TW227553B - Method of making 2,3- dihydrogen-1,4,5,8- tetrahydroxy -9,10 anthryl diketone - Google Patents

Method of making 2,3- dihydrogen-1,4,5,8- tetrahydroxy -9,10 anthryl diketone

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Publication number
TW227553B
TW227553B TW81106131A TW81106131A TW227553B TW 227553 B TW227553 B TW 227553B TW 81106131 A TW81106131 A TW 81106131A TW 81106131 A TW81106131 A TW 81106131A TW 227553 B TW227553 B TW 227553B
Authority
TW
Taiwan
Prior art keywords
anthryl
quinone
dihydroxy
tetrahydroxy
dihydrogen
Prior art date
Application number
TW81106131A
Other languages
Chinese (zh)
Inventor
Pong Chang
Original Assignee
Chinese Health Inst
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chinese Health Inst filed Critical Chinese Health Inst
Priority to TW81106131A priority Critical patent/TW227553B/en
Application granted granted Critical
Publication of TW227553B publication Critical patent/TW227553B/en

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  • Gas Separation By Absorption (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Method of making 2,3- dihydrogen -1,4,5,8- tetrahydroxy -9,10 anthryl diketone comprises: mixing 5-45% of fumed acid, 1,8- dihydroxy anthryl quinone and 1-3 equivalent of boric acid according to the equivalent of 1,8- dihydroxy anthryl quinone, adding nitric acid drop by drop to nitrify 1,8- dihydroxy anthryl quinone to produce 1,8- dihydroxy -4,5- dinitro anthryl quinone, washing the mixture with solvent and extracting the product with a solvent containing dimethyl amide at -10-50 deg.C; adding 60-90% of sulfuric acid and iron powder to reduce 1,8- dihydroxy -4,5- dinitro anthryl quinone into 1,8- dihydroxy -4,5- diamino anthryl quinone at 60-120 deg.C; adding alkaline solution with 5-25% oforganic solvent and 0.1-0.25 mole of sodium hydrosulfite to reduce 1,8- dihydroxy -4,5- diamino anthryl quinone into 2,3- dihydrogen -1,4,5,8- tetrahydroxy -9,10- anthryl diketone.
TW81106131A 1992-08-03 1992-08-03 Method of making 2,3- dihydrogen-1,4,5,8- tetrahydroxy -9,10 anthryl diketone TW227553B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
TW81106131A TW227553B (en) 1992-08-03 1992-08-03 Method of making 2,3- dihydrogen-1,4,5,8- tetrahydroxy -9,10 anthryl diketone

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
TW81106131A TW227553B (en) 1992-08-03 1992-08-03 Method of making 2,3- dihydrogen-1,4,5,8- tetrahydroxy -9,10 anthryl diketone

Publications (1)

Publication Number Publication Date
TW227553B true TW227553B (en) 1994-08-01

Family

ID=51348426

Family Applications (1)

Application Number Title Priority Date Filing Date
TW81106131A TW227553B (en) 1992-08-03 1992-08-03 Method of making 2,3- dihydrogen-1,4,5,8- tetrahydroxy -9,10 anthryl diketone

Country Status (1)

Country Link
TW (1) TW227553B (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101118901B (en) * 2007-06-29 2010-06-09 日月光半导体制造股份有限公司 Stack type chip packaging structure and manufacture process
US8110928B2 (en) 2007-10-05 2012-02-07 Advanced Semiconductor Engineering, Inc. Stacked-type chip package structure and method of fabricating the same

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101118901B (en) * 2007-06-29 2010-06-09 日月光半导体制造股份有限公司 Stack type chip packaging structure and manufacture process
US8110928B2 (en) 2007-10-05 2012-02-07 Advanced Semiconductor Engineering, Inc. Stacked-type chip package structure and method of fabricating the same

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Legal Events

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MM4A Annulment or lapse of patent due to non-payment of fees