SU574463A1 - Method of preparing phytosterol - Google Patents
Method of preparing phytosterolInfo
- Publication number
- SU574463A1 SU574463A1 SU7602363266A SU2363266A SU574463A1 SU 574463 A1 SU574463 A1 SU 574463A1 SU 7602363266 A SU7602363266 A SU 7602363266A SU 2363266 A SU2363266 A SU 2363266A SU 574463 A1 SU574463 A1 SU 574463A1
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- solution
- soap
- phytosterol
- preparing phytosterol
- preparing
- Prior art date
Links
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Fats And Perfumes (AREA)
Description
(54) СПОСОБ ПОЛУЧЕНИЯ ФИТОСГЕРИНА(54) METHOD OF OBTAINING PHYTOSGERIN
1one
Изобретение относитс к медицинской промышленностк и касаетс получени медицинских препаратов.FIELD OF THE INVENTION The invention relates to the medical industry and the provision of medical preparations.
Известен способ получени фитостерина из спиртоводньгх растворов сульфатного мыла путем экстрагировани еги и обрапотки раствора органическим растворителем 1.A method of obtaining phytosterol from alcoholic solutions of sulphate soap by extracting erg and treating a solution with an organic solvent 1 is known.
Однако известный способ Ht обеспечивает высокою выхода щлевокз продукт .However, the known method Ht provides a high yield product.
С целью увеличени выхода целевого продукта экстракцию осуществл ют низкомоле«ул рным спиртом, например эти.11)вым.In order to increase the yield of the target product, the extraction is carried out with a low-mole "street alcohol, for example, these 11).
Пример. Сульфатное мыло смешивают с этиловым спиртом в соотношении 1:0,2. Смесь раствор ют при 50°С и nept мешив.пог в течение 30 мин. Гор чий спиртовой раствор сульфатного мыла отстаивают в течение 1 час, затем , части раствора отдел ют декантацией , а насыщенную загр знител ми нижнюю часть раствора фильтруют от примесейExample. Sulfate soap is mixed with ethyl alcohol in a ratio of 1: 0.2. The mixture was dissolved at 50 ° C and nept. Mixed for 30 minutes. The hot alcohol solution of sulphate soap is allowed to settle for 1 hour, then, parts of the solution are separated by decantation, and the bottom of the solution, which is saturated with contaminants, is filtered from impurities.
Полученные растворы Объедин ют и экстрагируют непол рным растворителем б -нзином при 50°С. Соотношение сульфатное мыло :бен.ин равно 1 : 2. После экстракции бензиновый раствор фотостерина отдел ют от спиртомыльного раствора. Из бензинового раствора регенерируют растворитель. Полученный фито :терик очищают изнестнымл способами , напр1;мср кр1 стллл;.чааие 1.The resulting solutions are combined and extracted with a non-polar solvent b-sinzine at 50 ° C. The ratio of sulphate soap: ben.in is 1: 2. After extraction, the petrol solution of photosterol is separated from the alcohol solution. The solvent is regenerated from the gasoline solution. The obtained phyto: terik is cleaned using methods, for example, msr cr1 stll; chaie 1.
Предлагаемый способ обеспечивает высокий вых(;д нелев)-о продукта.The proposed method provides high output (; d nelev) -o product.
Ф о р м л а и о 6 р о т с ;: .-i Ф о рм л and and about 6 p about t with;:.-I
Способ получени фитсстерп;:; путем экстрагировани с}льфатного мыла, обработки растьорз органическим раствори-телем. от .1 и ч а ;О i и и с тс.м, ЧТО, С цслью увел} ченич выхода, целсзого проду :та, экстракцию осушествл ют ниакомолеку.1 рным слирто.м, например этиловы.м.The method of obtaining the fitss; by extracting from a soap soap, treating the plants with an organic solvent. from .1 and h a; O i and with tsm, THAT, With tslyu increased the yield, the whole product, the extraction is carried out by a molecular molecule, for example, ethyl m.
Источники информации, прин тые во внимание при экспертизеSources of information taken into account in the examination
1. .Авторское свидетельство СССР 48963, кл. С 11D 15/00. 1435.1.. The author's certificate of the USSR 48963, cl. From 11D to 15/00. 1435.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
SU7602363266A SU574463A1 (en) | 1976-05-12 | 1976-05-12 | Method of preparing phytosterol |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
SU7602363266A SU574463A1 (en) | 1976-05-12 | 1976-05-12 | Method of preparing phytosterol |
Publications (1)
Publication Number | Publication Date |
---|---|
SU574463A1 true SU574463A1 (en) | 1977-09-30 |
Family
ID=20662405
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
SU7602363266A SU574463A1 (en) | 1976-05-12 | 1976-05-12 | Method of preparing phytosterol |
Country Status (1)
Country | Link |
---|---|
SU (1) | SU574463A1 (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
RU2569688C1 (en) * | 2015-02-09 | 2015-11-27 | Общество с ограниченной ответственностью "Макорус" | Method of producing phytosterol |
-
1976
- 1976-05-12 SU SU7602363266A patent/SU574463A1/en active
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
RU2569688C1 (en) * | 2015-02-09 | 2015-11-27 | Общество с ограниченной ответственностью "Макорус" | Method of producing phytosterol |
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