TW202426713A - Device, method and control system for crystal growth - Google Patents

Device, method and control system for crystal growth Download PDF

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TW202426713A
TW202426713A TW112143844A TW112143844A TW202426713A TW 202426713 A TW202426713 A TW 202426713A TW 112143844 A TW112143844 A TW 112143844A TW 112143844 A TW112143844 A TW 112143844A TW 202426713 A TW202426713 A TW 202426713A
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Taiwan
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crystal
water
heat shield
cooled heat
crystal growth
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TW112143844A
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Chinese (zh)
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毛志飛
沈偉民
魏星
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大陸商上海新昇半導體科技有限公司
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Publication of TW202426713A publication Critical patent/TW202426713A/en

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Abstract

This application provides a device, a method and a control system for crystal growth. The device for crystal growth comprises: a furnace body; a crucible located in the furnace body for carry a silicon melt; a pulling device on the top of the furnace body for pulling the crystal from the silicon melt; a water-cooling heat shield surrounding the crystal and having an absorption surface for absorbing thermal radiation from the crystal surface, wherein the water-cooling heat shield is used to decrease temperature of local area of the crystal surface and increase vertical temperature gradient of the crystal; a thermal insulator located between the crystal and the water-cooling heat shield for shielding the water-cooling heat shield to reduce the area of the absorption surface; lifting devices respectively connecting to and adjusting the water-cooling heat shield and the thermal insulator to make the exposed absorption surface match with the local area of the crystal surface. The device for crystal growth is able to finely regulate vertical temperature gradient of the crystal.

Description

一種晶體生長裝置、方法和控制系統A crystal growth device, method and control system

本發明關於晶體生長領域,具體而言關於一種晶體生長裝置、方法和控制系統。The present invention relates to the field of crystal growth, and more particularly to a crystal growth device, method and control system.

目前,製備大尺寸單晶矽的方法主要為提拉法(Czochralski method),即在坩堝中將多晶矽熔融,將籽晶浸漬於矽熔體的液面內,緩慢地提拉籽晶,由此育成具有與籽晶相同的結晶方向的矽單晶。在製備大尺寸矽單晶過程中,半導體矽晶體的點缺陷與晶體的溫度變化有很大關係,通過改變晶棒在某一溫度段的時間,可以減少晶棒內部點缺陷的形成。根據Vornkov晶體生長理論,晶體內部的缺陷類型和V/G值相關。V為晶體的提拉速度(mm/min),G為晶體固液界面的垂直溫度梯度(K/mm)。在工業化生產中,為了提升產量,在保證晶棒品質情況下,希望採用盡可能高的拉速,而更高的拉速需要更大的溫度梯度。At present, the main method for preparing large-sized single-crystal silicon is the Czochralski method, which is to melt polycrystalline silicon in a crucible, immerse the seed crystal in the liquid surface of the silicon melt, and slowly pull the seed crystal to grow a silicon single crystal with the same crystallization direction as the seed crystal. In the process of preparing large-sized silicon single crystals, the point defects of semiconductor silicon crystals are closely related to the temperature change of the crystal. By changing the time that the crystal rod is in a certain temperature range, the formation of point defects inside the crystal rod can be reduced. According to Vornkov's crystal growth theory, the defect type inside the crystal is related to the V/G value. V is the pulling speed of the crystal (mm/min), and G is the vertical temperature gradient of the solid-liquid interface of the crystal (K/mm). In industrial production, in order to increase output and ensure the quality of the crystal rod, it is hoped to adopt the highest possible pulling speed, and a higher pulling speed requires a larger temperature gradient.

半導體矽晶體生長過程中為了獲得更佳的晶棒冷卻溫度梯度,通常會在熱場裡設置一個水冷熱屏。水冷熱屏由內層熱屏環、外層熱屏環、中層冷卻水通道、一個進水通道、一個出水通道組成。水冷熱屏裡有冷卻水流動,可以帶走大量的熱量,受到冷卻的部位能快速降溫,晶棒受到冷卻區域會有較大的冷卻溫度梯度,增加晶體在該區域的冷卻速度,抑制缺陷的形核與長大。然而,現有水冷熱屏的尺寸固定,能夠冷卻的區域的大小也固定,因此,在晶體生長過程中水冷熱屏可調節溫度梯度的範圍有限,無法靈活調節水冷熱屏帶走的熱量。現有的水冷熱屏及晶體生長裝置不能精細和靈活地調節晶棒的溫度梯度以滿足製備高階矽片的需求。In order to obtain a better cooling temperature gradient for the crystal rod during the growth of semiconductor silicon crystals, a water-cooled heat shield is usually set up in the hot field. The water-cooled heat shield consists of an inner heat shield ring, an outer heat shield ring, a middle cooling water channel, a water inlet channel, and a water outlet channel. Cooling water flows in the water-cooled heat shield, which can take away a large amount of heat. The cooled part can be cooled quickly, and the cooled area of the crystal rod will have a larger cooling temperature gradient, which increases the cooling rate of the crystal in this area and inhibits the nucleation and growth of defects. However, the size of the existing water-cooled heat shield is fixed, and the size of the area that can be cooled is also fixed. Therefore, the range of the temperature gradient that can be adjusted by the water-cooled heat shield during the crystal growth process is limited, and the heat taken away by the water-cooled heat shield cannot be flexibly adjusted. Existing water-cooled heat shields and crystal growth devices cannot precisely and flexibly adjust the temperature gradient of the crystal ingot to meet the requirements for manufacturing high-end silicon wafers.

因此,有必要提出一種晶體生長裝置、方法和控制系統,以至少部分地解決上述問題。Therefore, it is necessary to provide a crystal growth device, method and control system to at least partially solve the above problems.

在發明內容部分中引入了一系列簡化形式的概念,這將在具體實施方式部分中進一步詳細說明。本發明的發明內容部分並不意味著要試圖限定出所要求保護的技術方案的關鍵特徵和必要技術特徵,更不意味著試圖確定所要求保護的技術方案的保護範圍。A series of simplified concepts are introduced in the invention content section, which will be further described in detail in the specific implementation method section. The invention content section of the present invention does not mean to attempt to limit the key features and essential technical features of the technical solution claimed for protection, nor does it mean to attempt to determine the scope of protection of the technical solution claimed for protection.

針對相關技術的不足,本發明提供一種晶體生長裝置包括:爐體;坩堝,設置於所述爐體的內部,用以容納矽熔體;提拉裝置,設置於所述爐體的頂部,用以從所述矽熔體內提拉出晶體;水冷熱屏,圍繞所述晶體四周設置並具有用於吸收所述晶體的熱輻射的吸收表面,所述水冷熱屏用於降低所述晶體的局部區域的溫度並增大所述晶體的縱向溫度梯度;隔熱筒,設置於所述晶體與所述水冷熱屏之間,所述隔熱筒用於遮擋所述水冷熱屏以減小所述吸收表面的面積;升降裝置,設置於所述爐體的頂部並分別連接於所述水冷熱屏和所述隔熱筒,所述升降裝置用於分別調節所述水冷熱屏和所述隔熱筒的高度以及所述水冷熱屏與所述隔熱筒之間的高度差,以使所述吸收表面的位置和面積大小與所述晶體的所述局部區域相對應。In view of the shortcomings of the related art, the present invention provides a crystal growth device comprising: a furnace; a crucible, arranged inside the furnace, for accommodating a silicon melt; a pulling device, arranged at the top of the furnace, for pulling a crystal out of the silicon melt; a water-cooled heat shield, arranged around the crystal and having an absorbing surface for absorbing the thermal radiation of the crystal, the water-cooled heat shield is used to reduce the temperature of a local area of the crystal and increase the longitudinal temperature gradient of the crystal; a heat insulation cylinder, The heat-insulating cylinder is arranged between the crystal and the water-cooled heat shield, and is used to shield the water-cooled heat shield to reduce the area of the absorption surface; the lifting device is arranged at the top of the furnace body and is respectively connected to the water-cooled heat shield and the heat-insulating cylinder, and the lifting device is used to respectively adjust the height of the water-cooled heat shield and the heat-insulating cylinder and the height difference between the water-cooled heat shield and the heat-insulating cylinder, so that the position and area size of the absorption surface correspond to the local area of the crystal.

示例地,當所述高度差增加時,所述吸收表面的面積增加,所述水冷熱屏吸收的晶體的熱輻射增加;當所述高度差減小時,所述吸收表面的面積減小,所述水冷熱屏吸收的晶體的熱輻射減少。For example, when the height difference increases, the area of the absorption surface increases, and the thermal radiation of the crystal absorbed by the water-cooled heat shield increases; when the height difference decreases, the area of the absorption surface decreases, and the thermal radiation of the crystal absorbed by the water-cooled heat shield decreases.

示例地,所述隔熱筒可以完全遮擋所述水冷熱屏,也可以完全不遮擋所述水冷熱屏。For example, the heat-insulating cylinder may completely shield the water-cooled heat shield, or may not completely shield the water-cooled heat shield.

示例地,所述隔熱筒包括內層、外層和設置在所述內層和所述外層之間的中間層。For example, the heat-insulating cylinder includes an inner layer, an outer layer, and a middle layer disposed between the inner layer and the outer layer.

示例地,所述內層和所述外層的材料設置為石墨材料。For example, the material of the inner layer and the outer layer is set to be graphite material.

示例地,所述中間層的材料包括碳素纖維氈。Illustratively, the material of the middle layer includes carbon fiber felt.

一種晶體生長方法,包括:獲取晶體的當前縱向溫度梯度;計算所述晶體的所述當前縱向溫度梯度與預設縱向溫度梯度的偏差;基於縱向溫度梯度的所述偏差,確定需要降溫的所述晶體的局部區域的位置;基於經確定的需要降溫的所述晶體的所述局部區域的位置,調整水冷熱屏和隔熱筒的高度以及所述水冷熱屏與所述隔熱筒之間的高度差,以使所述水冷熱屏的冷卻表面的位置和面積大小與所述晶體的所述局部區域對應。A crystal growth method comprises: obtaining a current longitudinal temperature gradient of a crystal; calculating a deviation between the current longitudinal temperature gradient of the crystal and a preset longitudinal temperature gradient; determining the position of a local area of the crystal that needs to be cooled based on the deviation of the longitudinal temperature gradient; and adjusting the height of a water-cooled heat shield and an insulation tube and the height difference between the water-cooled heat shield and the insulation tube based on the determined position of the local area of the crystal that needs to be cooled, so that the position and area size of the cooling surface of the water-cooled heat shield correspond to the local area of the crystal.

一種晶體生長控制系統,包括處理器、存儲器以及存儲在所述存儲器上且在所述處理器上運行的計算機程序,所述處理器執行所述計算機程序時,實現如上述的晶體生長方法。A crystal growth control system includes a processor, a memory, and a computer program stored in the memory and running on the processor. When the processor executes the computer program, the crystal growth method as described above is implemented.

本發明提供的晶體生長裝置、方法和控制系統,通過調整隔熱筒和水冷熱屏相對位置,以及調節水冷熱屏吸收晶體熱輻射的吸收面積,以與晶體需要降溫的局部區域的位置和大小對應,進而在較大範圍調節水冷熱屏帶走熱量,從而調整晶體的縱向溫度梯度。本發明提供的晶體生長裝置、方法和控制系統能夠根據生產製程來以抑制晶體缺陷形核和長大,熱歷史活動空間大,使水冷熱屏能夠更精細、靈活地發揮作用。The crystal growth device, method and control system provided by the present invention adjust the relative position of the heat insulation cylinder and the water-cooled heat shield, and adjust the absorption area of the water-cooled heat shield to absorb the thermal radiation of the crystal, so as to correspond to the position and size of the local area of the crystal that needs to be cooled, thereby adjusting the heat taken away by the water-cooled heat shield in a larger range, thereby adjusting the longitudinal temperature gradient of the crystal. The crystal growth device, method and control system provided by the present invention can suppress the nucleation and growth of crystal defects according to the production process, and the thermal history activity space is large, so that the water-cooled heat shield can play a more precise and flexible role.

在下文的描述中,給出了大量具體的細節以便提供對本發明更為徹底的理解。然而,對於本領域技術人員而言顯而易見的是,本發明可以無需一個或多個這些細節而得以實施。在其他的例子中,為了避免與本發明發生混淆,對於本領域習知的一些技術特徵未進行描述。In the following description, a large number of specific details are given in order to provide a more thorough understanding of the present invention. However, it is obvious to those skilled in the art that the present invention can be implemented without one or more of these details. In other examples, some technical features known in the art are not described in order to avoid confusion with the present invention.

應當理解的是,本發明能夠以不同形式實施,而不應當解釋為局限於這裡提出的實施例。相反地,提供這些實施例將使公開徹底和完全,並且將本發明的範圍完全地傳遞給本領域技術人員。在附圖中,為了清楚,層和區的尺寸以及相對尺寸可能被誇大。自始至終相同附圖標記表示相同的元件。It should be understood that the present invention can be implemented in different forms and should not be construed as limited to the embodiments set forth herein. Rather, these embodiments are provided so that the disclosure will be thorough and complete and will fully convey the scope of the present invention to those skilled in the art. In the accompanying drawings, the sizes and relative sizes of layers and regions may be exaggerated for clarity. The same figure numbers throughout represent the same elements.

應當明白,當元件或層被稱為“在...上”、“與...相鄰”、“連接到”或“耦合到”其它元件或層時,其可以直接地在其它元件或層上、與之相鄰、連接或耦合到其它元件或層,或者可以存在居間的元件或層。相反,當元件被稱為“直接在...上”、“與...直接相鄰”、“直接連接到”或“直接耦合到”其它元件或層時,則不存在居間的元件或層。應當明白,儘管可使用術語第一、第二、第三等描述各種元件、部件、區、層和/或部分,這些元件、部件、區、層和/或部分不應當被這些術語限制。這些術語僅僅用來區分一個元件、部件、區、層或部分與另一個元件、部件、區、層或部分。因此,在不悖離本發明教導之下,下面討論的第一元件、部件、區、層或部分可表示為第二元件、部件、區、層或部分。It should be understood that when an element or layer is referred to as being "on," "adjacent to," "connected to," or "coupled to" another element or layer, it may be directly on, adjacent to, connected to, or coupled to the other element or layer, or there may be intervening elements or layers. Conversely, when an element is referred to as being "directly on," "directly adjacent to," "directly connected to," or "directly coupled to" another element or layer, there are no intervening elements or layers. It should be understood that although the terms first, second, third, etc. may be used to describe various elements, components, regions, layers, and/or portions, these elements, components, regions, layers, and/or portions should not be limited by these terms. These terms are only used to distinguish one element, component, region, layer, or portion from another element, component, region, layer, or portion. Thus, a first element, component, region, layer or section discussed below could be termed a second element, component, region, layer or section without departing from the teachings of the present invention.

空間關係術語例如“在...下”、“在...下面”、“下面的”、“在...之下”、“在...之上”、“上面的”等,在這裡可為了方便描述而被使用從而描述圖中所示的一個元件或特徵與其它元件或特徵的關係。應當明白,除了圖中所示的取向以外,空間關係術語意圖還包括使用和操作中的裝置的不同取向。例如,如果附圖中的裝置翻轉,然後,描述為“在其它元件下面”或“在其之下”或“在其下”元件或特徵將取向為在其它元件或特徵“上”。因此,示例性術語“在...下面”和“在...下”可包括上和下兩個取向。裝置可以另外地取向(旋轉90度或其它取向)並且在此使用的空間描述語相應地被解釋。Spatially related terms such as "under", "below", "below", "under", "above", "above", etc., may be used here for convenience of description to describe the relationship between an element or feature shown in the figure and other elements or features. It should be understood that in addition to the orientation shown in the figure, the spatial relationship terms are intended to include different orientations of the device in use and operation. For example, if the device in the accompanying drawings is turned over, then the elements or features described as "under other elements" or "under it" or "under it" will be oriented as "on" other elements or features. Therefore, the exemplary terms "under" and "under" can include both upper and lower orientations. The device can be oriented otherwise (rotated 90 degrees or other orientations) and the spatial descriptors used herein are interpreted accordingly.

在此使用的術語的目的僅在於描述具體實施例並且不作為本發明的限制。在此使用時,單數形式的“一”、“一個”和“所述/該”也意圖包括複數形式,除非上下文清楚指出另外的方式。還應明白術語“組成”和/或“包括”,當在該說明書中使用時,確定所述特徵、整數、步驟、操作、元件和/或部件的存在,但不排除一個或更多其它的特徵、整數、步驟、操作、元件、部件和/或組的存在或添加。在此使用時,術語“和/或”包括相關所列項目的任何及所有組合。The purpose of the terms used herein is only to describe specific embodiments and is not intended to be limiting of the present invention. When used herein, the singular forms "a", "an", and "said/the" are also intended to include the plural forms, unless the context clearly indicates otherwise. It should also be understood that the terms "consisting of" and/or "comprising", when used in this specification, determine the presence of the features, integers, steps, operations, elements and/or parts, but do not exclude the presence or addition of one or more other features, integers, steps, operations, elements, parts and/or groups. When used herein, the term "and/or" includes any and all combinations of the relevant listed items.

這裡參考作為本發明的理想實施例(和中間結構)的示意圖的橫截面圖來描述發明的實施例。這樣,可以預期由於例如製造技術和/或容差導致的從所示形狀的變化。因此,本發明的實施例不應當侷限於在此所示的區的特定形狀,而是包括由於例如製造導致的形狀偏差。例如,顯示為矩形的注入區在其邊緣通常具有圓的或彎曲特徵和/或注入濃度梯度,而不是從注入區到非注入區的二元改變。同樣,通過注入形成的埋藏區可導致該埋藏區和注入進行時所經過的表面之間的區中的一些注入。因此,圖中顯示的區實質上是示意性的,它們的形狀並不意圖顯示裝置的區的實際形狀且並不意圖限定本發明的範圍。Embodiments of the invention are described herein with reference to cross-sectional views which are schematic diagrams of idealized embodiments (and intermediate structures) of the invention. As such, variations from the shapes shown due to, for example, manufacturing techniques and/or tolerances are to be expected. Accordingly, embodiments of the invention should not be limited to the particular shapes of the regions shown herein, but rather include deviations in shape due to, for example, manufacturing. For example, an implanted region shown as a rectangle typically has rounded or curved features and/or an implant concentration gradient at its edges rather than a binary change from an implanted region to a non-implanted region. Similarly, a buried region formed by implantation may result in some implantation in the region between the buried region and the surface through which the implantation is performed. Accordingly, the regions shown in the figures are schematic in nature, and their shapes are not intended to illustrate the actual shape of the regions of the device and are not intended to limit the scope of the invention.

為了徹底理解本發明,將在下列的描述中提出詳細的結構,以便闡釋本發明提出的技術方案。本發明的較佳實施例詳細描述如下,然而除了這些詳細描述外,本發明還可以具有其他實施方式。In order to thoroughly understand the present invention, a detailed structure will be proposed in the following description to explain the technical solution proposed by the present invention. The preferred embodiments of the present invention are described in detail below, but in addition to these detailed descriptions, the present invention can also have other implementation methods.

目前,製備大尺寸單晶矽的方法主要為提拉法,即在坩堝中將多晶矽熔融為矽熔體,將籽晶浸漬於矽熔體的液面內,緩慢地提拉籽晶,由此育成具有與籽晶相同的結晶方向的矽單晶。At present, the main method for preparing large-size single crystal silicon is the pulling method, that is, melting polycrystalline silicon into silicon melt in a crucible, immersing a seed crystal in the liquid surface of the silicon melt, and slowly pulling the seed crystal to grow a silicon single crystal with the same crystallization direction as the seed crystal.

根據相關研究,半導體矽晶體的點缺陷與晶體的溫度變化有很大關係,通過改變晶棒在某一溫度段的時間,可以減少晶棒內部點缺陷的形成。在工業化生產中,為了提升產量,在保證品質情況下,希望採用盡可能大的拉速,根據Vornkov晶體生長理論,晶體內部的缺陷類型和V/G值相關,其中,V為晶體的提拉速度(mm/min),G為晶體固液界面的垂直溫度梯度(K/mm),更高的拉速需要更大的溫度梯度。因此如何合理的增大晶棒的溫度梯度一直是重要研究課題。According to relevant research, the point defects of semiconductor silicon crystals are closely related to the temperature change of the crystal. By changing the time that the crystal rod is in a certain temperature range, the formation of point defects inside the crystal rod can be reduced. In industrial production, in order to increase production, while ensuring quality, it is hoped to use the largest possible pulling speed. According to Vornkov's crystal growth theory, the defect type inside the crystal is related to the V/G value, where V is the pulling speed of the crystal (mm/min) and G is the vertical temperature gradient of the solid-liquid interface of the crystal (K/mm). A higher pulling speed requires a larger temperature gradient. Therefore, how to reasonably increase the temperature gradient of the crystal rod has always been an important research topic.

半導體矽晶體生長過程中為了獲得更優的晶棒冷卻溫度梯度,通常會在熱場裡設置一個水冷熱屏。如圖1所示,在晶體生長裝置100的熱場裡,導流筒130設置在熱場的正上方以用於保溫,並防止大量熱量流失,同時為了保證晶體能有較佳的溫度梯度,加快冷卻速度,在導流筒內部環繞晶體四周設置了一個水冷熱屏170,水冷熱屏170可以帶走晶棒的大量熱量。該水冷熱屏由內層熱屏環、外層熱屏環、中層冷卻水通道、一個進水通道、一個出水通道組成。水冷熱屏裡有冷卻水流動,可以帶走大量的熱量,晶棒受到冷卻區域會有較大的冷卻溫度梯度,受到冷卻的部位能快速降溫,從而增大熱場上部的溫度梯度,增加晶體在該區域的冷卻速度,抑制缺陷的形成與長大。In order to obtain a better crystal rod cooling temperature gradient during the growth process of semiconductor silicon crystals, a water-cooled heat shield is usually set in the hot field. As shown in FIG1 , in the hot field of the crystal growth device 100, the guide tube 130 is set directly above the hot field for heat preservation and to prevent a large amount of heat loss. At the same time, in order to ensure that the crystal can have a better temperature gradient and speed up the cooling speed, a water-cooled heat shield 170 is set around the crystal inside the guide tube. The water-cooled heat shield 170 can take away a large amount of heat from the crystal rod. The water-cooled heat shield consists of an inner heat shield ring, an outer heat shield ring, a middle cooling water channel, a water inlet channel, and a water outlet channel. There is cooling water flowing in the water-cooled heat screen, which can take away a large amount of heat. The cooled area of the crystal rod will have a large cooling temperature gradient. The cooled part can cool down quickly, thereby increasing the temperature gradient in the upper part of the heat field, increasing the cooling rate of the crystal in this area, and inhibiting the formation and growth of defects.

在相關技術中,生長出來的單晶矽在水冷熱屏的冷卻下可以獲得一定的溫度梯度,但是無法連續地調節水冷熱屏吸收的熱量。水冷熱屏裡冷卻水直接帶走大量由晶棒表面熱輻射過來的熱量。整個水冷熱屏內表面都在吸收熱量,水冷熱屏由升降裝置帶動升降,由於晶棒距離液面越近溫度越高,經過升降後不同高度位置的水冷熱屏因晶棒表面溫度不同接收到的熱量不同,這樣只能比較粗糙的調節水冷熱屏帶走熱量。因此,上述水冷熱屏及晶體生長裝置不能滿足製備高階矽片的需求。In the related technology, the grown single crystal silicon can obtain a certain temperature gradient under the cooling of the water-cooled heat screen, but the heat absorbed by the water-cooled heat screen cannot be continuously adjusted. The cooling water in the water-cooled heat screen directly takes away a large amount of heat radiated from the surface of the crystal rod. The entire inner surface of the water-cooled heat screen is absorbing heat. The water-cooled heat screen is driven up and down by the lifting device. Since the closer the crystal rod is to the liquid surface, the higher the temperature, the water-cooled heat screens at different heights after lifting receive different amounts of heat due to the different surface temperatures of the crystal rod. In this way, the heat taken away by the water-cooled heat screen can only be roughly adjusted. Therefore, the above-mentioned water-cooled heat screen and crystal growth device cannot meet the needs of preparing high-end silicon wafers.

本發明從傳熱上考慮在晶棒和水冷熱屏之間設置一個隔熱筒,通過隔熱筒調節晶棒表面的對應位置的散熱,以符合預設溫度梯度,這樣能在在提高拉速的情況下抑制缺陷的形成與長大,從而保證晶棒品質。The present invention considers heat transfer by arranging a heat-insulating tube between the crystal rod and the water-cooled heat shield, and adjusts the heat dissipation of the corresponding position on the surface of the crystal rod through the heat-insulating tube to meet the preset temperature gradient. In this way, the formation and growth of defects can be suppressed when the pulling speed is increased, thereby ensuring the quality of the crystal rod.

為了更精細調整晶棒溫度梯度。在水冷熱屏和晶棒之間設置一個可以升降的隔熱筒。隔熱筒在晶棒和水冷熱屏之間,可以隔絕晶棒至少部分表面直接對水冷熱屏的熱輻射。水冷熱屏受到隔熱筒遮擋後,直接接收晶棒的熱輻射會直接減少,能帶走的熱量也會減少。通過調節隔熱筒的位置,來調節水冷熱屏吸收晶棒熱輻射的吸收表面的面積的大小,以連續地調節水冷熱屏帶走的熱量,從而在晶棒上形成可控的溫度梯度。在大矽片參數要求越來越高的條件下,需要更精細調整晶棒溫度梯度,因此設計一種可調節的水冷熱屏的吸收表面的面積大小的結構就非常必要。In order to more precisely adjust the temperature gradient of the crystal rod, a heat-insulating cylinder that can be raised and lowered is set between the water-cooled heat shield and the crystal rod. The heat-insulating cylinder is between the crystal rod and the water-cooled heat shield, and can isolate at least part of the surface of the crystal rod from direct thermal radiation to the water-cooled heat shield. After the water-cooled heat shield is shielded by the heat-insulating cylinder, the thermal radiation directly received by the crystal rod will be directly reduced, and the amount of heat that can be taken away will also be reduced. By adjusting the position of the heat-insulating cylinder, the size of the absorption surface area of the water-cooled heat shield that absorbs the thermal radiation of the crystal rod is adjusted to continuously adjust the amount of heat taken away by the water-cooled heat shield, thereby forming a controllable temperature gradient on the crystal rod. Under the condition that the parameter requirements of large silicon wafers are getting higher and higher, it is necessary to adjust the temperature gradient of the crystal rod more precisely. Therefore, it is very necessary to design a structure with an adjustable area size of the absorption surface of the water-cooled heat shield.

下面將參照圖2,對本發明一實施例的晶體生長裝置做詳細描述。其中,圖2為根據本發明一實施例的晶體生長裝置的結構示意圖。The crystal growth device according to an embodiment of the present invention will be described in detail below with reference to Fig. 2. Fig. 2 is a schematic structural diagram of the crystal growth device according to an embodiment of the present invention.

如圖2所示,本發明所提供的晶體生長裝置200為用於採用提拉法生長矽單晶的晶體生長裝置200。晶體生長裝置200包括爐體201;坩堝210,設置於爐體201的內部,用以容納矽熔體203;提拉裝置250,設置於爐體201的頂部,用以從矽熔體203內提拉出晶體202;水冷熱屏270,圍繞晶體202四周設置並具有用於吸收晶體202的熱輻射的吸收表面,水冷熱屏270用於降低晶體202的局部區域的溫度並增大晶體202的縱向溫度梯度;隔熱筒211,設置於晶體202與水冷熱屏270之間,隔熱筒211用於遮擋水冷熱屏270以減小所述吸收表面的面積,其中水冷熱屏270的表面包括被隔離筒遮擋的部分和未遮擋的部分,其中未遮擋的部分為水冷熱屏170的吸收表面;升降裝置280,設置於爐體201的頂部並分別連接於水冷熱屏270和隔熱筒211,升降裝置280用於分別調節水冷熱屏270的高度和隔熱筒211的高度以及水冷熱屏270與隔熱筒211之間的高度差,以使所述吸收表面的位置和面積大小與晶體202的所述局部區域對應。參考圖2,當所述高度差增加時,所述吸收表面的面積增加,水冷熱屏270吸收的晶體202熱輻射增加;當所述高度差減小時,所述吸收表面的面積減小,水冷熱屏270吸收的晶體202的熱輻射減少。As shown in FIG. 2 , the crystal growth device 200 provided by the present invention is a crystal growth device 200 for growing silicon single crystals using the Czochralski method. The crystal growth device 200 includes a furnace 201; a crucible 210, which is arranged inside the furnace 201 and is used to accommodate a silicon melt 203; a pulling device 250, which is arranged at the top of the furnace 201 and is used to pull a crystal 202 out of the silicon melt 203; a water-cooled heat shield 270, which is arranged around the crystal 202 and has an absorbing surface for absorbing the thermal radiation of the crystal 202, and the water-cooled heat shield 270 is used to reduce the temperature of a local area of the crystal 202 and increase the longitudinal temperature gradient of the crystal 202; an insulating cylinder 211, which is arranged between the crystal 202 and the water-cooled heat shield 270, and the insulating cylinder 211 is used to shield the crystal 202 from the heat radiation of the crystal 202. A water-cooled heat shield 270 is provided to reduce the area of the absorption surface, wherein the surface of the water-cooled heat shield 270 includes a portion blocked by the isolation tube and an unblocked portion, wherein the unblocked portion is the absorption surface of the water-cooled heat shield 170; a lifting device 280 is arranged at the top of the furnace body 201 and is respectively connected to the water-cooled heat shield 270 and the insulation tube 211, and the lifting device 280 is used to respectively adjust the height of the water-cooled heat shield 270 and the height of the insulation tube 211 as well as the height difference between the water-cooled heat shield 270 and the insulation tube 211, so that the position and area size of the absorption surface correspond to the local area of the crystal 202. 2 , when the height difference increases, the area of the absorption surface increases, and the thermal radiation of the crystal 202 absorbed by the water-cooled heat shield 270 increases; when the height difference decreases, the area of the absorption surface decreases, and the thermal radiation of the crystal 202 absorbed by the water-cooled heat shield 270 decreases.

在一個實施例中,坩堝用於容納多晶矽原料,該多晶矽原料用於生長單晶矽,坩堝包括石英坩堝和石墨坩堝,多晶矽原料位於石英坩堝中,石英坩堝位於石墨坩堝中。In one embodiment, a crucible is used to contain polycrystalline silicon raw materials, and the polycrystalline silicon raw materials are used to grow single crystal silicon. The crucible includes a quartz crucible and a graphite crucible. The polycrystalline silicon raw materials are located in the quartz crucible, and the quartz crucible is located in the graphite crucible.

繼續參考圖2,加熱器220可以為石墨加熱器,其位於爐體201內,用於加熱坩堝210,從而使坩堝210內的多晶矽原料變成熔體203,並保持熔融的狀態,其中,加熱器220設置在坩堝210的外側。2 , the heater 220 may be a graphite heater, which is located in the furnace body 201 and is used to heat the crucible 210 , so that the polycrystalline silicon raw material in the crucible 210 becomes a melt 203 and maintains the melted state, wherein the heater 220 is disposed on the outer side of the crucible 210 .

繼續參考圖2,導流筒230(也稱為熱屏)位於爐體201內且位於坩堝210中熔體203液面的上方環繞晶體202的生長區域,其通常是由石墨材料製成的倒錐形屏蔽物,用於調節氬氣的流向和流速,使向下吹的氬氣集中到晶體202的生長界面附近,以及阻止高溫的液面和坩堝210對冷卻中的晶體202的熱輻射傳遞,提高晶體202表面對周圍的熱輸出,提高晶體熱傳出速率和晶體的溫度梯度。Continuing with reference to FIG. 2 , the guide tube 230 (also called a heat shield) is located in the furnace body 201 and above the liquid surface of the melt 203 in the crucible 210, surrounding the growth area of the crystal 202. It is usually an inverted cone-shaped shield made of graphite material, which is used to adjust the flow direction and flow rate of the argon gas, so that the downwardly blown argon gas is concentrated near the growth interface of the crystal 202, and to prevent the high-temperature liquid surface and the crucible 210 from transmitting heat radiation to the cooling crystal 202, thereby increasing the heat output from the surface of the crystal 202 to the surrounding area, and increasing the heat transfer rate of the crystal and the temperature gradient of the crystal.

繼續參考圖2,真空泵290與爐體201底部連通,用於不斷地從爐體201由內向外抽氣,保持爐體201內真空度的穩定,且使爐體201內保持負壓。在晶體202生長過程中,採用減壓技術,保持惰性氣體經由導流筒230自上而下地貫穿整個爐體201,及時地由真空泵290抽走由於高溫而產生出來的矽氧化物和雜質揮發物,保持爐體201真空度穩定,減少外界因素對爐體201內真空度的影響,確保晶體202的品質。Continuing to refer to FIG. 2 , the vacuum pump 290 is connected to the bottom of the furnace body 201 and is used to continuously pump gas from the inside to the outside of the furnace body 201 to maintain the stability of the vacuum degree in the furnace body 201 and keep the negative pressure in the furnace body 201. During the growth process of the crystal 202, the decompression technology is adopted to keep the inert gas from top to bottom through the guide tube 230 throughout the entire furnace body 201, and the silicon oxide and impurity volatiles generated by the high temperature are promptly pumped away by the vacuum pump 290 to maintain the stability of the vacuum degree of the furnace body 201, reduce the influence of external factors on the vacuum degree in the furnace body 201, and ensure the quality of the crystal 202.

繼續參考圖2,保溫層240可以為碳氈,其位於爐體201內且位於加熱器220與爐體201之間,用於保持爐內的溫度。Continuing to refer to FIG. 2 , the insulation layer 240 may be carbon felt, which is located inside the furnace body 201 and between the heater 220 and the furnace body 201 to maintain the temperature inside the furnace.

繼續參考圖2,提拉裝置250(也稱為提拉頭)與爐體201固定連接,其可以包括快速電機、慢速電機、旋轉電機、鋼纜、籽晶稱重頭等部件,其用於使籽晶提升及旋轉,且記錄晶體202重量、位移等數據。Continuing with reference to FIG. 2 , the lifting device 250 (also referred to as the lifting head) is fixedly connected to the furnace body 201 , and may include a fast motor, a slow motor, a rotating motor, a steel cable, a seed crystal weighing head and other components, which are used to lift and rotate the seed crystal and record data such as the weight and displacement of the crystal 202 .

繼續參考圖2,坩堝升降單元260與爐體201固定連接,其可以包括滾珠直線導軌、高精度絲杆、提升電機和旋轉電機等部件,用於帶動坩堝210升降及旋轉。Continuing to refer to FIG. 2 , the crucible lifting unit 260 is fixedly connected to the furnace body 201 , and may include components such as a ball linear guide rail, a high-precision screw rod, a lifting motor, and a rotating motor, and is used to drive the crucible 210 to lift and rotate.

在一個實施例中,提拉裝置包括豎直設置的籽晶軸,坩堝升降單元包括豎直設置的坩堝軸,籽晶軸設置在坩堝的上方,坩堝軸設置在坩堝的底部,籽晶軸的底部通過夾具安裝有籽晶,其頂部連接籽晶軸驅動裝置,使其能夠一邊旋轉一邊向上緩慢提拉,出於對單晶的長度和行程的考慮,所述籽晶軸採用鋼絲式鉸鏈製成。坩堝軸的底部設有坩堝軸驅動裝置,使坩堝軸能夠帶動坩堝進行旋轉。In one embodiment, the pulling device includes a vertically arranged seed crystal shaft, and the crucible lifting unit includes a vertically arranged crucible shaft. The seed crystal shaft is arranged above the crucible, and the crucible shaft is arranged at the bottom of the crucible. The seed crystal shaft is mounted with a seed crystal through a clamp at the bottom, and the top of the seed crystal shaft is connected to a seed crystal shaft driving device, so that it can be slowly pulled upward while rotating. Considering the length and stroke of the single crystal, the seed crystal shaft is made of a wire hinge. The bottom of the crucible shaft is provided with a crucible shaft driving device, so that the crucible shaft can drive the crucible to rotate.

在晶體生長裝置200工作時,首次在坩堝210中投放矽料,接著加熱器220通過坩堝210將矽料熔融為矽熔體203。將籽晶浸漬於矽熔體203的液面內,提拉裝置250緩慢地提拉籽晶,由此育成晶體202。隨著提拉裝置250的提拉,晶體202通過水冷熱屏270被隔離筒210未遮擋的部分和遮擋的部分,其中,所述未遮擋的部分(即吸收表面)增大晶體202固液界面附近的冷卻速率,抑制缺陷的形核過程,使得晶體202內的缺陷形核較少;遮擋部分降低晶體202在該部分的冷卻速率,利於使晶體202內部的缺陷保持一定的形體不發生其他變化;使得獲得的晶體缺陷在要求的特徵線寬之下,使得製備的矽片滿足高階芯片製造業的要求。When the crystal growth device 200 is working, silicon material is first put into the crucible 210, and then the heater 220 melts the silicon material into silicon melt 203 through the crucible 210. The seed crystal is immersed in the liquid surface of the silicon melt 203, and the pulling device 250 slowly pulls the seed crystal, thereby growing the crystal 202. As the pulling device 250 is pulled, the crystal 202 is separated from the unshielded portion and the shielded portion of the cylinder 210 by the water-cooled heat shield 270, wherein the unshielded portion (i.e., the absorption surface) increases the cooling rate near the solid-liquid interface of the crystal 202, suppresses the nucleation process of defects, and reduces the nucleation of defects in the crystal 202; the shielded portion reduces the cooling rate of the crystal 202 in this portion, which is beneficial for the defects in the crystal 202 to maintain a certain shape without other changes; the obtained crystal defects are within the required characteristic line width, so that the prepared silicon wafers meet the requirements of the high-end chip manufacturing industry.

在其他實施例中,隔熱筒可以完全遮擋水冷熱屏,也可以完全不遮擋水冷熱屏,具體可根據製程要求進行調節。In other embodiments, the heat-insulating cylinder may completely block the water-cooled heat shield, or may not block the water-cooled heat shield at all, and the specific adjustment may be made according to the process requirements.

在其他實施例中,本領域技術人員可以根據不同的熱場與製程對上述水冷熱屏和隔離筒的尺寸和相對位置進行調整,以增大調節晶體的縱向溫度梯度的調節範圍。In other embodiments, those skilled in the art may adjust the size and relative position of the water-cooled heat shield and the isolation cylinder according to different thermal fields and processes to increase the adjustment range of the longitudinal temperature gradient of the crystal.

在本發明的實施例中,由於在水冷熱屏和晶體之間設置了一個可以升降的隔熱筒,並且隔熱筒設置在晶體和水冷熱屏之間,可以隔絕晶體直接對水冷熱屏的熱輻射。水冷熱屏受到隔熱筒遮擋後,直接接收晶體的熱輻射會直接減少,能帶走的熱量也會減少。因此通過調節隔熱筒的高度,來調節遮擋的部分和未遮擋的部分(即吸收表面)的大小,進而調節了水冷熱屏吸收表面的面積大小,可以直接調節水冷熱屏帶走的熱量,以改變晶體的縱向溫度梯度。In the embodiment of the present invention, a heat-insulating cylinder that can be raised and lowered is provided between the water-cooled heat shield and the crystal, and the heat-insulating cylinder is provided between the crystal and the water-cooled heat shield, so that the heat radiation of the crystal directly to the water-cooled heat shield can be isolated. After the water-cooled heat shield is shielded by the heat-insulating cylinder, the heat radiation directly received by the crystal will be directly reduced, and the amount of heat that can be taken away will also be reduced. Therefore, by adjusting the height of the heat-insulating cylinder, the size of the shielded part and the unshielded part (i.e., the absorption surface) can be adjusted, and then the area size of the absorption surface of the water-cooled heat shield can be adjusted, and the amount of heat taken away by the water-cooled heat shield can be directly adjusted to change the longitudinal temperature gradient of the crystal.

在一個實施例中,隔熱筒由三層結構組成,包括內層、外層和設置在所述內層和所述外層之間的中間層,其中內層和外層由高純石墨材料加工而成,中間層由碳素纖維氈、或其他隔熱的發泡多空材料(例如玻璃纖維、石棉、岩棉和軟氈)加工而成。具有三層結構的該隔熱筒,可以更好的隔絕水冷熱屏和晶體間熱輻射。In one embodiment, the heat-insulating cylinder is composed of a three-layer structure, including an inner layer, an outer layer, and a middle layer disposed between the inner layer and the outer layer, wherein the inner layer and the outer layer are processed from high-purity graphite material, and the middle layer is processed from carbon fiber felt, or other heat-insulating foamed porous materials (such as glass fiber, asbestos, rock wool, and soft felt). The heat-insulating cylinder with a three-layer structure can better isolate the water-cooled heat shield and the thermal radiation between the crystals.

本發明提供的晶體生長裝置、方法和控制系統,通過調整隔熱筒和水冷熱屏相對位置,以及調節水冷熱屏吸收晶體熱輻射的吸收面積,以與晶體需要降溫的局部區域的位置和大小對應,進而在較大範圍調節水冷熱屏帶走熱量,從而調整晶體的縱向溫度梯度。本發明提供的晶體生長裝置、方法和控制系統能夠根據生產製程來以抑制晶體缺陷形核和長大,熱歷史活動空間大,使水冷熱屏能夠更精細、靈活地發揮作用。The crystal growth device, method and control system provided by the present invention adjust the relative position of the heat insulation cylinder and the water-cooled heat shield, and adjust the absorption area of the water-cooled heat shield to absorb the thermal radiation of the crystal, so as to correspond to the position and size of the local area of the crystal that needs to be cooled, thereby adjusting the heat taken away by the water-cooled heat shield in a larger range, thereby adjusting the longitudinal temperature gradient of the crystal. The crystal growth device, method and control system provided by the present invention can suppress the nucleation and growth of crystal defects according to the production process, and the thermal history activity space is large, so that the water-cooled heat shield can play a more precise and flexible role.

參見圖3,本發明還提供了一種晶體生長方法,該方法可以基於如上所述的晶體生長裝置,其包括如下步驟: S1:獲取晶體的當前縱向溫度梯度; S2:計算所述晶體的所述當前縱向溫度梯度與預設縱向溫度梯度的偏差; S3:基於縱向溫度梯度的所述偏差,確定需要降溫的所述晶體的局部區域的位置; S4:基於經確定的需要降溫的所述晶體的所述局部區域的位置,調整水冷熱屏和隔熱筒的高度以及所述水冷熱屏與所述隔熱筒之間的高度差,以使所述水冷熱屏的冷卻表面的位置和面積大小與所述晶體的所述局部區域對應;其中,所述高度差是指隔離筒的下端與水冷熱屏的下端之間的垂直距離。 Referring to FIG. 3 , the present invention also provides a crystal growth method, which can be based on the crystal growth device as described above, and includes the following steps: S1: obtaining the current longitudinal temperature gradient of the crystal; S2: calculating the deviation between the current longitudinal temperature gradient of the crystal and the preset longitudinal temperature gradient; S3: determining the position of the local area of the crystal that needs to be cooled based on the deviation of the longitudinal temperature gradient; S4: based on the determined position of the local area of the crystal that needs to be cooled, adjusting the height of the water-cooled heat shield and the insulation cylinder and the height difference between the water-cooled heat shield and the insulation cylinder, so that the position and area size of the cooling surface of the water-cooled heat shield correspond to the local area of the crystal; wherein the height difference refers to the vertical distance between the lower end of the insulation cylinder and the lower end of the water-cooled heat shield.

圖4顯示根據本發明一實施例的晶體生長控制系統400的結構示意圖。晶體生長控制系統400包括存儲器410和處理器420。FIG4 is a schematic diagram showing the structure of a crystal growth control system 400 according to an embodiment of the present invention. The crystal growth control system 400 includes a memory 410 and a processor 420.

存儲器410存儲用於實現上述實施例的晶體生長方法中的相應步驟的程序代碼。The memory 410 stores program codes for implementing corresponding steps in the crystal growth method of the above-mentioned embodiment.

處理器420用於運行所述存儲器410中存儲的程序代碼,以實現上述實施例的晶體生長方法中的相應步驟。The processor 420 is used to run the program code stored in the memory 410 to implement the corresponding steps in the crystal growth method of the above embodiment.

本發明還提供了一種計算機可讀存儲介質,該存儲介質上存儲有程序指令,該程序指令被計算機或處理器運行時用於執行上述實施例的晶體直徑控制方法的相應步驟。該存儲介質例如可以包括平板電腦的存儲部件、個人電腦的硬碟、唯讀記憶體(ROM,Read Only Memory)、可擦除可規劃式唯讀記憶體(EPROM,Erasable Programmable Read-Only Memory)、唯讀記憶光碟(CD-ROM))、USB存儲器、或者上述存儲介質的任意組合所述計算機可讀存儲介質可以是一個或多個計算機可讀存儲介質的任意組合。The present invention also provides a computer-readable storage medium, on which program instructions are stored, and when the program instructions are run by a computer or a processor, they are used to execute the corresponding steps of the crystal diameter control method of the above embodiment. The storage medium may include, for example, a storage component of a tablet computer, a hard disk of a personal computer, a read-only memory (ROM), an erasable programmable read-only memory (EPROM), a read-only memory compact disc (CD-ROM), a USB memory device, or any combination of the above storage media. The computer-readable storage medium may be any combination of one or more computer-readable storage media.

儘管這裡已經參考附圖描述了示例實施例,應理解上述示例實施例僅僅是示例性的,並且不意圖將本發明的範圍限制於此。本領域普通技術人員可以在其中進行各種改變和修改,而不偏離本發明的範圍和精神。所有這些改變和修改意在被包括在所附請求項所要求的本發明的範圍之內。Although example embodiments have been described herein with reference to the accompanying drawings, it should be understood that the above example embodiments are exemplary only and are not intended to limit the scope of the present invention thereto. Various changes and modifications may be made therein by a person of ordinary skill in the art without departing from the scope and spirit of the present invention. All such changes and modifications are intended to be included within the scope of the present invention as claimed in the appended claims.

本領域普通技術人員可以意識到,結合本文中所公開的實施例描述的各示例的單元及算法步驟,能夠以電子硬件、或者計算機軟件和電子硬件的結合來實現。這些功能究竟以硬件還是軟件方式來執行,取決於技術方案的特定應用和設計約束條件。專業技術人員可以對每個特定的應用來使用不同方法來實現所描述的功能,但是這種實現不應認為超出本發明的範圍。It will be appreciated by those skilled in the art that the units and algorithm steps of the various examples described in the embodiments disclosed herein can be implemented in electronic hardware, or in a combination of computer software and electronic hardware. Whether these functions are implemented in hardware or software depends on the specific application and design constraints of the technical solution. Professional and technical personnel may use different methods to implement the described functions for each specific application, but such implementation should not be considered beyond the scope of the present invention.

在本發明所提供的幾個實施例中,應該理解到,所揭露的設備和方法,可以通過其它的方式實現。例如,以上所描述的設備實施例僅僅是示意性的,例如,所述單元的劃分,僅僅為一種邏輯功能劃分,實際實現時可以有另外的劃分方式,例如多個單元或組件可以結合或者可以集成到另一個設備,或一些特徵可以忽略,或不執行。In the several embodiments provided by the present invention, it should be understood that the disclosed devices and methods can be implemented in other ways. For example, the device embodiments described above are only schematic, for example, the division of the units is only a logical function division, and there may be other division methods in actual implementation, such as multiple units or components can be combined or integrated into another device, or some features can be ignored or not executed.

在此處所提供的說明書中,說明了大量具體細節。然而,能夠理解,本發明的實施例可以在沒有這些具體細節的情況下實踐。在一些實例中,並未詳細示出習知的方法、結構和技術,以便不模糊對本說明書的理解。In the description provided herein, numerous specific details are described. However, it is understood that embodiments of the present invention can be practiced without these specific details. In some instances, well-known methods, structures, and techniques are not shown in detail so as not to obscure the understanding of this description.

類似地,應當理解,為了精簡本發明並幫助理解各個發明方面中的一個或多個,在對本發明的示例性實施例的描述中,本發明的各個特徵有時被一起分組到單個實施例、圖、或者對其的描述中。然而,並不應將該本發明的方法解釋成反映如下意圖:即所要求保護的本發明要求比在每個請求項中所明確記載的特徵更多的特徵。更確切地說,如相應的請求項所反映的那樣,其發明點在於可以用少於某個公開的單個實施例的所有特徵的特徵來解決相應的技術問題。因此,遵循具體實施方式的請求項由此明確地併入該具體實施方式,其中每個請求項本身都作為本發明的單獨實施例。Similarly, it should be understood that in order to simplify the present invention and assist in understanding one or more of the various inventive aspects, in the description of the exemplary embodiments of the present invention, the various features of the present invention are sometimes grouped together into a single embodiment, figure, or description thereof. However, this method of the present invention should not be interpreted as reflecting the following intention: the claimed invention requires more features than those explicitly recited in each claim. More precisely, as reflected in the corresponding claim, the invention lies in that the corresponding technical problem can be solved with fewer features than all the features of a single disclosed embodiment. Therefore, the claims that follow a specific embodiment are hereby expressly incorporated into the specific embodiment, wherein each claim itself serves as a separate embodiment of the present invention.

本領域的技術人員可以理解,除了特徵之間相互排斥之外,可以採用任何組合對本說明書(包括伴隨的請求項、摘要和附圖)中公開的所有特徵以及如此公開的任何方法或者設備的所有過程或單元進行組合。除非另外明確陳述,本說明書(包括伴隨的請求項、摘要和附圖)中公開的每個特徵可以由提供相同、等同或相似目的替代特徵來代替。It will be understood by those skilled in the art that all features disclosed in this specification (including the accompanying claims, abstracts and drawings) and all processes or units of any method or apparatus disclosed in this specification (including the accompanying claims, abstracts and drawings) may be combined in any combination, except where the features are mutually exclusive. Unless expressly stated otherwise, each feature disclosed in this specification (including the accompanying claims, abstracts and drawings) may be replaced by an alternative feature that provides the same, equivalent or similar purpose.

此外,本領域的技術人員能夠理解,儘管在此所述的一些實施例包括其它實施例中所包括的某些特徵而不是其它特徵,但是不同實施例的特徵的組合意味著處於本發明的範圍之內並且形成不同的實施例。例如,在請求項書中,所要求保護的實施例的任意之一都可以以任意的組合方式來使用。In addition, those skilled in the art will appreciate that, although some embodiments described herein include certain features included in other embodiments but not other features, the combination of features of different embodiments is meant to be within the scope of the present invention and form different embodiments. For example, in the claims, any one of the claimed embodiments may be used in any combination.

應該注意的是上述實施例對本發明進行說明而不是對本發明進行限制,並且本領域技術人員在不悖離所附請求項的範圍的情況下可設計出替換實施例。在請求項中,不應將位於括號之間的任何參考符號構造成對請求項的限制。本發明可以借助於包括有若干不同元件的硬件以及借助於適當編程的計算機來實現。在列舉了若干裝置的單元請求項中,這些裝置中的若干個可以是通過同一個硬件項來具體體現。單詞第一、第二、以及第三等的使用不表示任何順序。可將這些單詞解釋為名稱。It should be noted that the above-described embodiments illustrate rather than limit the present invention, and that those skilled in the art may devise alternative embodiments without departing from the scope of the appended claims. In the claims, any reference symbols between parentheses should not be construed as limiting the claims. The present invention may be implemented with the aid of hardware comprising a number of different elements and with the aid of a suitably programmed computer. In a unit claim enumerating a number of devices, several of these devices may be embodied by the same item of hardware. The use of the words first, second, and third, etc., does not indicate any order. These words may be interpreted as names.

100:晶體生長裝置 130:導流筒 170:水冷熱屏 200:晶體生長裝置 201:爐體 202:晶體 203:熔體 210:坩堝 220:加熱器 230:導流筒 240:保溫層 250:提拉裝置 260:坩堝升降單元 270:水冷熱屏 280:升降裝置 290:真空泵 211:隔熱筒 S1、S2、S3、S4:步驟 400:晶體生長控制系統 410:存儲器 420:處理器 100: Crystal growth device 130: Flow guide tube 170: Water-cooled heat shield 200: Crystal growth device 201: Furnace 202: Crystal 203: Melt 210: Crucible 220: Heater 230: Flow guide tube 240: Insulation layer 250: Lifting device 260: Crucible lifting unit 270: Water-cooled heat shield 280: Lifting device 290: Vacuum pump 211: Insulation tube S1, S2, S3, S4: Steps 400: Crystal growth control system 410: Memory 420: Processor

圖1為一種晶體生長裝置的示意圖。FIG1 is a schematic diagram of a crystal growth apparatus.

圖2為本發明一實施例所提供的晶體生長裝置的示意圖。FIG. 2 is a schematic diagram of a crystal growth device provided in an embodiment of the present invention.

圖3為本發明一實施例所提供的晶體生長方法的流程圖。FIG3 is a flow chart of a crystal growth method provided in an embodiment of the present invention.

圖4為本發明一實施例所提供的晶體生長控制系統的示意圖。FIG4 is a schematic diagram of a crystal growth control system provided by an embodiment of the present invention.

200:晶體生長裝置 200: Crystal growth device

201:爐體 201: Furnace body

202:晶體 202: Crystal

203:熔體 203: Melt

210:坩堝 210: Crucible

220:加熱器 220: Heater

230:導流筒 230: Guide tube

240:保溫層 240: Insulation layer

250:提拉裝置 250: Lifting device

260:坩堝升降單元 260: Crucible lifting unit

270:水冷熱屏 270: Water-cooled heat shield

280:升降裝置 280: Lifting device

290:真空泵 290: Vacuum pump

211:隔熱筒 211: Insulation tube

Claims (8)

一種晶體生長裝置,包括: 爐體; 坩堝,設置於所述爐體的內部,用以容納矽熔體; 提拉裝置,設置於所述爐體的頂部,用以從所述矽熔體內提拉出晶體; 水冷熱屏,圍繞所述晶體四周設置並具有用於吸收所述晶體的熱輻射的吸收表面,所述水冷熱屏用於降低所述晶體的局部區域的溫度並增大所述晶體的縱向溫度梯度; 隔熱筒,設置於所述晶體與所述水冷熱屏之間,所述隔熱筒用於遮擋所述水冷熱屏以減小所述吸收表面的面積; 升降裝置,設置於所述爐體的頂部並分別連接於所述水冷熱屏和所述隔熱筒,所述升降裝置用於分別調節所述水冷熱屏的高度和所述隔熱筒的高度以及所述水冷熱屏與所述隔熱筒之間的高度差,以使所述吸收表面的位置和面積大小與所述晶體的所述局部區域相對應。 A crystal growth device, comprising: a furnace; a crucible, arranged inside the furnace, for containing silicon melt; a pulling device, arranged at the top of the furnace, for pulling out the crystal from the silicon melt; a water-cooled heat shield, arranged around the crystal and having an absorbing surface for absorbing the thermal radiation of the crystal, the water-cooled heat shield being used to reduce the temperature of the local area of the crystal and increase the longitudinal temperature gradient of the crystal; an insulating cylinder, arranged between the crystal and the water-cooled heat shield, the insulating cylinder being used to shield the water-cooled heat shield to reduce the area of the absorbing surface; A lifting device is arranged at the top of the furnace body and is respectively connected to the water-cooled heat shield and the insulation tube. The lifting device is used to respectively adjust the height of the water-cooled heat shield and the insulation tube and the height difference between the water-cooled heat shield and the insulation tube, so that the position and area size of the absorption surface correspond to the local area of the crystal. 如請求項1所述的晶體生長裝置,其中, 當所述高度差增加時,所述吸收表面的面積增加,所述水冷熱屏吸收的晶體的熱輻射增加; 當所述高度差減小時,所述吸收表面的面積減小,所述水冷熱屏吸收的晶體的熱輻射減少。 The crystal growth device as described in claim 1, wherein, when the height difference increases, the area of the absorption surface increases, and the thermal radiation of the crystal absorbed by the water-cooled heat shield increases; when the height difference decreases, the area of the absorption surface decreases, and the thermal radiation of the crystal absorbed by the water-cooled heat shield decreases. 如請求項1所述的晶體生長裝置,其中,所述隔熱筒可以完全遮擋所述水冷熱屏,也可以完全不遮擋所述水冷熱屏。A crystal growth device as described in claim 1, wherein the thermal insulation tube may completely cover the water-cooled heat shield or may not completely cover the water-cooled heat shield. 如請求項1所述的晶體生長裝置,其中,所述隔熱筒包括內層、外層和設置在所述內層和所述外層之間的中間層。A crystal growth device as described in claim 1, wherein the thermal insulation tube includes an inner layer, an outer layer, and a middle layer arranged between the inner layer and the outer layer. 如請求項4所述的晶體生長裝置,其中,所述內層和所述外層的材料設置為石墨材料。A crystal growth device as described in claim 4, wherein the material of the inner layer and the outer layer is set to graphite material. 如請求項4所述的晶體生長裝置,其中,所述中間層的材料包括碳素纖維氈。A crystal growth device as described in claim 4, wherein the material of the middle layer includes carbon fiber felt. 一種晶體生長方法,包括: 獲取晶體的當前縱向溫度梯度; 計算所述晶體的所述當前縱向溫度梯度與預設縱向溫度梯度的偏差; 基於縱向溫度梯度的所述偏差,確定需要降溫的所述晶體的局部區域的位置; 基於經確定的需要降溫的所述晶體的所述局部區域的位置,調整水冷熱屏和隔熱筒的高度以及所述水冷熱屏與所述隔熱筒之間的高度差,以使所述水冷熱屏的冷卻表面的位置和面積大小與所述晶體的所述局部區域相對應。 A crystal growth method, comprising: Obtaining the current longitudinal temperature gradient of the crystal; Calculating the deviation between the current longitudinal temperature gradient of the crystal and the preset longitudinal temperature gradient; Determining the position of the local area of the crystal that needs to be cooled based on the deviation of the longitudinal temperature gradient; Based on the determined position of the local area of the crystal that needs to be cooled, adjusting the height of the water-cooled heat shield and the insulation tube and the height difference between the water-cooled heat shield and the insulation tube, so that the position and area size of the cooling surface of the water-cooled heat shield correspond to the local area of the crystal. 一種晶體生長控制系統,包括處理器、存儲器以及存儲在所述存儲器上且在所述處理器上運行的計算機程序,其特徵在於,所述處理器執行所述計算機程序時,實現如請求項7所述的晶體生長方法。A crystal growth control system includes a processor, a memory, and a computer program stored in the memory and running on the processor, wherein when the processor executes the computer program, the crystal growth method as described in claim 7 is implemented.
TW112143844A 2022-12-30 2023-11-14 Device, method and control system for crystal growth TW202426713A (en)

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