SU852860A1 - Adduct of n,n-dimethylacetamide with chlorine as frost-resistant additive to aqueous dispersion adhesive compositions - Google Patents
Adduct of n,n-dimethylacetamide with chlorine as frost-resistant additive to aqueous dispersion adhesive compositions Download PDFInfo
- Publication number
- SU852860A1 SU852860A1 SU782648490A SU2648490A SU852860A1 SU 852860 A1 SU852860 A1 SU 852860A1 SU 782648490 A SU782648490 A SU 782648490A SU 2648490 A SU2648490 A SU 2648490A SU 852860 A1 SU852860 A1 SU 852860A1
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- chlorine
- dimethylacetamide
- adduct
- frost
- aqueous dispersion
- Prior art date
Links
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Description
Вычислено, % С 39,2; Н 7,3;N 11,5 С1 29,0.Calculated,% C 39.2; H 7.3; N 11.5 C1 29.0.
.При мер 2. В 8,7 г(0,1 моль) Ы,Ы-диметилацетамида при впускают 3,9 г (0,055 моль) хлора. Через 1 ч после добавлени хлора в реакционной смеси по вл ютс белые кристаллы , количество которых постепенно увеличиваетс , пока вс масса превращаетс в криста ллы. Полученный продукт промывают сухим диэтиловым эфиром и высушивают в экстракторе в вакууме. После сушки получают гидроскопичные кристаллы белого цвета, т.пл. 78°С, .Выход 11,7 9 (93,1%).Example 2. In 8.7 g (0.1 mol) N, N-dimethylacetamide at 3.9 g (0.055 mol) of chlorine are admitted. After 1 h after the addition of chlorine, white crystals appear in the reaction mixture, the amount of which gradually increases until the entire mass turns into crystals. The resulting product is washed with dry diethyl ether and dried in an extractor under vacuum. After drying, white hydroscopic crystals are obtained, mp. 78 ° C. Exit 11.7 9 (93.1%).
Найдено, %: С 38,4; Н 7,6;N 10,8; С1 28,4.Found,%: C 38.4; H 7.6; N 10.8; C1 28.4.
Вычислено, % С 39,2; Н 7,3;N 11,5 С1 29,0.Calculated,% C 39.2; H 7.3; N 11.5 C1 29.0.
Предлагаемый способ получени нового вещества - аддукта N, N-диметилацетамида с хлором технологичен. Полученный продукт можно использовать как морозостойкую добавку к различным водно-дисперсионным системам. Клей на основе нового аддукта стоек при -25°С.The proposed method for the preparation of a new substance - the adduct of N, N-dimethylacetamide with chlorine is technological. The resulting product can be used as a frost-resistant additive to various water-dispersion systems. Glue based on new adduct racks at -25 ° C.
Claims (2)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
SU782648490A SU852860A1 (en) | 1978-07-24 | 1978-07-24 | Adduct of n,n-dimethylacetamide with chlorine as frost-resistant additive to aqueous dispersion adhesive compositions |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
SU782648490A SU852860A1 (en) | 1978-07-24 | 1978-07-24 | Adduct of n,n-dimethylacetamide with chlorine as frost-resistant additive to aqueous dispersion adhesive compositions |
Publications (1)
Publication Number | Publication Date |
---|---|
SU852860A1 true SU852860A1 (en) | 1981-08-07 |
Family
ID=20778713
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
SU782648490A SU852860A1 (en) | 1978-07-24 | 1978-07-24 | Adduct of n,n-dimethylacetamide with chlorine as frost-resistant additive to aqueous dispersion adhesive compositions |
Country Status (1)
Country | Link |
---|---|
SU (1) | SU852860A1 (en) |
-
1978
- 1978-07-24 SU SU782648490A patent/SU852860A1/en active
Similar Documents
Publication | Publication Date | Title |
---|---|---|
MX6174E (en) | PROCEDURE FOR THE PREPARATION OF (4-TRIFLUOROMETIL) -ANILIDA ACID 5-METHYL-ISOXAZOL-4-CARBOXILICO | |
NO794010L (en) | PROCEDURE FOR THE PREPARATION OF AMINO ACID DERIVATIVES | |
ATE18863T1 (en) | PROCESS FOR PRODUCTION OF FREE-FLOWING ETHYL CELLULOSE MICROCAPSULES. | |
NO150106C (en) | APPLICATION OF AN N-ACYL-ALFA AMINO ACID AS EMULSANT FOR THE PREPARATION OF EMULSIONS | |
BR7605322A (en) | PROCESS FOR THE PREPARATION OF PHOSPHORIC ACID OF HIGH DEGREE OF PURITY FROM PHOSPHORIC ACID OF PROCESS TO WET | |
SU852860A1 (en) | Adduct of n,n-dimethylacetamide with chlorine as frost-resistant additive to aqueous dispersion adhesive compositions | |
AR223663A1 (en) | PROCEDURE FOR THE PREPARATION OF DERIVATIVES 1,6-DISSTITUTED ACID 4-PIRIDON-3-CARBOXILICO | |
IT7829966A0 (en) | COMPOSITIONS OF PAINTS AND PROCEDURE FOR THEIR PREPARATION. | |
DK369079A (en) | FIVE-METHOD OF PREPARING SUBSTITUTED OMEGA-AROYL (PROPIONYL OR BUTYRYL) -L-PROLINES OR ESTERS OR SALTS THEREOF | |
DK430379A (en) | PROCEDURE FOR THE PREPARATION OF 2,6-DIAMINONEBULARIN OR ACID ADDITION SALTS THEREOF | |
ES480265A0 (en) | A PROCEDURE FOR THE PREPARATION OF ACID DERIVATIVES 7-OXO-1-AZA-BICYCLE (3,2,0) HEPT-2-EN-2-CARBOXILICO | |
GB1505020A (en) | Substituted 2-phenylimino-thiazolines a process for their preparation and their use as ectoparasiticides | |
DK135800B (en) | Analogous process for the preparation of (L) -1- (4-hydroxyphenoxy) -2-hydroxy-3-isopropylaminopropane or acid addition salts thereof. | |
IT1035464B (en) | PROCEDURE FOR THE PREPARATION OF CYANURIC ACID | |
DK153539C (en) | PROCEDURE FOR THE PREPARATION OF 3,3-DIMETHYL-2-OXOCHORIC ACID OR SALTS THEREOF | |
AR218217A1 (en) | PROCESS FOR THE PREPARATION OF 3,6-DICHLOROPYCOLINIC ACID | |
DE2960583D1 (en) | Novel 2-substituted-3-heterocyclylindoles, their preparation and pharmaceutical compositions containing them | |
SU777373A1 (en) | Lead cake drying method | |
SU529171A1 (en) | Method for preparing 1,8-oxazadecalon-4 derivatives | |
SU525739A1 (en) | Adhesive to attach the seed to the seed holders in the process of obtaining artificial crystals | |
ES502947A0 (en) | PROCEDURE FOR THE OBTAINING OF ESTERS OF DIMETH ACID-CRYLIC | |
IT1162589B (en) | PHENYLIC ESTERS OF CARBAMIC ACID, PROCEDURE FOR THE PREPARATION OF THESE COMPOUNDS AS WELL AS HERBICIDE CONTAINING THEM | |
SU765229A1 (en) | Inhibitor of gypsum hardening period | |
JPS54117454A (en) | Acylsteroid derivative | |
SU667130A3 (en) | Method of producing salt of lysine and alpha-methyl-(2-isopropyl-5-indanyl) of acetic acid |