TW200706493A - Method for producing dodecahydrododecaborates - Google Patents

Method for producing dodecahydrododecaborates

Info

Publication number
TW200706493A
TW200706493A TW095121321A TW95121321A TW200706493A TW 200706493 A TW200706493 A TW 200706493A TW 095121321 A TW095121321 A TW 095121321A TW 95121321 A TW95121321 A TW 95121321A TW 200706493 A TW200706493 A TW 200706493A
Authority
TW
Taiwan
Prior art keywords
dodecahydrododecaborates
producing
tetrahydroborates
lewis
acid
Prior art date
Application number
TW095121321A
Other languages
English (en)
Inventor
Sergei Vladimirovich Ivanov
Baldomero Casas
Original Assignee
Air Prod & Chem
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Air Prod & Chem filed Critical Air Prod & Chem
Publication of TW200706493A publication Critical patent/TW200706493A/zh

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F5/00—Compounds containing elements of Groups 3 or 13 of the Periodic System
    • C07F5/02—Boron compounds
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B6/00—Hydrides of metals including fully or partially hydrided metals, alloys or intermetallic compounds ; Compounds containing at least one metal-hydrogen bond, e.g. (GeH3)2S, SiH GeH; Monoborane or diborane; Addition complexes thereof
    • C01B6/06—Hydrides of aluminium, gallium, indium, thallium, germanium, tin, lead, arsenic, antimony, bismuth or polonium; Monoborane; Diborane; Addition complexes thereof
    • C01B6/10—Monoborane; Diborane; Addition complexes thereof
    • C01B6/13—Addition complexes of monoborane or diborane, e.g. with phosphine, arsine or hydrazine
    • C01B6/15—Metal borohydrides; Addition complexes thereof
    • C01B6/19—Preparation from other compounds of boron
    • C01B6/21—Preparation of borohydrides of alkali metals, alkaline earth metals, magnesium or beryllium; Addition complexes thereof, e.g. LiBH4.2N2H4, NaB2H7

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
TW095121321A 2005-06-16 2006-06-14 Method for producing dodecahydrododecaborates TW200706493A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US69122205P 2005-06-16 2005-06-16
US11/448,021 US20060286020A1 (en) 2005-06-16 2006-06-07 Method for producing dodecahydrododecaborates

Publications (1)

Publication Number Publication Date
TW200706493A true TW200706493A (en) 2007-02-16

Family

ID=36955658

Family Applications (1)

Application Number Title Priority Date Filing Date
TW095121321A TW200706493A (en) 2005-06-16 2006-06-14 Method for producing dodecahydrododecaborates

Country Status (6)

Country Link
US (1) US20060286020A1 (zh)
EP (1) EP1734003A3 (zh)
JP (1) JP2006347874A (zh)
KR (1) KR100758573B1 (zh)
CN (1) CN100584756C (zh)
TW (1) TW200706493A (zh)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7718154B2 (en) * 2005-06-16 2010-05-18 Air Products And Chemicals, Inc. Process for producing boranes
JP2009114174A (ja) * 2007-11-05 2009-05-28 Rohm & Haas Co ＭｎＢ１２Ｈ１２の調製
EP2206680A3 (en) * 2009-01-09 2011-04-06 Rohm and Haas Company Synthesis of Alkali Metal Dodecaborates
WO2013115889A2 (en) 2011-11-18 2013-08-08 The Curators Of The University Of Missouri Process and device for the production of polyhedral boranes
CN105210151B (zh) 2013-03-15 2017-07-14 赛瑞丹公司 使核反应堆冷却的方法以及包含多面体硼烷阴离子或碳硼烷阴离子的核反应堆
WO2015117119A1 (en) * 2014-02-03 2015-08-06 The Curators Of The University Of Missouri Synthesis of borane compounds
WO2015117123A1 (en) * 2014-02-03 2015-08-06 The Curators Of The University Of Missouri Synthesis of amine boranes and polyhedral boranes
CA2946854A1 (en) * 2014-04-25 2015-10-29 Ceradyne, Inc. Pool including aqueous solution of polyhedral boron hydride anions or carborane anions and methods of using the same
CN104557570B (zh) * 2015-01-27 2016-06-08 郑州西格玛化工有限公司 一种十二氢十二硼酸双四乙基铵的制备方法
RU2647733C1 (ru) * 2016-10-27 2018-03-19 Федеральное государственное бюджетное учреждение науки Институт органического синтеза им. И.Я. Постовского Уральского отделения Российской академии наук Способ получения солей додекагидрододекабората B12H12 2-
CN106829865A (zh) * 2017-01-21 2017-06-13 北京理工大学 一种制备k2b12h12的方法
CN107473184B (zh) * 2017-08-02 2019-09-13 河南师范大学 一种锂的硼氢化合物LiB3H8的合成方法
CZ308510B6 (cs) * 2019-08-07 2020-10-07 Katchem Spol. S R.O. Způsob přípravy bezvodých solí aniontu B12H12 2- s kationty I.A a II.A skupiny
CN111573624B (zh) * 2020-06-28 2021-10-15 郑州原理生物科技有限公司 利用十氢十硼双四乙基铵盐的副产物制备十二氢十二硼双钠盐的方法

Family Cites Families (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2830070A (en) * 1954-12-01 1958-04-08 Callery Chemical Co Preparation of trimethyl borate
US2927124A (en) * 1955-05-16 1960-03-01 Callery Chemical Co Preparation of trimethoxyboroxine
US2969274A (en) * 1955-06-09 1961-01-24 Callery Chemical Co Cyclic process for production of sodium borohydride
US3013016A (en) * 1957-05-24 1961-12-12 Bayer Ag Trialkylamine boranes and their preparation
US3257455A (en) * 1959-08-07 1966-06-21 Ethyl Corp Preparation of boron hydrides and amine boranes
US3169045A (en) * 1960-05-20 1965-02-09 Du Pont Dodecahydrododecaborate compounds
US3127448A (en) * 1960-09-21 1964-03-31 Metal Hydrides Inc Method for preparing tertiary amine boranes
US3355261A (en) * 1963-04-29 1967-11-28 Du Pont Chemical process
US3265737A (en) * 1964-11-03 1966-08-09 Du Pont Boron amines and process for formation thereof
US3328134A (en) * 1964-12-28 1967-06-27 Du Pont Process for preparing polyhydropolyborates
US3961017A (en) * 1975-03-24 1976-06-01 Mine Safety Appliances Company Production of dodecahydrododecaborate (2-)
US5144032A (en) * 1988-10-05 1992-09-01 E. I. Du Pont De Nemours And Company Preparation of tertiary amine borane adducts
US5262544A (en) * 1993-05-10 1993-11-16 The United States Of America As Represented By The Secretary Of The Navy 5,7-dinitro-5,7-diaza-1,3-dioxabicyclo(3:3:0)octan-2-one
US5886229A (en) * 1998-05-29 1999-03-23 Mine Safety Appliances Company Method of synthesis of alkali metal trisubstituted borohydride reagents
US7247286B2 (en) * 2003-02-25 2007-07-24 Rohm And Haas Company Process for production of sodium borohydride from sodium aluminum hydride with recycle of byproducts
US7311993B2 (en) * 2003-09-04 2007-12-25 Air Products And Chemicals, Inc. Polyfluorinated boron cluster anions for lithium electrolytes
US7718154B2 (en) * 2005-06-16 2010-05-18 Air Products And Chemicals, Inc. Process for producing boranes

Also Published As

Publication number Publication date
EP1734003A2 (en) 2006-12-20
EP1734003A3 (en) 2009-04-15
KR20060131693A (ko) 2006-12-20
JP2006347874A (ja) 2006-12-28
CN100584756C (zh) 2010-01-27
US20060286020A1 (en) 2006-12-21
CN1880221A (zh) 2006-12-20
KR100758573B1 (ko) 2007-09-14

Similar Documents

Publication Publication Date Title
TW200706493A (en) Method for producing dodecahydrododecaborates
TW200606581A (en) A chemically amplified positive resist composition, a haloester derivative and a process for producing the same
GB0401088D0 (en) Phosphoramidate derivatives
WO2004027822A3 (en) Oriented nanostructures and methods of preparing
WO2006027705A3 (en) Synthesis of triethylenetetramines
UA94833C2 (en) Substituted bicyclolactams
TW200744588A (en) Pharmaceutical composition for external use
MX2009003698A (es) Preparacion de azoxistrobina.
TW200733880A (en) Method for low light cultivation and plant growth-promoting agent
BRPI0518188A (pt) modificador de espuma, espumas preparadas a partir deste modificador de espuma, e processo para a preparação dessas espumas
WO2008058235A3 (en) Processes for the preparation of cinacalcet
WO2007023342A3 (en) Process of making geminal bisphosphonic acids and pharmaceutically acceptable salts and/or hydrates thereof
DK1606242T3 (da) Azidfri fremgangsmåde til fremstilling af 1,2-diaminoforbindelser
PT2049480E (pt) Derivados de 2-arilindole como inibidores da mpges-i
WO2007016029A3 (en) Diazepinoquinolines, synthesis thereof, and intermediates thereto
TW200720233A (en) Hydroxynaphthalenedicarboxylic acid hydrazide dimer and derivatives thereof as well as process for preparing them
WO2008015584A3 (en) Improved process for synthesizing desvenlafaxine free base and salts or solvates thereof
EP1598346A4 (en) PROCESS FOR PRODUCING AN ACID ADDITION SALT OF A POLYACID COMPOUND
UA96149C2 (en) Method for producing 4-oxoquinoline compound
YU101103A (en) Technical synthesis method for producing tropenol
NO20053208L (no) Metode for reduktiv dehalogenering.
ITMI20020933A1 (it) Procedimento per la sintesi di clopidogrel
WO2005075490A3 (en) Synthesis of polysulfated uronic acid glycosides
EP2420471A3 (en) Method of producing (NH2(R2)) and/or hydrogen
WO2007030848A3 (de) Nichtfluoreszierende chlorophyllkataboliten