TW202225434A - Sputtering target-backing plate assembly, production method therefor, and sputtering target recovery method - Google Patents
Sputtering target-backing plate assembly, production method therefor, and sputtering target recovery method Download PDFInfo
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K20/00—Non-electric welding by applying impact or other pressure, with or without the application of heat, e.g. cladding or plating
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
- C23C14/22—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
- C23C14/34—Sputtering
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- G—PHYSICS
- G11—INFORMATION STORAGE
- G11B—INFORMATION STORAGE BASED ON RELATIVE MOVEMENT BETWEEN RECORD CARRIER AND TRANSDUCER
- G11B5/00—Recording by magnetisation or demagnetisation of a record carrier; Reproducing by magnetic means; Record carriers therefor
- G11B5/84—Processes or apparatus specially adapted for manufacturing record carriers
- G11B5/851—Coating a support with a magnetic layer by sputtering
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Abstract
Description
本發明係關於一種用於設置在濺鍍裝置之較佳之濺鍍靶材-背板接合體、其製造方法及濺鍍靶材之回收方法,上述濺鍍裝置用於HDD(Hard Disk Drive,硬碟)、半導體等之製造步驟中。The present invention relates to a preferred sputtering target-backplate assembly for setting in a sputtering device, a method for producing the same, and a method for recovering the sputtering target. The above-mentioned sputtering device is used for HDD (Hard Disk Drive, hard disk drive) disk), semiconductors, etc. manufacturing steps.
為了將濺鍍靶材設置於HDD、半導體等之製造步驟中所使用之濺鍍裝置,一般使用將濺鍍靶材接合於被稱為背板之構件而成之濺鍍靶材-背板接合體。於濺鍍靶材-背板接合體中,藉由將背板固定,而介隔背板將濺鍍靶材設置於濺鍍裝置。In order to install a sputtering target in a sputtering apparatus used in the manufacturing steps of HDDs, semiconductors, etc., a sputtering target-backing bonding in which a sputtering target is joined to a member called a backing plate is generally used body. In the sputtering target material-backing plate joint body, by fixing the backing plate, the sputtering target material is installed in the sputtering apparatus through the backing plate.
背板係支持濺鍍靶材之構件,又,係用以抑制因暴露於電漿而導致之濺鍍靶材之溫度上升之負責冷卻之構件,故而由銅系材料、鋁系材料等熱傳導較高之材料形成。又,濺鍍靶材與背板必須維持密接性以實現熱傳導。The back plate is a member that supports the sputtering target, and is a member responsible for cooling to suppress the temperature rise of the sputtering target caused by exposure to plasma. Made of high material. In addition, the sputtering target and the backing plate must maintain adhesion to achieve thermal conduction.
關於濺鍍靶材與背板之接合,通常實施以下方法:使用銦或錫等低熔點且真空下之蒸氣壓較低之材料作為嵌入材的被稱為鍵合(bonding)之接合方法、或者使用具有導電性之樹脂來接合之方法。For the bonding of the sputtering target and the backing plate, the following methods are usually implemented: a bonding method called bonding using a material with a low melting point such as indium or tin and a low vapor pressure under vacuum as an embedded material, or A method of bonding using conductive resin.
但是,若濺鍍靶材之溫度升高至用作嵌入材之銦或錫等之熔點以上,則存在銦或錫因揮發而以雜質之形式混入所形成之膜中之情況,於要求高純度之用途中,成為致命性問題。However, if the temperature of the sputtering target material is raised above the melting point of indium or tin used as the embedded material, indium or tin may be mixed into the formed film as impurities due to volatilization, and high purity is required. It has become a fatal problem in its use.
為了解決鍵合之問題,有不使用低熔點金屬作為嵌入材而對濺鍍靶材與背板施加相對之壓力,並於升高溫度後之狀態下花費時間進行擴散接合之技術(例如,參照專利文獻1~3)。In order to solve the problem of bonding, there is a technique of applying relative pressure to the sputtering target and the backing plate without using a low-melting-point metal as an embedded material, and spending time in a state where the temperature is raised to perform diffusion bonding (for example, refer to
於專利文獻1中,揭示有相對於容許應力15~20 kgf/mm
2之包含鉭之濺鍍靶材,背板採用其容許應力與濺鍍靶材之容許應力相同或較其高之材料,製成由濺鍍靶材與背板擴散接合而成之組件,藉此,控制因熱膨脹與收縮而產生之濺鍍靶材之翹曲之方向。
In
於專利文獻2中,揭示有藉由對熔點為1000℃以上之靶材、選自熔點較該靶材之熔點低之金屬或合金中之1種以上之嵌入材、及背板進行固相擴散接合,而獲得接合率為100%之較高之密接性及較高之接合強度。In
於專利文獻3中,揭示有藉由如下操作製作總成之方法,即,於製成嵌埋濺鍍靶材之整個面之夾層構造之後,藉由熱等靜壓(HIP)或單軸熱壓(UHP)於400~600℃實施加熱壓縮使其擴散接合,其後,對濺鍍靶材及背板進行切削。
[先前技術文獻]
[專利文獻]
In
[專利文獻1]日本專利特開2015-183258號公報 [專利文獻2]日本專利特開平06-108246號公報 [專利文獻3]日本專利特表2014-511436號公報 [Patent Document 1] Japanese Patent Laid-Open No. 2015-183258 [Patent Document 2] Japanese Patent Laid-Open No. 06-108246 [Patent Document 3] Japanese Patent Publication No. 2014-511436
[發明所欲解決之問題][Problems to be Solved by Invention]
但是,如專利文獻1記載之發明,於濺鍍靶材係由撓曲強度較低之材料形成之情形時,若濺鍍靶材與背板之線膨脹係數差大為不同,則存在高溫下擴散接合之後進行冷卻並熱收縮時,濺鍍靶材發生破損之情況。因此,有時亦於低溫下進行擴散接合,但要麼擴散接合無法進行,要麼無法獲得充分之強度。However, as in the invention described in
又,即便藉由加熱與加壓對線膨脹係數差大為不同之濺鍍靶材與背板僅進行擴散接合,於使用濺鍍靶材時,若溫度反覆上升下降,則亦存在接合界面越來越疲勞而破裂、剝離之情況。In addition, even if the sputtering target and the backing plate with greatly different linear expansion coefficients are only diffusion-bonded by heating and pressing, when the sputtering target is used, if the temperature rises and falls repeatedly, the bonding interface may deteriorate. The condition of cracking and peeling due to fatigue.
又,於專利文獻2記載之發明中,在使用濺鍍靶材時,若溫度上升至嵌入材之熔點,則亦存在嵌入材發生熔融導致濺鍍靶材剝離之情況。此種傾向容易於使用大型靶材、要求高純度之半導體製造中出現。Moreover, in the invention described in
又,為了減小線膨脹係數之差,亦有放入線膨脹係數為濺鍍靶材與背板之中間值左右之嵌入材等緩解應力之方法,但與藉由鍵合進行金屬接合時或使用導電性樹脂進行接合時同樣,會發生嵌入材揮發,無法解決雜質混入之問題。In addition, in order to reduce the difference in the coefficient of linear expansion, there is also a method to relieve stress, such as inserting a material whose linear expansion coefficient is about the middle value of the sputtering target material and the backing plate, etc., but when metal bonding is performed by bonding or Similarly, when using conductive resin for bonding, volatilization of the insert material occurs, and the problem of contamination of impurities cannot be solved.
又,於專利文獻3記載之發明中,對濺鍍靶材與背板進行處理直至形成牢固之擴散接合,因此,濺鍍靶材與背板之線膨脹係數之差較大,且根據濺鍍靶材之材質,有可能於濺鍍靶材之擴散接合步驟中發生濺鍍靶材之破裂。Furthermore, in the invention described in
因此,本發明之目的在於提供一種濺鍍靶材-背板接合體、其製造方法及濺鍍靶材之回收方法,該濺鍍靶材-背板接合體即便於使用撓曲強度較低之濺鍍靶材之情形時或者濺鍍靶材與背板之線膨脹係數差大為不同之情形時,亦能抑制濺鍍靶材之破損及剝離,又,能夠抑制因雜質之揮發造成之污染,進而,既能抑制用作靶材之高價材料之損耗,又能容易地進行靶材之剝離回收。 [解決問題之技術手段] Therefore, an object of the present invention is to provide a sputtering target-backplate assembly, a method for manufacturing the same, and a method for recovering a sputtering target, which even when using a sputtering target-backplate assembly with a low flexural strength In the case of sputtering targets or when the difference between the linear expansion coefficients of the sputtering target and the backing plate is greatly different, damage and peeling of the sputtering target can be suppressed, and contamination caused by volatilization of impurities can be suppressed. Furthermore, the loss of the expensive material used as the target can be suppressed, and the target can be easily peeled and recovered. [Technical means to solve problems]
本發明者等人專心研究,結果發現藉由製成如下構造,能夠解決上述課題,從而完成本發明,即,於背板設置鉤狀部或鉤支承部中任一者,於濺鍍靶材之外周側面設置鉤狀部或鉤支承部中另一者,使鉤狀部抵接於鉤支承部而將濺鍍靶材固定於背板之構造。即,本發明之濺鍍靶材-背板接合體係將濺鍍靶材接合於背板而成者,其特徵在於:上述背板具有板表面、板背面、及板側面,上述濺鍍靶材具有靶材表面、與上述板表面相對之靶材背面、及外周側面,上述背板及上述濺鍍靶材中任一者進而具有鉤狀部,另一者進而具有鉤支承部,該鉤狀部與該鉤支承部相互抵接,上述濺鍍靶材之鉤狀部或鉤支承部設置於上述濺鍍靶材之外周側面,且藉由使上述鉤狀部抵接於上述鉤支承部,而將上述濺鍍靶材固定於上述背板。As a result of intensive research, the inventors of the present invention have found that the above-mentioned problems can be solved by having a structure in which either a hook-shaped portion or a hook support portion is provided on the back plate, and the sputtering target The other of the hook-shaped part or the hook support part is provided on the outer peripheral side surface, and the hook-shaped part is abutted on the hook support part, and the sputtering target is fixed to the backing plate. That is, the sputtering target-back plate bonding system of the present invention is formed by bonding a sputtering target to a backing plate, wherein the backing plate has a plate surface, a plate back surface, and a plate side surface, and the sputtering target material is characterized in that It has a target surface, a target back surface opposite to the plate surface, and an outer peripheral side surface, either one of the back plate and the sputtering target further has a hook-shaped portion, and the other one further has a hook support portion, and the hook-shaped The hook-shaped part or the hook-supporting part of the sputtering target is provided on the outer peripheral side surface of the sputtering target, and by making the hook-shaped part abut against the hook-supporting part, And the said sputtering target is fixed to the said backplate.
於本發明之濺鍍靶材-背板接合體中,較佳為上述背板於上述板表面具有凸部,該凸部具有上述鉤狀部或上述鉤支承部。除了能提高濺鍍靶材之側面方向上之濺鍍靶材與背板之接合強度以外,於濺鍍靶材之厚度方向上亦能提高濺鍍靶材與背板之接合強度,其結果為,能夠保持濺鍍靶材使用時之接合強度,將熱傳導保持良好。In the sputtering target material-back plate assembly of the present invention, it is preferable that the back plate has a convex portion on the plate surface, and the convex portion has the hook-shaped portion or the hook support portion. In addition to improving the bonding strength of the sputtering target and the backing plate in the lateral direction of the sputtering target, the bonding strength of the sputtering target and the backing plate can also be improved in the thickness direction of the sputtering target. The result is: , can maintain the bonding strength of the sputtering target during use, and maintain good thermal conductivity.
於本發明之濺鍍靶材-背板接合體中,較佳為上述背板於上述板表面或上述板側面具有卡子,該卡子具有上述鉤狀部或上述鉤支承部。除了能提高濺鍍靶材之側面方向上之濺鍍靶材與背板之接合強度以外,於濺鍍靶材之厚度方向上亦能提高濺鍍靶材與背板之接合強度,其結果為,能夠保持濺鍍靶材使用時之接合強度,將熱傳導保持良好。In the sputtering target material-back plate assembly of the present invention, it is preferable that the back plate has a clip on the plate surface or the plate side surface, and the clip has the hook portion or the hook support portion. In addition to improving the bonding strength of the sputtering target and the backing plate in the lateral direction of the sputtering target, the bonding strength of the sputtering target and the backing plate can also be improved in the thickness direction of the sputtering target. The result is: , can maintain the bonding strength of the sputtering target during use, and maintain good thermal conductivity.
於本發明之濺鍍靶材-背板接合體中,較佳為上述卡子留下側面之一部分而進入上述外周側面,上述卡子固定於上述背板。除了能提高濺鍍靶材之側面方向上之濺鍍靶材與背板之接合強度以外,於濺鍍靶材之厚度方向上亦能提高濺鍍靶材與背板之接合強度,其結果為,能夠保持濺鍍靶材使用時之接合強度,將熱傳導保持良好。In the sputtering target-back plate assembly of the present invention, it is preferable that the clip leaves a part of the side surface and enters the outer peripheral side surface, and the clip is fixed to the back plate. In addition to improving the bonding strength of the sputtering target and the backing plate in the lateral direction of the sputtering target, the bonding strength of the sputtering target and the backing plate can also be improved in the thickness direction of the sputtering target. The result is: , can maintain the bonding strength of the sputtering target during use, and maintain good thermal conductivity.
於本發明之濺鍍靶材-背板接合體中,較佳為上述卡子之側面自上述外周側面突出,至少上述卡子之突出部分固定於上述背板。即便在將卡子固定於上述濺鍍靶材之外周側面之後,亦能將卡子固定於上述背板。In the sputtering target-back plate assembly of the present invention, it is preferable that the side surface of the clip protrudes from the outer peripheral side surface, and at least the protruding portion of the clip is fixed to the back plate. Even after the clip is fixed to the outer peripheral side surface of the sputtering target, the clip can be fixed to the back plate.
於本發明之濺鍍靶材-背板接合體中,較佳為上述背板於上述板表面具有凹部,上述背板於上述凹部具有卡子,該卡子具有上述鉤狀部或上述鉤支承部,上述濺鍍靶材之至少一部分與上述卡子之至少一部分嵌入至上述凹部,上述卡子固定於上述背板之凹部。能夠相對於背板之板表面調整卡子之位置,並且將卡子固定於背板。In the sputtering target material-back plate assembly of the present invention, it is preferable that the back plate has a concave portion on the surface of the plate, the back plate has a clip in the concave portion, and the clip has the hook-shaped portion or the hook support portion, At least a part of the sputtering target and at least a part of the clip are fitted into the concave part, and the clip is fixed to the concave part of the back plate. The position of the clip can be adjusted relative to the board surface of the backboard, and the clip can be fixed to the backboard.
於本發明之濺鍍靶材-背板接合體中,較佳為上述背板於上述板表面具有凹部,上述背板於上述凹部之內周側面具有上述鉤狀部或上述鉤支承部,上述濺鍍靶材之一部分嵌入至上述凹部。除了能提高濺鍍靶材之側面方向上之濺鍍靶材與背板之接合強度以外,於濺鍍靶材之厚度方向上亦能提高濺鍍靶材與背板之接合強度,其結果為,能夠保持濺鍍靶材使用時之接合強度,將熱傳導保持良好。In the sputtering target material-backing plate assembly of the present invention, it is preferable that the backing plate has a concave portion on the surface of the plate, the backing plate has the hook-shaped portion or the hook supporting portion on the inner peripheral side of the concave portion, and the A part of the sputtering target is embedded in the above-mentioned concave portion. In addition to improving the bonding strength of the sputtering target and the backing plate in the lateral direction of the sputtering target, the bonding strength of the sputtering target and the backing plate can also be improved in the thickness direction of the sputtering target. The result is: , can maintain the bonding strength of the sputtering target during use, and maintain good thermal conductivity.
於本發明之濺鍍靶材-背板接合體中,較佳為上述鉤狀部具有第1凹凸形狀部,上述鉤支承部具有與上述第1凹凸形狀部相應之第2凹凸形狀部。除了能提高濺鍍靶材之側面方向上之濺鍍靶材與背板之接合強度以外,於濺鍍靶材之厚度方向上亦能提高濺鍍靶材與背板之接合強度,其結果為,能夠保持濺鍍靶材使用時之接合強度,將熱傳導保持良好。In the sputtering target-back plate assembly of the present invention, it is preferable that the hook portion has a first concavo-convex portion, and the hook support portion has a second concavo-convex portion corresponding to the first concavo-convex portion. In addition to improving the bonding strength of the sputtering target and the backing plate in the lateral direction of the sputtering target, the bonding strength of the sputtering target and the backing plate can also be improved in the thickness direction of the sputtering target. The result is: , can maintain the bonding strength of the sputtering target during use, and maintain good thermal conductivity.
於本發明之濺鍍靶材-背板接合體中,較佳為上述鉤狀部具有自上述背板至上述濺鍍表面之方向上之鉤前端成為最大鉤掛位置之鉤形,上述鉤支承部具有與上述鉤形相應之鉤孔。除了能提高濺鍍靶材之側面方向上之濺鍍靶材與背板之接合強度以外,於濺鍍靶材之厚度方向上亦能提高濺鍍靶材與背板之接合強度,其結果為,能夠保持濺鍍靶材使用時之接合強度,將熱傳導保持良好。In the sputtering target material-back plate assembly of the present invention, it is preferable that the hook-shaped portion has a hook shape such that the front end of the hook in the direction from the back plate to the sputtering surface becomes a maximum hook position, and the hook supports The portion has a hook hole corresponding to the above hook shape. In addition to improving the bonding strength of the sputtering target and the backing plate in the lateral direction of the sputtering target, the bonding strength of the sputtering target and the backing plate can also be improved in the thickness direction of the sputtering target. The result is: , can maintain the bonding strength of the sputtering target during use, and maintain good thermal conductivity.
於本發明之濺鍍靶材-背板接合體中,較佳為於上述濺鍍靶材與上述背板之界面具有2.5 mm以下之中間層,該中間層包括包含Ni、Cr、Al、Cu中至少任一種金屬或含有Ni、Cr、Al、Cu中至少任一種之合金之板材、粉末、或該板材與該粉末之組合。藉由設置中間層,能夠提高濺鍍靶材之靶材背面與背板之板表面或凹部底面之接合強度,並且提高密接性,將熱傳導保持良好。又,由於中間層由背板與濺鍍靶材覆蓋,故而能夠抑制中間層之材質揮發成為雜質而附著於基板。。In the sputtering target-backplate assembly of the present invention, it is preferable to have an intermediate layer of 2.5 mm or less at the interface between the sputtering target and the backplate, and the intermediate layer includes Ni, Cr, Al, Cu A sheet, powder, or a combination of the sheet and the powder of at least any metal or an alloy containing at least any one of Ni, Cr, Al, and Cu. By providing the intermediate layer, the bonding strength between the back surface of the sputtering target and the plate surface of the back plate or the bottom surface of the concave portion can be improved, the adhesion can be improved, and the heat conduction can be kept good. In addition, since the intermediate layer is covered with the back plate and the sputtering target, it is possible to prevent the material of the intermediate layer from volatilizing into impurities and adhering to the substrate. .
於本發明之濺鍍靶材-背板接合體中,較佳為於上述濺鍍靶材與上述背板之界面具有10 μm以下之中間層,該中間層係包含Ni、Cr、Al、Cu中至少任一種金屬或含有Ni、Cr、Al、Cu中至少任一種之合金之薄膜。藉由設置中間層,能夠提高濺鍍靶材之靶材背面與背板之板表面或凹部底面之接合強度,並且提高密接性,將熱傳導保持良好。又,由於中間層由背板與濺鍍靶材覆蓋,故而能夠抑制中間層之材質揮發成為雜質而附著於基板。。In the sputtering target-backplate assembly of the present invention, it is preferable to have an intermediate layer of 10 μm or less at the interface between the sputtering target and the backplate, and the intermediate layer contains Ni, Cr, Al, Cu A thin film of at least any metal or an alloy containing at least any one of Ni, Cr, Al, and Cu. By providing the intermediate layer, the bonding strength between the back surface of the sputtering target and the plate surface of the back plate or the bottom surface of the concave portion can be improved, the adhesion can be improved, and the heat conduction can be kept good. In addition, since the intermediate layer is covered with the back plate and the sputtering target, it is possible to prevent the material of the intermediate layer from volatilizing into impurities and adhering to the substrate. .
於本發明之濺鍍靶材-背板接合體中,較佳為於上述濺鍍靶材與上述背板之界面具有1.0 mm以下之中間層,該中間層包括包含In、Zn中至少任一種金屬或含有In、Zn中至少任一種之合金之板材、粉末、或該板材與該粉末之組合。藉由設置中間層,能夠提高濺鍍靶材之靶材背面與背板之板表面或凹部底面之接合強度,並且提高密接性,將熱傳導保持良好。又,由於中間層由背板與濺鍍靶材覆蓋,故而能夠抑制中間層之材質揮發成為雜質而附著於基板。。In the sputtering target-backplate assembly of the present invention, it is preferable to have an intermediate layer of 1.0 mm or less at the interface between the sputtering target and the backplate, and the intermediate layer includes at least any one of In and Zn. A sheet, powder, or a combination of the sheet and the powder of a metal or an alloy containing at least one of In, Zn. By providing the intermediate layer, the bonding strength between the back surface of the sputtering target and the plate surface of the back plate or the bottom surface of the concave portion can be improved, the adhesion can be improved, and the heat conduction can be kept good. In addition, since the intermediate layer is covered with the back plate and the sputtering target, it is possible to prevent the material of the intermediate layer from volatilizing into impurities and adhering to the substrate. .
於本發明之濺鍍靶材-背板接合體中,較佳為於上述濺鍍靶材與上述背板之界面具有2層以上之中間層,該中間層包括:2.5 mm以下之板材、粉末、或該板材與該粉末之組合,其包含Ni、Cr、Al、Cu中至少任一種金屬或含有Ni、Cr、Al、Cu中至少任一種之合金;10 μm以下之薄膜,其包含Ni、Cr、Al、Cu中至少任一種金屬或含有Ni、Cr、Al、Cu中至少任一種之合金;或者1.0 mm以下之板材、粉末、或該板材與該粉末之組合,其包含In、Zn中至少任一種金屬或含有In、Zn中至少任一種之合金。藉由設置2層中間層,能夠提高濺鍍靶材之靶材背面與背板之板表面或凹部底面之接合強度,並且提高密接性,將熱傳導保持良好。又,由於中間層由背板與濺鍍靶材覆蓋,故而能夠抑制中間層之材質揮發成為雜質而附著於基板。。In the sputtering target material-back plate assembly of the present invention, it is preferable to have at least two intermediate layers at the interface between the sputtering target material and the back plate, and the intermediate layers include: a plate with a thickness of 2.5 mm or less, powder , or the combination of the plate and the powder, which contains at least any metal of Ni, Cr, Al, and Cu or an alloy containing at least any of Ni, Cr, Al, and Cu; the thin film below 10 μm, which contains Ni, Cr, Al, and Cu. At least any one of Cr, Al, Cu or an alloy containing at least any one of Ni, Cr, Al, Cu; or a sheet, powder, or a combination of the sheet and the powder below 1.0 mm, which contains In, Zn At least any metal or an alloy containing at least any one of In and Zn. By providing two intermediate layers, the bonding strength between the back surface of the target of the sputtering target and the plate surface of the backing plate or the bottom surface of the recess can be improved, and the adhesion can be improved to maintain good thermal conductivity. In addition, since the intermediate layer is covered with the back plate and the sputtering target, it is possible to prevent the material of the intermediate layer from volatilizing into impurities and adhering to the substrate. .
於本發明之濺鍍靶材-背板接合體中,較佳為上述濺鍍靶材之材質為Al-Sc合金、Ru、Ru合金、Ir或Ir合金。即便為1000℃以上之高熔點材料亦能抑制濺鍍靶材之翹曲或破裂,並且提高濺鍍靶材與背板之接合強度。In the sputtering target-back plate assembly of the present invention, preferably, the material of the sputtering target is Al-Sc alloy, Ru, Ru alloy, Ir or Ir alloy. Even with a high melting point material of 1000°C or higher, warpage or cracking of the sputtering target can be suppressed, and the bonding strength between the sputtering target and the backing plate can be improved.
於本發明之濺鍍靶材-背板接合體中,較佳為上述濺鍍靶材之材質為Li系氧化物、Co系氧化物、Ti系氧化物或Mg系氧化物。即便為1000℃以上之高熔點材料亦能抑制濺鍍靶材之翹曲或破裂,並且提高濺鍍靶材與背板之接合強度。In the sputtering target-back plate assembly of the present invention, it is preferable that the material of the sputtering target is Li-based oxide, Co-based oxide, Ti-based oxide or Mg-based oxide. Even with a high melting point material of 1000°C or higher, warpage or cracking of the sputtering target can be suppressed, and the bonding strength between the sputtering target and the backing plate can be improved.
於本發明之濺鍍靶材-背板接合體中,較佳為上述背板之材質為Al、Al合金、Cu、Cu合金、Fe或Fe合金,上述背板之線膨脹係數為30.0×10 -6/℃以下。藉由使用背板之熱傳導性良好者,加熱時背板膨脹,能夠將濺鍍靶材插入於背板之凸部或凹部之內周側面,並且藉由冷卻時背板收縮,使背板之凸部或凹部之內周側面與濺鍍靶材之外周側面抵接,能夠形成接合體。 In the sputtering target material-back plate assembly of the present invention, preferably, the material of the back plate is Al, Al alloy, Cu, Cu alloy, Fe or Fe alloy, and the linear expansion coefficient of the back plate is 30.0×10 -6 /℃ or less. By using a backing plate with good thermal conductivity, the backing plate expands when heated, and the sputtering target can be inserted into the inner peripheral side of the convex or concave portion of the backing plate, and the backing plate shrinks when cooling, so that the The inner peripheral side surface of the convex portion or the concave portion is in contact with the outer peripheral side surface of the sputtering target to form a joined body.
本發明之濺鍍靶材-背板接合體之製造方法之特徵在於包括:步驟1,其係準備具有板表面、板背面、板側面、及鉤狀部或鉤支承部中任一者之背板、以及具有靶材表面、靶材背面、外周側面、及設置於該外周側面之上述鉤狀部或上述鉤支承部中另一者之濺鍍靶材;步驟2,其係加熱上述背板使其熱膨脹;步驟3,其係以上述板表面與上述靶材背面相對之方式,且以上述鉤支承部與上述鉤狀部相對之方式配置上述濺鍍靶材與上述背板;及步驟4,其係藉由將上述濺鍍靶材與上述背板冷卻使上述鉤狀部抵接於上述鉤支承部,而將上述濺鍍靶材固定於上述背板。藉由利用熱膨脹及熱收縮使鉤狀部與鉤支承部抵接,能容易地製造濺鍍靶材-背板接合體。The manufacturing method of the sputtering target material-back plate joint body of the present invention is characterized by comprising:
於本發明之濺鍍靶材-背板接合體之製造方法中,較佳為於藉由將上述濺鍍靶材與上述背板冷卻使上述鉤狀部抵接於上述鉤支承部,而將上述濺鍍靶材固定於上述背板之步驟4之後,將自上述濺鍍靶材之上述靶材表面對上述背板之按壓或者上述濺鍍靶材及上述背板之加熱與自上述濺鍍靶材之上述靶材表面對上述背板之按壓這一步驟、以及上述濺鍍靶材與上述背板之冷卻步驟作為1組而進行1次或重複進行2次以上。能夠抑制濺鍍靶材之翹曲,並且進一步提高濺鍍靶材之靶材背面與背板之板表面或凹部底面之接合強度,能夠提高密接性,效率良好地進行熱傳導。In the manufacturing method of the sputtering target material-backing plate joint body of this invention, it is preferable to cool the said sputtering target material and the said backing plate so that the said hook-shaped part abuts on the said hook support part, and is After the
本發明之濺鍍靶材-背板接合體之特徵在於包括:步驟1,其係準備具有板表面、板背面、及板側面之背板、具有鉤狀部或鉤支承部中任一者之卡子、以及具有靶材表面、靶材背面、外周側面、及該外周側面上之上述鉤狀部或上述鉤支承部中另一者之濺鍍靶材;步驟2,其係以上述板表面與上述靶材背面相對之方式配置上述濺鍍靶材與上述背板;步驟3,其係將上述卡子配置於上述板表面或上述板側面,且以上述鉤支承部與上述鉤狀部相對之方式配置上述濺鍍靶材與上述卡子;及步驟4,其係以該步驟3之配置狀態將上述卡子固定於上述背板。藉由將鉤狀部或鉤支承部設置於卡子,能容易地使鉤狀部與鉤支承部抵接,從而能容易地製造濺鍍靶材-背板接合體。The sputtering target material-backing plate joint body of the present invention is characterized by comprising:
於本發明之濺鍍靶材-背板接合體之製造方法中,較佳為於以上述步驟3之配置狀態將上述卡子固定於上述背板之步驟4之後,將自上述濺鍍靶材之上述靶材表面對上述背板之按壓或者上述濺鍍靶材及上述背板之加熱與自上述濺鍍靶材之上述靶材表面對上述背板之按壓這一步驟、以及上述濺鍍靶材與上述背板之冷卻步驟作為1組而進行1次或重複進行2次以上。能夠抑制濺鍍靶材之翹曲,並且進一步提高濺鍍靶材之靶材背面與背板之板表面或凹部底面之接合強度,能夠提高密接性,效率良好地進行熱傳導。In the manufacturing method of the sputtering target material-back plate assembly of the present invention, preferably after the
本發明之濺鍍靶材之回收方法之特徵在於包括:步驟A,其係加熱本發明之濺鍍靶材-背板接合體,使其熱膨脹直至上述鉤狀部離開上述鉤支承部;及步驟B,其係自上述背板卸除上述濺鍍靶材,自上述濺鍍靶材-背板接合體回收上述濺鍍靶材。The sputtering target recovery method of the present invention is characterized by comprising: step A, which is to heat the sputtering target-back plate assembly of the present invention to thermally expand it until the hook-shaped portion leaves the hook support portion; and step A B, it removes the said sputtering target material from the said backplate, and collects the said sputtering target material from the said sputtering target material-backplate assembly.
本發明之濺鍍靶材之回收方法之特徵在於:其係自利用卡子將濺鍍靶材固定於背板之濺鍍靶材-背板接合體回收上述濺鍍靶材之方法,且該回收方法包括自上述背板卸除上述卡子,自上述濺鍍靶材-背板接合體回收上述濺鍍靶材之步驟C。 [發明之效果] The sputtering target recovery method of the present invention is characterized in that it is a method for recovering the above-mentioned sputtering target material from a sputtering target material-backplane assembly in which the sputtering target material is fixed to the backing plate by means of a clip, and the recovery The method includes the step C of removing the clip from the backplane, and recovering the sputtering target from the sputtering target-backplane assembly. [Effect of invention]
本發明可提供一種濺鍍靶材-背板接合體、其製造方法及濺鍍靶材之回收方法,該濺鍍靶材-背板接合體即便於使用撓曲強度較低之濺鍍靶材之情形時或者濺鍍靶材與背板之線膨脹係數差大為不同之情形時,亦能抑制濺鍍靶材之破損及剝離,又,能夠抑制因雜質之揮發造成之污染,進而,既能抑制用作靶材之高價材料之損耗,又能容易地進行靶材之剝離回收。The present invention can provide a sputtering target material-back plate assembly, a method for manufacturing the same, and a method for recovering a sputtering target material. The sputtering target material-back plate assembly can be used even when a sputtering target with low flexural strength is used. In such cases or when the difference in the coefficient of linear expansion between the sputtering target and the backing plate is greatly different, the damage and peeling of the sputtering target can be suppressed, and the contamination caused by the volatilization of impurities can be suppressed. The loss of the expensive material used as the target can be suppressed, and the target can be easily peeled and recovered.
以下,示出實施方式對本發明詳細進行說明,但本發明不限定於該等記載來解釋。只要起到本發明之效果,則實施方式亦可進行各種變化。圖中,於各接合體中,對相同名稱之部位,無論形狀如何均標註相同符號。Hereinafter, the present invention will be described in detail with reference to the embodiments, but the present invention should not be construed as being limited to these descriptions. As long as the effects of the present invention are exhibited, the embodiment may be changed in various ways. In the figure, in each joint body, the parts with the same names are denoted by the same symbols regardless of their shapes.
<濺鍍靶材-背板接合體>
(形態1-1:背板具有鉤狀部,濺鍍靶材具有鉤支承部之形態)
參照圖1及圖2,對本實施方式之濺鍍靶材-背板接合體進行說明。本實施方式之濺鍍靶材-背板接合體100係濺鍍靶材2接合於背板1而成者,且背板1具有板表面3、板背面4、及板側面5,濺鍍靶材2具有靶材表面7、與板表面3相對之靶材背面8、及外周側面9,背板1及濺鍍靶材2中,背板1進而具有鉤狀部6,濺鍍靶材2進而具有鉤支承部10,鉤狀部6與鉤支承部10相互抵接,濺鍍靶材2之鉤支承部10設置於濺鍍靶材2之外周側面9,且藉由使鉤狀部6抵接於鉤支承部10,而將濺鍍靶材2固定於背板1。藉由使鉤狀部6抵接於鉤支承部10,能夠於背板1之板表面3之側面方向上固定濺鍍靶材2,並且於背板1之板表面3之厚度方向上固定濺鍍靶材2。
<Sputtering target-back plate assembly>
(Form 1-1: Form in which the back plate has a hook-shaped portion, and the sputtering target has a hook support portion)
Referring to FIGS. 1 and 2 , the sputtering target-back plate assembly of the present embodiment will be described. The sputtering target material-
於圖1及圖2所示之形態中,係背板1於板表面3具有凸部13,凸部13具有鉤狀部6之形態。對背板1進行切削而形成凸部13,於凸部13之內側形成鉤狀部6。鉤狀部6與背板1一體化,故而能夠將濺鍍靶材2固定。In the form shown in FIG. 1 and FIG. 2, the
關於圖2中之鉤狀部6與鉤支承部10,較佳為遍及濺鍍靶材2之外周形狀之全周使鉤狀部6與鉤支承部10抵接。於圖1中,環狀陰影位置表示設置於背板1之板表面3之凸部13之頂面,表示凸部13位於濺鍍靶材2之外周形狀之全周。但是,當能抑制濺鍍靶材2之破損及剝離,且能抑制因雜質之揮發造成之污染時,亦可局部地形成2個以上鉤狀部6及鉤支承部10並使其等抵接。As for the hook-shaped
關於圖2中之鉤狀部6與鉤支承部10,亦可採用圖2(A)~圖2(N)所示之鉤狀部、鉤支承部之形態使其等抵接。About the hook-shaped
又,若鉤狀部6與鉤支承部10抵接,則能夠保證背板1與濺鍍靶材2之接合強度,但除了需要接合強度以外,亦需要背板1與濺鍍靶材2之密接性時,較佳為於使鉤狀部6與鉤支承部10抵接時,自鉤狀部6朝向鉤支承部10按壓。Moreover, if the hook-shaped
於圖1及圖2中,示出了圓板形狀之濺鍍靶材2接合於圓板形狀之背板1之形態,但亦可為如圖3所示,長方形之濺鍍靶材2接合於長方形之背板1之形態。B-B剖面具有與圖2所示之A-A剖面相同之形狀。又,長方形之形狀包括正方形之形狀。圖3中,環狀陰影位置亦表示設置於背板1之板表面3之凸部13之頂面。In FIGS. 1 and 2 , the disc-shaped
(形態1-2:背板具有鉤支承部,濺鍍靶材具有鉤狀部之形態)
參照圖4及圖5,對本實施方式之濺鍍靶材-背板接合體之另一形態進行說明。本實施方式之濺鍍靶材-背板接合體101係將濺鍍靶材2接合於背板1而成者,且背板1具有板表面3、板背面4、及板側面5,濺鍍靶材2具有靶材表面7、與板表面3相對之靶材背面8、及外周側面9,背板1及濺鍍靶材2中,背板1進而具有鉤支承部10,濺鍍靶材2進而具有鉤狀部6,鉤狀部6與鉤支承部10相互抵接,濺鍍靶材2之鉤狀部6設置於濺鍍靶材2之外周側面9,且藉由使鉤狀部6抵接於鉤支承部10,而將濺鍍靶材2固定於背板1。藉由使鉤狀部6抵接於鉤支承部10,能夠於背板1之板表面3之側面方向上固定濺鍍靶材2,並且於背板1之板表面3之厚度方向上固定濺鍍靶材2。
(Form 1-2: Form in which the back plate has a hook support portion, and the sputtering target has a hook portion)
4 and 5, another form of the sputtering target-back plate assembly of the present embodiment will be described. The sputtering target material-
於圖4及圖5所示之形態中,係背板1於板表面3具有凸部13,凸部13具有鉤支承部10之形態。對背板1進行切削而形成凸部13,於凸部13之內側形成鉤支承部10。鉤支承部10與背板1一體化,故而能夠將濺鍍靶材2固定。In the form shown in FIGS. 4 and 5 , the
關於圖5中之鉤狀部6與鉤支承部10,較佳為遍及濺鍍靶材2之外周形狀之全周使鉤狀部6與鉤支承部10抵接,但是,當能抑制濺鍍靶材2之破損及剝離,且能抑制因雜質之揮發造成之污染時,亦可局部地形成2個以上鉤狀部6及鉤支承部10並使其等抵接。Regarding the hook-shaped
關於圖5中之鉤狀部6及鉤支承部10,亦可採用圖5(A)~圖5(L)等所示之鉤狀部、鉤支承部之形態使其等抵接。About the hook-shaped
又,若鉤狀部6與鉤支承部10抵接,則能夠保證背板1與濺鍍靶材2之接合強度,但除了需要接合強度以外,亦需要背板1與濺鍍靶材2之密接性時,較佳為於使鉤狀部6與鉤支承部10抵接時,自鉤支承部10朝向鉤狀部6按壓。Moreover, if the hook-shaped
於圖4及圖5中,示出了圓板形狀之濺鍍靶材2接合於圓板形狀之背板1之形態,但亦可為如圖6所示,長方形之濺鍍靶材2接合於長方形之背板1之形態。B-B剖面具有與圖5所示之A-A剖面相同之形狀。又,長方形之形狀包括正方形之形狀。於圖6中,環狀陰影位置亦表示設置於背板1之板表面3之凸部13之頂面。In FIGS. 4 and 5 , the disc-shaped
以下,示出各種濺鍍靶材-背板接合體之剖面概略圖,進一步對本實施方式進行說明。濺鍍靶材-背板接合體可為圓板形狀、長方形板狀或正方形板狀中任一種。Hereinafter, the present embodiment will be further described by showing schematic cross-sectional views of various sputtering target-backplate assemblies. The sputtering target-back plate joint body may be any of a circular plate shape, a rectangular plate shape, or a square plate shape.
(形態2-1:背板具有卡子,卡子具有鉤狀部之形態)
如圖7所示,於本實施方式之濺鍍靶材-背板接合體200中,較佳為背板1具有卡子14,卡子14具有鉤狀部6。濺鍍靶材2具有鉤支承部10,鉤狀部6抵接於鉤支承部10。於形態1-1中,係背板1於板表面3具有凸部13,凸部13具有鉤狀部6之形態,與此相對,於形態2-1中,具有卡子14以代替凸部13。藉由背板1具有卡子14,卡子14發揮與凸部13相同之作用。藉由背板1具有卡子14,能夠便於加工,便於組裝接合體。如圖7所示,於本實施方式之濺鍍靶材-背板接合體200中,較佳為卡子14之側面自外周側面9突出,至少卡子14之突出部分固定於背板1。與圖2所示之形態之差異在於:與背板1及濺鍍靶材2分開地準備卡子,於卡子之與濺鍍靶材2相接之側形成鉤狀部6,於濺鍍靶材2之外周側面9形成鉤支承部10,於使卡子14之鉤狀部6與濺鍍靶材2之鉤支承部10抵接後,自未被濺鍍靶材2覆蓋之位置之卡子朝向背板1進行固定,藉此,能夠將濺鍍靶材2固定於背板1。關於固定,例如於螺固位置11藉由螺固而固定。藉由製成此種構造,背板1之鉤狀部6之外側位於較濺鍍靶材2之外周側面9更外側,當鉤狀部6抵接於鉤支承部10時,濺鍍靶材2於背板1之板表面3之側面方向上被固定,並且亦能於背板1之板表面3之厚度方向上固定濺鍍靶材2。卡子14除了藉由螺固固定於背板1以外,亦可藉由擴散接合、熔接等接合方法來固定。於圖7中,示出了在螺固位置11處,藉由螺固將卡子14固定於背板1之板表面3之形態,但亦可以不僅固定於板表面3,還固定於背板1之側面或背面。
(Form 2-1: The back plate has a clip, and the clip has a hook-shaped part)
As shown in FIG. 7 , in the sputtering target-
於圖7所示之形態中,可與圖2所示之形態同樣地使鉤狀部6與鉤支承部10抵接,但進而亦可製成如下構造。
(1)較佳為遍及濺鍍靶材2之外周形狀之全周使鉤狀部6與鉤支承部10抵接,但亦可局部地形成2個以上鉤狀部6及鉤支承部10並使其等抵接。
(2)關於鉤狀部6與鉤支承部10,亦可採用圖7(A)~圖7(N)等所示之鉤狀部及鉤支承部之形態使其等抵接。
(3)除了需要接合強度以外,亦需要背板1與濺鍍靶材2之密接性時,亦可於鉤狀部6與鉤支承部10抵接時,自鉤狀部6朝向鉤支承部10按壓。
In the form shown in FIG. 7, the hook-shaped
(形態2-2:背板具有卡子,卡子具有鉤支承部之形態)
與形態1-1和形態1-2之關係,即鉤狀部與鉤支承部之配置為顛倒關係同樣地,亦可將形態2-1中鉤狀部6與鉤支承部10之配置顛倒(未圖示)。
(Form 2-2: The back plate has a clip, and the clip has a hook support part)
Similar to the relationship between the form 1-1 and the form 1-2, that is, the disposition of the hook-shaped part and the hook support part is reversed, the disposition of the hook-shaped
(形態3-1:背板具有卡子,卡子具有鉤狀部之形態)
如圖8所示,於本實施方式之濺鍍靶材-背板接合體201中,較佳為卡子14留下側面之一部分而進入外周側面9,卡子14固定於背板1。由於卡子14包含於濺鍍靶材2之形狀中,故而能夠減少卡子14之角部之露出。又,藉由製成此種構造,當鉤狀部6抵接於鉤支承部10時,濺鍍靶材2於背板1之板表面3之側面方向上被固定,並且能夠於背板1之板表面3之厚度方向上固定濺鍍靶材2。卡子14除了藉由螺固固定於背板1以外,亦可藉由擴散接合、熔接等接合方法來固定。於圖8中,示出了在螺固位置11處,藉由螺固將卡子14固定於背板1之板表面3之形態,但亦可以不僅固定於板表面3,還固定於背板1之側面或背面。
(Form 3-1: The back plate has a clip, and the clip has a hook-shaped part)
As shown in FIG. 8 , in the sputtering target-
於圖8所示之形態中,可與圖2所示之形態同樣地使鉤狀部6與鉤支承部10抵接,但進而亦可製成如下構造。
(1)較佳為遍及濺鍍靶材2之外周形狀之全周使鉤狀部6與鉤支承部10抵接,但亦可局部地形成2個以上鉤狀部6及鉤支承部10並使其等抵接。
(2)關於鉤狀部6與鉤支承部10,亦可採用圖8(A)~圖8(N)等所示之鉤狀部及鉤支承部之形態使其等抵接。
(3)除了需要接合強度以外,亦需要背板1與濺鍍靶材2之密接性時,亦可於鉤狀部6與鉤支承部10抵接時,自鉤狀部6朝向鉤支承部10按壓。
In the form shown in FIG. 8, the hook-shaped
(形態3-2:背板具有卡子,卡子具有鉤支承部之形態)
與形態1-1和形態1-2之關係,即鉤狀部與鉤支承部之配置為顛倒關係同樣地,亦可將形態3-1中鉤狀部6與鉤支承部10之配置顛倒(未圖示)。
(Form 3-2: The back plate has a clip, and the clip has a hook support part)
Similar to the relationship between the form 1-1 and the form 1-2, that is, the disposition of the hook-shaped part and the hook support part is reversed, the disposition of the hook-shaped
(形態4-1:背板具有凹部,凹部具有鉤狀部之形態)
如圖9所示,於本實施方式之濺鍍靶材-背板接合體300中,較佳為背板1於板表面3具有凹部17,背板1於凹部17之內周側面16具有鉤狀部6,濺鍍靶材2之一部分嵌入至凹部17。於圖9之形態中,藉由在濺鍍靶材2之外周側面9設置鉤支承部10,使鉤狀部6抵接於鉤支承部10,能夠於背板1之板表面3之側面方向上固定濺鍍靶材2,並且於背板1之板表面3之厚度方向上固定濺鍍靶材2。與圖2所示之形態之差異在於:與背板1之凹部17之深度相應地將濺鍍靶材2之底部嵌埋於凹部17內,故而能夠於背板1之板表面3之側面方向上固定濺鍍靶材2,並且於背板1之板表面3之厚度方向上固定濺鍍靶材2。
(Form 4-1: The back plate has a concave part, and the concave part has a hook-shaped part)
As shown in FIG. 9 , in the sputtering target-
於圖9所示之形態中,可與圖2所示之形態同樣地使鉤狀部6與鉤支承部10抵接,但進而亦可製成如下構造。
(1)較佳為遍及濺鍍靶材2之外周形狀之全周使鉤狀部6與鉤支承部10抵接,但亦可局部地形成2個以上鉤狀部6及鉤支承部10並使其等抵接。
(2)關於鉤狀部6與鉤支承部10,亦可採用圖9(A)~圖9(N)等所示之鉤狀部及鉤支承部之形態使其等抵接。
(3)除了需要接合強度以外,亦需要背板1與濺鍍靶材2之密接性時,亦可於鉤狀部6與鉤支承部10抵接時,自鉤狀部6朝向鉤支承部10按壓。
In the form shown in FIG. 9, the hook-shaped
(形態4-2:背板具有凹部,凹部具有鉤支承部之形態)
與形態1-1和形態1-2之關係,即鉤狀部與鉤支承部之配置為顛倒關係同樣地,亦可將形態4-1中鉤狀部6與鉤支承部10之配置顛倒(未圖示)。
(Form 4-2: The back plate has a concave part, and the concave part has a hook support part)
Similar to the relationship between the form 1-1 and the form 1-2, that is, the disposition of the hook-shaped part and the hook support part is reversed, the disposition of the hook-shaped
(形態5-1:背板具有凹部,卡子具有鉤狀部之形態)
如圖10所示,於本實施方式之濺鍍靶材-背板接合體400中,較佳為背板1於板表面3具有凹部17,背板1於凹部17具有卡子14,卡子14具有鉤狀部6,濺鍍靶材2之至少一部分與卡子14之至少一部分嵌入至凹部17,卡子14固定於背板1之凹部17。與圖9所示之形態之差異在於:與背板1及濺鍍靶材2分開地準備卡子14,於卡子14之與濺鍍靶材2相接之側形成鉤狀部6,於濺鍍靶材2之外周側面9形成鉤支承部10,於使卡子14之鉤狀部6與濺鍍靶材2之鉤支承部10抵接後,將卡子14與濺鍍靶材2嵌埋於背板1之凹部17,自未被濺鍍靶材2覆蓋之位置之卡子14朝向背板1進行固定,藉此,能夠將濺鍍靶材2固定於背板1。能夠於背板1之板表面3之側面方向上固定濺鍍靶材2,並且於背板1之板表面3之厚度方向上固定上述濺鍍靶材2。卡子14除了藉由螺固固定於背板1以外,亦可藉由擴散接合、熔接等接合方法來固定。
(Form 5-1: The back plate has a concave part and the clip has a hook part)
As shown in FIG. 10 , in the sputtering target-
於圖10所示之形態中,可與圖9所示之形態同樣地使鉤狀部6與鉤支承部10抵接,但進而亦可製成如下構造。
(1)較佳為遍及濺鍍靶材2之外周形狀之全周使鉤狀部6與鉤支承部10抵接,但亦可局部地形成2個以上鉤狀部6及鉤支承部10並使其等抵接。
(2)關於鉤狀部6與鉤支承部10,亦可採用圖10(A)~圖10(N)等所示之鉤狀部及鉤支承部之形態使其等抵接。
(3)除了需要接合強度以外,亦需要背板1與濺鍍靶材2之密接性時,亦可於鉤狀部6與鉤支承部10抵接時,自鉤狀部6朝向鉤支承部10按壓。
In the form shown in FIG. 10, the hook-shaped
(形態5-2:背板具有凹部,卡子具有鉤支承部之形態)
與形態1-1和形態1-2之關係,即鉤狀部與鉤支承部之配置為顛倒關係同樣地,亦可將形態5-1中鉤狀部6與鉤支承部10之配置顛倒(未圖示)。
(Form 5-2: The back plate has a concave part, and the clip has a hook support part)
Similar to the relationship between the form 1-1 and the form 1-2, that is, the disposition of the hook-shaped part and the hook support part is reversed, the disposition of the hook-shaped
(鉤狀部及鉤支承部之形狀之變化例1)
於本實施方式之濺鍍靶材-背板接合體中,較佳為鉤狀部6具有第1凹凸形狀部,鉤支承部10具有與第1凹凸形狀部相應之第2凹凸形狀部。除了能提高濺鍍靶材之側面方向上之濺鍍靶材與背板之接合強度以外,於濺鍍靶材之厚度方向上亦能提高濺鍍靶材與背板之接合強度,其結果為,能夠保持濺鍍靶材使用時之接合強度,將熱傳導保持良好。此處,與第1凹凸形狀部相應之第2凹凸形狀部包括凹凸形狀部彼此無間隙地相互接觸之形態,此外還包括凹凸形狀部彼此有間隙,但相互卡住無偏移之形態。作為具有此種形態之例,例如示於圖2(L)、圖2(M)、圖2(N)、圖5(J)、圖5(K)、圖5(L)、圖7(L)、圖7(M)、圖7(N)、圖8(L)、圖8(M)、圖8(N)、圖9(L)、圖9(M)、圖9(N)、圖10(L)、圖10(M)或圖10(N)。
(
(鉤狀部及鉤支承部之形狀之變化例2)
於本實施方式之濺鍍靶材-背板接合體中,較佳為鉤狀部6具有自背板1至濺鍍表面之方向上之鉤前端成為最大鉤掛位置之鉤形,鉤支承部10具有與鉤形相應之鉤孔。除了能提高濺鍍靶材2之側面方向上之濺鍍靶材2與背板1之接合強度以外,於濺鍍靶材2之厚度方向上亦能提高濺鍍靶材2與背板1之接合強度,其結果為,能夠保持濺鍍靶材使用時之接合強度,將熱傳導保持良好。此處,鉤支承部具有與鉤形相應之鉤孔包括鉤孔無間隙地嵌合於鉤形之形態,此外還包括將鉤形插入於鉤孔時有間隙,但相互卡住無偏移之形態。作為具有此種形態之例,例如示於圖2(D)、圖2(F)、圖7(D)、圖7(F)、圖8(D)、圖8(F)、圖9(D)、圖9(F)、圖10(D)或圖10(F)。
(
(形態6-1:具有中間層之形態)
如圖11所示,於本實施方式之濺鍍靶材-背板接合體500中,較佳為於濺鍍靶材2與背板1之界面具有2.5 mm以下之中間層12,中間層12包括包含Ni、Cr、Al、Cu中至少任一種金屬或含有Ni、Cr、Al、Cu中至少任一種之合金之板材、粉末、或該板材與該粉末之組合。藉由利用中間層12減小濺鍍靶材2與背板1之線膨脹係數之差,能夠進一步抑制因加熱膨脹或冷卻收縮反覆發生而導致之濺鍍靶材2之破損及翹曲。又,藉由設置中間層12,能夠提高濺鍍靶材2之靶材背面8與背板之板表面3之接合強度,並且提高密接性,將熱傳導保持良好。又,於在濺鍍靶材2之外周側面9之全周設置有背板1之鉤狀部6之情形時,中間層12設置於由背板1之板表面3、背板1之設置有鉤狀部6之內側之部位及濺鍍靶材2之靶材背面8所包圍的位置。其結果為,中間層12由濺鍍靶材2覆蓋,故而能夠抑制中間層12之材質揮發成為雜質而附著於基板。對中間層12選擇元素Ni、Cr、Al、Cu之原因在於:就密接性、熱傳導及線膨脹係數之觀點而言較為適宜。於中間層12為板材之情形時,若板材較2.5 mm厚,則必須將背板1之設置有鉤狀部6之位置之高度設置得更高。於中間層12為粉末層之情形時,藉由加熱,存在呈粉末狀態之形態、粉末燒結後之形態、或粉末經加熱而熔融之形態。再者,粉末經加熱而熔融之形態與中間層12為板材之形態類似。中間層12較佳為設置於濺鍍靶材2之靶材背面8與背板1之板表面3之間,但除此以外,進而亦可設置於濺鍍靶材2之包含鉤支承部10之外周側面9與背板1之設置有鉤狀部6之內側之位置的界面。關於鉤狀部6與鉤支承部10,亦可採用圖8(A)~圖8(N)等所示之鉤狀部及鉤支承部之形態使其等抵接。
(Form 6-1: Form with an intermediate layer)
As shown in FIG. 11 , in the sputtering target-
(形態6-2:具有中間層之形態)
於圖11所示之濺鍍靶材-背板接合體500中,對在設置於背板1之板表面3上之鉤狀部6之形態中設置中間層12進行了說明,但是於如圖12所示之濺鍍靶材-背板接合體501,在背板1之板表面3形成有凹部17之情形時,亦可同樣地設置2.5 mm以下之中間層12。
(Form 6-2: Form with an intermediate layer)
In the sputtering target-
(形態7-1:具有中間層之形態)
與圖11所示之形態同樣地,本實施方式之濺鍍靶材-背板接合體較佳為於濺鍍靶材2與背板1之界面具有10 μm以下之中間層12,中間層12係包含Ni、Cr、Al、Cu中至少任一種金屬或含有Ni、Cr、Al、Cu中至少任一種之合金之薄膜。藉由利用中間層12減小濺鍍靶材2與背板1之線膨脹係數之差,能夠進一步抑制因加熱膨脹或冷卻收縮反覆發生而導致之濺鍍靶材2之破損及翹曲。即便中間層12之膜厚較10 μm厚,亦只需要形成中間層12之時間,作為中間層12之效果與10 μm以下者之效果相比變化不大。又,藉由設置中間層12,能夠提高濺鍍靶材2之靶材背面8與背板1之板表面3之接合強度,並且提高密接性,將熱傳導保持良好。又,於在濺鍍靶材2之外周側面9之全周設置有背板1之鉤狀部6之情形時,中間層12設置於由背板1之板表面3、背板1之設置有鉤狀部6之內側之部位及濺鍍靶材2之靶材背面8所包圍的位置。其結果為,中間層12由濺鍍靶材2覆蓋,故而能夠抑制中間層12之材質揮發成為雜質而附著於基板。對中間層12選擇元素Ni、Cr、Al、Cu之原因在於:就密接性、熱傳導及線膨脹係數之觀點而言較為適宜。薄膜較佳為利用濺鍍所得之薄膜,且成膜於背板1之板表面3為佳。又,亦可以是厚度為10 μm以下之箔。中間層12較佳為設置於濺鍍靶材2之靶材背面8與背板1之板表面3之間,但除此以外,進而亦可設置於濺鍍靶材2之包含鉤支承部10之外周側面9與背板1之設置有鉤狀部6之內側之位置的界面。關於鉤狀部6與鉤支承部10,亦可採用圖8(A)~圖8(N)等所示之鉤狀部及鉤支承部之形態使其等抵接。
(Form 7-1: Form with an intermediate layer)
Similar to the form shown in FIG. 11 , the sputtering target-backplate assembly of the present embodiment preferably has an
(形態7-2:具有中間層之形態)
於圖11所示之濺鍍靶材-背板接合體500中,對在設置於背板1之板表面3上之鉤狀部6之形態中設置中間層12進行了說明,但是於如圖12所示之濺鍍靶材-背板接合體501,在背板1之板表面3形成有凹部17之情形時,亦可同樣地設置10 μm以下之中間層12。
(Form 7-2: Form with an intermediate layer)
In the sputtering target-
(形態8-1:具有中間層之形態)
與圖11所示之形態同樣地,本實施方式之濺鍍靶材-背板接合體較佳為於濺鍍靶材2與背板1之界面具有1.0 mm以下之中間層12,中間層12包括包含In、Zn中至少任一種金屬或含有In、Zn中至少任一種之合金之板材、粉末、或該板材與該粉末之組合。藉由利用中間層12減小濺鍍靶材2與背板1之線膨脹係數之差,能夠進一步抑制因加熱膨脹或冷卻收縮反覆發生而導致之濺鍍靶材2之破損及翹曲。對中間層12選擇元素In、Zn之原因在於:就密接性、熱傳導及線膨脹係數之觀點而言較為適宜。於中間層12為板材之情形時,若板材較1.0 mm厚,則由於In或Zn為易氧化之材料,故而存在硬度上升而發生破裂之情況。又,藉由設置中間層12,能夠提高濺鍍靶材2之靶材背面8與背板1之板表面3之接合強度,並且提高密接性,將熱傳導保持良好。又,於在濺鍍靶材2之外周側面9之全周設置有背板1之鉤狀部6之情形時,中間層12設置於由背板1之板表面3、背板1之設置有鉤狀部6之內側之部位及濺鍍靶材2之靶材背面8所包圍的位置。其結果為,中間層12由濺鍍靶材2覆蓋,故而能夠抑制中間層12之材質揮發成為雜質而附著於基板。於中間層12為粉末層之情形時,藉由加熱,存在呈粉末狀態之形態、粉末燒結後之形態、或粉末經加熱而熔融之形態。再者,粉末經加熱而熔融之形態與中間層12為板材之形態類似。中間層12較佳為設置於濺鍍靶材2之靶材背面8與背板1之板表面3之間,但除此以外,進而亦可設置於濺鍍靶材2之包含鉤支承部10之外周側面9與背板1之設置有鉤狀部6之內側之位置的界面。關於鉤狀部6與鉤支承部10,亦可採用圖8(A)~圖8(N)等所示之鉤狀部及鉤支承部之形態使其等抵接。
(Form 8-1: Form with an intermediate layer)
Similar to the form shown in FIG. 11 , the sputtering target material-backing plate assembly of the present embodiment preferably has an
(形態8-2:具有中間層之形態)
於圖11所示之濺鍍靶材-背板接合體500中,對在設置於背板1之板表面3上之鉤狀部6之形態中設置中間層12進行了說明,但是於如圖12所示之濺鍍靶材-背板接合體501,在背板1之板表面3形成有凹部17之情形時,亦可同樣地設置1.0 mm以下之中間層12。
(Form 8-2: Form with an intermediate layer)
In the sputtering target-
(形態9-1:具有中間層之形態)
如圖13所示,本實施方式之濺鍍靶材-背板接合體600較佳為於濺鍍靶材2與背板1之界面具有2層中間層12,中間層12a包含以下構成中之任一種:2.5 mm以下之板材、粉末、或該板材與該粉末之組合,其包含Ni、Cr、Al、Cu中至少任一種金屬或含有Ni、Cr、Al、Cu中至少任一種之合金;10 μm以下之薄膜,其包含Ni、Cr、Al、Cu中至少任一種金屬或含有Ni、Cr、Al、Cu中至少任一種之合金;或者1.0 mm以下之板材、粉末、或該板材與該粉末之組合,其包含In、Zn中至少任一種金屬或含有In、Zn中至少任一種之合金;且中間層12b包含以下構成中之任一種:2.5 mm以下之板材、粉末、或該板材與該粉末之組合,其包含Ni、Cr、Al、Cu中至少任一種金屬或含有Ni、Cr、Al、Cu中至少任一種之合金;10 μm以下之薄膜,其包含Ni、Cr、Al、Cu中至少任一種金屬或含有Ni、Cr、Al、Cu中至少任一種之合金;或者1.0 mm以下之板材、粉末、或該板材與該粉末之組合,其包含In、Zn中至少任一種金屬或含有In、Zn中至少任一種之合金。藉由利用中間層12減小濺鍍靶材2與背板1之線膨脹係數之差,能夠進一步抑制因加熱膨脹或冷卻收縮反覆發生而導致之濺鍍靶材2之破損及翹曲。由包含Ni、Cr、Al、Cu中至少任一種金屬或含有Ni、Cr、Al、Cu中至少任一種之合金、包含In、Zn中至少任一種金屬或含有In、Zn中至少任一種之合金之各種形態之材料形成在與背板1之界面設置的中間層12a之原因在於:就密接性、熱傳導及線膨脹係數之觀點而言較為適宜。又,由包含Ni、Cr、Al、Cu中至少任一種金屬或含有Ni、Cr、Al、Cu中至少任一種之合金、包含In、Zn中至少任一種金屬或含有In、Zn中至少任一種之合金之各種形態之材料形成在與濺鍍靶材2之界面設置的中間層12b之原因在於:就密接性、熱傳導及線膨脹係數之觀點而言較為適宜。再者,於圖13中示出了中間層為2層之形態,但亦可以是中間層為3層以上之形態,只要能獲得上述說明之中間層之效果即可。中間層12較佳為設置於濺鍍靶材2之靶材背面8與背板1之板表面3之間,但除此以外,進而亦可設置於濺鍍靶材2之包含鉤支承部10之外周側面9與背板1之設置有鉤狀部6之內側之位置的界面。關於鉤狀部6與鉤支承部10,亦可採用圖8(A)~圖8(N)等所示之鉤狀部及鉤支承部之形態使其等抵接。
(Form 9-1: Form with an intermediate layer)
As shown in FIG. 13 , the sputtering target-backplate assembly 600 of this embodiment preferably has two intermediate layers 12 at the interface between the sputtering target 2 and the backing plate 1 , and the intermediate layer 12 a includes the following structures Any one: a sheet, powder, or a combination of the sheet and the powder with a thickness of 2.5 mm or less, which contains at least any one of Ni, Cr, Al, and Cu, or an alloy containing at least any one of Ni, Cr, Al, and Cu; A thin film of 10 μm or less, which contains at least any metal of Ni, Cr, Al, and Cu or an alloy containing at least any of Ni, Cr, Al, and Cu; or a sheet, powder, or the sheet and the A combination of powders, which includes at least one metal in In, Zn or an alloy containing at least any one in In, Zn; and the intermediate layer 12b includes any one of the following structures: a sheet with a thickness of 2.5 mm or less, a powder, or the sheet and the The combination of the powder, which contains at least any metal of Ni, Cr, Al, and Cu, or an alloy containing at least any one of Ni, Cr, Al, and Cu; the thin film with a thickness of 10 μm or less, which contains Ni, Cr, Al, Cu At least any one of the metals or alloys containing at least any one of Ni, Cr, Al, and Cu; or a sheet, powder, or a combination of the sheet and the powder below 1.0 mm, which contains at least any one of In, Zn. Metal or An alloy containing at least one of In and Zn. By using the
(形態9-2:具有中間層之形態)
於圖13所示之濺鍍靶材-背板接合體600中,對在設置於背板1之板表面3上之鉤狀部6之形態中設置中間層12進行了說明,但是於如圖14所示之濺鍍靶材-背板接合體601,在背板1之板表面3形成有凹部17之情形時,亦可同樣地設置中間層12。
(Form 9-2: Form with an intermediate layer)
In the sputtering target-
(濺鍍靶材之材質)
本實施方式之濺鍍靶材-背板接合體中,濺鍍靶材2之材質可使用Al-Sc合金、Ru、Ru合金、Ir或Ir合金。又,亦可使用Li系氧化物、Co系氧化物、Ti系氧化物或Mg系氧化物等。即便為1000℃以上之高熔點材料亦能抑制濺鍍靶材之翹曲或破裂,並且提高濺鍍靶材與背板之接合強度。。
(Material of sputtering target)
In the sputtering target-back plate assembly of the present embodiment, the material of the
本實施方式之濺鍍靶材-背板接合體較佳為,背板1之材質為Al、Al合金、Cu、Cu合金、Fe或Fe合金,線膨脹係數為30.0×10
-6/℃以下。線膨脹係數較佳為28.5×10
-6/℃以下,進而較佳為27.3×10
-6/℃以下。若線膨脹係數大於30.0×10
-6/℃,則因背板1之加熱膨脹或冷卻收縮反覆發生而出現濺鍍靶材之破裂或翹曲,故而線膨脹係數較佳為30.0×10
-6/℃以下。又,藉由使用背板之熱傳導性良好者,加熱時背板膨脹,能夠將濺鍍靶材插入於由背板1之板表面3、背板1之設置有鉤狀部6之內側之部位及濺鍍靶材2之靶材背面8所包圍的位置或者背板之凹部,並且藉由冷卻時背板收縮,由背板之鉤狀部6抵接或者抵接與按壓濺鍍靶材之鉤支承部10,能夠形成接合體。線膨脹係數之下限較佳為6.0×10
-6/℃以上。
Preferably, in the sputtering target material-back plate assembly of the present embodiment, the material of the
[包含線膨脹係數之關係式](ΔT共通)
亦可於鉤狀部6與鉤支承部10抵接時,藉由用抵接面自背板對濺鍍靶材施加按壓,而將上述濺鍍靶材更牢固地固定於上述背板。將鉤狀部6與鉤支承部10抵接時,自背板對濺鍍靶材施加按壓之背板之面稱為按壓面。又,將自背板受到按壓之濺鍍靶材之面稱為接觸面。
由背板1之按壓面按壓濺鍍靶材2之接觸面時,較佳為上述按壓面至少具有配置於隔著上述接觸面相對之位置的成對之面,且該成對之按壓面彼此之距離與和上述成對之按壓面接觸的接觸面彼此之距離之關係滿足(數1)~(數5)。
(數1) D
TG>D
BP(數2) D
BP=D
TG-ΔD×C
(數3) ΔD=D
BP×ΔT×CTE
BP-D
TG×ΔT×CTE
TG(數4) D
TG-ΔD×4.0≦D
BP≦D
TG-ΔD×0.5
(數5) CTE
BP>CTE
TG其中,D
BP、D
TG、ΔD、C、T、ΔT、CTE
BP及CTE
TG之含義分別如下。
D
BP:室溫下之上述成對之按壓面彼此之距離(mm)
D
TG:室溫下之與上述成對之按壓面接觸的接觸面彼此之距離(mm)
T:使背板熱膨脹而使濺鍍靶材嵌合之溫度(℃)(其中,T>室溫)
ΔT:T-室溫(℃)
CTE
BP:溫度T下之背板之線膨脹係數(1/℃)
CTE
TG:溫度T下之濺鍍靶材之線膨脹係數(1/℃)
C:係數(其中,C=0.5~4.0)
ΔD:自室溫升溫至溫度T時之背板與濺鍍靶材之熱膨脹量之差(mm)
此處,當背板1之平面形狀為長方形時,使濺鍍靶材2之長邊與背板1之長邊對應,使濺鍍靶材2之短邊與背板1之短邊對應。如(數1)所示,室溫下,濺鍍靶材2之接觸面彼此之距離大於背板1之按壓面彼此之距離,無法將濺鍍靶材2放入背板1之按壓面之內側。此處,室溫設為25℃。此處,作為形態(1),想到使背板1與濺鍍靶材2兩者升溫至溫度T之形態。若將背板1自室溫升溫至使背板熱膨脹之溫度T,則背板1之按壓面彼此之距離以由(D
BP×ΔT×CTE
BP)求出之長度熱膨脹。又,若使濺鍍靶材2自室溫升溫至溫度T,則濺鍍靶材2之接觸面彼此之距離以由(D
TG×ΔT×CTE
TG)求出之長度熱膨脹。因此,關於線膨脹係數,(數5)之關係成立時,若將背板1與濺鍍靶材2兩者升溫至溫度T,則背板1之按壓面發生之熱膨脹較濺鍍靶材2之接觸面發生之熱膨脹多ΔD之長度。若藉由該熱膨脹使得背板1之按壓面彼此之距離與濺鍍靶材2之接觸面彼此之距離相同或較其大,則能夠將濺鍍靶材2嵌入至背板1之按壓面之內側。而且,若降溫至室溫,則根據(數1)所示之關係,由背板1之按壓面按壓濺鍍靶材2之接觸面。於上述形態(1)中,為了能夠由背板1之按壓面按壓濺鍍靶材2之接觸面,必須藉由背板1之熱膨脹,將背板1之按壓面彼此之距離與濺鍍靶材2之接觸面彼此之距離反轉。因此,表示可以將室溫下之背板1之按壓面彼此之距離設定為較室溫下之濺鍍靶材2之接觸面彼此之距離小多少這一關係的是(數2)及(數4)。於(數2)及(數4)中,C為係數,當C為0.5~4.0之範圍內時,由背板1之按壓面按壓濺鍍靶材2之接觸面而將濺鍍靶材與背板接合,此時能夠抑制濺鍍靶材之破裂或翹曲。
[Relational Expression Including Linear Expansion Coefficient] (Common to ΔT) When the hook-shaped
於本實施方式中,不僅包括上述說明之將背板1與濺鍍靶材2兩者升溫至溫度T之形態(1),還包括將背板1升溫至溫度T,將濺鍍靶材2僅升溫至低於溫度T之溫度T
1之形態(2);及將背板1升溫至溫度T,不使濺鍍靶材2升溫之形態(3)。
In this embodiment, not only the mode (1) of raising the temperature of both the
[包含線膨脹係數之關係式](於ΔT(BP)與ΔT1(TG)中不同)
由背板1之按壓面按壓濺鍍靶材2之接觸面時,較佳為上述按壓面至少具有配置於隔著上述接觸面相對之位置的成對之面,且該成對之按壓面彼此之距離與和上述成對之按壓面接觸的接觸面彼此之距離之關係滿足(數6)~(數10)。
(數6) D
TG>D
BP(數7) D
BP=D
TG-ΔD×C
(數8) ΔD=D
BP×ΔT×CTE
BP-D
TG×ΔT
1×CT
1E
TG(數9) D
TG-ΔD×4.0≦D
BP≦D
TG-ΔD×0.5
(數10) CTE
BP>CT
1E
TG其中,D
BP、D
TG、ΔD、C、T、ΔT、T
1、ΔT
1、CTE
BP及CT
1E
TG之含義分別如下。
D
BP:室溫下之上述成對之按壓面彼此之距離(mm)
D
TG:室溫下之與上述成對之按壓面接觸的接觸面彼此之距離(mm)
T:使背板熱膨脹而使濺鍍靶材嵌合時之背板之溫度(℃)(其中,T>室溫、T>T
1)
ΔT:T-室溫(℃)
T
1:使背板熱膨脹而使濺鍍靶材嵌合時之濺鍍靶材之溫度(℃)(其中,T
1≧室溫、T>T
1)
ΔT
1:T
1-室溫(℃)
CTE
BP:溫度T下之背板之線膨脹係數(1/℃)
CT
1E
TG:溫度T
1下之濺鍍靶材之線膨脹係數(1/℃)
C:係數(其中,C=0.5~4.0)
ΔD:自室溫升溫至溫度T時之背板與自室溫升溫至溫度T
1時之濺鍍靶材之熱膨脹量之差(mm)
此處,於形態(3)中,若同樣地進行研究,將背板1自室溫升溫至使背板熱膨脹之溫度T,則背板1之按壓面彼此之距離以由(D
BP×ΔT×CTE
BP)求出之長度熱膨脹。又,由於濺鍍靶材2保持室溫不變,故而濺鍍靶材2之接觸面彼此之距離不熱膨脹。如此,若藉由僅將背板1升溫至溫度T而使其熱膨脹,則背板1之按壓面彼此之距離以由(D
BP×ΔT×CTE
BP)求出之長度熱膨脹,藉由背板1之按壓面彼此之距離相較於濺鍍靶材2之接觸面彼此之距離熱膨脹,能夠將濺鍍靶材2嵌入至背板1之按壓面之內側。而且,若降溫至室溫,則根據(數6)所示之關係,由背板1之按壓面按壓濺鍍靶材2之接觸面。於上述形態(3)中,為了能夠由背板1之按壓面按壓濺鍍靶材2之接觸面,必須藉由背板1之熱膨脹,將背板1之按壓面彼此之距離與濺鍍靶材2之接觸面彼此之距離反轉。因此,表示可以將室溫下之背板1之按壓面彼此之距離設定為較室溫下之濺鍍靶材2之接觸面彼此之距離小多少這一關係的是(數7)及(數9)。於(數7)及(數9)中,C為係數,當C為0.5~4.0之範圍內時,由背板1之按壓面按壓濺鍍靶材2之接觸面而將濺鍍靶材與背板接合,此時能夠抑制濺鍍靶材之破裂或翹曲。
[Relational Expression Including Linear Expansion Coefficient] (Different in ΔT(BP) and ΔT1(TG)) When pressing the contact surface of the
形態(2)由於是形態(1)與形態(3)之中間形態,故而同樣地由背板1之按壓面按壓濺鍍靶材2之接觸面。Since the form (2) is an intermediate form between the form (1) and the form (3), the contact surface of the
<濺鍍靶材-背板接合體之製造方法>
[製造方法之第1例]
(步驟1)
接下來,參照圖15,對圖2所示之濺鍍靶材-背板接合體100之製造方法進行說明。首先,如圖15(A)所示,準備背板1、及具備靶材表面7、與背板之板表面3相對之靶材背面8、外周側面9之濺鍍靶材2。接下來,如圖15(B)所示,於背板1形成板表面3、板背面4、板側面5、能形成鉤狀部6之程度之凸部13。作為背板1之形成方法,可藉由使用車床之切削加工等進行。再者,凸部13之內側之板表面亦作為板表面3。只要濺鍍靶材2與背板1可接合,則凸部13之內側之板表面3與凸部13之外側之板表面的高度可一致,亦可不同。接下來,如圖15(B)所示,考慮形成於背板1之凸部13之高度及寬度,將濺鍍靶材2之外周側面9之下部除去,直至形成於凸部13之鉤狀部6與形成於濺鍍靶材2之外周側面9之下部的鉤支承部10能夠抵接之程度。作為濺鍍靶材2之外周側面9之下部之除去方法,可藉由使用車床之切削加工等進行。再者,被除去之位置之外周亦作為外周側面9。接下來,如圖15(C)所示,於與濺鍍靶材2之外周側面9之下部相對之位置,在形成於背板1之凸部13形成鉤狀部6。鉤狀部6之形成可藉由使用車床之切削加工等進行。再者,凸部13之鉤狀部6可相對於濺鍍靶材2之外周側面9全周地設置,只要濺鍍靶材2不會自背板1剝離,則亦可相對於濺鍍靶材2之外周側面9局部地設置。接下來,如圖15(C)所示,在能與形成於背板1之凸部13之鉤狀部6抵接之位置,於濺鍍靶材2之外周側面9之下部形成鉤支承部10。鉤支承部10之形成可藉由使用車床之切削加工等進行。再者,濺鍍靶材2之鉤支承部10可於濺鍍靶材2之外周側面9全周地設置,只要濺鍍靶材2不會自背板1剝離,則亦可於濺鍍靶材2之外周側面9局部地設置,但必須設置於與鉤狀部6抵接之位置。
<Method for producing sputtering target-back plate assembly>
[The first example of the manufacturing method]
(step 1)
Next, with reference to FIG. 15, the manufacturing method of the sputtering target material-
(步驟2)
接下來,如圖15(D)所示,加熱背板1使其熱膨脹,直至能將濺鍍靶材2之外周側面9之下部插入於背板1之鉤狀部6的內側之程度。此時,只要達到將濺鍍靶材2之外周側面9之下部插入於背板1之鉤狀部6的內側之目的,則亦可於加熱背板1時,對濺鍍靶材2進行加熱。加熱例如可藉由熱壓燒結法(HP)、熱均壓燒結法(HIP)、放電電漿燒結法(SPS)或利用加熱板之加熱法等進行。再者,於背板1與濺鍍靶材2之界面設置中間層時,較佳為於圖15(D)之步驟內或圖15(D)之步驟之前後進行,換言之,較佳為於圖15(C)與圖15(D)之間之步驟、進行圖15(D)期間或圖15(D)與圖15(E)之間之步驟中形成中間層(圖15中未示出)。
(step 2)
Next, as shown in FIG. 15(D) , the
(步驟3)
接下來,如圖15(E)所示,將濺鍍靶材2之外周側面9之下部插入於背板1之鉤狀部6的內側,將濺鍍靶材2之靶材背面8與背板1之板表面3合併,以濺鍍靶材2之鉤支承部10與背板1之鉤狀部6相對之方式進行配置。此時,只要背板1之鉤狀部6及濺鍍靶材2之鉤支承部10不發生變形,則亦可自濺鍍靶材2之靶材表面7朝向背板1施加按壓。
(step 3)
Next, as shown in FIG. 15(E), the lower part of the outer
(步驟4)
接下來,如圖15(F)所示,將背板1冷卻使其熱收縮,而使濺鍍靶材2之鉤支承部10與背板1之鉤狀部6抵接,藉此抑制濺鍍靶材2之側面方向之移動,並且抑制濺鍍靶材2之厚度方向之移動,故而能夠確保背板1與濺鍍靶材2之接合強度。關於冷卻,例如可於藉由熱壓燒結法(HP)、熱均壓燒結法(HIP)、放電電漿燒結法(SPS)或利用加熱板之加熱法等調整溫度之同時進行冷卻,但亦可停止藉由熱壓燒結法(HP)、熱均壓燒結法(HIP)、放電電漿燒結法(SPS)或利用加熱板之加熱法等進行之加熱而自然冷卻。
(step 4)
Next, as shown in FIG. 15(F), the
(步驟4之後之附加步驟)
再者,欲進一步確保背板1與濺鍍靶材2之密接性時,亦可於步驟4之後,將自濺鍍靶材2之靶材表面7對背板1之按壓或者濺鍍靶材2及背板1之加熱與自濺鍍靶材2之靶材表面7對背板1之按壓這一步驟、以及濺鍍靶材2與背板1之冷卻步驟作為1組而進行1次或重複進行2次以上。又,對背板1之凸部13之位置、濺鍍靶材2之外周側面9之下部之除去量、鉤狀部6之位置、鉤支承部10之位置等進行調整,可自背板1之鉤狀部6側向濺鍍靶材2之鉤支承部10側施加按壓,亦可自濺鍍靶材2之靶材背面8對背板1之板表面3施加按壓。
(Additional step after step 4)
Furthermore, to further ensure the adhesion between the
[製造方法之第2例]
(步驟1)
接下來,參照圖16,對圖8所示之濺鍍靶材-背板接合體201之製造方法進行說明。本實施方式之濺鍍靶材-背板接合體201之製造方法首先如圖16(A)所示,準備具備板表面3、板背面4及板側面5之背板1、具備靶材表面7、與板表面3相對之靶材背面8、及外周側面9之濺鍍靶材2、以及卡子14。接下來,如圖16(B)所示,考慮固定於背板1之卡子14之高度及寬度,將濺鍍靶材2之外周側面9之下部除去,直至形成於卡子14之鉤狀部6與形成於濺鍍靶材2之外周側面9之下部的鉤支承部10能夠抵接之程度。作為濺鍍靶材2之外周側面9之下部之除去方法,可藉由使用車床之切削加工等進行。再者,上述被除去之位置之外周亦作為外周側面9。接下來,考慮使形成於卡子14之鉤狀部6與形成於濺鍍靶材之外周側面9之下部的鉤支承部10抵接,將卡子14固定於背板1之板表面3。作為將卡子14固定於背板1之板表面3之方法,除了藉由螺固進行之固定以外,還可藉由擴散接合、熔接等接合方法進行。接下來,如圖16(C)所示,於與濺鍍靶材2之外周側面9之下部相對之位置,在固定於背板1之卡子14上形成鉤狀部6。鉤狀部6之形成可藉由使用車床之切削加工等進行。再者,卡子14之鉤狀部6可相對於濺鍍靶材2之外周側面9全周地設置,只要濺鍍靶材2不會自背板1剝離,則亦可相對於濺鍍靶材2之外周側面9局部地設置。接下來,如圖16(C)所示,在能與固定於背板1之卡子14之鉤狀部6抵接之位置,於濺鍍靶材2之外周側面9之下部形成鉤支承部10。鉤支承部10之形成可藉由使用車床之切削加工等進行。再者,濺鍍靶材2之鉤支承部10可於濺鍍靶材2之外周側面9全周地設置,只要濺鍍靶材2不會自背板1剝離,則亦可於濺鍍靶材2之外周側面9局部地設置,但必須設置於與卡子14之鉤狀部6抵接之位置。
[The second example of the manufacturing method]
(step 1)
Next, with reference to FIG. 16, the manufacturing method of the sputtering target material-
(步驟2)
接下來,如圖16(D)所示,加熱背板1使其熱膨脹,直至能夠將濺鍍靶材2之外周側面9之下部插入於設置在背板1之卡子14之鉤狀部6的內側之程度。此時,只要達到將濺鍍靶材2之外周側面9之下部插入於設置在背板1之卡子14之鉤狀部6的內側之目的,則亦可於加熱背板1時,對濺鍍靶材2進行加熱。加熱例如可藉由熱壓燒結法(HP)、熱均壓燒結法(HIP)、放電電漿燒結法(SPS)或利用加熱板之加熱法等進行。再者,於背板1與濺鍍靶材2之界面設置中間層時,較佳為於圖16(D)之步驟內或圖16(D)之步驟之前後進行,換言之,較佳為於圖16(C)與圖16(D)之間之步驟、進行圖16(D)期間或圖16(D)與圖16(E)之間之步驟中形成中間層(圖16中未示出)。
(step 2)
Next, as shown in FIG. 16(D) , the
(步驟3)
接下來,如圖16(E)所示,將濺鍍靶材2之外周側面9之下部插入於設置在背板1之卡子14之鉤狀部6的內側,將濺鍍靶材2之靶材背面8與背板1之板表面3合併,以濺鍍靶材2之鉤支承部10與設置於背板1之卡子14之鉤狀部6相對的方式進行配置。此時,只要設置於背板1之卡子14之鉤狀部6及濺鍍靶材2之鉤支承部10不發生變形,則亦可自濺鍍靶材2之靶材表面7朝向背板1施加按壓。
(step 3)
Next, as shown in FIG. 16(E), the lower part of the outer
(步驟4)
接下來,如圖16(F)所示,將背板1冷卻使其熱收縮,而使濺鍍靶材2之鉤支承部10與設置於背板1之卡子14之鉤狀部6抵接,藉此抑制濺鍍靶材2之側面方向之移動,並且抑制濺鍍靶材2之厚度方向之移動,故而能夠確保背板1與濺鍍靶材2之接合強度。關於冷卻,例如可於藉由熱壓燒結法(HP)、熱均壓燒結法(HIP)、放電電漿燒結法(SPS)或利用加熱板之加熱法等調整溫度之同時進行冷卻,但亦可停止藉由熱壓燒結法(HP)、熱均壓燒結法(HIP)、放電電漿燒結法(SPS)或利用加熱板之加熱法等進行之加熱而自然冷卻。
(step 4)
Next, as shown in FIG. 16(F), the
(步驟4之後之附加步驟)
再者,欲進一步確保背板1與濺鍍靶材2之密接性時,亦可於步驟4之後,將自濺鍍靶材2之靶材表面7對背板1之按壓或者濺鍍靶材2及背板1之加熱與自濺鍍靶材2之靶材表面7對背板1之按壓這一步驟、以及濺鍍靶材2與背板1之冷卻步驟作為1組而進行1次或重複進行2次以上。又,對背板1之卡子14之位置、濺鍍靶材2之外周側面9之下部之除去量、鉤狀部6之位置、鉤支承部10之位置等進行調整,可自設置於背板1之卡子14之鉤狀部6側向濺鍍靶材2之鉤支承部10側施加按壓,亦可自濺鍍靶材2之靶材背面8對背板1之板表面3施加按壓。
(Additional step after step 4)
Furthermore, to further ensure the adhesion between the
[製造方法之第3例]
(步驟1)
接下來,參照圖17,對圖8所示之濺鍍靶材-背板接合體201之製造方法之另一形態進行說明。本實施方式之濺鍍靶材-背板接合體201之製造方法首先如圖17(A)所示,準備具備板表面3、板背面4及板側面5之背板1、具備靶材表面7、與上述板表面3相對之靶材背面8、外周側面9之濺鍍靶材2、以及卡子14。接下來,如圖17(B)所示,考慮固定於背板1之卡子14之高度及寬度,將濺鍍靶材2之外周側面9之下部除去,直至形成於卡子14之鉤狀部6與形成於濺鍍靶材2之外周側面9之下部的鉤支承部10能夠抵接之程度。作為濺鍍靶材2之外周側面9之下部之除去方法,可藉由使用車床之切削加工等進行。再者,上述被除去之位置之外周亦作為外周側面9。接下來,於與濺鍍靶材2之外周側面9之下部相對之位置,在固定於背板1之卡子14上形成鉤狀部6。鉤狀部6之形成可藉由使用車床之切削加工等進行。再者,卡子14之鉤狀部6可相對於濺鍍靶材2之外周側面9全周地設置,只要濺鍍靶材2不會自背板1剝離,則亦可相對於濺鍍靶材2之外周側面9局部地設置。接下來,如圖17(C)所示,在能與固定於背板1之卡子14之鉤狀部6抵接之位置,於濺鍍靶材2之外周側面9之下部形成鉤支承部10。鉤支承部10之形成可藉由使用車床之切削加工等進行。再者,濺鍍靶材2之鉤支承部10可於濺鍍靶材2之外周側面9全周地設置,只要濺鍍靶材2不會自背板1剝離,則亦可於濺鍍靶材2之外周側面9局部地設置,但必須設置於與卡子14之鉤狀部6抵接之位置。接下來,如圖17(C)所示,考慮使形成於卡子14之鉤狀部6與形成於濺鍍靶材2之外周側面9之下部的鉤支承部10抵接,將卡子14固定於背板1之板表面3。作為將卡子14固定於背板1之板表面3之方法,除了藉由螺固進行之固定以外,還可藉由擴散接合、熔接等接合方法進行。
[The third example of the manufacturing method]
(step 1)
Next, with reference to FIG. 17, another form of the manufacturing method of the sputtering target material-
(步驟2)
接下來,如圖17(D)所示,加熱背板1使其熱膨脹,直至能夠將濺鍍靶材2之外周側面9之下部插入於設置在背板1之卡子14之鉤狀部6的內側之程度。此時,只要達到將濺鍍靶材2之外周側面9之下部插入於設置在背板1之卡子14之鉤狀部6的內側之目的,則亦可於加熱背板1時,對濺鍍靶材2進行加熱。加熱例如可藉由熱壓燒結法(HP)、熱均壓燒結法(HIP)、放電電漿燒結法(SPS)或利用加熱板之加熱法等進行。再者,於背板1與濺鍍靶材2之界面設置中間層時,較佳為於圖17(D)之步驟內或圖17(D)之步驟之前後進行,換言之,較佳為於圖17(C)與圖17(D)之間之步驟、進行圖17(D)期間或圖17(D)與圖17(E)之間之步驟中形成中間層(圖17中未示出)。
(step 2)
Next, as shown in FIG. 17(D) , the
(步驟3)
接下來,如圖17(E)所示,將濺鍍靶材2之外周側面9之下部插入於設置在背板1之卡子14之鉤狀部6的內側,將濺鍍靶材2之靶材背面8與背板1之板表面3合併,以濺鍍靶材2之鉤支承部10與設置於背板1之卡子14之鉤狀部6相對的方式進行配置。此時,只要設置於背板1之卡子14之鉤狀部6及濺鍍靶材2之鉤支承部10不發生變形,則亦可自濺鍍靶材2之靶材表面7朝向背板1施加按壓。
(step 3)
Next, as shown in FIG. 17(E), the lower part of the outer
(步驟4)
接下來,如圖17(F)所示,將背板1冷卻使其熱收縮,而使濺鍍靶材2之鉤支承部10與設置於背板1之卡子14之鉤狀部6抵接,藉此抑制濺鍍靶材2之側面方向之移動,並且抑制濺鍍靶材2之厚度方向之移動,故而能夠確保背板1與濺鍍靶材2之接合強度。關於冷卻,例如可於藉由熱壓燒結法(HP)、熱均壓燒結法(HIP)、放電電漿燒結法(SPS)或利用加熱板之加熱法等調整溫度之同時進行冷卻,但亦可停止藉由熱壓燒結法(HP)、熱均壓燒結法(HIP)、放電電漿燒結法(SPS)或利用加熱板之加熱法等進行之加熱而自然冷卻。
(step 4)
Next, as shown in FIG. 17(F) , the
(步驟4之後之附加步驟)
再者,欲進一步確保背板1與濺鍍靶材2之密接性時,亦可於步驟4之後,將自濺鍍靶材2之靶材表面7對背板1之按壓或者濺鍍靶材2及背板1之加熱與自濺鍍靶材2之靶材表面7對背板1之按壓這一步驟、以及濺鍍靶材2與背板1之冷卻步驟作為1組而進行1次或重複進行2次以上。又,對背板1之卡子14之位置、濺鍍靶材2之外周側面9之下部之除去量、鉤狀部6之位置、鉤支承部10之位置等進行調整,可自設置於背板1之卡子14之鉤狀部6側向濺鍍靶材2之鉤支承部10側施加按壓,亦可自濺鍍靶材2之靶材背面8對背板1之板表面3施加按壓。
(Additional step after step 4)
Furthermore, to further ensure the adhesion between the
[製造方法之第4例]
(步驟1)
接下來,參照圖18,對圖7所示之濺鍍靶材-背板接合體200之製造方法進行說明。本實施方式之濺鍍靶材-背板接合體200之製造方法首先如圖18(A)所示,準備具備板表面3、板背面4及板側面5之背板1、具備靶材表面7、與上述板表面3相對之靶材背面8、外周側面9之濺鍍靶材2、以及卡子14。接下來,如圖18(B)所示,考慮將濺鍍靶材2之外周側面9之下部固定於背板1之卡子14的高度及寬度,將濺鍍靶材2之外周側面9之下部除去,直至形成於卡子14之鉤狀部6與形成於濺鍍靶材2之外周側面9之下部的鉤支承部10能夠抵接之程度。作為濺鍍靶材2之外周側面9之下部之除去方法,可藉由使用車床之切削加工等進行。再者,上述被除去之位置之外周亦作為外周側面9。接下來,如圖18(C)所示,於與濺鍍靶材2之外周側面9之下部相對之位置,在固定於背板1之卡子14上形成鉤狀部6。卡子14之鉤狀部6之形成可藉由使用車床之切削加工等進行。再者,卡子14之鉤狀部6可相對於濺鍍靶材2之外周側面9全周地設置,只要濺鍍靶材2不會自背板1剝離,則亦可相對於濺鍍靶材2之外周側面9局部地設置。接下來,如圖18(C)所示,在能與固定於背板1之卡子14之鉤狀部6抵接之位置,於濺鍍靶材2之外周側面9之下部形成鉤支承部10。鉤支承部10之形成可藉由使用車床之切削加工等進行。再者,濺鍍靶材2之鉤支承部10可於濺鍍靶材2之外周側面9全周地設置,只要濺鍍靶材2不會自背板1剝離,則亦可於濺鍍靶材2之外周側面9局部地設置,但必須設置於與卡子14之鉤狀部6抵接之位置。
[The 4th example of the manufacturing method]
(step 1)
Next, with reference to FIG. 18, the manufacturing method of the sputtering target material-
(步驟2)
如圖18(C)所示,以板表面3與靶材背面8相對之方式配置濺鍍靶材2與背板1。
(step 2)
As shown in FIG. 18(C) , the
(步驟3)
接下來,如圖18(D)所示,使形成於卡子14之鉤狀部6與形成於濺鍍靶材2之外周側面9之下部的鉤支承部10抵接。接下來,如圖18(E)所示,將卡子14配置於板表面3,且以鉤支承部10與鉤狀部6相對之方式配置濺鍍靶材2與卡子14。
(step 3)
Next, as shown in FIG. 18(D) , the
(步驟4)
接下來,於圖18(E)中,以步驟3之配置狀態將卡子14固定於背板1之板表面3,藉此抑制濺鍍靶材2之側面方向之移動,並且抑制濺鍍靶材2之厚度方向之移動,故而能夠確保背板1與濺鍍靶材2之接合強度。作為將卡子14固定於背板1之板表面3之方法,除了藉由螺固進行之固定以外,還可藉由擴散接合、熔接等接合方法進行。
(step 4)
Next, in FIG. 18(E), the
(步驟4之後之附加步驟)
再者,欲進一步確保背板1與濺鍍靶材2之密接性時,亦可於步驟4之後,將自濺鍍靶材2之靶材表面7對背板1之按壓或者濺鍍靶材2及背板1之加熱與自濺鍍靶材2之靶材表面7對背板1之按壓之步驟、以及濺鍍靶材2與背板1之冷卻步驟作為1組而進行1次或重複進行2次以上。
(Additional step after step 4)
Furthermore, to further ensure the adhesion between the
[製造方法之第5例]
(步驟1)
接下來,參照圖19,對具有與圖7所示之濺鍍靶材-背板接合體200類似之構造的接合體202之製造方法進行說明。本實施方式之濺鍍靶材-背板接合體202之製造方法首先如圖19(A)所示,準備具備板表面3、板背面4及板側面5之背板1、具備靶材表面7、與上述板表面3相對之靶材背面8、外周側面9之濺鍍靶材2、以及卡子14。此時,卡子14之底部設為能夠覆蓋濺鍍靶材2之靶材背面8之形狀。接下來,如圖19(B)所示,考慮將濺鍍靶材2之外周側面9之下部固定於背板1之卡子14的高度及寬度,將濺鍍靶材2之外周側面9之下部除去,直至形成於卡子14之鉤狀部6與形成於濺鍍靶材2之外周側面9之下部的鉤支承部10能夠抵接之程度。作為濺鍍靶材2之外周側面9之下部之除去方法,可藉由使用車床之切削加工等進行。再者,上述被除去之位置之外周亦作為外周側面9。接下來,如圖19(C)所示,於與濺鍍靶材2之外周側面9之下部相對之位置,在固定於背板1之卡子14上形成鉤狀部6。鉤狀部6之形成可藉由使用車床之切削加工等進行。再者,卡子14之鉤狀部6可相對於濺鍍靶材2之外周側面9全周地設置,只要濺鍍靶材2不會自背板1剝離,則亦可相對於濺鍍靶材2之外周側面9局部地設置。接下來,如圖19(C)所示,在能與固定於背板1之卡子14之鉤狀部6抵接之位置,於濺鍍靶材2之外周側面9之下部形成鉤支承部10。鉤支承部10之形成可藉由使用車床之切削加工等進行。再者,濺鍍靶材2之鉤支承部10可於濺鍍靶材2之外周側面9全周地設置,只要濺鍍靶材2不會自背板1剝離,則亦可於濺鍍靶材2之外周側面9局部地設置,但必須設置於與卡子14之鉤狀部6抵接之位置。
[The 5th example of the manufacturing method]
(step 1)
Next, with reference to FIG. 19, the manufacturing method of the joined
(步驟2)
如圖19(C)所示,以板表面3與靶材背面8相對之方式配置濺鍍靶材2與背板1。
(step 2)
As shown in FIG. 19(C) , the
(步驟3)
接下來,如圖19(D)所示,使形成於卡子14之鉤狀部6與形成於濺鍍靶材2之外周側面9之下部的鉤支承部10抵接。此時,較佳為覆蓋濺鍍靶材2之靶材背面8之卡子14之底部與濺鍍靶材2的背面8抵接。接下來,如圖19(E)所示,將卡子14配置於板表面3,且以鉤支承部10與鉤狀部6相對之方式配置濺鍍靶材2與卡子14。
(step 3)
Next, as shown in FIG. 19(D) , the
(步驟4)
接下來,於圖19(E)中,以步驟3之配置狀態將卡子14固定於背板1之板表面3,藉此抑制濺鍍靶材2之側面方向之移動,並且抑制濺鍍靶材2之厚度方向之移動,故而能夠確保背板1與濺鍍靶材2之接合強度。作為將卡子14固定於背板1之板表面3之方法,除了藉由螺固進行之固定以外,還可藉由擴散接合、熔接等接合方法進行。
(step 4)
Next, in FIG. 19(E), the
(步驟4之後之附加步驟)
再者,欲進一步確保背板1與濺鍍靶材2之密接性時,亦可於步驟4之後,將自濺鍍靶材2之靶材表面7對背板1之按壓或者濺鍍靶材2及背板1之加熱與自濺鍍靶材2之靶材表面7對背板1之按壓這一步驟、以及濺鍍靶材2與背板1之冷卻步驟作為1組而進行1次或重複進行2次以上。
(Additional step after step 4)
Furthermore, to further ensure the adhesion between the
[製造方法之第6例]
(步驟1)
接下來,參照圖20,對圖9所示之濺鍍靶材-背板接合體300之製造方法進行說明。本實施方式之濺鍍靶材-背板接合體300之製造方法首先如圖20(A)所示,準備具備板表面3、板背面4、板側面5之背板1、及具備靶材表面7、與背板之板表面3相對之靶材背面8、外周側面9之濺鍍靶材2。接下來,如圖20(B)所示,形成用於將濺鍍靶材2之靶材背面8嵌入至背板1之板表面3之具有凹部底面15與凹部側面16的凹部17。此時,背板1之凹部底面15之大小必須考慮形成於背板1之凹部側面16之鉤狀部6的寬度。作為背板1之凹部17之形成方法,可藉由使用車床之切削加工等進行。再者,於將背板1與濺鍍靶材2固定時,背板1之凹部底面15與濺鍍靶材2之靶材背面8抵接為佳。接下來,如圖20(B)所示,考慮背板1之凹部側面16之高度及形成於背板1之凹部側面16之鉤狀部6的寬度,將濺鍍靶材2之外周側面9之下部除去,直至形成於背板1之凹部側面16之鉤狀部6與形成於濺鍍靶材2之外周側面9之下部的鉤支承部10能夠抵接之程度。作為濺鍍靶材2之外周側面9之下部之除去方法,可藉由使用車床之切削加工等進行。再者,上述被除去之位置之外周亦作為外周側面9。接下來,如圖20(C)所示,於與濺鍍靶材2之外周側面9之下部相對之位置,在背板1之凹部側面16形成鉤狀部6。鉤狀部6之形成可藉由使用車床之切削加工等進行。再者,背板1之凹部側面16之鉤狀部6可相對於濺鍍靶材2之外周側面9全周地設置,只要濺鍍靶材2不會自背板1剝離,則亦可相對於濺鍍靶材2之外周側面9局部地設置。接下來,如圖20(C)所示,在能與背板1之凹部側面16之鉤狀部6抵接之位置,於濺鍍靶材2之外周側面9之下部形成鉤支承部10。鉤支承部10之形成可藉由使用車床之切削加工等進行。再者,濺鍍靶材2之鉤支承部10可於濺鍍靶材2之外周側面9全周地設置,只要濺鍍靶材2不會自背板1剝離,則亦可於濺鍍靶材2之外周側面9局部地設置,但必須設置於與上述鉤狀部6抵接之位置。
[The sixth example of the manufacturing method]
(step 1)
Next, with reference to FIG. 20, the manufacturing method of the sputtering target material-
(步驟2)
接下來,如圖20(D)所示,加熱背板1使其熱膨脹,直至能將濺鍍靶材2之外周側面9之下部插入於背板1之鉤狀部6的內側之程度。此時,只要達到將濺鍍靶材2之外周側面9之下部插入於背板1之鉤狀部6的內側之目的,則亦可於加熱背板1時,對濺鍍靶材2進行加熱。加熱例如可藉由熱壓燒結法(HP)、熱均壓燒結法(HIP)、放電電漿燒結法(SPS)或利用加熱板之加熱法等進行。再者,於背板1與濺鍍靶材2之界面設置中間層時,較佳為於圖20(D)之步驟內或圖20(D)之步驟之前後進行,換言之,較佳為於圖20(C)與圖20(D)之間之步驟、進行圖20(D)期間或圖20(D)與圖20(E)之間之步驟中形成中間層(圖20中未示出)。
(step 2)
Next, as shown in FIG. 20(D) , the
(步驟3)
接下來,如圖20(E)所示,將濺鍍靶材2之外周側面9之下部插入於背板1之鉤狀部6的內側,將濺鍍靶材2之靶材背面8與背板1之凹部底面15合併,以濺鍍靶材2之鉤支承部10與背板1之鉤狀部6相對之方式進行配置。此時,只要背板1之鉤狀部6及濺鍍靶材2之鉤支承部10不發生變形,則亦可自濺鍍靶材2之靶材表面7朝向背板1施加按壓。
(step 3)
Next, as shown in FIG. 20(E), the lower part of the outer
(步驟4)
接下來,如圖20(F)所示,將背板1冷卻使其熱收縮,而使濺鍍靶材2之鉤支承部10與背板1之鉤狀部6抵接,藉此抑制濺鍍靶材2之側面方向之移動,並且抑制濺鍍靶材2之厚度方向之移動,故而能夠確保背板1與濺鍍靶材2之接合強度。關於冷卻,例如可於藉由熱壓燒結法(HP)、熱均壓燒結法(HIP)、放電電漿燒結法(SPS)或利用加熱板之加熱法等調整溫度之同時進行冷卻,但亦可停止藉由熱壓燒結法(HP)、熱均壓燒結法(HIP)、放電電漿燒結法(SPS)或利用加熱板之加熱法等進行之加熱而自然冷卻。
(step 4)
Next, as shown in FIG. 20(F), the
(步驟4之後之附加步驟)
再者,欲進一步確保背板1與濺鍍靶材2之密接性時,亦可於步驟4之後,將自濺鍍靶材2之靶材表面7對背板1之按壓或者濺鍍靶材2及背板1之加熱與自濺鍍靶材2之靶材表面7對背板1之按壓這一步驟、以及濺鍍靶材2與背板1之冷卻步驟作為1組而進行1次或重複進行2次以上。又,對背板1之凹部底面15之大小、濺鍍靶材2之外周側面9之下部之除去量、鉤狀部6之位置、鉤支承部10之位置等進行調整,可自背板1之鉤狀部6側向濺鍍靶材2之鉤支承部10側施加按壓,亦可自濺鍍靶材2之靶材背面8對背板1之凹部底面15施加按壓。
(Additional step after step 4)
Furthermore, to further ensure the adhesion between the
[製造方法之第7例]
(步驟1)
接下來,參照圖21,對具有與圖9所示之濺鍍靶材-背板接合體300類似之構造且使用卡子14的接合體301之製造方法進行說明。本實施方式之濺鍍靶材-背板接合體301之製造方法首先如圖21(A)所示,準備具備板表面3、板背面4、板側面5之背板1、具備靶材表面7、與背板1之板表面3相對之靶材背面8、外周側面9之濺鍍靶材2、以及卡子14。接下來,如圖21(B)所示,形成用於將濺鍍靶材2之靶材背面8嵌入至背板1之板表面3之具有凹部底面15與凹部側面16的凹部17。此時,背板1之凹部底面15之大小必須考慮卡子14之寬度。作為背板1之凹部17之形成方法,可藉由使用車床之切削加工等進行。再者,於將背板1與濺鍍靶材2固定時,背板1之凹部底面15與濺鍍靶材2之靶材背面8抵接為佳。接下來,如圖21(B)所示,考慮背板1之凹部側面16之高度、固定於背板1之凹部底面15或凹部側面16之卡子14之高度及寬度,將濺鍍靶材2之外周側面9之下部除去,直至在固定於背板1之凹部17之卡子14上形成之鉤狀部6與形成於濺鍍靶材2之外周側面9之下部的鉤支承部10能夠抵接之程度。作為濺鍍靶材2之外周側面9之下部之除去方法,可藉由使用車床之切削加工等進行。再者,上述被除去之位置之外周亦作為外周側面9。接下來,如圖21(B)所示,於與濺鍍靶材2之外周側面9之下部相對之位置,在固定於背板1之凹部底面15或凹部側面16之卡子14上形成鉤狀部6。鉤狀部6之形成可藉由使用車床之切削加工等進行。再者,卡子14之鉤狀部6可相對於濺鍍靶材2之外周側面9全周地設置,只要濺鍍靶材2不會自背板1剝離,則亦可相對於濺鍍靶材2之外周側面9局部地設置。接下來,如圖21(C)所示,在能與固定於背板1之凹部底面15或凹部側面16之卡子14上形成的鉤狀部6抵接之位置,於濺鍍靶材2之外周側面9之下部形成鉤支承部10。鉤支承部10之形成可藉由使用車床之切削加工等進行。再者,濺鍍靶材2之鉤支承部10可於濺鍍靶材2之外周側面9全周地設置,只要濺鍍靶材2不會自背板1剝離,則亦可於濺鍍靶材2之外周側面9局部地設置,但必須設置於與卡子14之鉤狀部6抵接之位置。接下來,考慮使形成於卡子14之鉤狀部6與形成於濺鍍靶材2之外周側面9之下部的鉤支承部10抵接,將卡子14固定於背板1之凹部底面15或凹部側面16。作為將卡子14固定於背板1之凹部底面15或凹部側面16之方法,除了藉由螺固進行之固定以外,還可藉由擴散接合、熔接等接合方法進行。
[The seventh example of the manufacturing method]
(step 1)
Next, referring to FIG. 21 , a description will be given of a method of manufacturing a joined
(步驟2)
接下來,如圖21(D)所示,加熱背板1使其熱膨脹,直至能夠將濺鍍靶材2之外周側面9之下部插入於設置在背板1之卡子14之鉤狀部6的內側之程度。此時,只要達到將濺鍍靶材2之外周側面9之下部插入於設置在背板1之卡子14之鉤狀部6的內側之目的,則亦可於加熱背板1時,對濺鍍靶材2進行加熱。加熱例如可藉由熱壓燒結法(HP)、熱均壓燒結法(HIP)、放電電漿燒結法(SPS)或利用加熱板之加熱法等進行。再者,於背板1與濺鍍靶材2之界面設置中間層時,較佳為於圖21(D)之步驟內或圖21(D)之步驟之前後進行,換言之,較佳為於圖21(C)與圖21(D)之間之步驟、進行圖21(D)期間或圖21(D)與圖21(E)之間之步驟中形成中間層(圖21中未示出)。
(step 2)
Next, as shown in FIG. 21(D), the
(步驟3)
接下來,如圖21(E)所示,將濺鍍靶材2之外周側面9之下部插入於設置在背板1之卡子14之鉤狀部6的內側,將濺鍍靶材2之靶材背面8與背板1之凹部底面15合併,以濺鍍靶材2之鉤支承部10與設置於背板1之卡子14之鉤狀部6相對的方式進行配置。此時,只要設置於背板1之卡子14之鉤狀部6及濺鍍靶材2之鉤支承部10不發生變形,則亦可自濺鍍靶材2之靶材表面7朝向背板1施加按壓。
(step 3)
Next, as shown in FIG. 21(E), the lower part of the outer
(步驟4)
接下來,如圖21(F)所示,將背板1冷卻使其熱收縮,而使濺鍍靶材2之鉤支承部10與設置於背板1之卡子14之鉤狀部6抵接,藉此抑制濺鍍靶材2之側面方向之移動,並且抑制濺鍍靶材2之厚度方向之移動,故而能夠確保背板1與濺鍍靶材2之接合強度。關於冷卻,例如可於藉由熱壓燒結法(HP)、熱均壓燒結法(HIP)、放電電漿燒結法(SPS)或利用加熱板之加熱法等調整溫度之同時進行冷卻,但亦可停止藉由熱壓燒結法(HP)、熱均壓燒結法(HIP)、放電電漿燒結法(SPS)或利用加熱板之加熱法等進行之加熱而自然冷卻。
(step 4)
Next, as shown in FIG. 21(F) , the
(步驟4之後之附加步驟)
再者,欲進一步確保背板1與濺鍍靶材2之密接性時,亦可於步驟4之後,將自濺鍍靶材2之靶材表面7對背板1之按壓或者濺鍍靶材2及背板1之加熱與自濺鍍靶材2之靶材表面7對背板1之按壓這一步驟、以及濺鍍靶材2與背板1之冷卻步驟作為1組而進行1次或重複進行2次以上。又,對背板1之凹部底面15之大小、濺鍍靶材2之外周側面9之下部之除去量、鉤狀部6之位置、鉤支承部10之位置等進行調整,可自設置於背板1之卡子14之鉤狀部6側向濺鍍靶材2之鉤支承部10側施加按壓,亦可自濺鍍靶材2之靶材背面8對背板1之凹部底面15施加按壓。
(Additional step after step 4)
Furthermore, to further ensure the adhesion between the
[製造方法之第8例]
(步驟1)
接下來,參照圖22,對具有與圖10所示之濺鍍靶材-背板接合體400類似之構造且不使用卡子的接合體401之製造方法進行說明。本實施方式之濺鍍靶材-背板接合體401之製造方法首先如圖22(A)所示,準備具備板表面3、板背面4、板側面5之背板1、及具備靶材表面7、與背板之板表面3相對之靶材背面8、外周側面9之濺鍍靶材2。接下來,如圖22(B)所示,形成用於將濺鍍靶材2之靶材背面8嵌入至背板1之板表面3之具有凹部底面15與凹部側面16的凹部17。此時,背板1之凹部底面15之大小必須考慮形成於背板1之凹部側面16之鉤狀部6的寬度。作為背板1之凹部17之形成方法,可藉由使用車床之切削加工等進行。再者,於將背板1與濺鍍靶材2固定時,背板1之凹部底面15與濺鍍靶材2之靶材背面8抵接為佳。接下來,如圖22(C)所示,於與濺鍍靶材2之外周側面9之下部相對之位置,在背板1之凹部側面16形成鉤狀部6。鉤狀部6之形成可藉由使用車床之切削加工等進行。再者,背板1之凹部側面16之鉤狀部6可相對於濺鍍靶材2之外周側面9全周地設置,只要濺鍍靶材2不會自背板1剝離,則亦可相對於濺鍍靶材2之外周側面9局部地設置。接下來,如圖22(C)所示,在能與背板1之凹部側面16之鉤狀部6抵接之位置,於濺鍍靶材2之外周側面9之下部形成鉤支承部10。鉤支承部10之形成可藉由使用車床之切削加工等進行。再者,濺鍍靶材2之鉤支承部10可於濺鍍靶材2之外周側面9全周地設置,只要濺鍍靶材2不會自背板1剝離,則亦可於濺鍍靶材2之外周側面9局部地設置,但必須設置於與上述鉤狀部6抵接之位置。
[The 8th example of the manufacturing method]
(step 1)
Next, referring to FIG. 22 , a description will be given of a method of manufacturing a joined
(步驟2)
接下來,如圖22(D)所示,加熱背板1使其熱膨脹,直至能將濺鍍靶材2之外周側面9之下部插入於背板1之鉤狀部6的內側之程度。此時,只要達到將濺鍍靶材2之外周側面9之下部插入於背板1之鉤狀部6的內側之目的,則亦可於加熱背板1時,對濺鍍靶材2進行加熱。加熱例如可藉由熱壓燒結法(HP)、熱均壓燒結法(HIP)、放電電漿燒結法(SPS)或利用加熱板之加熱法等進行。再者,於背板1與濺鍍靶材2之界面設置中間層時,較佳為於圖22(D)之步驟內或圖22(D)之步驟之前後進行,換言之,較佳為於圖22(C)與圖22(D)之間之步驟、進行圖22(D)期間或圖22(D)與圖22(E)之間之步驟中形成中間層(圖22中未示出)。
(step 2)
Next, as shown in FIG. 22(D) , the
(步驟3)
接下來,如圖22(E)所示,將濺鍍靶材2之外周側面9之下部插入於背板1之鉤狀部6的內側,將濺鍍靶材2之靶材背面8與背板1之凹部底面15合併,以濺鍍靶材2之鉤支承部10與背板1之鉤狀部6相對之方式進行配置。此時,只要背板1之鉤狀部6及濺鍍靶材2之鉤支承部10不發生變形,則亦可自濺鍍靶材2之靶材表面7朝向背板1施加按壓。
(step 3)
Next, as shown in FIG. 22(E), the lower part of the outer
(步驟4)
接下來,如圖22(F)所示,將背板1冷卻使其熱收縮,而使濺鍍靶材2之鉤支承部10與背板1之鉤狀部6抵接,藉此抑制濺鍍靶材2之側面方向之移動,並且抑制濺鍍靶材2之厚度方向之移動,故而能夠確保背板1與濺鍍靶材2之接合強度。關於冷卻,例如可於藉由熱壓燒結法(HP)、熱均壓燒結法(HIP)、放電電漿燒結法(SPS)或利用加熱板之加熱法等調整溫度之同時進行冷卻,但亦可停止藉由熱壓燒結法(HP)、熱均壓燒結法(HIP)、放電電漿燒結法(SPS)或利用加熱板之加熱法等進行之加熱而自然冷卻。
(step 4)
Next, as shown in FIG. 22(F) , the
(步驟4之後之附加步驟)
再者,欲進一步確保背板1與濺鍍靶材2之密接性時,亦可於步驟4之後,將自濺鍍靶材2之靶材表面7對背板1之按壓或者濺鍍靶材2及背板1之加熱與自濺鍍靶材2之靶材表面7對背板1之按壓這一步驟、以及濺鍍靶材2與背板1之冷卻步驟作為1組而進行1次或重複進行2次以上。又,對背板1之凹部底面15之大小、鉤狀部6之位置、鉤支承部10之位置等進行調整,可自背板1之鉤狀部6側向濺鍍靶材2之鉤支承部10側施加按壓,亦可自濺鍍靶材2之靶材背面8對背板1之凹部底面15施加按壓。
(Additional step after step 4)
Furthermore, to further ensure the adhesion between the
[製造方法之第9例]
(步驟1)
接下來,參照圖23,對圖10所示之濺鍍靶材-背板接合體400之製造方法進行說明。本實施方式之濺鍍靶材-背板接合體400之製造方法首先如圖23(A)所示,準備具備板表面3、板背面4、板側面5之背板1、具備靶材表面7、與背板之板表面3相對之靶材背面8、外周側面9之濺鍍靶材2、以及卡子14。接下來,如圖23(B)所示,形成用於將濺鍍靶材2之靶材背面8嵌入至背板1之板表面3之具有凹部底面15與凹部側面16的凹部17。此時,背板1之凹部底面15之大小必須考慮卡子14之寬度。作為背板1之凹部17之形成方法,可藉由使用車床之切削加工等進行。再者,於將背板1與濺鍍靶材2固定時,背板1之凹部底面15與濺鍍靶材2之靶材背面8抵接為佳。接下來,如圖23(B)所示,於與濺鍍靶材2之外周側面9之下部相對之位置,在固定於背板1之凹部底面15或凹部側面16之卡子14上形成鉤狀部6。鉤狀部6之形成可藉由使用車床之切削加工等進行。再者,卡子14之鉤狀部6可相對於濺鍍靶材2之外周側面9全周地設置,只要濺鍍靶材2不會自背板1剝離,則亦可相對於濺鍍靶材2之外周側面9局部地設置。接下來,如圖23(B)所示,在能與固定於背板1之凹部底面15或凹部側面16之卡子14上形成的鉤狀部6抵接之位置,於濺鍍靶材2之外周側面9之下部形成鉤支承部10。鉤支承部10之形成可藉由使用車床之切削加工等進行。再者,濺鍍靶材2之鉤支承部10可於濺鍍靶材2之外周側面9全周地設置,只要濺鍍靶材2不會自背板1剝離,則亦可於濺鍍靶材2之外周側面9局部地設置,但必須設置於與卡子14之鉤狀部6抵接之位置。接下來,如圖23(C)所示,考慮使形成於卡子14之鉤狀部6與形成於濺鍍靶材之外周側面9之下部的鉤支承部10抵接,將卡子14固定於背板1之凹部底面15或凹部側面16。作為將卡子14固定於背板1之凹部底面15或凹部側面16之方法,除了藉由螺固進行之固定以外,還可藉由擴散接合、熔接等接合方法進行。
[The ninth example of the manufacturing method]
(step 1)
Next, with reference to FIG. 23, the manufacturing method of the sputtering target material-
(步驟2)
接下來,如圖23(D)所示,加熱背板1使其熱膨脹,直至能夠將濺鍍靶材2之外周側面9之下部插入於設置在背板1之卡子14之鉤狀部6的內側之程度。此時,只要達到將濺鍍靶材2之外周側面9之下部插入於設置在背板1之卡子14之鉤狀部6的內側之目的,則亦可於加熱背板1時,對濺鍍靶材2進行加熱。加熱例如可藉由熱壓燒結法(HP)、熱均壓燒結法(HIP)、放電電漿燒結法(SPS)或利用加熱板之加熱法等進行。再者,於背板1與濺鍍靶材2之界面設置中間層時,較佳為於圖23(D)之步驟內或圖23(D)之步驟之前後進行,換言之,較佳為於圖23(C)與圖23(D)之間之步驟、進行圖23(D)期間或圖23(D)與圖23(E)之間之步驟中形成中間層(圖23中未示出)。
(step 2)
Next, as shown in FIG. 23(D) , the
(步驟3)
接下來,如圖23(E)所示,將濺鍍靶材2之外周側面9之下部插入於設置在背板1之卡子14之鉤狀部6的內側,將濺鍍靶材2之靶材背面8與背板1之凹部底面15合併,以濺鍍靶材2之鉤支承部10與設置於背板1之卡子14之鉤狀部6相對的方式進行配置。此時,只要設置於背板1之卡子14之鉤狀部6及濺鍍靶材2之鉤支承部10不發生變形,則亦可自濺鍍靶材2之靶材表面7朝向背板1施加按壓。
(step 3)
Next, as shown in FIG. 23(E), the lower part of the outer
(步驟4)
接下來,如圖23(F)所示,將背板1冷卻使其熱收縮,而使濺鍍靶材2之鉤支承部10與設置於背板1之卡子14之鉤狀部6抵接,藉此抑制濺鍍靶材2之側面方向之移動,並且抑制濺鍍靶材2之厚度方向之移動,故而能夠確保背板1與濺鍍靶材2之接合強度。關於冷卻,例如可於藉由熱壓燒結法(HP)、熱均壓燒結法(HIP)、放電電漿燒結法(SPS)或利用加熱板之加熱法等調整溫度之同時進行冷卻,但亦可停止藉由熱壓燒結法(HP)、熱均壓燒結法(HIP)、放電電漿燒結法(SPS)或利用加熱板之加熱法等進行之加熱而自然冷卻。
(step 4)
Next, as shown in FIG. 23(F), the
(步驟4之後之附加步驟)
再者,欲進一步確保背板1與濺鍍靶材2之密接性時,亦可於步驟4之後,將自濺鍍靶材2之靶材表面7對背板1之按壓或者濺鍍靶材2及背板1之加熱與自濺鍍靶材2之靶材表面7對背板1之按壓這一步驟、以及濺鍍靶材2與背板1之冷卻步驟作為1組而進行1次或重複進行2次以上。又,對背板1之凹部底面15之大小、濺鍍靶材2之外周側面9之下部之除去量、鉤狀部6之位置、鉤支承部10之位置等進行調整,可自設置於背板1之卡子14之鉤狀部6側向濺鍍靶材2之鉤支承部10側施加按壓,亦可自濺鍍靶材2之靶材背面8對背板1之凹部底面15施加按壓。
(Additional step after step 4)
Furthermore, to further ensure the adhesion between the
[製造方法之第10例]
(步驟1)
接下來,參照圖24,對圖10所示之濺鍍靶材-背板接合體400之製造方法之另一形態進行說明。本實施方式之濺鍍靶材-背板接合體400之製造方法首先如圖24(A)所示,準備具備板表面3、板背面4及板側面5之背板1、具備靶材表面7、與上述板表面3相對之靶材背面8、外周側面9之濺鍍靶材2、以及卡子14。接下來,如圖24(B)所示,形成用於將濺鍍靶材2之靶材背面8嵌入至背板1之板表面3之具有凹部底面15與凹部側面16的凹部17。此時,背板1之凹部底面15之大小必須考慮卡子14之寬度。作為背板1之凹部17之形成方法,可藉由使用車床之切削加工等進行。再者,於將背板1與濺鍍靶材2固定時,背板1之凹部底面15與濺鍍靶材2之靶材背面8抵接為佳。接下來,如圖24(B)所示,以與濺鍍靶材2之外周側面9相對之方式在固定於背板1之卡子14上形成鉤狀部6。卡子14之鉤狀部6之形成可藉由使用車床之切削加工等進行。再者,卡子14之鉤狀部6可相對於濺鍍靶材2之外周側面9全周地設置,只要濺鍍靶材2不會自背板1剝離,則亦可相對於濺鍍靶材2之外周側面9局部地設置。接下來,如圖24(B)所示,在能與固定於背板1之卡子14之鉤狀部6抵接之位置,於濺鍍靶材2之外周側面9形成鉤支承部10。鉤支承部10之形成可藉由使用車床之切削加工等進行。再者,濺鍍靶材2之鉤支承部10可於濺鍍靶材2之外周側面9全周地設置,只要濺鍍靶材2不會自背板1剝離,則亦可於濺鍍靶材2之外周側面9局部地設置,但必須設置於與卡子14之鉤狀部6抵接之位置。
[The tenth example of the manufacturing method]
(step 1)
Next, with reference to FIG. 24, another aspect of the manufacturing method of the sputtering target material-
(步驟2)
如圖24(C)所示,以板表面3與靶材背面8相對之方式配置濺鍍靶材2與背板1。
(step 2)
As shown in FIG. 24(C), the
(步驟3)
接下來,如圖24(C)所示,使形成於卡子14之鉤狀部6與形成於濺鍍靶材之外周側面9之下部的鉤支承部10抵接。接下來,如圖24(D)所示,將卡子14配置於板表面3,且以鉤支承部10與鉤狀部6相對之方式配置濺鍍靶材2與卡子14。
(step 3)
Next, as shown in FIG.24(C), the hook-shaped
(步驟4)
接下來,於圖24(D)中,以步驟3之配置狀態將卡子14固定於背板1之凹部底面15或凹部側面16,藉此抑制濺鍍靶材2之側面方向之移動,並且抑制濺鍍靶材2之厚度方向之移動,故而能夠確保背板1與濺鍍靶材2之接合強度。作為將卡子14固定於背板1之板表面3之方法,除了藉由螺固進行之固定以外,還可藉由擴散接合、熔接等接合方法進行。
(step 4)
Next, in FIG. 24(D), the
(步驟4之後之附加步驟)
再者,欲進一步確保背板1與濺鍍靶材2之密接性時,亦可於步驟4之後,將自濺鍍靶材2之靶材表面7對背板1之按壓或者濺鍍靶材2及背板1之加熱與自濺鍍靶材2之靶材表面7對背板1之按壓這一步驟、以及濺鍍靶材與背板之冷卻步驟作為1組而進行1次或重複進行2次以上。
(Additional step after step 4)
Furthermore, to further ensure the adhesion between the
[製造方法之第11例]
(步驟1)
接下來,參照圖25,對具有與圖10所示之濺鍍靶材-背板接合體400類似之構造的接合體402之製造方法進行說明。本實施方式之濺鍍靶材-背板接合體402之製造方法首先如圖25(A)所示,準備具備板表面3、板背面4及板側面5之背板1、具備靶材表面7、與上述板表面3相對之靶材背面8、外周側面9之濺鍍靶材2、以及卡子14。此時,卡子14之底部設為能夠覆蓋濺鍍靶材2之靶材背面8之形狀。接下來,如圖25(B)所示,形成用於將濺鍍靶材2之靶材背面8嵌入至背板1之板表面3之具有凹部底面15與凹部側面16的凹部17。此時,背板1之凹部底面15之大小必須考慮卡子14之寬度。作為背板1之凹部17之形成方法,可藉由使用車床之切削加工等進行。再者,於將背板1與濺鍍靶材2固定時,背板1之凹部底面15與濺鍍靶材2之靶材背面8抵接為佳。接下來,如圖25(B)所示,以與濺鍍靶材2之外周側面9相對之方式在固定於背板1之卡子14上形成鉤狀部6。卡子14之鉤狀部6之形成可藉由使用車床之切削加工等進行。再者,卡子14之鉤狀部6可相對於濺鍍靶材2之外周側面9全周地設置,只要濺鍍靶材2不會自背板1剝離,則亦可相對於濺鍍靶材2之外周側面9局部地設置。接下來,如圖25(B)所示,在能與固定於背板1之卡子14之鉤狀部6抵接之位置,於濺鍍靶材2之外周側面9之下部形成鉤支承部10。鉤支承部10之形成可藉由使用車床之切削加工等進行。再者,濺鍍靶材2之鉤支承部10可於濺鍍靶材2之外周側面9全周地設置,只要濺鍍靶材2不會自背板1剝離,則亦可於濺鍍靶材2之外周側面9局部地設置,但必須設置於與卡子14之鉤狀部6抵接之位置。
[The 11th example of the manufacturing method]
(step 1)
Next, with reference to FIG. 25 , a method of manufacturing a joined
(步驟2)
如圖25(C)所示,以板表面3與靶材背面8相對之方式配置濺鍍靶材2與背板1。
(step 2)
As shown in FIG. 25(C) , the
(步驟3)
接下來,如圖25(C)所示,使形成於卡子14之鉤狀部6與形成於濺鍍靶材之外周側面9之下部的鉤支承部10抵接。此時,較佳為覆蓋濺鍍靶材2之靶材背面8之卡子14之底部與濺鍍靶材2的背面8抵接。接下來,如圖25(D)所示,將卡子14配置於板表面3並將卡子14嵌入至凹部17,且以鉤支承部10與鉤狀部6相對之方式配置濺鍍靶材2與卡子14。
(step 3)
Next, as shown in FIG.25(C), the hook-shaped
(步驟4)
接下來,於圖25(D)中,以步驟3之配置狀態將卡子14固定於背板1之凹部底面15或凹部側面16,藉此抑制濺鍍靶材2之側面方向之移動,並且抑制濺鍍靶材2之厚度方向之移動,故而能夠確保背板1與濺鍍靶材2之接合強度。作為將卡子14固定於背板1之板表面3之方法,除了藉由螺固進行之固定以外,還可藉由擴散接合、熔接等接合方法進行。
(step 4)
Next, in FIG. 25(D), the
(步驟4之後之附加步驟)
再者,欲進一步確保背板1與濺鍍靶材2之密接性時,亦可於步驟4之後,將自濺鍍靶材2之靶材表面7對背板1之按壓或者濺鍍靶材2及背板1之加熱與自濺鍍靶材2之靶材表面7對背板1之按壓這一步驟、以及濺鍍靶材2與背板1之冷卻步驟作為1組而進行1次或重複進行2次以上。
(Additional step after step 4)
Furthermore, to further ensure the adhesion between the
(濺鍍靶材之回收方法之第1例)
對本實施方式之濺鍍靶材-背板接合體安裝於濺鍍裝置並使用,且濺鍍靶材被消耗之情形進行說明。本實施方式之濺鍍靶材之回收方法包括:步驟A,其係加熱本實施方式之濺鍍靶材-背板接合體,使其熱膨脹直至鉤狀部6離開鉤支承部10;及步驟B,其係自背板1卸除濺鍍靶材2,自濺鍍靶材-背板接合體回收濺鍍靶材。將濺鍍靶材2卸除之形態包括將濺鍍靶材2直接卸除之形態、及對濺鍍靶材2施加衝擊來卸除之形態。
(The first example of the recovery method of sputtering targets)
The case where the sputtering target-back plate assembly of the present embodiment is installed and used in a sputtering apparatus and the sputtering target is consumed will be described. The recovery method of the sputtering target material of this embodiment includes: step A, which is to heat the sputtering target material-back plate joint body of this embodiment to thermally expand until the hook-shaped
(濺鍍靶材之回收方法之第2例)
背板1上固定有卡子14之濺鍍靶材-背板接合體中之濺鍍靶材之回收方法包括自背板1卸除卡子14,自濺鍍靶材-背板接合體回收濺鍍靶材2之步驟C。卸除濺鍍靶材2之形態中,包括直接卸除濺鍍靶材2之形態、及對濺鍍靶材2施加衝擊而卸除之形態。
[實施例]
(The second example of the recovery method of sputtering targets)
The method for recovering the sputtering target material in the sputtering target material with the
以下,示出實施例,更詳細地對本發明進行說明,但本發明不限定於實施例來解釋。Hereinafter, although an Example is shown and this invention is demonstrated in detail, this invention is not limited to an Example, and should be interpreted.
(實施例1)
製作與圖9相當之接合體。首先,準備利用熔解法製作之Φ156×9t(單位:mm)之釕濺鍍靶材2、及Φ240×20t(單位:mm)之黃銅之背板1。關於線膨脹係數,釕為6.75×10
-6/℃,黃銅為21.2×10
-6/℃。接下來,利用車床,於濺鍍靶材2之外周側面9沿著側面之圓周方向形成成為鉤支承部10之0.5 mm之環狀凹部。藉此,於濺鍍靶材2之外周側面9形成以環狀凹部之底面為基準而凸出之環狀凸部。接下來,於背板1之設置濺鍍靶材2之位置,利用車床加工出較濺鍍靶材2之直徑小0.4 mm且深度為4 mm之凹部17。進而,在與濺鍍靶材2之鉤狀部6相對應之位置之背板的凹部內周側面16形成0.5 mm之鉤支承部10。接下來,於背板1之凹部底面15填充厚度為0.1 mm的Ni之板材及微量之In粉末。該微量之In粉末填充於Ni之板材周圍之間隙。接下來,於背板1之凹部17之上設置濺鍍靶材2。接下來,使用放電電漿燒結機於10 Pa以下之減壓氣體氛圍下升溫至250℃後,將濺鍍靶材2填充於背板之凹部17。填充後,以10 MPa自濺鍍靶材2之靶材表面7加壓,並且進一步升溫至400℃,保持1小時進行擴散接合,之後冷卻而進行抵接。將其結果示於圖26。接合體具有濺鍍靶材2之外周側面9之凹凸部分與背板1之凹部內周側面16之凹凸部分相互嵌入的構造。如圖26所示,濺鍍靶材2之外周側面9與背板1之凹部17之內周側面16藉由抵接而固定,靶材背面8亦無間隙地由Ni、In填充,熱傳導良好地進行擴散接合,並且不發生濺鍍靶材2之破裂。
(Example 1) A joined body corresponding to FIG. 9 was produced. First, a
(比較例1)
準備撓曲強度為138 MPa之Φ70×7t(單位:mm)之Al-30原子%之Sc濺鍍靶材、及Φ80×8t(單位:mm)之Al合金即A6061之背板。關於線膨脹係數,Al-30原子%之Sc為13.5×10
-6/℃,A6061為23.6×10
-6/℃。接下來,於背板1上設置Al-30原子%之Sc濺鍍靶材。接下來,使用放電電漿燒結機於真空氣體氛圍下升溫至500℃後,以10 MPa自濺鍍靶材之靶材表面加壓,並且保持1小時進行擴散接合。將其結果示於圖27。如圖27所示,濺鍍靶材與背板雖被接合,但線膨脹係數之差較大,因此,背板冷卻時,濺鍍靶材受到壓縮之應力而破裂。
(Comparative Example 1) A flexural strength of 138 MPa was prepared as a Φ70×7t (unit: mm) Al-30 atomic % Sc sputtering target, and a Φ80×8t (unit: mm) Al alloy, namely the back of A6061 plate. Regarding the coefficient of linear expansion, Sc in Al-30 atomic % was 13.5×10 -6 /°C, and A6061 was 23.6×10 -6 /°C. Next, an Al-30 atomic % Sc sputtering target is set on the
(比較例2)
準備撓曲強度為138 MPa之Φ70×7t(單位:mm)之Al-30原子%之Sc濺鍍靶材、及Φ80×8t(單位:mm)之Al合金即鋁青銅之背板。關於線膨脹係數,Al-30原子%之Sc為13.5×10
-6/℃,鋁青銅為16.5×10
-6/℃。接下來,於背板1上設置Al-30原子%之Sc濺鍍靶材。接下來,使用放電電漿燒結機於真空氣體氛圍下升溫至500℃後,以10 MPa自濺鍍靶材之靶材表面加壓,並且保持1小時進行擴散接合。將其結果示於圖28。如圖28所示,雖試圖使濺鍍靶材之線膨脹係數與背板之線膨脹係數相較於比較例1更接近,但仍存在濺鍍靶材與背板之線膨脹係數之差,因此,濺鍍靶材2受到壓縮之應力而破裂,並且於背板上之接合不充分,故而濺鍍靶材自背板剝離。
(Comparative Example 2) A flexural strength of 138 MPa, Φ70×7t (unit: mm), Al-30 atomic % Sc sputtering target, and Φ80×8t (unit: mm) Al alloy, that is, aluminum bronze were prepared. backplane. Regarding the coefficient of linear expansion, Sc of Al-30 atomic % is 13.5×10 -6 /°C, and aluminum bronze is 16.5×10 -6 /°C. Next, an Al-30 atomic % Sc sputtering target is set on the
(比較例3) 利用燒結法準備Φ194×10t(單位:mm)之釕濺鍍靶材、及Φ240×20t(單位:mm)之無氧銅之背板。關於線膨脹係數,釕為6.75×10 -6/℃,無氧銅為16.2×10 -6/℃。接下來,於背板上設置釕濺鍍靶材。接下來,使用放電電漿燒結機於真空氣體氛圍下升溫至700℃後,以10 MPa自濺鍍靶材之靶材表面加壓,並且保持1小時進行擴散接合。將其結果示於圖29。如圖29所示,存在濺鍍靶材與背板之線膨脹係數之差,因此,濺鍍靶材受到壓縮之應力而破裂。 (Comparative Example 3) A ruthenium sputtering target of Φ194×10t (unit: mm) and an oxygen-free copper backplate of Φ240×20t (unit: mm) were prepared by a sintering method. Regarding the coefficient of linear expansion, ruthenium was 6.75×10 -6 /°C, and oxygen-free copper was 16.2×10 -6 /°C. Next, a ruthenium sputtering target is set on the backing plate. Next, the temperature was raised to 700° C. in a vacuum atmosphere using a spark plasma sintering machine, and then the target surface of the sputtering target was pressurized at 10 MPa and held for 1 hour to perform diffusion bonding. The results are shown in FIG. 29 . As shown in FIG. 29 , there is a difference between the linear expansion coefficients of the sputtering target and the backing plate, so that the sputtering target is cracked due to compressive stress.
(比較例4)
利用燒結法準備Φ180×5t(單位:mm)之釕濺鍍靶材及背板,該背板係在由無氧銅製作之被稱為CAN之厚度15 mm之容器上形成有Φ180.1 mm且深度10 mm之凹部者。關於線膨脹係數,釕為6.75×10
-6/℃,無氧銅為16.2×10
-6/℃。接下來,將濺鍍靶材內包於CAN後,自其上將由無氧銅製作之Φ180×5t之蓋放置於濺鍍靶材之上,將CAN內真空密封。接下來,使用HIP裝置升溫至500℃後,以100 MPa對CAN加壓而進行擴散接合。此時,容器之所有面受到加壓,容器與濺鍍靶材擴散接合。擴散接合後,使用車床對濺鍍靶材2及背板進行切削。將其結果示於圖30。如圖30所示,發生了擴散接合,但存在濺鍍靶材與背板之線膨脹係數之差,因此,濺鍍靶材受到壓縮之應力,自中央部向外周呈放射狀出現細小之裂痕而破裂。
(Comparative Example 4) A ruthenium sputtering target of Φ180×5t (unit: mm) and a backing plate were prepared by the sintering method. The backing plate was formed on a container with a thickness of 15 mm called CAN made of oxygen-free copper. Those with a concave portion of Φ180.1 mm and a depth of 10 mm. Regarding the coefficient of linear expansion, ruthenium was 6.75×10 -6 /°C, and oxygen-free copper was 16.2×10 -6 /°C. Next, after wrapping the sputtering target in the CAN, a Φ180×5t cover made of oxygen-free copper was placed on the sputtering target, and the CAN was vacuum-sealed. Next, after the temperature was raised to 500° C. using a HIP apparatus, the CAN was pressurized at 100 MPa to perform diffusion bonding. At this time, all surfaces of the container are pressurized, and the container and the sputtering target are diffusion bonded. After the diffusion bonding, the
1:背板 2:濺鍍靶材 3:背板之板表面 4:背板之板背面 5:背板之側面 6:鉤狀部 7:濺鍍靶材之靶材表面 8:濺鍍靶材之靶材背面 9:濺鍍靶材之外周側面 10:鉤支承部 11:螺固位置 12:中間層 12a:設置於與背板之界面之中間層 12b:設置於與濺鍍靶材之界面之中間層 13:設置於背板之板表面之凸部 14:卡子 15:背板之凹部底面 16:背板之凹部側面 17:凹部 50:濺鍍靶材-背板接合體 60:濺鍍靶材-背板接合體 100:濺鍍靶材-背板接合體 101:濺鍍靶材-背板接合體 200:濺鍍靶材-背板接合體 201:濺鍍靶材-背板接合體 202:濺鍍靶材-背板接合體 300:濺鍍靶材-背板接合體 301:濺鍍靶材-背板接合體 400:濺鍍靶材-背板接合體 401:濺鍍靶材-背板接合體 402:濺鍍靶材-背板接合體 500:濺鍍靶材-背板接合體 501:濺鍍靶材-背板接合體 600:濺鍍靶材-背板接合體 601:濺鍍靶材-背板接合體 1: Backplane 2: Sputtering target 3: The surface of the backplane 4: The back of the board of the backplane 5: The side of the back panel 6: Hook part 7: Target surface of sputtering target 8: The back of the target of the sputtering target 9: Outer peripheral side of sputtering target 10: Hook support part 11: Screw position 12: middle layer 12a: The intermediate layer at the interface with the backplane 12b: interlayer disposed at the interface with the sputtering target 13: The convex part on the surface of the back plate 14: clip 15: The bottom surface of the concave part of the back plate 16: The side of the concave part of the back plate 17: Recess 50: Sputtering target-back plate joint 60: Sputtering target-back plate joint 100: Sputtering target-back plate joint 101: Sputtering target-back plate joint 200: Sputtering target-back plate joint 201: Sputtering target-backplane joint 202: Sputtering target-backplate joint 300: Sputtering target-back plate joint 301: Sputtering target-back plate joint 400: Sputtering target-back plate joint 401: Sputtering target-back plate joint 402: Sputtering target-back plate joint 500: Sputtering target-back plate joint 501: Sputtering target-backplane joint 600: Sputtering target-backplane joint 601: Sputtering target-backplane joint
圖1係本實施方式之圓板狀之濺鍍靶材-背板接合體之俯視概略圖。 圖2係圖1之第1例之A-A剖面概略圖,表示形態1-1。 圖2(A)係由圖2之虛線所包圍之部分之另一形態(1)之概略圖。 圖2(B)係由圖2之虛線所包圍之部分之另一形態(2)之概略圖。 圖2(C)係由圖2之虛線所包圍之部分之另一形態(3)之概略圖。 圖2(D)係由圖2之虛線所包圍之部分之另一形態(4)之概略圖。 圖2(E)係由圖2之虛線所包圍之部分之另一形態(5)之概略圖。 圖2(F)係由圖2之虛線所包圍之部分之另一形態(6)之概略圖。 圖2(G)係由圖2之虛線所包圍之部分之另一形態(7)之概略圖。 圖2(H)係由圖2之虛線所包圍之部分之另一形態(8)之概略圖。 圖2(I)係由圖2之虛線所包圍之部分之另一形態(9)之概略圖。 圖2(J)係由圖2之虛線所包圍之部分之另一形態(10)之概略圖。 圖2(K)係由圖2之虛線所包圍之部分之另一形態(11)之概略圖。 圖2(L)係由圖2之虛線所包圍之部分之另一形態(12)之概略圖。 圖2(M)係由圖2之虛線所包圍之部分之另一形態(13)之概略圖。 圖2(N)係由圖2之虛線所包圍之部分之另一形態(14)之概略圖。 圖3係本實施方式之長方形板狀之濺鍍靶材-背板接合體之俯視概略圖。 圖4係本實施方式之另一形態之圓板狀之濺鍍靶材-背板接合體的俯視概略圖。 圖5係圖4之第1例之A-A剖面概略圖,表示形態1-2。 圖5(A)係由圖5之虛線所包圍之部分之另一形態(1)之概略圖。 圖5(B)係由圖5之虛線所包圍之部分之另一形態(2)之概略圖。 圖5(C)係由圖5之虛線所包圍之部分之另一形態(3)之概略圖。 圖5(D)係由圖5之虛線所包圍之部分之另一形態(4)之概略圖。 圖5(E)係由圖5之虛線所包圍之部分之另一形態(5)之概略圖。 圖5(F)係由圖5之虛線所包圍之部分之另一形態(6)之概略圖。 圖5(G)係由圖5之虛線所包圍之部分之另一形態(7)之概略圖。 圖5(H)係由圖5之虛線所包圍之部分之另一形態(8)之概略圖。 圖5(I)係由圖5之虛線所包圍之部分之另一形態(9)之概略圖。 圖5(J)係由圖5之虛線所包圍之部分之另一形態(10)之概略圖。 圖5(K)係由圖5之虛線所包圍之部分之另一形態(11)之概略圖。 圖5(L)係由圖5之虛線所包圍之部分之另一形態(12)之概略圖。 圖6係本實施方式之另一形態之長方形板狀之濺鍍靶材-背板接合體的俯視概略圖。 圖7係形態2-1之剖面概略圖。 圖7(A)係由圖7之虛線所包圍之部分之另一形態(1)之概略圖。 圖7(B)係由圖7之虛線所包圍之部分之另一形態(2)之概略圖。 圖7(C)係由圖7之虛線所包圍之部分之另一形態(3)之概略圖。 圖7(D)係由圖7之虛線所包圍之部分之另一形態(4)之概略圖。 圖7(E)係由圖7之虛線所包圍之部分之另一形態(5)之概略圖。 圖7(F)係由圖7之虛線所包圍之部分之另一形態(6)之概略圖。 圖7(G)係由圖7之虛線所包圍之部分之另一形態(7)之概略圖。 圖7(H)係由圖7之虛線所包圍之部分之另一形態(8)之概略圖。 圖7(I)係由圖7之虛線所包圍之部分之另一形態(9)之概略圖。 圖7(J)係由圖7之虛線所包圍之部分之另一形態(10)之概略圖。 圖7(K)係由圖7之虛線所包圍之部分之另一形態(11)之概略圖。 圖7(L)係由圖7之虛線所包圍之部分之另一形態(12)之概略圖。 圖7(M)係由圖7之虛線所包圍之部分之另一形態(13)之概略圖。 圖7(N)係由圖7之虛線所包圍之部分之另一形態(14)之概略圖。 圖8係形態3-1之剖面概略圖。 圖8(A)係由圖8之虛線所包圍之部分之另一形態(1)之概略圖。 圖8(B)係由圖8之虛線所包圍之部分之另一形態(2)之概略圖。 圖8(C)係由圖8之虛線所包圍之部分之另一形態(3)之概略圖。 圖8(D)係由圖8之虛線所包圍之部分之另一形態(4)之概略圖。 圖8(E)係由圖8之虛線所包圍之部分之另一形態(5)之概略圖。 圖8(F)係由圖8之虛線所包圍之部分之另一形態(6)之概略圖。 圖8(G)係由圖8之虛線所包圍之部分之另一形態(7)之概略圖。 圖8(H)係由圖8之虛線所包圍之部分之另一形態(8)之概略圖。 圖8(I)係由圖8之虛線所包圍之部分之另一形態(9)之概略圖。 圖8(J)係由圖8之虛線所包圍之部分之另一形態(10)之概略圖。 圖8(K)係由圖8之虛線所包圍之部分之另一形態(11)之概略圖。 圖8(L)係由圖8之虛線所包圍之部分之另一形態(12)之概略圖。 圖8(M)係由圖8之虛線所包圍之部分之另一形態(13)之概略圖。 圖8(N)係由圖8之虛線所包圍之部分之另一形態(14)之概略圖。 圖9係形態4-1之剖面概略圖。 圖9(A)係由圖9之虛線所包圍之部分之另一形態(1)之概略圖。 圖9(B)係由圖9之虛線所包圍之部分之另一形態(2)之概略圖。 圖9(C)係由圖9之虛線所包圍之部分之另一形態(3)之概略圖。 圖9(D)係由圖9之虛線所包圍之部分之另一形態(4)之概略圖。 圖9(E)係由圖9之虛線所包圍之部分之另一形態(5)之概略圖。 圖9(F)係由圖9之虛線所包圍之部分之另一形態(6)之概略圖。 圖9(G)係由圖9之虛線所包圍之部分之另一形態(7)之概略圖。 圖9(H)係由圖9之虛線所包圍之部分之另一形態(8)之概略圖。 圖9(I)係由圖9之虛線所包圍之部分之另一形態(9)之概略圖。 圖9(J)係由圖9之虛線所包圍之部分之另一形態(10)之概略圖。 圖9(K)係由圖9之虛線所包圍之部分之另一形態(11)之概略圖。 圖9(L)係由圖9之虛線所包圍之部分之另一形態(12)之概略圖。 圖9(M)係由圖9之虛線所包圍之部分之另一形態(13)之概略圖。 圖9(N)係由圖9之虛線所包圍之部分之另一形態(14)之概略圖。 圖10係形態5-1之剖面概略圖。 圖10(A)係由圖10之虛線所包圍之部分之另一形態(1)之概略圖。 圖10(B)係由圖10之虛線所包圍之部分之另一形態(2)之概略圖。 圖10(C)係由圖10之虛線所包圍之部分之另一形態(3)之概略圖。 圖10(D)係由圖10之虛線所包圍之部分之另一形態(4)之概略圖。 圖10(E)係由圖10之虛線所包圍之部分之另一形態(5)之概略圖。 圖10(F)係由圖10之虛線所包圍之部分之另一形態(6)之概略圖。 圖10(G)係由圖10之虛線所包圍之部分之另一形態(7)之概略圖。 圖10(H)係由圖10之虛線所包圍之部分之另一形態(8)之概略圖。 圖10(I)係由圖10之虛線所包圍之部分之另一形態(9)之概略圖。 圖10(J)係由圖10之虛線所包圍之部分之另一形態(10)之概略圖。 圖10(K)係由圖10之虛線所包圍之部分之另一形態(11)之概略圖。 圖10(L)係由圖10之虛線所包圍之部分之另一形態(12)之概略圖。 圖10(M)係由圖10之虛線所包圍之部分之另一形態(13)之概略圖。 圖10(N)係由圖10之虛線所包圍之部分之另一形態(14)之概略圖。 圖11係形態6-1、形態7-1或形態8-1之剖面概略圖。 圖12係形態6-2、形態7-2或形態8-2之剖面概略圖。 圖13係形態9-1之剖面概略圖。 圖14係形態9-2之剖面概略圖。 圖15(A)~(F)係用於對本實施方式之濺鍍靶材-背板接合體之製造方法之第1例進行說明的概略步驟圖。 圖16(A)~(F)係用於對本實施方式之濺鍍靶材-背板接合體之製造方法之第2例進行說明的概略步驟圖。 圖17(A)~(F)係用於對本實施方式之濺鍍靶材-背板接合體之製造方法之第3例進行說明的概略步驟圖。 圖18(A)~(E)係用於對本實施方式之濺鍍靶材-背板接合體之製造方法之第4例進行說明的概略步驟圖。 圖19(A)~(E)係用於對本實施方式之濺鍍靶材-背板接合體之製造方法之第5例進行說明的概略步驟圖。 圖20(A)~(F)係用於對本實施方式之濺鍍靶材-背板接合體之製造方法之第6例進行說明的概略步驟圖。 圖21(A)~(F)係用於對本實施方式之濺鍍靶材-背板接合體之製造方法之第7例進行說明的概略步驟圖。 圖22(A)~(F)係用於對本實施方式之濺鍍靶材-背板接合體之製造方法之第8例進行說明的概略步驟圖。 圖23(A)~(F)係用於對本實施方式之濺鍍靶材-背板接合體之製造方法之第9例進行說明的概略步驟圖。 圖24(A)~(D)係用於對本實施方式之濺鍍靶材-背板接合體之製造方法之第10例進行說明的概略步驟圖。 圖25(A)~(D)係用於對本實施方式之濺鍍靶材-背板接合體之製造方法之第11例進行說明的概略步驟圖。 圖26係表示實施例1中之抵接部位之圖像。 圖27係表示比較例1中之接合結果之圖像。 圖28係表示比較例2中之接合結果之圖像。 圖29係表示比較例3中之接合結果之圖像。 圖30係表示比較例4中之接合結果之圖像。 FIG. 1 is a schematic plan view of a disk-shaped sputtering target-back plate assembly of the present embodiment. Fig. 2 is a schematic cross-sectional view taken along A-A of the first example of Fig. 1, showing a form 1-1. Fig. 2(A) is a schematic view of another form (1) of the portion surrounded by the dotted line in Fig. 2 . Fig. 2(B) is a schematic view of another form (2) of the portion surrounded by the dotted line in Fig. 2 . Fig. 2(C) is a schematic view of another form (3) of the portion surrounded by the dotted line in Fig. 2 . Fig. 2(D) is a schematic view of another form (4) of the portion surrounded by the dotted line in Fig. 2 . Fig. 2(E) is a schematic view of another form (5) of the portion surrounded by the dotted line in Fig. 2 . Fig. 2(F) is a schematic view of another form (6) of the portion surrounded by the dotted line in Fig. 2 . Fig. 2(G) is a schematic view of another form (7) of the portion surrounded by the dotted line in Fig. 2 . Fig. 2(H) is a schematic view of another form (8) of the portion surrounded by the dotted line in Fig. 2 . Fig. 2(I) is a schematic view of another form (9) of the portion surrounded by the dotted line in Fig. 2 . FIG. 2(J) is a schematic view of another form ( 10 ) of the portion surrounded by the dotted line in FIG. 2 . Fig. 2(K) is a schematic view of another form (11) of the portion surrounded by the dotted line in Fig. 2 . Fig. 2(L) is a schematic view of another form (12) of the portion surrounded by the dotted line in Fig. 2 . Fig. 2(M) is a schematic view of another form (13) of the portion surrounded by the dotted line in Fig. 2 . Fig. 2(N) is a schematic view of another form (14) of the portion surrounded by the dotted line in Fig. 2 . FIG. 3 is a schematic plan view of the sputtering target-back plate assembly in the form of a rectangular plate according to the present embodiment. FIG. 4 is a schematic plan view of a disk-shaped sputtering target-back plate assembly according to another aspect of the present embodiment. Fig. 5 is a schematic cross-sectional view taken along A-A of the first example of Fig. 4, and shows a form 1-2. Fig. 5(A) is a schematic view of another form (1) of the portion surrounded by the dotted line in Fig. 5 . Fig. 5(B) is a schematic view of another form (2) of the portion surrounded by the dotted line in Fig. 5 . Fig. 5(C) is a schematic view of another form (3) of the portion surrounded by the dotted line in Fig. 5 . Fig. 5(D) is a schematic view of another form (4) of the portion surrounded by the dotted line in Fig. 5 . Fig. 5(E) is a schematic view of another form (5) of the portion surrounded by the dotted line in Fig. 5 . Fig. 5(F) is a schematic view of another form (6) of the portion surrounded by the dotted line in Fig. 5 . Fig. 5(G) is a schematic view of another form (7) of the portion surrounded by the dotted line in Fig. 5 . Fig. 5(H) is a schematic view of another form (8) of the portion surrounded by the dotted line in Fig. 5 . Fig. 5(I) is a schematic view of another form (9) of the portion surrounded by the dotted line in Fig. 5 . Fig. 5(J) is a schematic view of another form (10) of the portion surrounded by the dotted line in Fig. 5 . Fig. 5(K) is a schematic view of another form (11) of the portion surrounded by the dotted line in Fig. 5 . Fig. 5(L) is a schematic view of another form (12) of the portion surrounded by the dotted line in Fig. 5 . FIG. 6 is a schematic plan view of a rectangular plate-shaped sputtering target-back plate assembly according to another aspect of the present embodiment. Fig. 7 is a schematic cross-sectional view of Form 2-1. Fig. 7(A) is a schematic view of another form (1) of the portion surrounded by the dotted line in Fig. 7 . Fig. 7(B) is a schematic view of another form (2) of the portion surrounded by the dotted line in Fig. 7 . Fig. 7(C) is a schematic view of another form (3) of the portion surrounded by the dotted line in Fig. 7 . Fig. 7(D) is a schematic view of another form (4) of the portion surrounded by the dotted line in Fig. 7 . Fig. 7(E) is a schematic view of another form (5) of the portion surrounded by the dotted line in Fig. 7 . Fig. 7(F) is a schematic view of another form (6) of the portion surrounded by the dotted line in Fig. 7 . Fig. 7(G) is a schematic view of another form (7) of the portion surrounded by the dotted line in Fig. 7 . Fig. 7(H) is a schematic view of another form (8) of the portion surrounded by the dotted line in Fig. 7 . Fig. 7(I) is a schematic view of another form (9) of the portion surrounded by the dotted line in Fig. 7 . Fig. 7(J) is a schematic view of another form (10) of the portion surrounded by the dotted line in Fig. 7 . Fig. 7(K) is a schematic view of another form (11) of the portion surrounded by the dotted line in Fig. 7 . Fig. 7(L) is a schematic view of another form (12) of the portion surrounded by the dotted line in Fig. 7 . Fig. 7(M) is a schematic view of another form (13) of the portion surrounded by the dotted line in Fig. 7 . Fig. 7(N) is a schematic view of another form (14) of the portion surrounded by the dotted line in Fig. 7 . Fig. 8 is a schematic cross-sectional view of Form 3-1. Fig. 8(A) is a schematic view of another form (1) of the portion surrounded by the dotted line in Fig. 8 . Fig. 8(B) is a schematic view of another form (2) of the portion surrounded by the dotted line in Fig. 8 . Fig. 8(C) is a schematic view of another form (3) of the portion surrounded by the dotted line in Fig. 8 . Fig. 8(D) is a schematic view of another form (4) of the portion surrounded by the dotted line in Fig. 8 . Fig. 8(E) is a schematic view of another form (5) of the portion surrounded by the dotted line in Fig. 8 . Fig. 8(F) is a schematic view of another form (6) of the portion surrounded by the dotted line in Fig. 8 . Fig. 8(G) is a schematic view of another form (7) of the portion surrounded by the dotted line in Fig. 8 . Fig. 8(H) is a schematic view of another form (8) of the portion surrounded by the dotted line in Fig. 8 . Fig. 8(I) is a schematic view of another form (9) of the portion surrounded by the dotted line in Fig. 8 . Fig. 8(J) is a schematic view of another form (10) of the portion surrounded by the dotted line in Fig. 8 . Fig. 8(K) is a schematic view of another form (11) of the portion surrounded by the dotted line in Fig. 8 . Fig. 8(L) is a schematic view of another form (12) of the portion surrounded by the dotted line in Fig. 8 . Fig. 8(M) is a schematic view of another form (13) of the portion surrounded by the dotted line in Fig. 8 . Fig. 8(N) is a schematic view of another form (14) of the portion surrounded by the dotted line in Fig. 8 . Fig. 9 is a schematic cross-sectional view of Form 4-1. Fig. 9(A) is a schematic view of another form (1) of the portion surrounded by the dotted line in Fig. 9 . Fig. 9(B) is a schematic view of another form (2) of the portion surrounded by the dotted line in Fig. 9 . Fig. 9(C) is a schematic view of another form (3) of the portion surrounded by the dotted line in Fig. 9 . Fig. 9(D) is a schematic view of another form (4) of the portion surrounded by the dotted line in Fig. 9 . Fig. 9(E) is a schematic view of another form (5) of the portion surrounded by the dotted line in Fig. 9 . Fig. 9(F) is a schematic view of another form (6) of the portion surrounded by the dotted line in Fig. 9 . Fig. 9(G) is a schematic view of another form (7) of the portion surrounded by the dotted line in Fig. 9 . Fig. 9(H) is a schematic view of another form (8) of the portion surrounded by the dotted line in Fig. 9 . Fig. 9(I) is a schematic view of another form (9) of the portion surrounded by the dotted line in Fig. 9 . Fig. 9(J) is a schematic view of another form (10) of the portion surrounded by the dotted line in Fig. 9 . Fig. 9(K) is a schematic view of another form (11) of the portion surrounded by the dotted line in Fig. 9 . Fig. 9(L) is a schematic view of another form (12) of the portion surrounded by the dotted line in Fig. 9 . Fig. 9(M) is a schematic view of another form (13) of the portion surrounded by the dotted line in Fig. 9 . Fig. 9(N) is a schematic view of another form (14) of the portion surrounded by the dotted line in Fig. 9 . Fig. 10 is a schematic cross-sectional view of Form 5-1. Fig. 10(A) is a schematic view of another form (1) of the portion surrounded by the dotted line in Fig. 10 . Fig. 10(B) is a schematic view of another form (2) of the portion surrounded by the dotted line in Fig. 10 . Fig. 10(C) is a schematic view of another form (3) of the portion surrounded by the dotted line in Fig. 10 . Fig. 10(D) is a schematic view of another form (4) of the portion surrounded by the dotted line in Fig. 10 . Fig. 10(E) is a schematic view of another form (5) of the portion surrounded by the dotted line in Fig. 10 . Fig. 10(F) is a schematic view of another form (6) of the portion surrounded by the dotted line in Fig. 10 . Fig. 10(G) is a schematic view of another form (7) of the portion surrounded by the dotted line in Fig. 10 . Fig. 10(H) is a schematic view of another form (8) of the portion surrounded by the dotted line in Fig. 10 . Fig. 10(I) is a schematic view of another form (9) of the portion surrounded by the dotted line in Fig. 10 . Fig. 10(J) is a schematic view of another form (10) of the portion surrounded by the dotted line in Fig. 10 . Fig. 10(K) is a schematic view of another form (11) of the portion surrounded by the dotted line in Fig. 10 . FIG. 10(L) is a schematic diagram of another form ( 12 ) of the portion surrounded by the dotted line in FIG. 10 . Fig. 10(M) is a schematic view of another form (13) of the portion surrounded by the dotted line in Fig. 10 . Fig. 10(N) is a schematic view of another form (14) of the portion surrounded by the dotted line in Fig. 10 . Fig. 11 is a schematic cross-sectional view of the form 6-1, the form 7-1 or the form 8-1. Fig. 12 is a schematic cross-sectional view of Form 6-2, Form 7-2 or Form 8-2. Fig. 13 is a schematic cross-sectional view of Form 9-1. Fig. 14 is a schematic cross-sectional view of Form 9-2. FIGS. 15(A) to (F) are schematic step diagrams for explaining the first example of the manufacturing method of the sputtering target material-back plate assembly of the present embodiment. FIGS. 16(A) to (F) are schematic process diagrams for explaining the second example of the method for producing the sputtering target-back plate assembly of the present embodiment. FIGS. 17(A) to (F) are schematic process diagrams for explaining the third example of the manufacturing method of the sputtering target-back plate assembly of the present embodiment. FIGS. 18(A) to (E) are schematic step diagrams for explaining a fourth example of the method for producing the sputtering target-back plate assembly of the present embodiment. FIGS. 19(A) to (E) are schematic step diagrams for explaining the fifth example of the method for producing the sputtering target-back plate assembly of the present embodiment. FIGS. 20(A) to (F) are schematic step diagrams for explaining the sixth example of the manufacturing method of the sputtering target-back plate assembly of the present embodiment. FIGS. 21(A) to (F) are schematic step diagrams for explaining a seventh example of the method for producing the sputtering target-back plate assembly of the present embodiment. FIGS. 22(A) to (F) are schematic step diagrams for explaining the eighth example of the manufacturing method of the sputtering target-back plate assembly of the present embodiment. FIGS. 23(A) to (F) are schematic process diagrams for explaining the ninth example of the manufacturing method of the sputtering target-back plate assembly of the present embodiment. FIGS. 24(A) to (D) are schematic step diagrams for explaining a tenth example of the manufacturing method of the sputtering target-back plate assembly of the present embodiment. FIGS. 25(A) to (D) are schematic process diagrams for explaining the eleventh example of the manufacturing method of the sputtering target material-back plate assembly of the present embodiment. FIG. 26 is an image showing the abutting portion in Example 1. FIG. FIG. 27 is an image showing the bonding result in Comparative Example 1. FIG. FIG. 28 is an image showing the bonding result in Comparative Example 2. FIG. FIG. 29 is an image showing the bonding result in Comparative Example 3. FIG. FIG. 30 is an image showing the bonding result in Comparative Example 4. FIG.
1:背板 1: Backplane
2:濺鍍靶材 2: Sputtering target
3:背板之板表面 3: The surface of the backplane
4:背板之板背面 4: The back of the board of the backplane
5:背板之側面 5: The side of the back panel
6:鉤狀部 6: Hook part
7:濺鍍靶材之靶材表面 7: Target surface of sputtering target
8:濺鍍靶材之靶材背面 8: The back of the target of the sputtering target
9:濺鍍靶材之外周側面 9: Outer peripheral side of sputtering target
10:鉤支承部 10: Hook support part
13:設置於背板之板表面之凸部 13: The convex part on the surface of the back plate
100:濺鍍靶材-背板接合體 100: Sputtering target-back plate joint
Claims (22)
Applications Claiming Priority (10)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2020-165872 | 2020-09-30 | ||
JP2020165872 | 2020-09-30 | ||
JP2020218600 | 2020-12-28 | ||
JP2020-218600 | 2020-12-28 | ||
JP2021013676 | 2021-01-29 | ||
JP2021-013676 | 2021-01-29 | ||
JP2021024010A JP7024128B1 (en) | 2020-09-30 | 2021-02-18 | Sputtering target-backing plate joint, its manufacturing method and recovery method of sputtering target |
JP2021-024010 | 2021-02-18 | ||
JP2021-144277 | 2021-09-03 | ||
JP2021144277A JP2022104518A (en) | 2020-12-28 | 2021-09-03 | Sputtering target-backing plate bonded body, method for manufacturing the same and method for collecting sputtering target |
Publications (1)
Publication Number | Publication Date |
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TW202225434A true TW202225434A (en) | 2022-07-01 |
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Family Applications (1)
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TW110135823A TW202225434A (en) | 2020-09-30 | 2021-09-27 | Sputtering target-backing plate assembly, production method therefor, and sputtering target recovery method |
Country Status (2)
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TW (1) | TW202225434A (en) |
WO (1) | WO2022070880A1 (en) |
Family Cites Families (3)
Publication number | Priority date | Publication date | Assignee | Title |
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JP2688243B2 (en) * | 1988-11-25 | 1997-12-08 | 東京エレクトロン株式会社 | Electrode structure |
JP6508774B2 (en) * | 2015-06-09 | 2019-05-08 | 株式会社高純度化学研究所 | Sputtering target assembly |
JP7033873B2 (en) * | 2017-09-20 | 2022-03-11 | Jx金属株式会社 | Sputtering target assembly and its manufacturing method |
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2021
- 2021-09-14 WO PCT/JP2021/033679 patent/WO2022070880A1/en active Application Filing
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