SU580824A3 - Method of preparing potassium phosphate - Google Patents
Method of preparing potassium phosphateInfo
- Publication number
- SU580824A3 SU580824A3 SU7101723375A SU1723375A SU580824A3 SU 580824 A3 SU580824 A3 SU 580824A3 SU 7101723375 A SU7101723375 A SU 7101723375A SU 1723375 A SU1723375 A SU 1723375A SU 580824 A3 SU580824 A3 SU 580824A3
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- phosphoric acid
- potassium phosphate
- solution
- treating
- taken
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
- Fertilizers (AREA)
Description
гидролизатом, характеризуетс мол рным соотношением фосфора и кали , равным 4:1.hydrolyzate, characterized by a molar ratio of phosphorus and potassium, equal to 4: 1.
Загр зненный фосфат кали осаждают путем добавлени метанола к жидкому гидролизату при соотношении 0,75:1 по весу. Твердые вешества отфильтровывают, промывают метанолом и удал ют из систем. Содержащий кислоту фильтрат подают в дистилл ционную колонну и удал ют метанол. Получаемый при перегонке кубовой раствор, содержаш,ий 56,1% Р205, упаривают с целью получени «суперфосфорной кнслоты 70,3% Р205. Одну треть упаренной кислоты вывод т из системы в виде «суперфосфорной кислоты, по существу не содержащей никаких посторонних примесей за исключением калк . Остающуюс «суперфосфорную кислоту возвращают обратно в реактор дл проведени реакции взаимодействи с хлористым калием. Чистый первичный кислый фосфорнокислый калий содержит 4&% PaOs и 31% KzO.The contaminated potassium phosphate is precipitated by adding methanol to the liquid hydrolyzate at a ratio of 0.75: 1 by weight. The solids are filtered, washed with methanol and removed from the systems. The acid-containing filtrate is fed to a distillation column and the methanol is removed. The distillation bottom solution, containing 56.1% of P205, is evaporated to obtain a superphosphoric acid of 70.3% of P205. One third of one stripped off acid is removed from the system in the form of "superphosphoric acid, which is essentially free of any impurities except calcium. The remaining " superphosphoric acid is returned back to the reactor for carrying out the reaction of reaction with potassium chloride. Pure potassium hydroxide contains 4 & PaOs and 31% KzO.
Пример 2. 250 г концентрированной, экстракционной фосфорной кислоты (100% НзР04) обрабатывают 93,2 г КС1 (60% КгО) при 260°С в течение 3 ч. Продукт содержит 63,3% PsOs и 20,0% КдО. Затем ввод т фосфорную кислоту (192 г 49% Р2О5) и смесь нагревают до 100°С в течение 1 часа. Добавл ют метанол к гидролизующей жидкости в отношении от 0,75 до 1% по весу. Осадок отфильтровывают , промывают метанолом и сушат. 166,1 г продукта содержит по данным анализа 45,4 Р205, 28,3;% К2О, что в расчете на калий составл ет 82%.Example 2. 250 g of concentrated, extraction phosphoric acid (100% HzP04) are treated with 93.2 g of KC1 (60% CgO) at 260 ° C for 3 hours. The product contains 63.3% PsOs and 20.0% CdO. Phosphoric acid (192 g, 49% P2O5) is then introduced, and the mixture is heated to 100 ° C for 1 hour. Methanol is added to the hydrolyzing liquid in a ratio of 0.75 to 1% by weight. The precipitate is filtered off, washed with methanol and dried. 166.1 g of the product contains, according to analysis, 45.4 P205, 28.3;% K2O, which is 82% based on potassium.
Claims (3)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB5995770 | 1970-12-17 |
Publications (1)
Publication Number | Publication Date |
---|---|
SU580824A3 true SU580824A3 (en) | 1977-11-15 |
Family
ID=10484746
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
SU7101723375A SU580824A3 (en) | 1970-12-17 | 1971-12-07 | Method of preparing potassium phosphate |
Country Status (15)
Country | Link |
---|---|
AU (1) | AU452587B2 (en) |
BE (1) | BE776793A (en) |
CA (1) | CA958870A (en) |
DD (1) | DD98892A5 (en) |
DE (1) | DE2161849B2 (en) |
ES (1) | ES397978A1 (en) |
FR (1) | FR2118701A5 (en) |
GB (1) | GB1318224A (en) |
IE (1) | IE35900B1 (en) |
IL (1) | IL38264A (en) |
IT (1) | IT945255B (en) |
MX (1) | MX3021E (en) |
NL (1) | NL155801B (en) |
SE (1) | SE370926B (en) |
SU (1) | SU580824A3 (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
RU2597117C1 (en) * | 2015-07-14 | 2016-09-10 | Открытое акционерное общество "Реатэкс" (ОАО "Реатэкс") | Method of producing disubstituted potassium phosphate |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB8825390D0 (en) * | 1988-10-31 | 1988-11-30 | Univ Waterloo | Production of chloride-free fertilizers-11 |
MXPA03011064A (en) | 2003-12-02 | 2004-04-28 | Grupo Cementos De Chihuahua S | Cementing compositions of containing anhydrite and procedures for its fabrication. |
CN116119634B (en) * | 2023-04-20 | 2023-06-20 | 诸城市浩天药业有限公司 | Method for improving clarity of potassium dihydrogen phosphate product prepared from corn soaking water |
-
1970
- 1970-12-17 GB GB5995770A patent/GB1318224A/en not_active Expired
-
1971
- 1971-11-30 IL IL38264A patent/IL38264A/en unknown
- 1971-11-30 NL NL7116474.A patent/NL155801B/en not_active IP Right Cessation
- 1971-12-03 IT IT54505/71A patent/IT945255B/en active
- 1971-12-07 SE SE7115679A patent/SE370926B/xx unknown
- 1971-12-07 SU SU7101723375A patent/SU580824A3/en active
- 1971-12-08 AU AU36630/71A patent/AU452587B2/en not_active Expired
- 1971-12-09 MX MX002426U patent/MX3021E/en unknown
- 1971-12-13 DE DE2161849A patent/DE2161849B2/en not_active Ceased
- 1971-12-15 ES ES397978A patent/ES397978A1/en not_active Expired
- 1971-12-15 DD DD159619A patent/DD98892A5/xx unknown
- 1971-12-16 IE IE1591/71A patent/IE35900B1/en unknown
- 1971-12-16 FR FR7145285A patent/FR2118701A5/fr not_active Expired
- 1971-12-16 BE BE776793A patent/BE776793A/en unknown
- 1971-12-17 CA CA130,364A patent/CA958870A/en not_active Expired
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
RU2597117C1 (en) * | 2015-07-14 | 2016-09-10 | Открытое акционерное общество "Реатэкс" (ОАО "Реатэкс") | Method of producing disubstituted potassium phosphate |
Also Published As
Publication number | Publication date |
---|---|
IL38264A (en) | 1974-10-22 |
FR2118701A5 (en) | 1972-07-28 |
ES397978A1 (en) | 1974-07-01 |
NL7116474A (en) | 1972-06-20 |
DE2161849B2 (en) | 1978-10-19 |
DD98892A5 (en) | 1973-07-12 |
AU3663071A (en) | 1973-06-14 |
SE370926B (en) | 1974-11-04 |
IT945255B (en) | 1973-05-10 |
NL155801B (en) | 1978-02-15 |
BE776793A (en) | 1972-04-17 |
GB1318224A (en) | 1973-05-23 |
IE35900L (en) | 1972-06-17 |
CA958870A (en) | 1974-12-10 |
AU452587B2 (en) | 1974-09-05 |
MX3021E (en) | 1980-02-13 |
DE2161849A1 (en) | 1972-06-22 |
IL38264A0 (en) | 1972-01-27 |
IE35900B1 (en) | 1976-06-23 |
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