SU949452A1 - Polymer material heat capacity determination method - Google Patents
Polymer material heat capacity determination method Download PDFInfo
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- SU949452A1 SU949452A1 SU813229922A SU3229922A SU949452A1 SU 949452 A1 SU949452 A1 SU 949452A1 SU 813229922 A SU813229922 A SU 813229922A SU 3229922 A SU3229922 A SU 3229922A SU 949452 A1 SU949452 A1 SU 949452A1
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- heat capacity
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Description
(54) СПОСОБ ИЗМЕРЕНИЯ ТЕПЛОЕМКОСТИ ПОЛИМЕРНОГО(54) METHOD OF MEASUREMENT OF POLYMERIC HEAT CAPACITY
МАТЕРИАЛАMATERIAL
Изобретение относитс к теплометрии и может быть использовано при изучении теплофизических свойств полимерных материалов.The invention relates to calorimetry and can be used in the study of the thermophysical properties of polymeric materials.
Известен способ определени теплоемкости , при котором теплоемкость какого-либо вещества определ ют путем передачи определенного количества тепла от нагревател к образцу исследуемого материала и измерени соответствующего изменени температуры образца. При этом количество переданного тепла определ ют либо непосредственными измерени ми мощности, выдел емой нагревателем, либо по эталонному образцу с известными характеристиками t A known method for determining the heat capacity in which the heat capacity of a substance is determined by transferring a certain amount of heat from the heater to the sample of the material under study and measuring the corresponding temperature change of the sample. In this case, the amount of heat transferred is determined either by direct measurements of the power released by the heater or by a reference sample with known characteristics t
Недостатком известного способа вл етс то, что при таких измерени х трудно избежать потери тепла через контактные сопротивлени при передаче его от нагревател к исследуемому образцу.The disadvantage of this method is that with such measurements it is difficult to avoid heat loss through contact resistances when transferring it from the heater to the sample under study.
Наиболее близким к изобретению техническим решением вл етс способ определени теплофизических свойств материалов, заключающийс в нагреве образца и измерении изменени температуры 2.The closest technical solution to the invention is a method for determining the thermophysical properties of materials, which consists in heating the sample and measuring the temperature change 2.
Однако обработка результатов измерений и расчет теплофизических параметров вещества очень трудоемки и требуют построени градуировочных графиков дл каждого исследуемого вещества.However, the processing of measurement results and the calculation of the thermophysical parameters of a substance are very laborious and require the construction of calibration curves for each test substance.
Целью изобретени вл етс упрощение и ускорение процесса измерени теплоемкости.The aim of the invention is to simplify and accelerate the process of measuring the heat capacity.
10ten
Цель достигаетс тем, что согласно способу измерени теплоемкости полимерного материала, заключающемс Ё нагреве образца и измерении изменени темйературы, образец теп15 лоизолируют от внешней среды, подвергают циклическому деформированию, измер ют параметры деформировани ; амплитуду и частоту колебаний, модуль упругости и модуль потерь и по The goal is achieved by the fact that, according to the method of measuring the heat capacity of a polymer material, which consists in heating the sample and measuring the change in temperature, the sample is isolated from the external environment, subjected to cyclic deformation, the deformation parameters are measured; amplitude and frequency of oscillation, elastic modulus and loss modulus and
20 измеренным величинам определ ют теплоемкость материала.20 measured values determine the heat capacity of the material.
Пример. Образец композиционного материала на основе эпоксидной смолы, жидкого каучука и минерально25 го наполнител изготовлен в виде стержн пр моугольного сечени . В процессе изготовлени в середину образца вмонтирована термопара (хромель - копель). Стержень изолирован Example. A sample of a composite material based on epoxy resin, liquid rubber and mineral filler is made in the form of a rectangular rod. In the process of manufacturing, a thermocouple (chromel - copel) is mounted in the middle of the sample. The rod is insulated
30 от теплообмена с внешней средой стек30 heat exchange with external environment stack
Claims (1)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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SU813229922A SU949452A1 (en) | 1981-01-05 | 1981-01-05 | Polymer material heat capacity determination method |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
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SU813229922A SU949452A1 (en) | 1981-01-05 | 1981-01-05 | Polymer material heat capacity determination method |
Publications (1)
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SU949452A1 true SU949452A1 (en) | 1982-08-07 |
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SU813229922A SU949452A1 (en) | 1981-01-05 | 1981-01-05 | Polymer material heat capacity determination method |
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SU (1) | SU949452A1 (en) |
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1981
- 1981-01-05 SU SU813229922A patent/SU949452A1/en active
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