TR201904928T4 - Method for the production of terephthalic acid diesters by recirculating alcohol dehydration. - Google Patents
Method for the production of terephthalic acid diesters by recirculating alcohol dehydration. Download PDFInfo
- Publication number
- TR201904928T4 TR201904928T4 TR2019/04928T TR201904928T TR201904928T4 TR 201904928 T4 TR201904928 T4 TR 201904928T4 TR 2019/04928 T TR2019/04928 T TR 2019/04928T TR 201904928 T TR201904928 T TR 201904928T TR 201904928 T4 TR201904928 T4 TR 201904928T4
- Authority
- TR
- Turkey
- Prior art keywords
- terephthalic acid
- production
- acid diesters
- alcohol dehydration
- recirculating
- Prior art date
Links
- KKEYFWRCBNTPAC-UHFFFAOYSA-N benzene-dicarboxylic acid Natural products OC(=O)C1=CC=C(C(O)=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-N 0.000 title abstract 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 title abstract 2
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- -1 terephthalic acid diesters Chemical class 0.000 title abstract 2
- 230000018044 dehydration Effects 0.000 title 1
- 238000006297 dehydration reaction Methods 0.000 title 1
- 238000000034 method Methods 0.000 title 1
- 230000003134 recirculating effect Effects 0.000 title 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
- C07C69/76—Esters of carboxylic acids having a carboxyl group bound to a carbon atom of a six-membered aromatic ring
- C07C69/80—Phthalic acid esters
- C07C69/82—Terephthalic acid esters
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00132—Controlling the temperature using electric heating or cooling elements
Abstract
Buluş tereftalik asit diesterler tereftalik asidin en azından bir alkol ile reaksiyonuyla üretilmesi için bir yöntem ile ilgilidir.The invention relates to a method for producing terephthalic acid diesters by reaction of terephthalic acid with at least one alcohol.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP14186143 | 2014-09-24 |
Publications (1)
Publication Number | Publication Date |
---|---|
TR201904928T4 true TR201904928T4 (en) | 2019-05-21 |
Family
ID=51660314
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
TR2019/04928T TR201904928T4 (en) | 2014-09-24 | 2015-09-21 | Method for the production of terephthalic acid diesters by recirculating alcohol dehydration. |
Country Status (12)
Country | Link |
---|---|
US (1) | US10207978B2 (en) |
EP (1) | EP3197859B1 (en) |
CN (1) | CN106715382A (en) |
BR (1) | BR112017005839A2 (en) |
CA (1) | CA2962305C (en) |
ES (1) | ES2724982T3 (en) |
MX (1) | MX2017003920A (en) |
PL (1) | PL3197859T3 (en) |
RU (1) | RU2668223C1 (en) |
TR (1) | TR201904928T4 (en) |
TW (1) | TW201612150A (en) |
WO (1) | WO2016046118A1 (en) |
Families Citing this family (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107849224B (en) | 2015-07-09 | 2021-06-08 | 巴斯夫欧洲公司 | Curable composition |
CN112439377A (en) * | 2019-08-29 | 2021-03-05 | 江苏察克润滑科技有限公司 | A reation kettle for preparing antirust liquid |
KR20220067385A (en) * | 2020-11-17 | 2022-05-24 | 주식회사 엘지화학 | Method for preparing diester compound |
CN115282894A (en) * | 2022-06-30 | 2022-11-04 | 福建久策气体股份有限公司 | Difluoro ethyl acetoacetate production device and working method thereof |
Family Cites Families (35)
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GB798439A (en) * | 1954-10-26 | 1958-07-23 | Bayer Ag | Process for the manufacture of terephthalic acid dimethyl ester |
DE1286003B (en) * | 1966-06-21 | 1969-01-02 | Metallgesellschaft Ag | Process for the continuous esterification of terephthalic and isophthalic acid with ethylene glycol |
US3617226A (en) * | 1968-04-26 | 1971-11-02 | Huels Chemische Werke Ag | Apparatus for the continuous preparation of esters |
BE789047A (en) * | 1971-09-20 | 1973-03-20 | Montedison Spa | PROCESS FOR THE CONTINUOUS ESTERIFICATION OF DICARBOXYLIC ACIDS AND ALCOHOLS |
BR8103970A (en) | 1980-10-20 | 1982-08-24 | Ad Ind Inc | GAS ETHANOL WATER STEAM REMOVAL PROCESS |
GB2088739B (en) | 1980-11-28 | 1983-11-30 | Coal Industry Patents Ltd | Drying organic solvents |
US4372857A (en) | 1981-03-05 | 1983-02-08 | Union Carbide Corporation | Liquid adsorption process and apparatus |
US4465875A (en) | 1982-09-27 | 1984-08-14 | Calgon Carbon Corporation | Process for dehydrating ethanol |
US4487614A (en) | 1983-11-16 | 1984-12-11 | Union Carbide Corporation | Adsorption separation cycle |
GB2151501A (en) | 1983-12-22 | 1985-07-24 | Coal Ind | Continuous sorption process |
US4726818A (en) | 1984-12-20 | 1988-02-23 | Union Carbide Corporation | Bulk removal of water from organic liquids |
GB8601082D0 (en) | 1986-01-17 | 1986-02-19 | Distillers Co Carbon Dioxide | Potable spirit production |
US4670580A (en) * | 1986-03-31 | 1987-06-02 | Celanese Corporation | Process for preparing oligomeric glycol esters of dicarboxylic acids |
DE69012682T2 (en) | 1989-06-12 | 1995-04-06 | Merck & Co Inc | Process for the removal of bacterial endotoxins from gram-negative polysaccharides. |
JPH04308543A (en) | 1991-04-06 | 1992-10-30 | Kobe Steel Ltd | Method for purifying hydrous ethanol |
DK0743948T4 (en) | 1994-02-07 | 2004-02-02 | Qiagen Gmbh | Chromatographic isolation of nucleic acids |
FR2719039B1 (en) | 1994-04-22 | 1996-06-21 | Interis | New alcohol dehydration process by adsorption / regeneration on molecular sieve, and installation for its implementation. |
AU4314099A (en) | 1998-06-01 | 1999-12-20 | Immune Response Corporation, The | Novel method of large scale plasmid purification |
DE10043545A1 (en) | 2000-09-05 | 2002-03-14 | Oxeno Olefinchemie Gmbh | Process for the preparation of carboxylic acid esters |
DE10056179A1 (en) | 2000-11-13 | 2002-05-29 | Basf Ag | Process for the preparation of esters of polybasic acids |
JP4996791B2 (en) | 2001-03-14 | 2012-08-08 | Jnc株式会社 | Endotoxin adsorbent and method for removing endotoxin using the same |
US20060189790A1 (en) | 2003-06-24 | 2006-08-24 | Akzo Nobel N.V. | Removal of lipopolysaccharides from protein-lipopolysaccharide complexes by non flammable solvents. |
US7531308B2 (en) | 2004-04-23 | 2009-05-12 | Sigma-Aldrich Co. | Process for the reduction of endotoxins in a plasmid preparation using a carbohydrate non-ionic detergent with silica chromatography |
US7799942B2 (en) * | 2005-08-12 | 2010-09-21 | Eastman Chemical Company | Production of terephthalic acid di-esters |
US7276621B2 (en) | 2005-08-12 | 2007-10-02 | Eastman Chemical Company | Production of di-(2-ethylhexyl) terephthalate |
JP4956945B2 (en) * | 2005-09-12 | 2012-06-20 | 三菱化学株式会社 | Method for producing terephthalic acid diester |
WO2007115046A1 (en) | 2006-03-31 | 2007-10-11 | Invitrogen Corporation | Low-endotoxin nucleic acid preparations |
US7714111B2 (en) | 2006-09-08 | 2010-05-11 | Wyeth Llc | Arginine derivative wash in protein purification using affinity chromatography |
US7943094B2 (en) | 2006-12-07 | 2011-05-17 | Grupo Petrotemex, S.A. De C.V. | Polyester production system employing horizontally elongated esterification vessel |
US8034970B2 (en) * | 2007-06-27 | 2011-10-11 | H R D Corporation | Method of making phthalic acid diesters |
ES2422262T3 (en) | 2008-12-16 | 2013-09-10 | Basf Se | Procedure for the preparation of a crude ester |
JP5780967B2 (en) | 2008-12-16 | 2015-09-16 | ビーエーエスエフ ソシエタス・ヨーロピアBasf Se | Method for producing carboxylic acid ester |
WO2012025308A1 (en) | 2010-08-25 | 2012-03-01 | Exxonmobil Chemical Patents Inc. | Processes for the production of esters |
TWI654177B (en) | 2013-10-31 | 2019-03-21 | 德商巴斯夫歐洲公司 | Process for preparing carboxylic acid esters and use thereof as plasticizer |
US9776949B2 (en) | 2014-04-22 | 2017-10-03 | Basf Se | Process for the production of carboxylic esters and use of these as plasticizers |
-
2015
- 2015-09-21 EP EP15766173.7A patent/EP3197859B1/en active Active
- 2015-09-21 RU RU2017113965A patent/RU2668223C1/en not_active IP Right Cessation
- 2015-09-21 CN CN201580051362.6A patent/CN106715382A/en active Pending
- 2015-09-21 TR TR2019/04928T patent/TR201904928T4/en unknown
- 2015-09-21 MX MX2017003920A patent/MX2017003920A/en unknown
- 2015-09-21 WO PCT/EP2015/071576 patent/WO2016046118A1/en active Application Filing
- 2015-09-21 US US15/513,757 patent/US10207978B2/en active Active
- 2015-09-21 BR BR112017005839A patent/BR112017005839A2/en not_active Application Discontinuation
- 2015-09-21 PL PL15766173T patent/PL3197859T3/en unknown
- 2015-09-21 ES ES15766173T patent/ES2724982T3/en active Active
- 2015-09-21 CA CA2962305A patent/CA2962305C/en not_active Expired - Fee Related
- 2015-09-23 TW TW104131415A patent/TW201612150A/en unknown
Also Published As
Publication number | Publication date |
---|---|
PL3197859T3 (en) | 2019-08-30 |
US10207978B2 (en) | 2019-02-19 |
MX2017003920A (en) | 2017-06-28 |
US20170297997A1 (en) | 2017-10-19 |
ES2724982T3 (en) | 2019-09-18 |
WO2016046118A1 (en) | 2016-03-31 |
TW201612150A (en) | 2016-04-01 |
EP3197859A1 (en) | 2017-08-02 |
CN106715382A (en) | 2017-05-24 |
CA2962305C (en) | 2019-06-11 |
RU2668223C1 (en) | 2018-09-27 |
CA2962305A1 (en) | 2016-03-31 |
BR112017005839A2 (en) | 2018-01-30 |
EP3197859B1 (en) | 2019-02-06 |
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