TW201906535A - candy - Google Patents

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Publication number
TW201906535A
TW201906535A TW107117326A TW107117326A TW201906535A TW 201906535 A TW201906535 A TW 201906535A TW 107117326 A TW107117326 A TW 107117326A TW 107117326 A TW107117326 A TW 107117326A TW 201906535 A TW201906535 A TW 201906535A
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extract
candy
present
peppermint
green tea
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TW107117326A
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Chinese (zh)
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藤原健太
藤原将平
山本雅
山下美保
湊孝文
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日商大正製藥股份有限公司
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Publication of TW201906535A publication Critical patent/TW201906535A/en

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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23GCOCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
    • A23G3/00Sweetmeats; Confectionery; Marzipan; Coated or filled products
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23GCOCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
    • A23G3/00Sweetmeats; Confectionery; Marzipan; Coated or filled products
    • A23G3/34Sweetmeats, confectionery or marzipan; Processes for the preparation thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/53Lamiaceae or Labiatae (Mint family), e.g. thyme, rosemary or lavender
    • A61K36/534Mentha (mint)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/82Theaceae (Tea family), e.g. camellia
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K47/00Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
    • A61K47/06Organic compounds, e.g. natural or synthetic hydrocarbons, polyolefins, mineral oil, petrolatum or ozokerite
    • A61K47/08Organic compounds, e.g. natural or synthetic hydrocarbons, polyolefins, mineral oil, petrolatum or ozokerite containing oxygen, e.g. ethers, acetals, ketones, quinones, aldehydes, peroxides
    • A61K47/14Esters of carboxylic acids, e.g. fatty acid monoglycerides, medium-chain triglycerides, parabens or PEG fatty acid esters
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K47/00Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
    • A61K47/06Organic compounds, e.g. natural or synthetic hydrocarbons, polyolefins, mineral oil, petrolatum or ozokerite
    • A61K47/16Organic compounds, e.g. natural or synthetic hydrocarbons, polyolefins, mineral oil, petrolatum or ozokerite containing nitrogen, e.g. nitro-, nitroso-, azo-compounds, nitriles, cyanates

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  • Health & Medical Sciences (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • General Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Animal Behavior & Ethology (AREA)
  • Epidemiology (AREA)
  • Biotechnology (AREA)
  • General Chemical & Material Sciences (AREA)
  • Microbiology (AREA)
  • Medical Informatics (AREA)
  • Botany (AREA)
  • Alternative & Traditional Medicine (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Mycology (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Confectionery (AREA)
  • Seasonings (AREA)
  • Medicinal Preparation (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

Provided is a candy which comprises (i) at least one component selected from the group consisting of ethyl-3-(p-menthane-3-carboxamido)acetate and monomenthyl succinate and (ii) at least one component selected from the group consisting of a green tea extract, a peppermint extract, an elderberry extract, sage, guava and a holy basil extract, and has both a long-lasting refreshing sensation and a good taste.

Description

糖果candy

本發明係關於糖果,其可利用在食品、醫藥部外品或醫藥品領域。The present invention relates to confectionery, which can be used in the field of foods, pharmaceutical products, or pharmaceutical products.

屬糖果類別的製品中,藉由薄荷腦等感到「清涼感」或藉由酸味感到「爽快感」等之給予包含咽喉的口腔內之官能性要素係受到重視。   就給予「清涼感」方面,胡椒薄荷(peppermint)精油、薄荷精油的主要構成成分之l-薄荷腦是已知會帶來清涼感的物質。但是,l-薄荷腦係有具高揮發性並且不能持續清涼感的點或添加到飲食物中時會感到苦味的點等缺點。Among the products belonging to the confectionery category, the functional elements given to the oral cavity including the throat by menthol, etc., for feeling "coolness" or by sourness, for example, are valued. In terms of giving a "cooling sensation", peppermint (peppermint) essential oil, the main constituent of mint essential oil, l-menthol is known to bring a cooling sensation. However, the l-menthol system has disadvantages such as a point with high volatility and the inability to continue cooling or a bitter taste when added to foods and drinks.

於牙膏組成物摻合薄荷腦、胡椒薄荷油、薄荷油等,給與清涼感係已被廣泛進行,有許多市售產品摻合此等成分。又,強化清涼感或持續清涼感的探討有多數係在進行,已知含有薄荷腦類與各種冷感劑的毛髮及身體洗淨劑組成物具有優良之清涼效果及其持續性,組合薄荷腦類與各種冷感劑而具有冷感效果的香料組成物係被摻合於口腔組成物中(專利文獻1及2)。但是,此等技術清涼感持續性均不充分,抑制口腔用組成物中薄荷腦的苦味亦非可滿足者。 [先前技術文獻] [專利文獻]Blending menthol, peppermint oil, peppermint oil, etc. into the toothpaste composition has been widely carried out to provide a cooling sensation system, and many commercial products have blended these ingredients. In addition, there are many studies on strengthening the cooling sensation or continuous cooling sensation. It is known that the hair and body cleansing composition containing menthol and various cold sensation agents has excellent cooling effect and continuity. A fragrance composition having a cold-sensing effect similar to various cold-sensing agents is blended into an oral composition (Patent Documents 1 and 2). However, none of these techniques have sufficient continuity of cooling sensation, nor is it satisfactory to suppress the bitterness of menthol in the oral composition. [Prior Technical Literature] [Patent Literature]

[專利文獻1]日本特開2005-8535號公報   [專利文獻2]日本特開2007-2005號公報[Patent Literature 1] Japanese Patent Application Publication No. 2005-8535 [Patent Literature 2] Japanese Patent Application Publication No. 2007-2005

[發明所欲解決之課題][Problems to be solved by the invention]

本發明的目的係提供兼具清涼感的持續性及良好風味的糖果。 [用以解決課題之手段]The object of the present invention is to provide a confectionery that has both a refreshing continuity and a good flavor. [Means to solve the problem]

本發明等人為了解決上述問題而深入探討的結果,發現藉由對冷涼成分之選自由乙基-3-p-薄荷烷-3-羧醯胺乙酸酯及琥珀酸單薄荷腦酯所成之群的至少一種,組合選自由綠茶萃取物、胡椒薄荷萃取物、接骨木萃取物、鼠尾草、番石榴及聖羅勒萃取物所成之群的至少一種,可調製兼具清涼感的持續性及良好風味的糖果。In order to solve the above problems, the inventors of the present invention have intensively studied and found that the cooling component is selected from ethyl-3-p-menthane-3-carboxamide acetate and monomenthol succinate. At least one of the group consisting of at least one selected from the group consisting of green tea extract, peppermint extract, elderberry extract, sage, guava, and holy basil extract, which can be prepared to maintain a cooling sensation Sex and good flavor candy.

藉由該見解所得之本發明態樣如下:   (1)一種糖果,其含有   (i)選自由乙基-3-p-薄荷烷-3-羧醯胺乙酸酯及琥珀酸單薄荷腦酯所成之群的至少一種,以及   (ii)選自由綠茶萃取物、胡椒薄荷萃取物、接骨木萃取物、鼠尾草、番石榴及聖羅勒萃取物所成之群的至少1種。   (2)如(1)之糖果,其中成分(ii)為選自由綠茶萃取物及胡椒薄荷萃取物所成之群的至少1種。   (3)如(1)或(2)之糖果,其中成分(i)含有乙基-3-p-薄荷烷-3-羧醯胺乙酸酯及琥珀酸單薄荷腦酯。   (4)如(2)或(3)之糖果,其中成分(ii)含有綠茶萃取物及胡椒薄荷萃取物。 [發明之效果]The aspects of the present invention obtained from this insight are as follows: (1) A candy containing (i) selected from the group consisting of ethyl-3-p-menthane-3-carboxamide acetate and monomenthol succinate At least one of the group, and (ii) at least one selected from the group consisting of green tea extract, peppermint extract, elderberry extract, sage, guava, and holy basil extract. (2) The candy according to (1), wherein the component (ii) is at least one kind selected from the group consisting of green tea extract and peppermint extract. (3) The candy as described in (1) or (2), wherein component (i) contains ethyl-3-p-menthane-3-carboxamide acetate and monomenthol succinate. (4) The candy as described in (2) or (3), wherein component (ii) contains green tea extract and peppermint extract. [Effect of invention]

藉由本發明,可提供兼具清涼感的持續性及良好風味的糖果。According to the present invention, it is possible to provide a confectionery having both a cooling continuity and a good flavor.

本發明中,「乙基-3-p-薄荷烷-3-羧醯胺乙酸酯」別名亦稱為WS-5,係可由例如Penta Manufacturing公司等購入市售品之冷涼感優良的化合物之一種,通常使用作為甜點類或清涼飲料等之添加劑的香料。   乙基-3-p-薄荷烷-3-羧醯胺乙酸酯的含量,相對於本發明之糖果總量,通常為0.00001~0.1W/W%,從本發明的效果面而言,0.0001~0.1W/W%較佳,0.001~0.1W/W%更佳,從亦包含不給予異味、異臭之觀點的總合觀點而言,更佳之含量為0.0001~0.01W/W%。當添加超過0.1W/W%的量時,因乙基-3-p-薄荷烷-3-羧醯胺乙酸酯引起令人不快的刺激味,而顯著降低服用感,故不佳。In the present invention, the alias of "ethyl-3-p-menthane-3-carboxamide acetate" is also known as WS-5, which is a compound with excellent cooling sensation that can be purchased from a commercial product such as Penta Manufacturing One is usually used as an additive for desserts or refreshing drinks. The content of ethyl-3-p-menthane-3-carboxamide acetate, relative to the total amount of confectionery of the present invention, is usually 0.00001 ~ 0.1W / W%, from the effect side of the present invention, 0.0001 It is preferably ~ 0.1 W / W%, more preferably 0.001 to 0.1 W / W%, and from a total point of view including no odor or odor, the more preferable content is 0.0001 to 0.01 W / W%. When added in an amount exceeding 0.1 W / W%, ethyl-3-p-menthane-3-carboxamide acetate causes an unpleasant irritating odor and significantly reduces the feeling of taking, so it is not good.

本發明中,「琥珀酸單薄荷腦酯」,係可由例如東京化成工業等購入市售品之冷涼感優良的化合物之一種,通常使用作為甜點類或清涼飲料等添加劑的香料。   琥珀酸單薄荷腦酯的摻合量,相對於本發明之糖果總量,係0.0001~1W/W%,較佳為0.004~0.5W/W%,更佳為0.01~0.5W/W%。摻合量未達0.0001W/W%無法充分得到清涼感之持續性,超過1W/W%毋寧會抑制清涼感,阻礙香味表現,使用上不佳。In the present invention, "monomenthyl succinate" is one of the compounds with excellent cooling sensation that can be purchased from, for example, Tokyo Chemical Industry Co., Ltd., and is usually used as an additive for desserts or refreshing drinks. The blending amount of menthol succinate relative to the total amount of confectionery of the present invention is 0.0001 to 1 W / W%, preferably 0.004 to 0.5 W / W%, and more preferably 0.01 to 0.5 W / W%. If the blending amount is less than 0.0001W / W%, the continuity of cooling sensation cannot be fully obtained. If it exceeds 1W / W%, it will rather suppress the cooling sensation, hinder the fragrance performance, and it is not good in use.

本發明中,「綠茶萃取物」,係可使用從例如Camellia屬(例如C. sinensis和C. assamica)的例如藪北(Yabukita)種或其等之雜種獲得的茶葉,將使其例如在40~140℃下加熱處理0.1分鐘~120小時的綠茶葉萃取液之濃縮物使用溶劑萃取或吸附劑等進行精製者。作為市售品例如亦可利用商品名「Purephenon」(小川香料(股)製造),商品名「Polyphenon」(東京Food Techno(股)製造),商品名「Theaflan」(伊藤園(股)製造),商品名 「Sunphenon」(太陽化學(股)製造)等。   綠茶萃取物的摻合量,相對於本發明糖果總量,係0.0001~10W/W%,較佳為0.01~5W/W%。摻合量10W/W%以上會展現強苦味,使用上不佳。In the present invention, "green tea extract" is a tea leaf obtained from, for example, Camellia (such as C. sinensis and C. assamica), such as Yabukita species or hybrids thereof. The concentrate of green tea leaf extract that has been heat-treated at ~ 140 ° C for 0.1 minute to 120 hours is purified by solvent extraction or adsorbent. As a commercially available product, for example, a trade name "Purephenon" (manufactured by Ogawa Spice Co., Ltd.), a trade name "Polyphenon" (manufactured by Tokyo Food Techno), and a trade name "Theaflan" (manufactured by Itoen Co., Ltd.), Trade name "Sunphenon" (made by Sun Chemical Co., Ltd.), etc. The blending amount of green tea extract is 0.0001 to 10 W / W%, preferably 0.01 to 5 W / W% relative to the total amount of confectionery of the present invention. If the blending amount is more than 10W / W%, it will show a strong bitter taste, which is not good in use.

本發明中,「胡椒薄荷萃取物」,係可使用例如自屬唇形科(Lamiaceae)的胡椒薄荷(Mentha pipertia L. 別名西洋薄荷)的葉或全草,藉由水、二氧化碳或乙醇等有機溶劑進行萃取,或藉由水蒸氣蒸餾所得之胡椒薄荷萃取液之濃縮物,使用溶劑萃取或吸附劑等所精製者。作為市售品例如可利用商品名「Peppermint萃取液BG」(丸善製藥(股)),商品名「Mint Polyphenol」(小川香料(股))等。   胡椒薄荷萃取物的摻合量,相對於本發明之糖果總量,係0.0001~10W/W%,較佳為0.001~5W/W%,更佳為0.01~5W/W%。摻合量10W/W%以上時、苦味/澀味強,使用上不佳。In the present invention, “pepper mint extract” can be, for example, the leaves or whole grass of peppermint (Mentha pipertia L. alias western mint) belonging to the family Lamiaceae (Lamiaceae), with water, carbon dioxide or ethanol, etc. Solvent extraction, or concentrate of peppermint extract obtained by steam distillation, refined using solvent extraction or adsorbent, etc. As a commercially available product, for example, a trade name "Peppermint extract BG" (Maruzen Pharmaceutical Co., Ltd.), a trade name "Mint Polyphenol" (Ogawa Spice Co., Ltd.), etc. can be used. The blending amount of the peppermint extract is 0.0001 to 10 W / W%, preferably 0.001 to 5 W / W%, and more preferably 0.01 to 5 W / W% relative to the total confectionery of the present invention. When the blending amount is more than 10W / W%, the bitterness / astringency is strong, and the use is not good.

本發明中「接骨木萃取物」係由接骨木屬(Sambucus)植物之西洋接骨木的果實萃取/純化的萃取物或粉末,例如可利用市售品的「接骨木果實色素」(TRADEPIA(股)),「接骨木萃取物粉末」((股)Life Health Care)等。The "elderberry extract" in the present invention is an extract or powder extracted or purified from the fruits of the western elderberry of the genus Sambucus, for example, commercially available "elderberry fruit pigment" (TRADEPIA (share )), "Elderberry Extract Powder" ((Share) Life Health Care), etc.

本發明中「鼠尾草」係藉由將唇形科植物的鼠尾草的葉子或穗狀花序粉碎或萃取/純化而得到的粉末或萃取物,例如可利用市售品的「鼠尾草粉末(Sage Powder)」(S&B食品(股))、「鼠尾草乾燥萃取物」(ASK 藥品(股)))等。In the present invention, "sage" refers to a powder or extract obtained by pulverizing or extracting / purifying the leaves or spikes of the sage of the Lamiaceae plant, for example, commercially available "sage" "Sage Powder" (S & B Foods (share)), "Sage Dry Extract" (ASK Pharmaceuticals (share)), etc.

本發明中「番石榴」係藉由將屬於桃金孃科(Myrtaceae)之植物的番石榴的葉子粉碎或萃取/純化而得到的粉末或萃取物,例如可利用「Guava Phenone」(備前化成 (股)),「番石榴之葉(粉末)」((股)P@life)等。In the present invention, "guava" is a powder or extract obtained by crushing or extracting / purifying guava leaves belonging to the Myrtaceae family, for example, "Guava Phenone" Stock)), "Guava Leaf (Powder)" ((Share) P @ life) etc.

本發明中「聖羅勒萃取物」係藉由將屬於唇形科之植物聖羅勒的葉子萃取/純化而得到的萃取物或粉末,例如可利用「聖羅勒萃取物」、「Tulsi SCFE」((股)Sabinsa Japan Corporation),「Holy Basil extract」(Bio Activities Japan (股))等。   接骨木萃取物、鼠尾草、番石榴、聖羅勒萃取物的各摻合量,相對於本發明之糖果總量,係0.0001~10W/W%,較佳為0.001~5W/W%。當摻合量10W/W%以上時,苦味/澀味強,使用上不佳。In the present invention, "holy basil extract" is an extract or powder obtained by extracting / purifying the leaves of the plant holy basil belonging to the family Lamiaceae, for example, "holy basil extract", "Tulsi SCFE" (( Shares) Sabinsa Japan Corporation), "Holy Basil extract" (Bio Activities Japan (shares)), etc. The blending amounts of elderberry extract, sage, guava, and holy basil extract are 0.0001-10 W / W%, preferably 0.001-5 W / W%, relative to the total amount of candy of the present invention. When the blending amount is more than 10W / W%, the bitterness / astringency is strong and the use is not good.

本發明之糖果之一實施態樣中,較佳含有選自由綠茶萃取物及胡椒薄荷萃取物所成之群的至少1種,特佳含有綠茶萃取物及胡椒薄荷萃取物。   本發明之糖果之別的實施態樣中,較佳含有乙基-3-p-薄荷烷-3-羧醯胺乙酸酯及琥珀酸單薄荷腦酯。   本發明之糖果進一步的實施態樣中,較佳含有乙基-3-p-薄荷烷-3-羧醯胺乙酸酯、琥珀酸單薄荷腦酯、綠茶萃取物。In one embodiment of the confectionery of the present invention, it is preferable to contain at least one kind selected from the group consisting of green tea extract and peppermint extract, and particularly preferably contain green tea extract and peppermint extract. In another embodiment of the confectionery of the present invention, it is preferable to contain ethyl-3-p-menthan-3-carboxamide acetate and monomenthol succinate. In a further embodiment of the confectionery of the present invention, it is preferable to contain ethyl-3-p-menthan-3-carboxamide acetate, monomenthol succinate, and green tea extract.

本發明之「糖果」,係以糖、糖醇、水飴等為主原料之於口腔內溶解及咀嚼而服用的固體物,例如可列舉硬糖果、軟糖果、口含錠、錠型糖果、薄膜劑,但不限定於此,又,其製造方法、形狀及容器等之包裝形態亦不限定。又,糖果中,於上述成分以外,亦可在不損及本發明之效果的範圍內適當摻合糖類或糖醇類(砂糖、葡萄糖、果糖、異構化糖、還原水飴、麥芽糖醇、山梨醇、異麥芽糖醇、丁四醇、寡糖等)、鹽類(食鹽等)、甘味料(阿斯巴甜、乙鮮舒泛鉀(Acesulfame potassium)、蔗糖素、Advantame、紐甜、阿洛酮糖等)、酸味料(檸檬酸、蘋果酸、酒石酸、富馬酸、抗壞血酸、磷酸等)、香料、著色料、保存劑、礦物質類、維生素類、胺基酸及其鹽類、生藥、生藥萃取物、咖啡因、蜂王漿、食物纖維等,作為其他成分。 [實施例]The "candy" of the present invention is a solid substance which is dissolved and chewed in the oral cavity by taking sugar, sugar alcohol, water syrup and the like as the main raw materials, for example, hard candy, soft candy, lozenge, lozenge candy, film The agent is not limited to this, and the manufacturing method, shape, and packaging form of the container are not limited. In addition, in the confectionery, in addition to the above-mentioned components, sugars or sugar alcohols (granose, glucose, fructose, isomerized sugar, reduced water syrup, maltitol, sorbitol) may be appropriately blended within a range that does not impair the effects of the present invention Alcohol, isomalt, butylol, oligosaccharides, etc.), salts (salt, etc.), sweeteners (aspartame, Acesulfame potassium), sucralose, Advantame, neotame, alo Ketoses, etc.), sour flavors (citric acid, malic acid, tartaric acid, fumaric acid, ascorbic acid, phosphoric acid, etc.), spices, coloring materials, preservatives, minerals, vitamins, amino acids and their salts, crude drugs , Crude drug extract, caffeine, royal jelly, dietary fiber, etc., as other ingredients. [Example]

以下列舉實施例,比較例及試驗例,以更詳細地說明本發明,但是此等並未對本發明的範圍有任何限定。Examples, comparative examples, and test examples are listed below to explain the present invention in more detail, but these do not limit the scope of the present invention in any way.

將60g水添加至167g砂糖和167g水飴中,以常規方法加熱溶解並煮濃以製備300g糖糰。然後將各成分添加到糖糰中使成為表1~6記載的組成,藉由並成形、冷卻硬化以獲得硬糖(1個2.3g,1處方40個)。試吃所獲得的1個樣品,實施例1~9及比較例1~4係由4名品評員,又,實施例10~13及比較例5~10係由3名品評員使用VAS(Visual Analog Scale)方法評估含完10分鐘後的清涼感。亦即,橫向繪製的直線左端係為「感覺不到清涼感」,右端係為「非常感到清涼感」,測定距左端的距離來對清涼感的程度評分。計算出各個樣品的平均值後,算出以各個控制組(實施例1、2為比較例1;實施例3~5為比較例2;實施例6~8、10~13、比較例5~8為比較例3;實施例9為比較例4;比較例10為比較例9)之清涼感為1時的值。此外,實施例的胡椒薄荷萃取物係使用小川香料(股)的「Mint Polyphenol」,綠茶萃取物係使用小川香料(股)的「Purephenon」,接骨木萃取物係使用TRADEPIA(股)的「接骨木果實色素」,鼠尾草粉末係使用S&B食品(股)的「鼠尾草粉末(Sage Powder)」,番石榴粉末係使用(股)P@life之「番石榴之葉(粉末)」,聖羅勒萃取物係使用(股)Sabinsa Japan Corporation的「Tulsi SCFE」。又,比較例的黑醋栗萃取物係使用(股)明治Food Materia的「明治黑醋栗多酚(AC10)」,蜂蜜係使用日新蜂蜜(股)的「純粹匈牙利產金合歡蜜」,接骨木花萃取物係使用由(股)生活之木的「有機接骨木花」使用熱水萃取者,蜂膠萃取物係使用(股)FAP Japan的「超臨界萃取蜂膠萃取物粉末」。又,表中的「香料※」不包括乙基-3-p-薄荷烷-3-羧醯胺乙酸酯(WS-5)、N,2,3-三甲基-2-(1-甲基乙基)丁醯胺(WS-23)及琥珀酸單薄荷腦酯。60g of water was added to 167g of sugar and 167g of water syrup, heated and dissolved in a conventional method and boiled to prepare 300g of sugar mass. Then, each component was added to the sugar mass to make the composition described in Tables 1 to 6, and was formed, cooled and hardened to obtain hard candy (1 2.3 g, 40 per prescription). For one sample obtained by trial eating, Examples 1 to 9 and Comparative Examples 1 to 4 were made by 4 reviewers, and Examples 10 to 13 and Comparative Examples 5 to 10 were made by 3 reviewers using VAS (Visual Analog Scale) method to evaluate the cooling sensation after 10 minutes. That is, the left end of the straight line drawn horizontally is "can't feel coolness" and the right end is "very coolness", and the distance from the left end is measured to rate the degree of coolness. After calculating the average value of each sample, calculate each control group (Examples 1 and 2 are Comparative Example 1; Examples 3 to 5 are Comparative Example 2; Examples 6 to 8, 10 to 13 and Comparative Examples 5 to 8 Comparative Example 3; Example 9 is Comparative Example 4; Comparative Example 10 is the value when the cooling feeling of Comparative Example 9) is 1. In addition, the peppermint extract of the examples used "Mint Polyphenol" of Ogawa Spice (share), the green tea extract used "Purephenon" of Ogawa Spice (share), and the elderberry extract used "Elderberry" of TRADEPIA (share) "Wood fruit pigment", Sage powder uses "Sage Powder" from S & B Foods Co., Ltd., and guava powder uses "Guava leaf (powder)" from P @ life, The holy basil extract uses "Tulsi SCFE" of Sabinsa Japan Corporation. In addition, the black currant extract of the comparative example uses Meiji Food Materia's "Meiji black currant polyphenol (AC10)", and the honey series uses Nissin Honey's "pure Hungarian acacia honey". The elderberry extract is made from "organic elderberry" made from living wood, and hot water extract is used, and the propolis extract is made from "supercritical extraction propolis extract powder" of FAP Japan. In addition, "perfume ※" in the table does not include ethyl-3-p-menthane-3-carboxamide acetate (WS-5), N, 2,3-trimethyl-2- (1- Methylethyl) Butylamide (WS-23) and monomenthol succinate.

相對於比較例1,觀察到實施例1及實施例2在10分鐘後的清涼感較強。   相對於比較例2,觀察到實施例3及實施例4在10分鐘後的清涼感較強,實施例5觀察到清涼感更強。   相對於比較例3,實施例6、10~13在10分鐘後的清涼感較強,實施例7及實施例8觀察到清涼感更強。   相對於比較例4,觀察到實施例9在10分鐘後的清涼感較強。   實施例1至13中,與作為對照組的比較例1~4相比,在含完10分鐘後觀察到清涼感之持續性之提高效果。又,觀察到比較例5~8的素材、比較例10的冷涼成分中,並無在含完10分鐘後之清涼感之持續性之提高效果。 [產業上之可利用性]Relative to Comparative Example 1, it was observed that Example 1 and Example 2 had a stronger cooling feeling after 10 minutes. Compared with Comparative Example 2, Example 3 and Example 4 were observed to have a stronger cooling feeling after 10 minutes, and Example 5 was observed to have a stronger cooling feeling. Compared to Comparative Example 3, Examples 6, 10 to 13 had a stronger cooling sensation after 10 minutes, and Examples 7 and 8 were observed to have a stronger cooling sensation. Compared to Comparative Example 4, Example 9 was observed to have a stronger cooling sensation after 10 minutes. In Examples 1 to 13, compared with Comparative Examples 1 to 4 as a control group, a sustained improvement effect of cooling sensation was observed after 10 minutes of inclusion. In addition, it was observed that among the materials of Comparative Examples 5 to 8, and the cooling component of Comparative Example 10, there was no effect of continuously improving the cooling sensation after 10 minutes. [Industry availability]

依本發明,可提供兼具清涼感之持續性與良好風味的糖果。因此,藉由將本發明作為醫藥品、醫藥部外品及食品來提供,此等產業的發達係受到期待。According to the present invention, it is possible to provide confectionery that has both the continuity of cooling and good flavor. Therefore, by providing the present invention as a medicinal product, a non-medicinal product, and a food product, the developed system of these industries is expected.

本申請案以2017年5月23日在日本申請的日本特願2017-101767號為基礎,其內容均包含在本說明書中。This application is based on Japanese Patent Application No. 2017-101767 filed in Japan on May 23, 2017, and its contents are included in this specification.

Claims (4)

一種糖果,其含有   (i)選自由乙基-3-p-薄荷烷-3-羧醯胺乙酸酯及琥珀酸單薄荷腦酯所成之群的至少一種,以及   (ii)選自由綠茶萃取物、胡椒薄荷萃取物、接骨木萃取物、鼠尾草、番石榴及聖羅勒萃取物所成之群的至少1種。A candy comprising (i) at least one selected from the group consisting of ethyl-3-p-menthan-3-carboxamide acetate and monomenthol succinate, and (ii) selected from green tea At least one species of extract, peppermint extract, elderberry extract, sage, guava, and holy basil extract. 如請求項1之糖果,其中成分(ii)為選自由綠茶萃取物及胡椒薄荷萃取物所成之群的至少1種。The candy according to claim 1, wherein the component (ii) is at least one selected from the group consisting of green tea extract and peppermint extract. 如請求項1或2之糖果,其中成分(i)含有乙基-3-p-薄荷烷-3-羧醯胺乙酸酯及琥珀酸單薄荷腦酯。The candy as claimed in claim 1 or 2, wherein the component (i) contains ethyl-3-p-menthane-3-carboxamide acetate and monomenthol succinate. 如請求項2或3之糖果,其中成分(ii)含有綠茶萃取物及胡椒薄荷萃取物。The candy according to claim 2 or 3, wherein the component (ii) contains green tea extract and peppermint extract.
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