TH72152B - Method for the production of a concentrated alkaline solution of organic compounds - Google Patents

Abstract

------18/07/2018------(OCR) Page 1 of 1 page Summary of Invention After aqueous solutions containing organic compounds with two or more hydrolysis groups The molecules at concentrations less than 40% by mass were adjusted to contain organic compounds at concentrations. equal to or greater than 40% by mass aqueous solution in which the organic compound concentration is adjusted equal to or greater than 40%, the mass is irradiated by ultrasonic waves for atomization and is dehydrated and concentrated. ------------ Revised Invention Summary 9 /03/2015 After aqueous solutions containing organic compounds with two or more hydrophilic groups The molecules at concentrations less than 40% by mass were adjusted to contain organic compounds at concentrations. equal to or greater than 40% by mass aqueous solution in which the organic compound concentration is adjusted equal to or greater than 40%, the mass is irradiated by ultrasonic waves to atomize water and is dewatered and concentrated. ---------------------------------------------------- ---------------- After aqueous solution containing organic compounds having two or more hydrophilic groups The molecules at concentrations less than 40% by mass were adjusted to contain organic compounds at concentrations. equal to or greater than 40% by mass aqueous solution in which the organic compound concentration is adjusted equal to or greater than 40%, the mass is irradiated by ultrasonic waves to atomize water and is dewatered and concentrated.

Claims (9)

Disclaimer (all) which will not appear on the advertisement page: Amendment 5 Jul 2019 No disclaimer -------------------------------------------------- ------------------------ ------ 18/07/2018 ------ (OCR) Page 1 of 4 pages Claims 1. Method for the production of a concentrated alkaline solution of organic compounds, which includes: a concentration adjustment procedure which consists of the adjustment of aqueous solution containing a compound. Organic at a concentration of less than 40% by mass to contain organic compounds at a concentration equal to or greater than 40% by mass, in which organic compounds have two or more hydrophilic groups in the molecule; And the process of removing the water concentration by dehydration, which includes light irradiation Aqueous solution in which the organic compound concentration is adjusted to or greater than 40% by mass at the ultrasonic concentration adjustment step for atomization 2. Method of claim 1, Where the concentration adjustment was done at the concentration adjustment step in such a way that Akvey solution containing organic compounds at a concentration of less than 40% by mass was mixed with Organic compounds or AKVI solutions containing organic compounds at a concentration greater than 40% by mass 3. Method of claim 1, which includes additions. The recovery process of a concentrated alkaline solution of the compound The organic compound is concentrated by dehydration at the water removal process. 4. Method of claim 1, which is a method for producing a concentrated alkaline solution of organic compounds. Such is Semi-set process 5. Method of claim 1, in which the method for producing a concentrated alkaline solution of such organic compounds is A semi-batch process in which the Aqueous solution is produced, at a concentration adjustment step, in such a way that Achilles solution containing organic compounds at concentrations of less than 40% with mass was adjusted to provide Organic compounds at a concentration equal to or greater than 40% by mass were continuously dosed or Periodically to aqueous solution of organic compounds which are dehydrated and concentrated at Elimination procedure above page 2 of the number 4. Page 6. Method of claim 5, in which the concentration adjustment procedure for adjusting the concentration of the ACV solution to provide It is supplied continuously or periodically to the acuity solution of the exposed organic compound. Dehydrate and concentrate at the dehydration process was performed along with the water removal process in such a way that the Aqueous solution containing organic compounds at concentrations less than 40% by mass was It is mixed with an organic compound AQUIES solution at a concentration greater than 40% by mass 7. Method of claim 6, in which part or all of the organic compound Akvey solution at a greater concentration 40% by mass is a concentrated Aqueous solution of organic compounds formed by concentrating with Dehydration at the elimination phase 8. Method of claim 1, in which the method for producing a concentrated alkaline solution of such organic compounds is A continuous process in which the Aqueous solution is produced, at a concentration adjustment step, in such a way that Aqueous solution containing organic compounds at concentrations less than 40% by mass was adjusted to provide Contains organic compounds at a concentration equal to or greater than 40% with a continuously dosed mass or Periodically to aqueous solution of organic compounds which are dehydrated and concentrated at The process of removing water and aqueous concentrate of organic compounds is continuously or periodically recycled. 9. Method of claim No. 1, in which the concentrated alkaline solution of the compound The organic is produced by a semi-batch process, where while the organic solution containing organic compounds at a concentration of less than 40% by mass is continuously or periodically dispensed to the AQUA solution. Of organic compounds Dehydration and concentration at the dehydration stage, the concentration modulation procedure was performed in the It is characterized by that the velocity of the distribution flow of a solution containing organic compounds at Less than 40% concentration by mass was controlled in such a way that the aquias solution of organic compounds, page 3 of the 4 p., Dehydrated and concentrated, contained organic compounds at a concentration equal to or greater. 40% by mass 1 0. Method of claim 1, in which a concentrated organic compound AQUIES solution is produced by a continuous process, while the AQUA solution containing organic compounds at The concentration of less than 40% by mass was continuously or periodically applied to the aquias solution of organic compound which was Dehydrate and make, concentrate at the \ 'process of removal of water, and 1 concentrate of aqueous solution, of the compound Organic matter, which is induced by dehydration concentrations at the water removal process is introduced. Back continuously or periodically, the procedure for adjusting the concentration has been done in such a way that The velocity of the discharge flow of the AKVA solution The mass and recovery flow of the concentrated AQUA solution were controlled in organic compounds with concentrations of less than 40%. The nature in that the acuity solution of the dehydrated and concentrated organic compound has Organic compounds at a concentration equal to or greater than 40% by mass 1 1. Method of claim 1, in which the temperature of the ultrasonic irradiated Aqueous solution at the water removal procedure is equal or higher. 10? C and equal to or less than 100? C 1 2. Method of claim 1, which Organic compounds, which are hydrothermal groups, have one or more groups of ash from the It consists of hydroxyl group, 1 shill of carboxyl group, carbonyl group, ester group, acanthal group, hemiachital group, ether group, moo. Amino, ammonium group, amid group, chulfonate group, chalfate ester group, phosphonate group, phosphate group, or uri group 1 ido 1 3. Method of claim 12, where organic compounds contain polyhydric alcohol 1 4. Method of claim 12, in which organic compounds contain carboxyl group organic compounds 1 5. Method of claim Rights 1, which Molecules of organic compounds have two or more carbon atoms and are equal to or page 4 of a number of 4 pages less than 22 carbon atoms 1 6. Method of claim 1, in which the molecular weight of an organic compound is equal to or greater than 50 and overlapped. Or less than 400 1 7. Method of claim 1, in which an organic compound, which is a hydrotilic group, has one or more groups selected from that group. Contains hi-litter or carboxyl group ------------ Amendment 09/03/2015 1. Method for the production of a concentrated Aqueous solution of organic compounds, which This includes: Concentration adjustment procedure for adjusting an ACU solution containing organic compounds at a concentration of less than 40% by mass to contain organic compounds at a concentration equal to or greater than 40% by mass, organic compounds with There are two or more hydrophilic groups in the molecule; And the dehydration process of the Aqueous irradiation, where the compound concentration The organic matter was adjusted to be equal to or greater than 40% by mass at the ultrasonic homogenization process. Sonic for atomizing water 2. Method of claim 1, where concentration adjustment is performed at the concentration adjustment step in the method that the AQUIUS solution There are organic compounds at concentrations less than 40% by mass being mixed with organic compounds or AQUIES solution containing organic compounds at a concentration greater than 40% by mass. 3. Method of claim 1 or 2, which includes additions: the process of recovery of AQUIZ solution. Concentration of organic compounds It is created by concentrating by water removal at the concentrated process by dehydration 4. Method of claim 1 to 3, where the concentration adjustment at the concentration adjustment procedure is performed. In the Al-type aerosol machine The ultrasonic seal, including the aerosol tank provided, has an ultrasonic generating device 5. Method of claim 1 to 4, where at the concentration adjustment step, A solution Quies in which the intensity of organic compounds was adjusted. Is equal to or greater than 40% by mass being supplied to the aerosol tank provided with an ultrasonic generating device 6. Method of claim 1 to 5, either, where AK solution The organic compound aqueous concentrate was produced by a batch operation 7. Method of claim 1 to 5, where the organic compound aqueous concentrate solution was produced by operation. Semi-set work where the AQUIUS solution was prepared at the calibration step with the Aquias solution method. Containing organic compounds at concentrations less than 40%, the mass was adjusted to contain organic compounds that Concentrations equal to or greater than 40% with the mass being supplied continuously or periodically to the solution. Aquias of organic compounds which are dehydrated and concentrated at the concentrate process by dehydration. 8. Method of claim 1 to 5. The concentrations of organic compounds are produced by a continuous process where Aquias solution was produced. At the process of adjusting the concentration by means of the AKVI solution that It contains organic compounds at concentrations less than 40%, with the mass adjusted to contain organic compounds that Concentrations equal to or greater than 40% with the mass being supplied continuously or periodically to the solution. Aquias of organic compounds, which are dehydrated and concentrated at the concentrated process by dehydration, and continuously or periodically recovered the concentrated aquias of organic compounds.9. The method of claim 7 or 8, where the concentration adjustment of the concentration adjustment step for the AQUA solution is to be It is continuously or periodically supplied to a solution of organic compound AQUIRE to dehydrate and To be concentrated at the concentrate process by dehydration with the concentrated process by dehydrating The method was that aqueous solution containing organic compounds at a concentration of less than 40% by mass was mixed with a solution containing organic compounds at a concentration of more than 40% by mass 1 0. Hold the 9th right, where part or all of aqueous solution containing organic compounds at a concentration of more than 40% by mass is a concentrated Aqueous solution of organic compounds created by concentrating. By dehydration at the dehydration concentrate process 1 1. Method of claim 1 to 5, where the Aqueous concentrated solution of Organic compounds are produced by a semi-series process where, while the organic compounds containing organic compounds at concentrations of less than 40% by mass are supplied continuously or periodically to the Aqueous solution of Organic compounds to be eliminated by water And concentrated at the concentrate process by dehydration, the concentration adjustment step in How to determine the flow rate of aqueous solution containing organic compounds at The concentration of less than 40% by mass was controlled so that the Aqueous solution of the organic compound was Eliminate water and concentrate organic compounds with a concentration equal to or greater than 40% by mass 1 2. Method of claim 1 to 5, where a concentrated Aqueous solution of organic compounds is produced. This is a continuous process where, while the organic compound Akuyase solution at a concentration less than 40% by mass is continuously or periodically applied to the organic compound AQUA solution which will Get rid of water And concentrated at the concentrated process by water removal And a concentrated Aquias solution of The organic compounds are created by concentrating by dehydration at the concentrate process by elimination. Water is continuously or periodically recovered, perform a thickening adjustment step in the method. It is said that the flow velocity of an organic compound AQUA solution at a concentration of less than 40% by the mass and the recovered flow rate of the concentrated AQUA solution is controlled so that Aqueous solution of organic compounds to be rubbed, dehydrated and concentrated. Concentration equal to or greater than 40% by mass. 1. 3. Method of claim 1 to 12, where the temperature of the ultrasonic irradiated Aqueous solution at the When doing intensive by Water removal equal to or above 10? C and equal to or less than 100? C 1 4. Method of claim 1 to 13, where one of the hydrophilic organic compounds, Or more selected from the Moo It consists of hydroxyl group, carboxyl group, carbonyl group, ester group, acetal group, hemiacetal group, ether group, ami group. No, ammonium group, amid group, sulfonate group, sulfate ester group, phosphonate group, phosphate group, or uriido group 1 5. Method of Claim 14, where organic compound contains polyhydric alcohol 1 6. Method of claim 14 or 15, where organic compound contains organic compound with carboxyl group 1 7. Method Of Clause 1 to 16, where the organic compound molecule has two or more carbon atoms and is equal to or less than 22 carbon atoms 1 8. Any method of claim 1 to 17. , Where the molecular weight of the organic compound is or greater than 50 and equal to or less than 400 1 9. Water removal method of concentration, which includes; The process of adjusting the organic compounds containing organic compounds at a concentration of less than 40% by mass to contain organic compounds at a concentration equal to or greater than 40% by mass, organic compounds with two hydrophilic groups. Moo or more in the molecule; And the process of irradiation, the Akvi solution in which the organic compound concentration was adjusted to Equal to or greater than 40%) by mass by ultrasonic waves to make water mist -------------------------------------------------- 1. Methods for the production of aqueous concentrate of organic compounds, which include: Concentration adjustment procedure for adjusting aqueous solution containing organic compounds at a concentration of less than 40% by Mass to contain organic compounds at a concentration equal to or greater than 40% by mass of organic compounds having two or more hydrophilic groups in the molecule; And the dehydration process of the Aqueous irradiation, where the compound concentration The organic matter was adjusted to be equal to or greater than 40% by mass at the ultrasonic homogenization process. Sonic for atomizing water 2. Method of claim 1 where concentration adjustment is performed at the concentration adjustment step. It contains organic compounds less than 40% by mass being mixed with organic compounds or AQUIES solution containing organic compounds at a concentration greater than 40% by mass. 3. Method of claim 1 or 2, which includes additions: the recovery process of the AQUIZ solution at Concentration of organic compounds 4. The method of claim 1 to 3, where the concentration adjustment at the concentration adjustment procedure is performed in Al type aerosol dispenser The ultrasonic seal, including the aerosol tank, is provided with an ultrasonic generating device. 5. Method of claim 1 to 4, where at the concentration adjustment step Akuyase solution in which the intensity of organic compounds was adjusted. Is equal to or greater than 40%, with the mass being dispensed into the aerosol tank provided with an ultrasonic generating device 6. Method of claim 1 to 5 any one where the AKV solution The concentrated organic compounds were produced by a batch operation 7. One of the No. 1 to 5 claim method, where the organic compound aqueous solution is produced by a series of operations. Semi-set, where the AQUIUS solution was prepared at the calibration step with the AKUY solution method. Containing organic compounds at concentrations less than 40%, the mass was adjusted to contain organic compounds that Concentrations equal to or greater than 40% with the mass being supplied continuously or periodically to the solution. Aquias of organic compounds, which are dehydrated and concentrated at the concentrate process by dehydration. 8. Method of claim 1 to 5, whereby the AQUIES solution is Concentration of organic compounds is produced by a continuous process where Aquias solution was produced. At the process of adjusting the concentration by means of the AKVI solution that It contains organic compounds at concentrations less than 40%, with the mass adjusted to contain organic compounds that Concentrations equal to or greater than 40% with the mass being supplied continuously or periodically to the solution. Aquias of organic compounds, which are dehydrated and concentrated at the concentrate process by dehydration, and the organic concentrate aqueous solution is continuously or periodically reversed. 9. Method of claim 7 or 8, where the concentration adjustment of the concentration adjustment procedure for the AQUA solution is to be It is continuously or periodically supplied to a solution of organic compound AQUIRE to dehydrate and To be concentrated at the concentrate process by dehydration with the concentrated process by dehydrating The method was that aqueous solution containing organic compounds at a concentration of less than 40% by mass was mixed with a solution containing organic compounds at a concentration of more than 40% by mass 1 0. Holds the ninth right where part or all of aqueous solution containing organic compounds at a concentration greater than 40% by mass is a concentrated Aqueous solution of organic compounds created by concentrating. By water removal at the concentrate step by water removal 1 1. Any method of terms 1 to 5 Where the concentrated AQUA solution of Organic compounds are produced in a semi-series process where On the other hand, aqueous solutions containing organic compounds at concentrations less than 40% by mass were supplied continuously or periodically to the Aqueous solution of organic compounds to be removed with water. And concentrated at the concentrated process by water removal Perform a concentration adjustment procedure in How to determine the flow rate of aqueous solution containing organic compounds at The concentration of less than 40% by mass was controlled so that the Aqueous solution of the organic compound was Removes water and concentrates organic compounds with a concentration equal to or greater than 40% by mass 1. 2. Method of claim 1 to 5 Clause one is where the concentrated alkaline solution of organic compound is produced by a continuous process where, while the compound Akviase solution Organics at concentrations less than 40% by mass were supplied continuously or periodically to the aquias solution of organic compounds which were then removed with water. And concentrated at the concentrate process by removing water, and the concentrated Aqueous solution of The organic compounds are created by concentrating by dehydration at the concentrate process over the removal. Water is recovered continuously or periodically. Perform the thickening adjustment procedure in the method. It is said that the speed of flow of aqueous solutions containing organic compounds at a concentration of less than 40% over the mass and the recovered flow rate of a concentrated Aqueous solution is controlled so that Aqueous solution of organic compounds to be rubbed, dehydrated and concentrated. The concentration is equal to or greater than 40% by mass 1. 3. Any method of Clause 1 to 12, where the temperature of an ultrasonic irradiated solution at the concentrated procedure by Water removal equal to or above 110 C and equal to or below 100 C 1 4. Any method of claim 1 through 13 where an organic compound, which is a hydrophilic group, is selected from that group. It consists of hydroxyl group, carboxyl group, carbonyl group, ester group, acetal group, hemiacetal group, ether group, ami group. No, ammonium group, amid group, sulfonate group, sulfate ester group, phosphonate group, phosphate group, or uriido 1 group. 5. Method of claim 14, where organic compounds contain polyhydric alcohols 1 6. Method of claim 14 or 15, where organic compounds contain organic compounds with carboxyl group 1. 7. Any method of claim 1 through 16 where organic compound molecules have two or more carbon atoms and equal or less than 22 carbon atoms 1. 8.Any method of claim 1 to 17 where the molecular weight of the organic compound is or greater than 50 and equal to or less than 400 1. 9. Concentration methods by dehydration, which include; The process of adjusting an organic compound containing organic compounds at a concentration of less than 40% by mass to contain organic compounds at a concentration equal to or greater than 40% by mass of organic compounds having two hydrophilic groups Or more in molecules; And the process of irradiation, the Akvi solution in which the organic compound concentration was adjusted to Equal to or more than 40%) by mass by ultrasonic waves to atomize water