TR201904928T4 - Method for the production of terephthalic acid diesters by recirculating alcohol dehydration. - Google Patents

Method for the production of terephthalic acid diesters by recirculating alcohol dehydration. Download PDF

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Publication number
TR201904928T4
TR201904928T4 TR2019/04928T TR201904928T TR201904928T4 TR 201904928 T4 TR201904928 T4 TR 201904928T4 TR 2019/04928 T TR2019/04928 T TR 2019/04928T TR 201904928 T TR201904928 T TR 201904928T TR 201904928 T4 TR201904928 T4 TR 201904928T4
Authority
TR
Turkey
Prior art keywords
terephthalic acid
production
acid diesters
alcohol dehydration
recirculating
Prior art date
Application number
TR2019/04928T
Other languages
Turkish (tr)
Inventor
Schraut Armin
Kaller Martin
BRONNEBERG Rob
STAMMER Jasmin
DAS Martin
HARNISCHMACHER Gerrit
Original Assignee
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Se filed Critical Basf Se
Publication of TR201904928T4 publication Critical patent/TR201904928T4/en

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00Preparation of carboxylic acid esters
    • C07C67/08Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/76Esters of carboxylic acids having a carboxyl group bound to a carbon atom of a six-membered aromatic ring
    • C07C69/80Phthalic acid esters
    • C07C69/82Terephthalic acid esters
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00132Controlling the temperature using electric heating or cooling elements

Abstract

Buluş tereftalik asit diesterler tereftalik asidin en azından bir alkol ile reaksiyonuyla üretilmesi için bir yöntem ile ilgilidir.The invention relates to a method for producing terephthalic acid diesters by reaction of terephthalic acid with at least one alcohol.

TR2019/04928T 2014-09-24 2015-09-21 Method for the production of terephthalic acid diesters by recirculating alcohol dehydration. TR201904928T4 (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
EP14186143 2014-09-24

Publications (1)

Publication Number Publication Date
TR201904928T4 true TR201904928T4 (en) 2019-05-21

Family

ID=51660314

Family Applications (1)

Application Number Title Priority Date Filing Date
TR2019/04928T TR201904928T4 (en) 2014-09-24 2015-09-21 Method for the production of terephthalic acid diesters by recirculating alcohol dehydration.

Country Status (12)

Country Link
US (1) US10207978B2 (en)
EP (1) EP3197859B1 (en)
CN (1) CN106715382A (en)
BR (1) BR112017005839A2 (en)
CA (1) CA2962305C (en)
ES (1) ES2724982T3 (en)
MX (1) MX2017003920A (en)
PL (1) PL3197859T3 (en)
RU (1) RU2668223C1 (en)
TR (1) TR201904928T4 (en)
TW (1) TW201612150A (en)
WO (1) WO2016046118A1 (en)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107849224B (en) 2015-07-09 2021-06-08 巴斯夫欧洲公司 Curable composition
CN112439377A (en) * 2019-08-29 2021-03-05 江苏察克润滑科技有限公司 A reation kettle for preparing antirust liquid
KR20220067385A (en) * 2020-11-17 2022-05-24 주식회사 엘지화학 Method for preparing diester compound
CN115282894A (en) * 2022-06-30 2022-11-04 福建久策气体股份有限公司 Difluoro ethyl acetoacetate production device and working method thereof

Family Cites Families (35)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB798439A (en) * 1954-10-26 1958-07-23 Bayer Ag Process for the manufacture of terephthalic acid dimethyl ester
DE1286003B (en) * 1966-06-21 1969-01-02 Metallgesellschaft Ag Process for the continuous esterification of terephthalic and isophthalic acid with ethylene glycol
US3617226A (en) * 1968-04-26 1971-11-02 Huels Chemische Werke Ag Apparatus for the continuous preparation of esters
BE789047A (en) * 1971-09-20 1973-03-20 Montedison Spa PROCESS FOR THE CONTINUOUS ESTERIFICATION OF DICARBOXYLIC ACIDS AND ALCOHOLS
BR8103970A (en) 1980-10-20 1982-08-24 Ad Ind Inc GAS ETHANOL WATER STEAM REMOVAL PROCESS
GB2088739B (en) 1980-11-28 1983-11-30 Coal Industry Patents Ltd Drying organic solvents
US4372857A (en) 1981-03-05 1983-02-08 Union Carbide Corporation Liquid adsorption process and apparatus
US4465875A (en) 1982-09-27 1984-08-14 Calgon Carbon Corporation Process for dehydrating ethanol
US4487614A (en) 1983-11-16 1984-12-11 Union Carbide Corporation Adsorption separation cycle
GB2151501A (en) 1983-12-22 1985-07-24 Coal Ind Continuous sorption process
US4726818A (en) 1984-12-20 1988-02-23 Union Carbide Corporation Bulk removal of water from organic liquids
GB8601082D0 (en) 1986-01-17 1986-02-19 Distillers Co Carbon Dioxide Potable spirit production
US4670580A (en) * 1986-03-31 1987-06-02 Celanese Corporation Process for preparing oligomeric glycol esters of dicarboxylic acids
DE69012682T2 (en) 1989-06-12 1995-04-06 Merck & Co Inc Process for the removal of bacterial endotoxins from gram-negative polysaccharides.
JPH04308543A (en) 1991-04-06 1992-10-30 Kobe Steel Ltd Method for purifying hydrous ethanol
DK0743948T4 (en) 1994-02-07 2004-02-02 Qiagen Gmbh Chromatographic isolation of nucleic acids
FR2719039B1 (en) 1994-04-22 1996-06-21 Interis New alcohol dehydration process by adsorption / regeneration on molecular sieve, and installation for its implementation.
AU4314099A (en) 1998-06-01 1999-12-20 Immune Response Corporation, The Novel method of large scale plasmid purification
DE10043545A1 (en) 2000-09-05 2002-03-14 Oxeno Olefinchemie Gmbh Process for the preparation of carboxylic acid esters
DE10056179A1 (en) 2000-11-13 2002-05-29 Basf Ag Process for the preparation of esters of polybasic acids
JP4996791B2 (en) 2001-03-14 2012-08-08 Jnc株式会社 Endotoxin adsorbent and method for removing endotoxin using the same
US20060189790A1 (en) 2003-06-24 2006-08-24 Akzo Nobel N.V. Removal of lipopolysaccharides from protein-lipopolysaccharide complexes by non flammable solvents.
US7531308B2 (en) 2004-04-23 2009-05-12 Sigma-Aldrich Co. Process for the reduction of endotoxins in a plasmid preparation using a carbohydrate non-ionic detergent with silica chromatography
US7799942B2 (en) * 2005-08-12 2010-09-21 Eastman Chemical Company Production of terephthalic acid di-esters
US7276621B2 (en) 2005-08-12 2007-10-02 Eastman Chemical Company Production of di-(2-ethylhexyl) terephthalate
JP4956945B2 (en) * 2005-09-12 2012-06-20 三菱化学株式会社 Method for producing terephthalic acid diester
WO2007115046A1 (en) 2006-03-31 2007-10-11 Invitrogen Corporation Low-endotoxin nucleic acid preparations
US7714111B2 (en) 2006-09-08 2010-05-11 Wyeth Llc Arginine derivative wash in protein purification using affinity chromatography
US7943094B2 (en) 2006-12-07 2011-05-17 Grupo Petrotemex, S.A. De C.V. Polyester production system employing horizontally elongated esterification vessel
US8034970B2 (en) * 2007-06-27 2011-10-11 H R D Corporation Method of making phthalic acid diesters
ES2422262T3 (en) 2008-12-16 2013-09-10 Basf Se Procedure for the preparation of a crude ester
JP5780967B2 (en) 2008-12-16 2015-09-16 ビーエーエスエフ ソシエタス・ヨーロピアBasf Se Method for producing carboxylic acid ester
WO2012025308A1 (en) 2010-08-25 2012-03-01 Exxonmobil Chemical Patents Inc. Processes for the production of esters
TWI654177B (en) 2013-10-31 2019-03-21 德商巴斯夫歐洲公司 Process for preparing carboxylic acid esters and use thereof as plasticizer
US9776949B2 (en) 2014-04-22 2017-10-03 Basf Se Process for the production of carboxylic esters and use of these as plasticizers

Also Published As

Publication number Publication date
PL3197859T3 (en) 2019-08-30
US10207978B2 (en) 2019-02-19
MX2017003920A (en) 2017-06-28
US20170297997A1 (en) 2017-10-19
ES2724982T3 (en) 2019-09-18
WO2016046118A1 (en) 2016-03-31
TW201612150A (en) 2016-04-01
EP3197859A1 (en) 2017-08-02
CN106715382A (en) 2017-05-24
CA2962305C (en) 2019-06-11
RU2668223C1 (en) 2018-09-27
CA2962305A1 (en) 2016-03-31
BR112017005839A2 (en) 2018-01-30
EP3197859B1 (en) 2019-02-06

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