TR202017274A2 - OBTAINING PROTEIN FROM GROUND PISTACHIO AND USING LEFT POSAN AS A FUNCTIONAL FOOD ADDITIVE - Google Patents

OBTAINING PROTEIN FROM GROUND PISTACHIO AND USING LEFT POSAN AS A FUNCTIONAL FOOD ADDITIVE Download PDF

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TR202017274A2
TR202017274A2 TR2020/17274A TR202017274A TR202017274A2 TR 202017274 A2 TR202017274 A2 TR 202017274A2 TR 2020/17274 A TR2020/17274 A TR 2020/17274A TR 202017274 A TR202017274 A TR 202017274A TR 202017274 A2 TR202017274 A2 TR 202017274A2
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proteins
protein
peanuts
pulp
obtaining
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TR2020/17274A
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Turkish (tr)
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Çeli̇k Mahi̇r
Kayacilar Can
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Kayacilar Can
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Abstract

Buluş, yer fıstığından isoelektrik pH yöntemi kullanılarak proteinlerin elde edilmesini ve ayrıca işlem sonucunda kalan posanın gıda katkı maddesi ve fonksiyonel gıda bileşeni olarak kullanılması ile ilgilidir. Buluş özellikle yer fıstığından, su ve sodyum hidroksit, potasyum hidroksit, kalsiyum karbonat, sodyum karbonat gibi pH yükseltici ajanlar eklenip, karıştırılarak özütün elde edilmesi ve dekantör aracılığıyla ayrıştırılan özütten, posa ve izole bitkisel proteinlerin elde edilmesi ile ilgilidir.The invention relates to obtaining proteins from peanuts by using the isoelectric pH method and also using the pulp remaining as a food additive and functional food ingredient. In particular, the invention relates to obtaining extract from peanuts by adding water and pH increasing agents such as sodium hydroxide, potassium hydroxide, calcium carbonate, sodium carbonate, mixing them, and obtaining pulp and isolated vegetable proteins from the extract separated by means of a decanter.

Description

TARIFNAME YER FISTIGINDAN PROTEIN ELDESI VE GERIYE KALAN POSANIN FONKSIYONEL GIDA KATKI MADDESI OLARAK KULLANILMASI TEKNIK ALAN Bulus, yerfistigindan isoelektrik pH yöntemi kullanilarak proteinlerin elde edilmesini ve ayrica islem sonucunda kalan posanin gida katki maddesi ve fonksiyonel gida bileseni olarak kullanilmasi ile ilgilidir. DESCRIPTION FUNCTIONAL FOOD ADDITIVE TO OBTAIN PROTEIN FROM PEASTEN AND REMAIN FRUIT USING AS AN INGREDIENT TECHNICAL FIELD The invention is to obtain proteins from peanuts using the isoelectric pH method and also The remaining fiber as a food additive and functional food component relates to its use.

Bulus özellikle; yer fistigina, su ve sodyum hidroksit, potasyum hidroksit, calcium carbonat, sodyum karbonat gibi pH yükseltici ajanlar eklenip, karistirilarak 1:10 su oraninda özütün elde edilmesi ve dekantör araciligiyla ayristirilan özütten, posa ve protein zengini solüsyonun ayri ayri elde edilmesi ile ilgilidir. The invention especially; ground fistigina, water and sodium hydroxide, potassium hydroxide, calcium carbonate, By adding pH increasing agents such as sodium carbonate and mixing, the extract is obtained at a ratio of 1:10 to water. The pulp and protein-rich solution is separated from the extract separated by the decanter. is related to the acquisition.

TEKNIGIN BILINEN DURUMU Gida katkilari/takviyeleri sagliginizi en iyi düzeye çikarmak için gerekli vitamin, mineral ve diger önemli besin ögelerini günlük Önerilen düzeyde alabilmenizin etkili bir yoludur. Zorunlu yasam kosullari, organik yiyeceklere ulasim imkaninin az olmasi ve alerji/intolerans durumlari nedeniye bazi yiyeceklerin diyetten çikarilmasi gibi etmenlerden dolayi her zaman tüm besin ögelerini almamiz mümkün olmamaktadir. Diyetinizi gida takviyeleri ile destekleyebilirsiniz. KNOWN STATE OF THE TECHNIQUE Food additives/supplements provide essential vitamins, minerals and other nutrients to optimize your health. It is an effective way to get important nutrients at the daily Recommended level. forced living conditions, lack of access to organic food, and allergy/intolerance situations always all nutrients due to factors such as the removal of certain foods from the diet It is not possible for us to receive items. You can supplement your diet with food supplements.

Burada sunu da belirtilmelidir ki gida takviyesi üretimi ile dogal yiyeceklerin yerini almak hedeflenmemektedir. Günümüzün gida takviyeleri; vitamin, mineral, amino asit, enzim, bitki tohumlari ve diger pek çok besin bilesenini bir arada içermektedir. Bu takviyeler geleneksel tablet, kapsül, tozlar ve sivi formlar, baska ürünlere eklenen takviyeler olmak üzere çok farkli seçenekte karsimiza çikmaktadir. It should also be mentioned here that with the production of food supplements, it is necessary to replace natural foods. is not targeted. Today's food supplements; vitamins, minerals, amino acids, enzymes, herbs It contains seeds and many other nutritional components together. These supplements are traditional tablets, capsules, powders and liquid forms, supplements added to other products. appears in the option.

Mevcut teknikte yer fistigindan pH bagimli izoelektrik nokta yöntemi kullanilarak yer fistigi proteinlerin yüksek verimde elde edilmesi ve elde edilen proteinlerin gidalarda kullanimlarinin saglanmasi bugüne kadar yapilmamistir. Elde edilecek yer fistigi proteinlerinin gidalarin protein degerlerinin arttirilmasinda kullanilmasi ve ayrica haricen protein destegi olarak kullanilmasi söz konusudur. Ülkemizde bu tarzda uygulamalar bulunmamaktadir. Ayrica islem sonrasinda yer fistigindan elde edilen posanin da fonksiyonel gida katki maddesi olarak kullanilmasi söz konusudur. In the current technique, peanuts are harvested using the pH-dependent isoelectric point method from peanuts. obtaining proteins in high efficiency and using the obtained proteins in foods provision has not been made to date. of peanut proteins to be obtained to be used to increase protein values and also as an external protein supplement is to be used. There are no such practices in our country. In addition, the transaction Afterwards, the pulp obtained from peanuts is also used as a functional food additive. is to be used.

Sonuç olarak, mevcut teknikte var olan yukarida belirtilen problemlerin çözümü için, yeni bir ekonomik, kullanisli bir yer fistigi proteinli gida katkisi/takviyesine duyulan gereksinim ve mevcut çözümlerin yetersizligi ilgili teknik alanda bir gelistirme yapmayi zorunlu kilmistir. As a result, for the solution of the above-mentioned problems existing in the current art, a new the need for an economical, useful peanut protein food additive/supplement, and The inadequacy of existing solutions has made it necessary to make an improvement in the relevant technical field.

BULUSUN AMACI Mevcut bulus yukarida bahsedilen dezavantajlari ortadan kaldirmak ve ilgili teknik alana yeni avantajlar getirmek üzere gelistirilen yer fistigindan isoelektrik pH yöntemi kullanilarak proteinlerin elde edilmesini ve ayrica islem sonucunda kalan posanin gida katki maddesi ve fonksiyonel gida bileseni olarak kullanilmasi ile ilgilidir. OBJECTIVE OF THE INVENTION The present invention is intended to eliminate the above mentioned disadvantages and to introduce new technologies into the relevant technical field. using the isoelectric pH method from peanuts, which was developed to bring advantages obtaining the proteins and also the remaining pulp as a result of the processing as a food additive and related to its use as a functional food ingredient.

Bulusun en önemli amaci, yer fistigindan yesil sentez yoluyla (yani gidaya uyumlu olmayan kimyasallar kullanmayarak) pH bagimli izoelektrik ayrimdan faydalanarak proteinlerin elde edilmesidir. Elde edilecek ürün en az %80 saflikta protein içermektedir. Izole Bitkisel Protein gida alaninda olarak kullanimi söz konusudur. The most important object of the invention is the green synthesis from peanuts (i.e. non-food compatible). without using chemicals) to obtain proteins by utilizing pH-dependent isoelectric separation. is to be done. The product to be obtained contains at least 80% pure protein. Isolated Vegetable Protein It is used in the field of food.

Bulusun diger bir amaci, yer fistigindan protein alinmasi sonrasinda elde edilen yer fistigi posasinin da gida katki maddesi olarak kullanilmasidir. Dengeli bir gida bilesen içerigine sahiptir. Yüksek lif, karbonhidrat ve protein içermektedir. Another aim of the invention is to obtain peanuts after taking protein from peanuts. Its pulp is also used as a food additive. A balanced food ingredient content has. It contains high fiber, carbohydrates and protein.

Bulusun yapisal ve karakteristik özellikleri ve tüm avantajlari asagida verilen detayli açiklama sayesinde daha net olarak anlasilacaktir ve bu nedenle degerlendirmenin de bu detayli açiklama göz önüne alinarak yapilmasi gerekmektedir. The structural and characteristic features of the invention and all its advantages are described in detail below. will be more clearly understood by means of must be made taking into account the description.

BULUSUN DETAYLI AÇIKLAMASI Bu detayli açiklamada, bir yer fistigindan elde edilen gida katkisi/takviyesinin tercih edilen yapilanmalari, sadece konunun daha iyi anlasilmasina yönelik olarak ve hiçbir sinirlayici etki olusturmayacak sekilde açiklanmaktadir. DETAILED DESCRIPTION OF THE INVENTION In this detailed description, the preferred food additive/supplement from a peanut structuring is only for a better understanding of the subject and has no limiting effect. described in a way that does not constitute.

Bulusumuz yer fistigindan yesil sentez yoluyla (yani gidaya uyumlu olmayan kimyasallar kullanmayarak) pH bagimli izoelektrik ayrimdan faydalanarak proteinlerin özütlenmesini içermektedir. Bulusumuz ile en az %80 saflikta protein elde edilmektedir. Izole Bitkisel Protein gida alaninda olarak kullanimi söz konusudur. Ayrica yer fistigindan protein ekstraksiyonu sonrasinda elde edilen yer fistigi posasinin da gida katki maddesi olarak kullanilmaktadir. Ortaya çikan bu posa dengeli bir gida bilesen içerigine sahiptir. Yüksek lif, karbonhidrat ve protein içermektedir. Our invention is through green synthesis from peanuts (ie chemicals that are not compatible with food). leaching of proteins by utilizing pH-dependent isoelectric separation. contains. With our invention, at least 80% pure protein is obtained. Herbal Isolated It is used in the field of protein food. Also protein from peanuts The peanut pulp obtained after the extraction is also used as a food additive. is used. The resulting pulp has a balanced food component content. high fiber, contains carbohydrates and protein.

Yer fistigindan protein elde edilmesi asagidaki sekilde gerçeklestirilmektedir: Yer fistiklari mikron ögütücüler kullanilarak ögütülür. Daha sonra yaginin çikarilmasi için yag çikartici makinelerde su ile islenir. Bu islemler yag fabrikalarinda yapilan sikma islemiyle benzerdir. Yagi alinmis yer fistiklari pH bagimli yöntemlerle protein izole edilmekte ve kalan posa da gida katki maddesi olarak kullanilacaktir. Obtaining protein from peanuts is carried out as follows: Peanuts are ground using micron grinders. Then oil to remove the oil It is processed with water in extractor machines. These processes are combined with the squeezing process in oil factories. is similar. Protein is isolated from the oiled peanuts using pH-dependent methods, and the remaining The pulp will also be used as a food additive.

Proteinler öncelikli olarak sodyum hidroksit, potasyum hidroksit, kalsiyum karbonat, sodyum karbonat gibi pH yükseltici ajanlar kullanilarak yagi alinmis yer fistigi ezmelerinden oda sicakliginda ya da en yüksek 100 derece sicaklik kullanilarak 1:10 oraninda su ile ekstrakte edilir. Bu islem öncesinde posalardan yaglarin ve fenolik bilesenlerin uzaklastirilmasi için %50 oraninda etanol içeren su posalardan geçirilebilir. Sonrasinda dekantör ile süzülür ve ekstraksiyona hazir hale getirilir. Ekstraksiyon karistirici bir tankin içerisinde gerçeklestirilir. Proteins are primarily sodium hydroxide, potassium hydroxide, calcium carbonate, sodium from peanut pastes degreased using pH-raising agents such as baking soda. Extract with water at a ratio of 1:10 using a maximum temperature of 100 degrees Celsius. is done. Before this process, 50% of the oils and phenolic components were removed from the pulp. water containing ethanol can be passed through the pulp. Then it is filtered with a decanter and prepared for extraction. Extraction is carried out in a mixing tank.

Ekstraksiyon için 1:10 ile 1:20 oranlari arasinda su kullanilir. Su ve içerisine konulan posanin pH derecesi bazik ajanlarla birlikte 12'ye getirilir. Bu sekilde en az 1 saat boyunca muamele edilir. Bu islem sirasinda sicaklik oda sicakliginda ya da en fazla 100 dereceye kadar getirilir. Water between 1:10 and 1:20 ratios is used for extraction. Water and the pulp put in it The pH is brought to 12 with basic agents. Treat in this way for at least 1 hour is done. During this process, the temperature is brought to room temperature or up to a maximum of 100 degrees.

Bu islem sonrasinda elde edilen özüt dekantör araciligiyla birbirinden ayristirilir. Posa ve protein zengini solüsyon ayri olarak dekantörden alinir. The extract obtained after this process is separated from each other by means of a decanter. pulp and The protein-rich solution is taken separately from the decanter.

Proteinli solüsyon ve posa daha sonra pH dengelemek amaciyla sitrik asitli su ile muamele Protein zengini solüsyon ise pH'si 4-5'e gelene kadar organik asitlerle ya da sitrik asit gibi gida katkilariyla muamele edilir. Solüsyonun pH'si 4-5'e gelmeye basladiginda proteinler kendiliginden çökmeye baslarlar. Bu süreçte solüsyon tekrardan dekantörden geçirilerek proteinler elde edilir. Proteinler safsizliklarindan arindirilmak için 1-2 defa sitrik asitle pH'si 4-5'e getirilmis su ile yikanir. Elde edilen proteinler tepsilere yayilarak konvansiyonel kurutucularda 50 derecelik sicaklikta kurutulur. Ya da püskürtmeli kurutucu kullanilarak püskürtülerek kurutulur. The protein solution and pulp are then treated with citric acid water to balance the pH. The protein-rich solution is mixed with organic acids or food such as citric acid until the pH reaches 4-5. treated with its contributions. When the pH of the solution starts to reach 4-5, the proteins they begin to collapse on their own. In this process, the solution is passed through the decanter again. proteins are obtained. To be purified of protein impurities, it is pHed 1-2 times with citric acid. It is washed with water brought to 4-5. Obtained proteins are spread on trays and conventional dried in dryers at a temperature of 50 degrees. Or using a spray dryer spray dried.

Elde edilen yer fistigi proteinlerinin gidalarin proteince zenginlestirilmesi ve haricen izole bitkisel protein olarak satilmasi amaçlanmaktadir. Bu amaç dogrultusunda ekmek ve unlu mamüller, süt ve süt ürünleri, pastacilik ürünleri, sporcu destekleri, çorbalar, hazir yemekler, kahvaltilik gevrekler ve saglikli atistirmaliklar gibi birçok uygulama alaninda proteince zenginlestirmeler gerçeklestirilecektir. Benzer alanlarda yer fistigi posasi da gida zenginlestirme ajani olarak kullanilacaktir. Ayrica elde edilecek yer fistigi posasi fonksiyonel gida ham maddesi ve haricen de dengeli beslenme katkisi olarak kullanilacaktir. Protein enrichment of the obtained peanut proteins and external isolation It is intended to be sold as vegetable protein. For this purpose, bread and flour products, milk and dairy products, pastry products, sports supplements, soups, ready meals, Protein content in many application areas such as breakfast cereals and healthy snacks. enhancements will be made. In similar areas, peanut pulp is also a food. used as enrichment agent. In addition, the peanut pulp to be obtained is functional. It will be used as food raw material and externally as a balanced nutrition additive.

Bu basvurunun koruma kapsami istemler kisminda belirlenmis olup yukarida kesinlikle örnekleme amaciyla anlatilanlarla sinirli tutulamaz teknikte uzman bir kisinin bulusta ortaya konan yeniligi, benzer yapilanmalari kullanaraktan ortaya koyabilecegi ve/veya bu yapilanmayi ilgili teknikte kullanilan benzer amaçli diger alanlara da uygulayabilecegi açiktir. Dolayisiyla böyle yapilanmalarin yenilik ve özellikle teknigin bilinen durumunun asilmasi kriterinden yoksun olacagi da asikârdir. The scope of protection of this application has been determined in the claims section and It cannot be limited to what is described for exemplary purposes. It is revealed in the invention by a person skilled in the art. that the innovation can be demonstrated by using similar structures and/or It is clear that it can also be applied to other fields with similar purposes used in the related technique. Therefore such structuring is one of the criteria of innovation and especially overcoming the state of the art. It is obvious that it will be lacking.

Claims (2)

ISTEMLERREQUESTS 1- Bulus yer fistigindan isoelektrik pH yöntemi kullanilarak proteinlerin elde edilmesi ile ilgili olup, özelligi; Yer fistiginin mikron ögütücüler ile ögütülüp, yaginin çikarilarak yer fistigi ezmesi elde edilmesi, Ezmeden yerine göre yaglarin ve fenolik bilesenlerin uzaklastirilmasi için küspenin etanol içeren sudan geçirilmesi, karistirici bir tank içerisine yer fistigi ezmesi, su ve sodyum hidroksit, potasyum hidroksit, kalsiyum karbonat, sodyum karbonat gibi pH yükseltici ajanlar eklenip, karistirilarak özütün elde edilmesi, dekantör araciligiyla ayristirilan özütten, posa ve protein zengini solüsyonun elde edilmesi, Protein zengini solüsyonun pH'si 4-5'e gelene kadar organik asitlerle ya da sitrik asit gibi gida katkilariyla muamele edilerek, proteinlerin kendiliginden çökmeye baslamasi, Proteinleri çökmeye baslayan solüsyonun tekrar dekantörden geçirilerek proteinlerin elde edilmesi, Proteinlerin, safsizliklarindan arinmasi için sitrik asitli pH'si 3-5'e getirilmis su ile yikanmasi, elde edilen proteinlerin konvansiyonel ya da püskürtmeli kurutucu kullanilarak kurutulmasi Islem adimlarini içermesi ile karakterize edilmesidir.1- The invention is about obtaining proteins from peanuts by using isoelectric pH method. Peanuts are ground with micron grinders and the oil is removed to obtain peanut paste, Passing the pulp through water containing ethanol to remove the oils and phenolic compounds from the crushing, peanut paste, water and sodium hydroxide, potassium hydroxide, sodium carbonate, Adding pH-raising agents such as carbonate and mixing to obtain the extract, Obtaining pulp and protein-rich solution from the extract separated by the decanter, Treating the protein-rich solution with organic acids or food additives such as citric acid until the pH of the protein-rich solution reaches 4-5, Proteins starting to precipitate on their own, Obtaining proteins by passing the solution that starts to precipitate through the decanter again, Washing the proteins with citric acid pH-adjusted water to 3-5 in order to purify them from their impurities, Drying the obtained proteins using conventional or spray dryers. is characterized by its resilience. 2- Istem 1'e uygun gida takviyesi ve fonksiyonel gida katki maddesi olup, özelligi; yer fistigindan proteinlerin elde edilmesi sirasinda ortaya çikan posanin pH'ni dengelemek amaciyla sitrik asitli su ile muamele edilerek elde edilmesi ile karakterize edilmesidir.2- It is a food supplement and functional food additive in accordance with claim 1, its feature is; It is characterized by the fact that it is obtained by treating the pulp that emerges during the extraction of proteins from peanuts with citric acid water in order to balance the pH.
TR2020/17274A 2020-10-29 2020-10-29 OBTAINING PROTEIN FROM GROUND PISTACHIO AND USING LEFT POSAN AS A FUNCTIONAL FOOD ADDITIVE TR202017274A2 (en)

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