儀的量測誤差。 依美國1998年Yu-Faye Chao等人專利 5706088 , Polarizer-Sample-Analyzer IntensityV. Description of the invention (l) The present invention is to add a rotatable platform to a unidirectional quartz crystal on a sample holder of a rotary ellipsometry to measure the rotation of the ellipse The resulting incident angle deviation (Figure 1) is generally recognized as a parasitic error of a rotating elliptical polarizer 〇 > Rotating elliptical polarizers have been widely used in spectral measurement because they do not require a complementary plate. However, because of the rotating element, unless the plane of the optical element has no oblique angle, the beam will move, which will cause the parasitic error of the incident angle. This error was disclosed in Zeidler JR et'al · Appl · Opt · as early as 1 974 13, 1938. In addition to the use of expensive optical components, the present invention uses an anisotropic uniaxial quartz to measure and evaluate the parasitic errors in the polarimeter ', thereby eliminating the measurement errors of the ellipsometry. According to US 1998 Yu-Faye Chao et al. Patent 5706088, Polarizer-Sample-Analyzer Intensity
Qudient ellipsometry,取一標準玻璃先校正偏光片及 析光片的穿透軸;將偏光片的穿透軸分別調放在± 4 5度 的位置,在樣品座上換放一可旋轉的異向單軸石英,當 析光片的穿透軸為零度時將樣品旋轉一周並量取其亮度, 稱,Ip±45」當析光片的穿透軸為9〇度時將樣品旋轉一周 並s取其党度’稱為is±45。依上述專利優化後的擴圓參Qudient ellipsometry, take a standard glass and first correct the transmission axis of the polarizer and the analyzer; adjust the transmission axis of the polarizer to ± 45 degrees, and place a rotatable anisotropy on the sample holder. For uniaxial quartz, when the transmission axis of the light analysis plate is zero degrees, the sample is rotated once and its brightness is measured. Weigh, Ip ± 45 ″ When the transmission axis of the light analysis plate is 90 degrees, the sample is rotated one time and s Taking its party degree 'is called is ± 45. Expanded ginseng optimized according to the above patent
第4頁 531638Page 4 531638
fr J ^ to—= 上11 U+« U (式1) 此橢圓偏光參數Aspnes D. Ε·在1 980年的j· 〇pt. S〇C· Am· 7〇, 1 275中指出:異向單軸晶體所量的橢圓偏 光參數等效於一無向介質(isotr〇pic medium)的偏光參 數,而此等效無向介質的折射率取決於此異向單軸的折射 率在反射面的分量。依此說法,本發明根據Lekne;r j· 1991年在J. Αρρ1· Phys· 34,5〇16所發展的異向單軸 介面的反射關係撰寫程式以供推算入射角偏差(表丨)。 本,明以一雙折射晶體石英校正轉動式橢圓偏光儀的 ^射=藉以減少其系統的量測誤差,並可將偏光片取代造 價昂貴的偏光晶體,亦可以同樣的方法量測異向單軸晶體 的折射率及光軸的位置。 本發明之一特徵在於提供一雙折射晶體石英,其一般 折射率(ordinary refractive index)及異常折射率 (extraordinary refractive index)相差很小以達分辨入 射角的微小誤差。 本發明之另一特徵在於利用校正入射角偏差後量測 異向單軸晶體之一般折射率(ordinary refractive index)、異常折射率(extra〇rdinary refractiVe index) 及其光軸與切面的夾角。 為了更進一步揭露本發明的架構、特徵及優點,茲 配合附圖說明實例於後。fr J ^ to— = above 11 U + «U (Equation 1) This elliptic polarization parameter Aspnes D. Ε · is indicated in j · 〇pt. S〇C · Am · 70, 1 275 in 1980: The elliptic polarization parameter measured by a uniaxial crystal is equivalent to the polarization parameter of an isotropic medium, and the refractive index of this equivalent nondirectional medium depends on the refractive index of the anisotropic uniaxial refractive index on the reflecting surface. Weight. According to this statement, the present invention compiles a program based on the reflection relationship of the anisotropic uniaxial interface developed in J. Αρρ1 · Phys · 34, 5016 in 1991 by Lekne; r j · for estimating the incident angle deviation (Table 丨). In this paper, Ming uses a birefringent crystal quartz to correct the rotation of an elliptical polarizer. This reduces the measurement error of the system, and can replace polarizers with expensive polarizers. The refractive index of the axial crystal and the position of the optical axis. One feature of the present invention is to provide a birefringent crystalline quartz, the difference between the ordinary refractive index and the extraordinary refractive index is small to achieve a small error in resolving the incident angle. Another feature of the present invention is to measure the ordinary refractive index, extraordinary refractiVe index, and the angle between the optical axis and the tangent plane of the anisotropic uniaxial crystal after correcting the deviation of the incident angle. In order to further disclose the structure, features, and advantages of the present invention, examples are described below with reference to the drawings.
531638 五、發明說明(3) 依美專利5706088架設一轉動式橢圓偏光儀(圖 1);雷射(10)發出之光經一偏光片(2〇),其方位角置於 ^ 45度處’在一特定入射角(25,本實例為45度)經石 央(3 5 )反射後’再經析光片(3 0 ),其方位角分別置於0 及90度’最後由光偵測器(40)測得之亮度由一數位轉換 器(50j輸入電腦(60)將之換算成橢圓偏光參數(參考式 lj。晶體的方位角可由其旋轉座(37)控制。本發明將石 央所置出的橢圓偏光參數與理論值比後(圖2 ),可清楚的 發覺由轉動系統所發生之誤差,當入射角設為44· 94度 則,論值與量測吻合(圖3)。並以同樣的方法量γν〇4則 可篁出此晶體的切面與光軸的夾角(圖4)。 雖然本發明已以較佳實例 定本發明,在不脫離本發明之 單軸異向晶體光軸與切面的量 常折射率的量測,單軸異向晶 均為本發明之保護範圍。 揭露如上,然其並非用以限 精神和範圍内,如其應用在 測,亦或其一般折射率及異 體光軸對參考座的相對位置 說明附圖 第1圖:(a)轉動式橢圓偏光儀的基本架構 (b)本發明石英晶體及轉台 重要元件符號說明531638 V. Description of the invention (3) According to US patent 5706088, a rotating elliptical polarizer (Figure 1) is set up; the light emitted by the laser (10) passes through a polarizer (20), and its azimuth is placed at ^ 45 degrees 'After being reflected by Shi Yang (3 5) at a specific incident angle (25, 45 degrees in this example)' and then passing through the light analysis sheet (3 0), the azimuth angles are set to 0 and 90 degrees, respectively. ' The brightness measured by the measuring device (40) is converted into an elliptical polarization parameter (refer to the formula lj) by a digital converter (50j input to the computer (60)). The azimuth of the crystal can be controlled by its rotating seat (37). The ratio of the elliptical polarization parameter set by the center to the theoretical value (Figure 2) can clearly detect the error caused by the rotation system. When the incident angle is set to 44.94 degrees, the theoretical value is consistent with the measurement (Figure 3) ). And by measuring γν〇4 in the same way, the angle between the cut plane of the crystal and the optical axis can be found out (Figure 4). Although the present invention has been determined by a preferred example, the uniaxial anisotropy does not depart from the invention The measurement of the constant refractive index of the optical axis and the tangent plane of the crystal, and the uniaxial anisotropic crystal are all within the protection scope of the present invention. However, it is not intended to limit the spirit and scope. If it is applied to the measurement, or its general refractive index and the relative position of the foreign body optical axis to the reference base will be described in the drawing. Figure 1: (a) Basics of a rotating ellipsometry Architecture (b) Symbol description of important components of the quartz crystal and turntable of the present invention
第6頁 531638Page 6 531638
五、發明說明(4) (10)光源(light source) (20)偏光片(polarizer) (30)析光片(analyzer) (37)待測架(sample holder) (40)偵測裝置(detector) (50)數位轉換器(a/D converter) (60)個人電腦(pc) 第2圖:當入射角為45度,石英晶體光軸之各方位下 橢圓參數值(-為理論計算值,•為量測值) 第3圖:當入射角為44.94度,石英晶體光軸之各方位 下的橢圓參數值(-為理論計算值,•為量測值),入 射角偏差為-0.06±0.01度。 第4圖:當入射角為44. 94 度,YV04晶體光軸之各方 位下的橢圓參數值(-為理論計算值,_為量測值), 所推算出的η〇 = 1·9929 ne = 2.2154 ;切面與光軸夾角為 136· 〇1 ± 0· 01 度 表1 :入射角偏差判別流程·V. Description of the invention (4) (10) Light source (20) Polarizer (30) Analyzer (37) Sample holder (40) Detector (detector) ) (50) digital converter (a / D converter) (60) personal computer (pc) Figure 2: When the incident angle is 45 degrees, the ellipse parameter values in the various positions of the optical axis of the quartz crystal (-is the theoretical calculation value, • is the measured value) Figure 3: When the incident angle is 44.94 degrees, the ellipse parameter values under the various directions of the optical axis of the quartz crystal (-is the theoretical calculation value, • is the measured value), the incident angle deviation is -0.06 ± 0.01 degrees. Figure 4: When the incident angle is 44. 94 degrees, the ellipse parameter values (-is the theoretical calculation value, _ is the measurement value) under each position of the optical axis of the YV04 crystal, the calculated η〇 = 1.9929 ne = 2.2154; The angle between the cut plane and the optical axis is 136 · 〇1 ± 0 · 01 degrees Table 1: Discrimination process of incident angle deviation ·
531638 五、發明說明(5)531638 V. Description of the invention (5)
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Cited By (1)
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TWI485374B (en) * | 2014-01-27 | 2015-05-21 | Univ Nat Chiao Tung | Ellipsometer and ellipsometric parameters measuring method utilizing the same |
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TWI485374B (en) * | 2014-01-27 | 2015-05-21 | Univ Nat Chiao Tung | Ellipsometer and ellipsometric parameters measuring method utilizing the same |
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