TW201028677A - Test equipment and test method - Google Patents

Test equipment and test method Download PDF

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TW201028677A
TW201028677A TW98102312A TW98102312A TW201028677A TW 201028677 A TW201028677 A TW 201028677A TW 98102312 A TW98102312 A TW 98102312A TW 98102312 A TW98102312 A TW 98102312A TW 201028677 A TW201028677 A TW 201028677A
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test
aerosol
buffer bottle
buffer
detecting device
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TW98102312A
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Chinese (zh)
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TWI385374B (en
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Li-May Chang
Shu-Ruey Chiu
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Taiwan Textile Res Inst
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Abstract

A method and equipment for testing filtration efficiency are provided. The equipment includes a buffer, a nebulizer, a chamber and a collector. The buffer has an inlet at its top and an outlet at its lateral side. The inlet and the outlet are respectively used for letting a spray enter and leave the buffer. The nebulizer disposed at the inlet is used for nebulizing a fluid into the spray. The spray that leaves the buffer enters the chamber. The collector is connected to the chamber for collecting the filtrated spray so as to test the filtration efficiency. In the method, the spray is provided to enter the buffer in an in-feed direction. Then, the spray is directed to leave the buffer in an out-feed direction that is unparallel to the in-feed direction. Afterwards, the spray is dispersed, filtrated, and collected in turn so as to test the filtration efficiency.

Description

201028677 六、發明說明: 【發明所屬之技術領域】 本發明是有關於一種檢測裴置及檢測方法,且特別是 有關於一種過濾效率之檢測裝置及檢測方法。 【先前技術】 隨著科技的發展,空氣品質日益下 粒對於人體的危害也*日俱氣中懸序微 源(污毕、、& 甶一個方面加以控制:發生 杀原)、傳輸途徑以及防護措施。其中防螬抖谂今為 使用個^護具,如面罩、防護衣^/情㈣施包含 作,界發展的面罩多利用多孔隙的纖維織物來製 織物的後=過=的檢測,以得知面” 據效率的檢㈣署 率的檢測,係發展出遇 ❹ 器將包冬裝置。一般而言,檢測裝置係利用氣霧產生 並將試驗==例如細菌)的試驗液霧化為試驗氣霧, 來進行滿ΐ霧通過欲進行測試的濾材(例如面罩等織物) 氣霧祐;的動作。接著,利用採樣器接收過濾後的試磁 率。’並檢測其中微粒誠餘量,藉轉知級的過遽衫 般的檢測裝置係 以 置於翁裳 '、…氣霧腔為主,氣霧產生器係設 在氣霧腔採樣器設置於氣霧腔下端’遽材則1 般霧通過濾材,以進行檢測。然而,氣霧產生器一 .、、、儿全將試驗液霧化為試驗氣霧,未被霧化的試驗液 201028677 便會形成液滴’直接滴落在渡材上,導致因覆蓋作用而影 響檢測結果的缺點。 另外,在進入實際檢測階段前,檢測裝置必須先經過 前置準備階段。在準備階段中,渡材未被放置入檢測裝置 内,檢測裝置先開始產生試驗氣霧’待試驗氣霧之流量穩 定,並且試驗氣霧粒子之粒徑達到試驗條件的要求後,再 將濾材置入檢測装置内。如此必須拆開並重新組裝檢測裝 置,大大降低了操作上的便利性。特別是進行多次檢測時, _ 需要反覆拆裝檢測裝置,此些拆裝動作會彳艮容易改變檢測 條件。如此便增加檢測條件的變異性,大幅降低檢測的穩 疋性再者’在拆裝檢測裝置的過程中,更增加了檢測裝 置中的元件以及濾材受到外部污染的機會。 【發明内容】 因此本發明的目的是在提供一種檢測襞置及檢測方 法,其係利用試驗氣霧分別由緩衝瓶頂端之進料口及緩衝 β瓶側邊之出料口進入及離開緩衝瓶之方式,使試驗氣霧進 入緩衝瓶之方向非平行於試驗氣霧離開緩衝瓶之方向。 根據本發明之上述目的,提出一種檢剛裝置,包括一 缓衝瓶、一霧化器、一氣霧腔以及一採樣器。緩衝瓶具有 一進料口及一出料口,分別用以使一試驗氣霧進入及離開 缓衝瓶,並且分別位於緩衝瓶之頂端及側邊。霧化器設置 於進料口,用以將一試驗液霧化為試驗氣霧。氣霧腔具有 一上端開口及一下端開口,離開緩衝瓶之試驗氣霧由上端 開口進入氣霧腔。採樣器經由下端開口連接於氣霧腔,用 201028677 以接收經由一慮材過滤後之试驗氣霧’藉以檢驗滤材之過 濾效率,濾材設置於氣霧腔及採樣器之間。 根據本發明之另一目的’提出一種檢測方法。首先’ 提供一試驗氣霧沿一進料方向進入一緩衝瓶。其次,導引 試驗氣霧由一出料方向離開緩衝瓶’進料方向非平行於出 料方向。再來,分散試驗氣霧於一氣霧腔中。接著,過濾 試驗氣霧。然後,接收過濾後之試驗氣霧,藉以檢測過濾 效率。 Φ 本發明之檢測裝置及檢測方法利用試驗氣霧進入緩衝 瓶之方向非平行於試驗氣霧離開緩衝瓶之方向的方式,由 緩衝瓶產生緩衝的功能,使離開緩衝瓶的試驗氣霧具有穩 定的流量以及均勻的平均粒徑,可提升操作便利性、提高 檢測穩定性,並且可避免濾材被污染的問題。 【實施方式】 依照本發明一較佳實施例之檢測裝置及檢測方法,係 ❹ 用以檢測一濾材之過濾效率。檢測裝置利用緩衝瓶之進料 口及出料口錯開設置的方式,使得超過檢測條件之粒徑範 圍的氣霧粒子以及未被霧化的試驗液,不會直接滴落至渡 材’藉以產生緩衝的作用。其係具有提升操作便利性、提 高檢測穩定性,以及避免濾材被污染等優點。 «用參照第1圖’其繪不依照本發明一較佳實施例之檢 測裝置之示意圖。本實施例之檢測裝置100主要包括一緩 衝瓶110、一霧化器120、一氣霧腔140以及一採樣器15〇。 緩衝瓶110具有一進料口 ll〇a及一出料口 11〇b,分別位於 201028677 緩衝瓶110之頂端及側邊’一試驗氣霧S係由進料口 110a 進入缓衝瓶110 ’並由出料口 110b離開緩衝瓶no。霧化 器120設置於進料口 110a,用以將一試驗液霧化為試驗氣 霧S。氣霧腔140具有一上端開口 140a及一下端開口 140b’離開缓衝瓶110之試驗氣霧S係由上端開口 i4〇a進 入氣霧腔140。本實施例中,出料口 ll〇b與缓衝瓶11〇底 部之距離大於出料口 110b與緩衝瓶11〇頂端之距離。採樣 器150經由下端開口 140b連接於氣霧腔140,用以接收被 設置於氣霧腔140與採樣器150之間的一濾材F過滤後的 參 試驗氣霧S,藉以檢驗濾材F之過濾效率。檢測裝置1〇〇 利用錯開設置的進料口 ll〇a及出料口 ii〇b,使緩衝瓶no 可產生緩衝的作用,讓超過檢測條件之粒徑範圍的試驗氣 霧S粒子以及未被霧化之試驗液,不會直接滴落在濾材ρ 上’可以避免濾材F被污染而影響檢測結果的問題。 更進一步來說’緩衝瓶110及氣霧腔140分別具有一 長軸方向L1及L2。緩衝瓶11〇之長轴方向L1及氣霧腔 140之長軸方向L2分別大致上垂直於一水平面,且緩衝瓶 ❹ 11〇之長轴方向L1較佳地大致平行於氣霧腔14〇之長軸方 向L2。依照本發明較佳之實施例中,緩衝瓶11()之進料口 ll〇a及氣霧腔140之上端開口 140a位於不同的長軸方向 上。此種配置方式係可確保试驗氣霧S由進料口 11 〇a進入 緩衝瓶110之後,不會直接經由上端開口 14〇a進入氣霧腔 140 内。 另一方面,檢測裝置100更包括一連接管13〇,其係 設置於緩衝瓶110及氣霧腔140之間。依照本發明一較佳 201028677 實施例中,連接管130垂直於緩衝瓶11〇之侧邊川,亦即 垂直於緩衝瓶110之長轴方向L卜如第1圖所示。連接管 130之兩端分別連接於出料卩服及上端開口偷。由出 料口 u〇b離開緩衝瓶110之試驗氣霧s係經由連接管13〇 導引至氣霧腔140。另外,在不同的實施方式中連接管 130亦可非垂直於緩衝瓶11〇之侧邊lu。請參照第2圖, 其繪示依照本發明另-較佳實施例之檢測裝置之緩衝瓶及 連接管的示意圖。連接管13〇’連接於緩衝瓶11〇之出料 • 口 11〇b處,尚於連接管13〇,連接於氣霧腔140之上端開 〇140a處。也就是說,連接管13〇,係朝向緩衝瓶11〇之 底部傾斜。 此外,檢測裝置100更包括一真空泵(vacuumpump) 160、一空氣泵170及一注射泵180。真空泵160用以提供 〜氣流通過緩衝瓶110、氣霧腔14〇及採樣器15〇,以帶動 試驗氣霧S。本實施例中,真空泵ι60係設置於採樣器15〇 支下游端’藉由抽氣使得氣流依序通過緩衝瓶110、氣霧 _ 脸及採樣器150。本實施例之霧化器120例如為一氣 ®式氣霧產生器。空氣泵170及注射泵180分別提供一高 ®氣體以及試驗液至霧化器120,霧化器120係利用由空 氣泵170提供之高壓氣體,將試驗液霧化成為微小之粒子。 檢測裝置100可例如是應用依照本發明一較佳實施例 ^檢測方法進行過濾效率之檢測。以下係針對依照本發明 〜較佳實施例之檢測方法進行說明。請參照第3圖,其繪 示依照本發明一較佳實施例之檢測方法的流程圖。本實施 例之檢測方法首先進行步驟S1,提供試驗氣霧S沿一進料 201028677 方向D1進入緩衝瓶11〇〇接著, 驗氣霧S由-出料方向m離開缓t步驟S2所示,導引試 m非平行於出料方向瓶,0,其中進料方向 進料口 ma沿進料方向D1進!^1巾’試驗氣霧s係由 口 110b沿出料方向D2離開緩衝沲 叶 .. 柯艰4 11〇。進料方向di大致 上垂直於出料方向D2,如第1圖也 蚁 由氣流帶動之嫌祕S可以_進人氣_⑽,連接 管130可朝向緩衝瓶110之底部傾斜,如第2圖所螬·示。 亦即’緩衝瓶110的側邊111對應於出料口 ll〇b及緩衝瓶 110底部之間的部分’與出料方向D2夾有一銳角Θ。 接下來’檢測方法進行分散試驗氣霧S的步驟,使試 驗氣霧S的粒子均勻分散在氣霧腔140中,如步驟S3所 示。然後,如步驟S4及S5所示,過濾試驗氣霧S,並且 接收過濾後之試驗氣霧S,藉以檢測過濾效率。 本實施例之檢測方法更可進一步包括霧化試驗液、提 供氣流以及分離試驗氣霧S及未霧化之試驗液的步驟。實 際應用上,係利用霧化器120將試驗液霧化成為試驗氣霧 參 S,並利用真空泵160提供氣流,由氣流帶動試驗氣霧S 依序通過緩衝瓶110、連接管130、氣霧腔140、濾材F以 及採樣器150。由於特定流量之氣流可以帶動特定粒徑範 圍之粒子,因此超過此範圍之粒徑的試驗氣霧s粒子係無 法由氣流帶動。再者,由於出料口 較靠近緩衝瓶110 之頂端,前述無法由氣流帶動之試驗氣霧s粒子便沿重力 方向沈降至缓衝瓶110底部。另外,未被霧化之試驗液亦 直接由進料口 ll〇a滴落至缓衝瓶110底部。如此一來,符 201028677 合檢測條件之試驗氣霧s粒子以及未被霧化之試驗液液滴 係完成分離的動作。進一步來說,在進行檢測的準備階段 以及實際檢測階段,未符合檢測條件的試驗氣霧S以及未 被霧化的試驗液液滴係滴落至緩衝瓶110底部。實際應用 上’藉由緩衝瓶110的設置,在前置準備階段中進行氣流 流量及試驗氣霧s粒徑的校正時,可以避免液滴污染採樣 器150及免去反覆拆裳檢測裝置1〇〇的動作,大幅提升操 作的便利性以及檢測效率。 春將本實施例之檢測裝置100應用美國材料試驗協會 (American Society for Testing and Materials ’ ASTM)F2101 標準試驗方法’進行細菌過滤效率(Bacteriai Fiitrati〇n Efficiency,BFE)之檢測試驗。試驗液中含有細菌,例如 金黃色葡萄球菌(Staphylococcus aureus),霧化器12〇係將 試驗液霧化成為包含細菌之試驗氣霧S,濾材ρ係為醫用 面罩。標準試驗之條件如下:真空泵16〇提供之氣流流量 為28.3L/min’试驗氣霧S粒子的平均粒徑為2.7〜3 3微米, 總菌落數為1700至2700之間。以下係針對應用前述條件 醫進行檢測之方式來進行說明,利用過濾前後細菌量之比 較,得到醫用面罩之細菌過渡效率。 首先針對有/無緩衝瓶之檢測装置所提供試驗氣霧之 粒子數量及粒徑的差異進行說明。以下係由同一人員針 對有/無加裝緩衝瓶之檢測裝置進行試驗,取得有緩衝瓶之 數據82組以及無緩衝瓶之數據4〇組,試驗結果係如表j 所示。 -試驗氣 201028677 平均值 標準差 平均值 標準差 有緩衝瓶 2196 273 2.89 0.11 無緩衝瓶 2168 365 2.95 —----. 0.16 表1 根據試驗結果,82組有緩衝瓶之數據係全數落入標準 試驗方法所規定之試驗氣霧粒子數量及粒徑範圍内;而無 缓衝瓶之數據中,僅有17組落於標準試驗方法所規定之^ 驗氣霧粒子數量及粒徑範圍内。此外’有緩衝瓶之數據的 φ 標準差小於無緩衝瓶之數據的標準差,顯示包含有緩衝瓶 的檢測裝置可依據氣流流量穩定產生特定粒徑及數量之試 驗氣霧,有效提高檢測過濾效率的有效性。接下來,請參 照第4圖,其繪示試驗氣霧粒子之數量及粒徑的分佈曲線 圖。曲線A及曲線B分別表示有緩衝瓶及無緩衝瓶之檢測 裝置提供的試驗氣霧粒子數量及粒徑分佈曲線。由第4圖 可知,有緩衝瓶之檢測裝置並不會顯著改變試驗氣霧粒子 的粒徑數量分佈’因此可完全適用於ASTM F2101或其他 標準試驗方法。 鲁 另一方面,以下係將本實施例之檢測裝置1〇〇與習知 之檢測裝置進行細菌過濾效率檢測能力的比對。其中係以 醫用面罩作為濾材進行過濾,分別取得五組過濾效率數 值,並將檢測結果做成表2。 本實施例之檢 測裝置 習知之檢測 裝置 試驗氣霧平均生菌菌落數 2464 CFU/mL 2640 CFU/mL 試驗氣霧粒徑 3.0微米 3.3微米 11 201028677 第一次細菌過渡效率 97.6% 99.6% 〜 第二次細菌過遽效率 97.1% 98.9% 第二么細菌過滤效率 97.6% 99.5% ~~〜 第四次細菌過濾效率 ---------- 97.5% 99.5% ^、 第五次細菌過濾效率 97.8% 98.9% 細菌過濾效率平均值~~ 97.5% 99.3% 標準差 〜~~ 0.26 0.35 〜 Z-Scores 0.9 ------^ 0·9 ❿ 表2 檢測裝置100提供之試驗氣霧s,其中平均生菌菌落 數為2464,平均粒徑為3 〇微米。由表2可知,本實施例 之檢測裝置1〇〇的過濾效率之平均值為97 5%,標準差為 〇·26。將此檢測結果依照ASTM D6674標準進行Z值 (Z-Sc〇res)分析,得到z值為〇 9。在z值分析中,乙值 之絕對值小於2係表示檢測能力良好(satisfact〇ry )。依照 本發明較佳實施例之檢測裝置100與習知之檢測裝置得出 ❹ 之Z值均為0.9’因此由結果可知檢測裝置100可提供與習 知之檢測裝置相類似之檢測能力。也就是說,當檢測裝置 i〇〇採用緩衝瓶110來進行緩衝的動作時,並不會改變檢 測裝置100對於濾材過渡效率之檢測能力。 上述依照本發明一較佳實施例之檢測裝置及檢測方 法’係設置緩衝瓶於霧化器及氣霧腔之間。利用緩衝瓶之 進料口及出料口係錯開設置,以及進料方向非平行於出料 方向的方式,使試驗氣霧中粒徑過大、無法由氣流帶動之 粒子,以及未被霧化器霧化之試驗液液滴,滴落至緩衝瓶 12 201028677 改善原本液滴會直接滴落在濾材F上,導致因覆蓋 $%響過濾效率檢測結果的缺點。另外,此種應用缓 過遠2行緩衝之方式,係完全利用氣流來帶動試驗氣霧通 • 接管進入氣霧腔中,排除重力、沈積作用的影響,使 得抵達氣霧腔的試驗氣霧符合需求的條件,可以增加檢測 的穩定性。此外,應用緩衝瓶進行緩衝的方式,可免去傳 統檢冽裴置需要在準備階段及測試階段之間重複拆裝裝 ^造成外界污染以及檢測條件變異的問題,進一步更可 • 提升操作的便利性以及檢測結果的可靠度。 雖然本發明已以實施例揭露如上,然其並非用以限定 本發明,任何熟習此技藝者,在不脫離本發明之精神和範 =内,當可作各種之更動與潤飾,因此本發明之保護範圍 當視後附之申請專利範圍所界定者為準。 【圖式簡單說明】 ^為讓本發明之上述和其他目的、特徵、優點與實施例 Φ 犯更明顯易懂,所附圖式之說明如下: 第1圖繪示依照本發明一較佳實施例之檢測裝置之示 意圖。 ,第2圖繪示依照本發明另一較佳實施例之檢測裝置之 緩衝瓶及連接管的示意圖。 第3圖鳍'示依照本發明一較佳實施例之檢測方法的流 程圖。 第4圖繪示試驗氣霧粒子之數量及粒徑的分佈曲線 圖。 201028677 【主要元件符號說明】 100 :檢測裝置 110 :緩衝瓶 110a :進料口 110b :出料口 111 :侧邊 120 :霧化器 130 :連接管 130’ :連接管 140 :氣霧腔 140a ··上端開口 140b :下端開口 150 :採樣器 160 :真空泵 170 :空氣泵 ® 180 :注射泵 A :曲線 B :曲線 D1 :進料方向 D2 :出料方向 D2’ :出料方向 F :滤材 L1 :緩衝瓶之長軸方向 L2 :氣霧腔之長軸方向 0 :銳角 S:試驗氣霧 14201028677 VI. Description of the Invention: [Technical Field] The present invention relates to a detection device and a detection method, and more particularly to a detection device and a detection method for filtration efficiency. [Prior Art] With the development of science and technology, the air quality is becoming more and more harmful to the human body. * The daily micro-source (staining, and & one control: killing), transmission route and Protective measures. Among them, the use of protective gears, such as masks, protective clothing, and (4) applications, the development of masks using more porous fabrics to make the fabric after the = = detection, to obtain According to the efficiency test (four), the detection of the rate of the device is to develop a device for the winter. In general, the test device uses a test solution that uses aerosol generation and tests == for example bacteria to atomize the test. The mist is used to carry out the action of the filter material (such as a fabric such as a mask) that is to be tested by the mist. Then, the sampler is used to receive the filtered magnetic permeability. The level-following-like detection device is mainly placed in Weng's..., the aerosol chamber, and the aerosol generator is installed in the aerosol chamber sampler at the lower end of the aerosol chamber. Through the filter material, the test is carried out. However, the gas mist generator, I., and the child completely atomize the test liquid into the test gas mist, and the test liquid that is not atomized will form a liquid droplet 'drop directly on the cross material. The disadvantage of affecting the detection result due to the covering effect In addition, before entering the actual detection stage, the detection device must first pass through the pre-preparation phase. In the preparation phase, the crossing material is not placed in the detection device, and the detection device begins to generate the test aerosol first. And after testing the particle size of the aerosol particles to meet the requirements of the test conditions, the filter material is placed in the detection device. Therefore, the detection device must be disassembled and reassembled, which greatly reduces the convenience of operation. When, _ need to repeatedly disassemble the detection device, these disassembly and assembly operations will easily change the detection conditions. This increases the variability of the detection conditions, greatly reducing the stability of the detection and then in the process of disassembling the detection device The invention further increases the chances of the components in the detecting device and the filter material being externally contaminated. SUMMARY OF THE INVENTION Accordingly, it is an object of the present invention to provide a detecting device and a detecting method which utilize the test gas mist respectively from the top of the buffer bottle. The inlet and the outlet of the buffered β bottle enter and leave the buffer bottle, so that the test aerosol enters the buffer bottle. According to the above object of the present invention, a cleaning device comprising a buffer bottle, an atomizer, an aerosol chamber and a sampler is provided. The buffer bottle has a The material inlet and the discharge port are respectively used to make a test aerosol enter and leave the buffer bottle, and are respectively located at the top and the side of the buffer bottle. The atomizer is disposed at the feed port for using a test liquid mist. The test chamber is provided with an upper end opening and a lower end opening, and the test aerosol leaving the buffer bottle enters the aerosol chamber from the upper end opening. The sampler is connected to the aerosol chamber via the lower end opening, and is received by 201028677. The test aerosol after filtering is used to test the filtration efficiency of the filter material, and the filter material is disposed between the aerosol chamber and the sampler. According to another object of the present invention, a detection method is proposed. First, a test aerosol is provided. Enter a buffer bottle along a feed direction. Secondly, the pilot test aerosol exits the buffer bottle from a discharge direction. The feed direction is non-parallel to the discharge direction. Again, the dispersion test aerosol is in an aerosol chamber. Next, the test aerosol was filtered. The filtered test aerosol is then received to detect filtration efficiency. Φ The detecting device and the detecting method of the invention use the test gas mist to enter the buffer bottle in a direction non-parallel to the direction in which the test gas mist leaves the buffer bottle, and the buffering function is generated by the buffer bottle, so that the test gas leaving the buffer bottle is stable. The flow rate and uniform average particle size improve handling convenience, improve detection stability, and avoid contamination of the filter material. [Embodiment] A detecting device and a detecting method according to a preferred embodiment of the present invention are used to detect the filtering efficiency of a filter medium. The detecting device uses the feeding port and the discharging port of the buffer bottle to be staggered, so that the aerosol particles exceeding the particle size range of the detection condition and the test liquid not atomized are not directly dripped to the ferry material. The role of buffering. It has the advantages of improved operation convenience, improved detection stability, and avoiding contamination of the filter material. «With reference to Fig. 1, a schematic view of a detecting device not according to a preferred embodiment of the present invention is shown. The detecting device 100 of this embodiment mainly comprises a buffer bottle 110, an atomizer 120, an aerosol chamber 140 and a sampler 15A. The buffer bottle 110 has a feed port 11a and a discharge port 11b, respectively located at the top and side of the 201028677 buffer bottle 110. A test aerosol S enters the buffer bottle 110' from the feed port 110a. The buffer bottle no is left from the discharge port 110b. The atomizer 120 is disposed at the inlet port 110a for atomizing a test liquid into the test gas mist S. The test mist S of the aerosol chamber 140 having an upper end opening 140a and a lower end opening 140b' exiting the buffer bottle 110 is introduced into the aerosol chamber 140 from the upper end opening i4〇a. In this embodiment, the distance between the discharge port 11b and the bottom of the buffer bottle 11b is greater than the distance between the discharge port 110b and the top end of the buffer bottle 11〇. The sampler 150 is connected to the aerosol chamber 140 via the lower end opening 140b for receiving the filtered test gas mist S filtered by a filter material F disposed between the aerosol chamber 140 and the sampler 150, thereby verifying the filtration efficiency of the filter material F. . The detecting device 1 uses the feed port 11〇a and the discharge port ii〇b which are staggered, so that the buffer bottle no can generate a buffering effect, and the test aerosol S particles exceeding the particle size range of the detection condition are not The atomized test solution does not drip directly on the filter material ρ' to avoid contamination of the filter material F and affect the detection result. Further, the buffer bottle 110 and the aerosol chamber 140 have a longitudinal direction L1 and L2, respectively. The long axis direction L1 of the buffer bottle 11〇 and the long axis direction L2 of the aerosol chamber 140 are respectively substantially perpendicular to a horizontal plane, and the long axis direction L1 of the buffer bottle ❹ 11〇 is preferably substantially parallel to the aerosol chamber 14 Long axis direction L2. In accordance with a preferred embodiment of the present invention, the feed port 11a of the buffer bottle 11() and the upper end opening 140a of the aerosol chamber 140 are located in different major axis directions. This configuration ensures that the test aerosol S enters the buffer bottle 110 from the feed port 11 〇a and does not enter the aerosol chamber 140 directly through the upper end opening 14〇a. On the other hand, the detecting device 100 further includes a connecting tube 13 设置 disposed between the buffer bottle 110 and the aerosol chamber 140. According to a preferred embodiment of the present invention, in the embodiment of 201028677, the connecting pipe 130 is perpendicular to the side of the buffer bottle 11, i.e., perpendicular to the long axis direction of the buffer bottle 110, as shown in Fig. 1. The two ends of the connecting pipe 130 are respectively connected to the discharge raft and the upper end opening. The test aerosol s leaving the buffer bottle 110 from the discharge port u〇b is guided to the aerosol chamber 140 via the connecting tube 13A. In addition, in various embodiments, the connecting tube 130 may also be non-perpendicular to the side lu of the buffer bottle 11〇. Referring to Figure 2, there is shown a schematic view of a buffer bottle and a connecting tube of a detecting device in accordance with another preferred embodiment of the present invention. The connecting pipe 13〇' is connected to the discharge of the buffer bottle 11〇, at the port 11〇b, still at the connecting pipe 13〇, and is connected to the upper end opening 140a of the aerosol chamber 140. That is, the connecting pipe 13〇 is inclined toward the bottom of the buffer bottle 11〇. In addition, the detecting device 100 further includes a vacuum pump 160, an air pump 170, and a syringe pump 180. The vacuum pump 160 is configured to provide a flow of air through the buffer bottle 110, the aerosol chamber 14A, and the sampler 15A to drive the test aerosol S. In the present embodiment, the vacuum pump ι 60 is disposed at the downstream end of the sampler 15 by air pumping so that the air flow sequentially passes through the buffer bottle 110, the aerosol _ face and the sampler 150. The atomizer 120 of the present embodiment is, for example, a gas-type aerosol generator. The air pump 170 and the syringe pump 180 respectively supply a high gas and a test liquid to the atomizer 120. The atomizer 120 uses the high pressure gas supplied from the air pump 170 to atomize the test liquid into minute particles. The detecting device 100 can, for example, apply the detection of the filtering efficiency in accordance with a preferred embodiment of the present invention. The following is a description of the detection method according to the present invention to the preferred embodiment. Referring to Figure 3, a flow chart of a method of detecting in accordance with a preferred embodiment of the present invention is shown. The detecting method of the embodiment first performs step S1 to provide the test aerosol S to enter the buffer bottle 11 along a direction D1 of feed 201028677. Next, the test mist S is separated from the discharge direction m by step t2, and the guide is shown. The test m is not parallel to the discharge direction bottle, 0, wherein the feed direction feed port ma enters along the feed direction D1! ^1 towel 'test aerosol s is exited from the buffer leaf by the port 110b along the discharge direction D2. Ke Qiang 4 11〇. The feed direction di is substantially perpendicular to the discharge direction D2. As shown in Fig. 1, the ant is driven by the airflow, and the connection pipe 130 can be tilted toward the bottom of the buffer bottle 110, as shown in Fig. 2.螬·Show. That is, the side 111 of the buffer bottle 110 corresponds to the portion ' between the discharge port 11b and the bottom of the buffer bottle 110' and the discharge direction D2 has an acute angle Θ. Next, the detecting method performs the step of dispersing the test aerosol S so that the particles of the test gas mist S are uniformly dispersed in the aerosol chamber 140 as shown in step S3. Then, as shown in steps S4 and S5, the test aerosol S is filtered, and the filtered test aerosol S is received, thereby detecting the filtration efficiency. The detecting method of this embodiment may further comprise the steps of atomizing the test liquid, supplying the gas stream, and separating the test gas mist S and the un-atomized test liquid. In practical application, the test liquid is atomized into the test gas mist S by the atomizer 120, and the air flow is provided by the vacuum pump 160, and the test gas mist S is sequentially driven by the air flow to pass through the buffer bottle 110, the connecting tube 130, and the aerosol chamber. 140, filter material F and sampler 150. Since the flow of a specific flow rate can drive particles of a specific particle size range, the test aerosol s particle system exceeding the particle size of this range cannot be driven by the gas flow. Further, since the discharge port is closer to the top end of the buffer bottle 110, the aforementioned test aerosol s particles which cannot be driven by the air flow settle to the bottom of the buffer bottle 110 in the direction of gravity. In addition, the test liquid which has not been atomized is also directly dropped from the feed port 11a to the bottom of the buffer bottle 110. In this way, the test aerosol particles s particles of the test conditions and the test liquid droplets that have not been atomized are separated. Further, in the preparation stage for performing the detection and the actual detection stage, the test aerosol S which does not meet the detection conditions and the test liquid droplets which are not atomized are dropped to the bottom of the buffer bottle 110. In practical application, by the setting of the buffer bottle 110, when the flow rate of the airflow and the particle size of the test aerosol are corrected in the pre-preparation stage, the droplet contamination sampler 150 and the re-disassembly detection device can be avoided. The embarrassing action greatly enhances the convenience of operation and the efficiency of detection. In the spring, the detection device 100 of the present embodiment was subjected to a test of bacterial filtration efficiency (Bacteriai Fiitrati〇n Efficiency, BFE) using the American Society for Testing and Materials (ASTM) F2101 standard test method. The test solution contains bacteria, such as Staphylococcus aureus, and the atomizer 12 atomizes the test liquid into a test aerosol S containing bacteria, and the filter material ρ is a medical mask. The conditions of the standard test were as follows: the flow rate of the gas supplied by the vacuum pump 16 was 28.3 L/min'. The average particle diameter of the test aerosol S particles was 2.7 to 3 3 μm, and the total number of colonies was between 1700 and 2700. The following description will be made on the method of applying the aforementioned conditional examination, and the bacterial transition efficiency of the medical mask is obtained by comparing the amounts of bacteria before and after filtration. First, the difference in the number and particle size of the test aerosol provided by the detection device with/without buffer bottle will be described. In the following, the same person is tested with or without a buffer bottle, and 82 sets of buffered data and 4 sets of unbuffered data are obtained. The test results are shown in Table j. -Test gas 201028677 Mean standard deviation Mean standard deviation Buffer bottle 2196 273 2.89 0.11 Buffer bottle 2168 365 2.95 —----. 0.16 Table 1 According to the test results, the data of 82 groups of buffer bottles are all in the standard. The test method specifies the number and particle size range of the test aerosol particles; while the data of the unbuffered bottles, only 17 groups fall within the range of the number and particle size of the aerosol particles specified by the standard test method. In addition, the standard deviation of the data of the buffered bottle is smaller than the standard deviation of the data of the unbuffered bottle. It is shown that the detecting device containing the buffer bottle can stably generate the test aerosol of a specific particle size and quantity according to the flow rate of the airflow, thereby effectively improving the detection and filtering efficiency. Effectiveness. Next, please refer to Figure 4, which shows the distribution of the number and particle size of the test aerosol particles. Curves A and B show the number of test aerosol particles and the particle size distribution curve provided by the detection device with buffer bottles and unbuffered bottles, respectively. As can be seen from Fig. 4, the detection device with the buffer bottle does not significantly change the particle size distribution of the test aerosol particles', so it can be fully applied to ASTM F2101 or other standard test methods. On the other hand, in the following, the detection device 1 of the present embodiment is compared with the conventional detection device for the bacterial filtration efficiency detection capability. Among them, a medical mask was used as a filter to filter, and five sets of filtration efficiency values were obtained, and the test results were shown in Table 2. The detection device of the detection device of the present embodiment tests the average number of bacterial colonies of the aerosol 2464 CFU/mL 2640 CFU/mL test aerosol particle size 3.0 micron 3.3 micron 11 201028677 first bacterial transition efficiency 97.6% 99.6% ~ second Secondary bacteria over-yield efficiency 97.1% 98.9% Second bacterial filtration efficiency 97.6% 99.5% ~~~ Fourth bacterial filtration efficiency---------- 97.5% 99.5% ^, fifth bacterial filtration efficiency 97.8% 98.9% Average bacterial filtration efficiency ~~ 97.5% 99.3% Standard deviation~~~ 0.26 0.35 ~ Z-Scores 0.9 ------^ 0·9 ❿ Table 2 Test aerosol s provided by the detection device 100, The average number of colonies was 2464 and the average particle size was 3 〇 microns. As is apparent from Table 2, the average filtration efficiency of the detecting device 1 of the present embodiment was 97 5%, and the standard deviation was 〇·26. The Z value (Z-Sc〇res) analysis was carried out according to the ASTM D6674 standard to obtain a z value of 〇 9. In the z-value analysis, the absolute value of the B value is less than 2, indicating that the detection ability is good (satisfact〇ry). The detecting apparatus 100 and the conventional detecting apparatus according to the preferred embodiment of the present invention have a Z value of 0.9'. Therefore, it is known from the results that the detecting apparatus 100 can provide a detecting capability similar to that of the conventional detecting apparatus. That is to say, when the detecting means i 〇〇 uses the buffer bottle 110 for the buffering operation, the detecting ability of the detecting device 100 for the filter material transition efficiency is not changed. The detecting device and the detecting method according to a preferred embodiment of the present invention are arranged to provide a buffer bottle between the atomizer and the aerosol chamber. The feed port and the discharge port of the buffer bottle are staggered, and the feeding direction is not parallel to the discharge direction, so that the particle size in the test gas is too large, the particles cannot be driven by the air flow, and the mist is not atomized. The test liquid droplets are dripped into the buffer bottle 12 201028677 The original droplets are directly dripped on the filter material F, resulting in the disadvantage of covering the detection result of the filtration efficiency of $%. In addition, this application relies on the far-distance 2-line buffering method, which completely utilizes the airflow to drive the test gas mist. The nozzle enters the aerosol chamber to eliminate the influence of gravity and sedimentation, so that the test aerosol reaching the aerosol chamber meets the test. The conditions of demand can increase the stability of the test. In addition, the use of buffer bottles for buffering eliminates the need for traditional inspections to require repeated disassembly and assembly between the preparation and testing phases, resulting in external contamination and variations in detection conditions, further improving the convenience of operation. Sex and the reliability of the test results. The present invention has been disclosed in the above embodiments, and is not intended to limit the present invention. Any one skilled in the art can make various modifications and retouchings without departing from the spirit and scope of the present invention. The scope is subject to the definition of the scope of the patent application attached. BRIEF DESCRIPTION OF THE DRAWINGS In order to make the above and other objects, features, advantages and embodiments of the present invention more obvious and obvious, the description of the drawings is as follows: Figure 1 shows a preferred embodiment of the present invention. A schematic diagram of a detection device. FIG. 2 is a schematic view showing a buffer bottle and a connecting tube of the detecting device according to another preferred embodiment of the present invention. Figure 3 is a flow diagram of a detection method in accordance with a preferred embodiment of the present invention. Figure 4 is a graph showing the distribution of the number and particle size of the test aerosol particles. 201028677 [Description of main component symbols] 100: Detection device 110: buffer bottle 110a: inlet port 110b: discharge port 111: side 120: atomizer 130: connection tube 130': connection tube 140: aerosol chamber 140a Upper end opening 140b: Lower end opening 150: Sampler 160: Vacuum pump 170: Air pump® 180: Syringe pump A: Curve B: Curve D1: Feeding direction D2: Discharge direction D2': Discharge direction F: Filter material L1 : The long axis direction of the buffer bottle L2: the long axis direction of the aerosol chamber 0: acute angle S: test aerosol 14

Claims (1)

201028677 七、申請專利範圍: 1. 一種檢測裝置,包括: 一緩衝瓶,具有一進料口及一出料口,分別用以使一 試驗氣霧進入及離開該緩衝瓶,並且分別位於該緩衝瓶之頂端 及侧邊; 一霧化器,設置於該進料口,用以將一試驗液霧化為 該試驗氣霧; 一氣霧腔,具有一上端開口及一下端開口,離開該緩 •衝瓶之該試驗氣霧由該上端開口進入該氣霧腔;以及 一採樣器,經由該下端開口連接於該氣霧腔,用以接 收經由一濾材過濾後之該試驗氣霧,藉以檢驗該濾材之過 濾效率,該濾材設置於該氣霧腔及該採樣器之間。 2. 如申請專利範圍第1項所述之檢測裝置,其中該 檢測裝置更包括: 一真空泵,用以提供一氣流通過該緩衝瓶、該氣霧腔 φ 及該採樣器,以帶動該試驗氣霧。 3. 如申請專利範圍第2項所述之檢測裝置,其中該 氣流係依序通過該緩衝瓶、該氣霧腔及該採樣器,該真空 泵設置於該採樣器之下游。 4. 如申請專利範圍第1項所述之檢測裝置,其中該 霧化器為一氣壓式氣霧產生器。 15 201028677 5·如申請專利範圍第1項所述之檢測裝置,其中未 被霧化之該試驗液係滴落至該緩衝瓶底部。 6.如申請專利範圍第1項所述之檢測裝置,其中該 緩衝瓶及該氣霧腔分別具有一長軸方向,該緩衝瓶之長軸 方向及該氣霧腔之長軸方向分別大致上垂直於一水平面。 ’ - • · ·. ··· . 7·如申請專利範圍第6項所述之檢測裝置,其中該 緩衝瓶之長軸方向大致平行於該氣霧腔之長轴方向。 8. 如申請專利範圍第7項所述之檢測裝置,其中該 進料口及該上端開口位於不同之長軸方向上。 9. 如申請專利範圍第6項所述之檢測裝置,其中該 檢測裝置更包括: Λ 一連接管,兩端分別連接於該出料口及該上端開口, 該連接管連接於該出料口處之高度大於該連接管連接於該 上端開口處之高度。 10. 如申請專利範圍第9項所述之檢測裴置,其中該 連接管係朝向該緩衝瓶之底部傾斜。 11 ·如申請專利範圍第1項所述之檢測裝置’其中該 16 201028677 檢測裝置更包括: 一連接管,兩端分別連接於該出料口及該上端開口, 該連接管垂直於該緩衝瓶之侧邊。 12.如申請專利範圍第1項所述之檢測裝置,其中該 出料口與該緩衝瓶底部之距離大於該出料口與該緩衝瓶頂 端之距離。 φ 13. —種過濾效率之檢測方法,包括: 提供一試驗氣霧沿一進料方向進入一緩衝瓶; 導引該試驗氣霧由一出料方向離開該緩衝瓶,該進料 方向非平行於該出料方向; 分散該試驗氣霧於一氣霧腔中; 過濾該試驗氣霧;以及 接收過濾後之該試驗氣霧,藉以檢測過濾效率。 ❿ 14.如申請專利範圍第13項所述之檢測方法,其中於 提供該試驗氣霧之該步驟前,該檢測方法更包括: 霧化一試驗液以形成該試驗氣霧。 15.如申請專利範圍第14項所述之檢測方法,其中於 導引該試驗氣霧之該步驟前,該檢測方法更包括: 分離該試驗氣霧及未被霧化之該試驗液。 17 201028677 16.如申請專利範圍第13項所述之檢測方法,其中該 檢測方法更包括: 提供一氣流通過該緩衝瓶及該氣霧腔,以帶動該試驗 氣霧。 17.如申請專利範圍第13項所述之檢測方法,其中於 提供該試驗氣霧之該步驟中,該試驗氣霧經由位於該緩衝 瓶頂端之一進料口沿該進料方向進入該緩衝瓶,並經由位 於該緩衝瓶之侧邊之一出料口沿該出料方向離開該緩衝 瓶0 18. 如申請專利範圍第17項所述之檢測方法,其中於 導引該試驗氣霧之該步驟中,該進料方向大致垂直於該出 料方向。 19. 如申請專利範圍第17項所述之檢測方法,其中於 φ 導引該試驗氣霧之該步驟中,該緩衝瓶之側邊對應於該出 料口及該緩衝瓶底部之間的部分,與該出料方向夾有一銳 角0 18201028677 VII. Patent application scope: 1. A detecting device comprising: a buffer bottle having a feeding port and a discharging port for respectively injecting a test aerosol into and out of the buffer bottle, and respectively located in the buffer a top end and a side of the bottle; an atomizer disposed at the feed port for atomizing a test liquid into the test gas mist; an aerosol chamber having an upper end opening and a lower end opening, leaving the slow The test aerosol of the rinsing bottle enters the aerosol chamber from the upper end opening; and a sampler is connected to the aerosol chamber via the lower end opening for receiving the test aerosol filtered through a filter material, thereby verifying the test The filtering efficiency of the filter medium is disposed between the aerosol chamber and the sampler. 2. The detecting device of claim 1, wherein the detecting device further comprises: a vacuum pump for providing an air flow through the buffer bottle, the aerosol chamber φ and the sampler to drive the test gas fog. 3. The detecting device of claim 2, wherein the air flow sequentially passes through the buffer bottle, the aerosol chamber, and the sampler, the vacuum pump being disposed downstream of the sampler. 4. The detecting device of claim 1, wherein the atomizer is a pneumatic aerosol generator. The test device of claim 1, wherein the test liquid that has not been atomized is dropped to the bottom of the buffer bottle. 6. The detecting device according to claim 1, wherein the buffer bottle and the aerosol chamber respectively have a long axis direction, and a longitudinal direction of the buffer bottle and a longitudinal direction of the aerosol chamber are substantially respectively Vertical to a horizontal plane. 7. The detecting device according to claim 6, wherein the buffer bottle has a major axis direction substantially parallel to a longitudinal direction of the aerosol chamber. 8. The detecting device of claim 7, wherein the feed port and the upper end opening are located in different major axis directions. 9. The detecting device of claim 6, wherein the detecting device further comprises: 连接 a connecting pipe, the two ends are respectively connected to the discharging port and the upper end opening, and the connecting pipe is connected to the discharging port The height is greater than the height at which the connecting tube is connected to the upper end opening. 10. The test device of claim 9, wherein the connecting tube is inclined toward the bottom of the buffer bottle. 11. The detecting device of claim 1, wherein the 16 201028677 detecting device further comprises: a connecting pipe, the two ends are respectively connected to the discharging port and the upper end opening, the connecting pipe is perpendicular to the buffer bottle Side. 12. The detecting device of claim 1, wherein the distance between the discharge opening and the bottom of the buffer bottle is greater than the distance between the discharge opening and the top end of the buffer bottle. Φ 13. A method for detecting filtration efficiency, comprising: providing a test gas mist into a buffer bottle along a feeding direction; guiding the test gas mist to leave the buffer bottle in a discharge direction, the feeding direction is non-parallel In the discharge direction; dispersing the test aerosol in an aerosol chamber; filtering the test aerosol; and receiving the filtered test aerosol to detect filtration efficiency. The method of claim 13, wherein before the step of providing the test aerosol, the detecting method further comprises: atomizing a test liquid to form the test aerosol. 15. The method according to claim 14, wherein the detecting method further comprises: separating the test aerosol and the test liquid that has not been atomized before the step of guiding the test aerosol. The method of claim 13, wherein the detecting method further comprises: providing a gas flow through the buffer bottle and the aerosol chamber to drive the test aerosol. 17. The method according to claim 13, wherein in the step of providing the test aerosol, the test gas mist enters the buffer in the feed direction via a feed port located at one of the top ends of the buffer bottle. a bottle, and exiting the buffer bottle in the discharge direction via a discharge port located at a side of the buffer bottle. 18. The test method of claim 17, wherein the test aerosol is guided In this step, the feed direction is substantially perpendicular to the discharge direction. 19. The method according to claim 17, wherein in the step of guiding the test aerosol, the side of the buffer bottle corresponds to a portion between the discharge port and the bottom of the buffer bottle. , with an acute angle of the discharge direction 0 18
TW98102312A 2009-01-21 2009-01-21 Test equipment and test method TWI385374B (en)

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JP2005189025A (en) * 2003-12-25 2005-07-14 Miura Co Ltd Method for collecting residual organic pollutant and sampler
EP1688731A1 (en) * 2005-02-03 2006-08-09 Air Products and Chemicals, Inc. System and method for measurement and/or analysis of particles in gas stream

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