SU524512A3 - Способ выделени арилгидроксилсоединений - Google Patents
Способ выделени арилгидроксилсоединенийInfo
- Publication number
- SU524512A3 SU524512A3 SU1881112A SU1881112A SU524512A3 SU 524512 A3 SU524512 A3 SU 524512A3 SU 1881112 A SU1881112 A SU 1881112A SU 1881112 A SU1881112 A SU 1881112A SU 524512 A3 SU524512 A3 SU 524512A3
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- extraction
- water
- isolating
- boiling point
- compounds
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims description 12
- 150000001875 compounds Chemical class 0.000 title claims description 5
- 238000000605 extraction Methods 0.000 claims description 14
- 238000009835 boiling Methods 0.000 claims description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 11
- 150000002576 ketones Chemical class 0.000 claims description 6
- 239000003960 organic solvent Substances 0.000 claims description 6
- 239000012670 alkaline solution Substances 0.000 claims description 2
- 125000004432 carbon atom Chemical group C* 0.000 claims description 2
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- 239000000243 solution Substances 0.000 description 5
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 4
- 150000002989 phenols Chemical class 0.000 description 4
- GEHJYWRUCIMESM-UHFFFAOYSA-L sodium sulfite Chemical compound [Na+].[Na+].[O-]S([O-])=O GEHJYWRUCIMESM-UHFFFAOYSA-L 0.000 description 4
- 239000012074 organic phase Substances 0.000 description 3
- 239000011734 sodium Substances 0.000 description 3
- 229910052708 sodium Inorganic materials 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- NTIZESTWPVYFNL-UHFFFAOYSA-N Methyl isobutyl ketone Chemical compound CC(C)CC(C)=O NTIZESTWPVYFNL-UHFFFAOYSA-N 0.000 description 2
- UIHCLUNTQKBZGK-UHFFFAOYSA-N Methyl isobutyl ketone Natural products CCC(C)C(C)=O UIHCLUNTQKBZGK-UHFFFAOYSA-N 0.000 description 2
- 239000003513 alkali Substances 0.000 description 2
- 239000008346 aqueous phase Substances 0.000 description 2
- LLEMOWNGBBNAJR-UHFFFAOYSA-N biphenyl-2-ol Chemical group OC1=CC=CC=C1C1=CC=CC=C1 LLEMOWNGBBNAJR-UHFFFAOYSA-N 0.000 description 2
- 238000004821 distillation Methods 0.000 description 2
- NGAZZOYFWWSOGK-UHFFFAOYSA-N heptan-3-one Chemical compound CCCCC(=O)CC NGAZZOYFWWSOGK-UHFFFAOYSA-N 0.000 description 2
- 239000012044 organic layer Substances 0.000 description 2
- FDPIMTJIUBPUKL-UHFFFAOYSA-N pentan-3-one Chemical compound CCC(=O)CC FDPIMTJIUBPUKL-UHFFFAOYSA-N 0.000 description 2
- 239000012071 phase Substances 0.000 description 2
- 235000011121 sodium hydroxide Nutrition 0.000 description 2
- 235000010265 sodium sulphite Nutrition 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- SRJCJJKWVSSELL-UHFFFAOYSA-N 2-methylnaphthalen-1-ol Chemical compound C1=CC=CC2=C(O)C(C)=CC=C21 SRJCJJKWVSSELL-UHFFFAOYSA-N 0.000 description 1
- 239000001856 Ethyl cellulose Substances 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 229920001249 ethyl cellulose Polymers 0.000 description 1
- 238000004880 explosion Methods 0.000 description 1
- 125000004356 hydroxy functional group Chemical group O* 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 125000003010 ionic group Chemical group 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 125000005487 naphthalate group Chemical group 0.000 description 1
- 235000010292 orthophenyl phenol Nutrition 0.000 description 1
- 230000020477 pH reduction Effects 0.000 description 1
- 238000003918 potentiometric titration Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- WEGDVNIPLOLRJC-UHFFFAOYSA-M sodium;naphthalene-1-carboxylate Chemical compound [Na+].C1=CC=C2C(C(=O)[O-])=CC=CC2=C1 WEGDVNIPLOLRJC-UHFFFAOYSA-M 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 125000000020 sulfo group Chemical group O=S(=O)([*])O[H] 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
- C07C37/68—Purification; separation; Use of additives, e.g. for stabilisation
- C07C37/70—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment
- C07C37/72—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment by liquid-liquid treatment
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2205227A DE2205227A1 (de) | 1972-02-04 | 1972-02-04 | Verfahren zur isolierung von arylhydroxy-verbindungen |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU524512A3 true SU524512A3 (ru) | 1976-08-05 |
Family
ID=5834993
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU1881112A SU524512A3 (ru) | 1972-02-04 | 1973-02-02 | Способ выделени арилгидроксилсоединений |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US3894095A (enExample) |
| JP (1) | JPS4885544A (enExample) |
| BE (1) | BE794992A (enExample) |
| CA (1) | CA1004690A (enExample) |
| CH (1) | CH589019A5 (enExample) |
| DD (1) | DD106160A5 (enExample) |
| DE (1) | DE2205227A1 (enExample) |
| FR (1) | FR2170260B1 (enExample) |
| GB (1) | GB1425226A (enExample) |
| IT (1) | IT978772B (enExample) |
| NL (1) | NL7301297A (enExample) |
| SU (1) | SU524512A3 (enExample) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5517304A (en) * | 1978-07-18 | 1980-02-06 | Hodogaya Chem Co Ltd | Preparation of 4, 4'-dihydroxybiphenyl |
| US4400553A (en) * | 1981-06-24 | 1983-08-23 | General Electric Company | Recovery of BPA and phenol from aqueous effluent streams |
| US4374283A (en) * | 1981-06-25 | 1983-02-15 | General Electric Company | Purification of aqueous effluent streams containing BPA and phenol |
| US4547596A (en) * | 1983-03-30 | 1985-10-15 | General Electric Company | Separation and recovery of alkylated phenols |
| US4705902A (en) * | 1985-10-03 | 1987-11-10 | Rohm And Haas Company | DDTR-free 1,1-bis(chlorophenyl)-2,2,2-trichloroethanol |
| GB0016336D0 (en) * | 2000-07-03 | 2000-08-23 | Zeneca Ltd | Chemical process |
| GB0016338D0 (en) * | 2000-07-03 | 2000-08-23 | Zeneca Ltd | Chemical process |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1314138A (en) * | 1919-08-26 | Nathan goodman and benjamin grubman | ||
| US1956570A (en) * | 1931-08-15 | 1934-05-01 | Rhone Poulenc Sa | Process of recovering resorcinol |
| US1991329A (en) * | 1932-05-02 | 1935-02-12 | Dow Chemical Co | Alkali-metal trichlorophenolates |
| US2137587A (en) * | 1937-05-13 | 1938-11-22 | Dow Chemical Co | Separation of phenols |
| US2334488A (en) * | 1941-06-18 | 1943-11-16 | Allied Chem & Dye Corp | Manufacture of aromatic hydroxy compounds |
-
0
- BE BE794992D patent/BE794992A/xx unknown
-
1972
- 1972-02-04 DE DE2205227A patent/DE2205227A1/de active Pending
-
1973
- 1973-01-30 US US328023A patent/US3894095A/en not_active Expired - Lifetime
- 1973-01-30 CA CA162,939A patent/CA1004690A/en not_active Expired
- 1973-01-30 NL NL7301297A patent/NL7301297A/xx not_active Application Discontinuation
- 1973-02-01 CH CH142973A patent/CH589019A5/xx not_active IP Right Cessation
- 1973-02-02 DD DD168637A patent/DD106160A5/xx unknown
- 1973-02-02 JP JP48013003A patent/JPS4885544A/ja active Pending
- 1973-02-02 IT IT19987/73A patent/IT978772B/it active
- 1973-02-02 SU SU1881112A patent/SU524512A3/ru active
- 1973-02-05 FR FR7303922A patent/FR2170260B1/fr not_active Expired
- 1973-02-05 GB GB560173A patent/GB1425226A/en not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| US3894095A (en) | 1975-07-08 |
| CA1004690A (en) | 1977-02-01 |
| GB1425226A (en) | 1976-02-18 |
| FR2170260A1 (enExample) | 1973-09-14 |
| DD106160A5 (enExample) | 1974-06-05 |
| DE2205227A1 (de) | 1973-08-16 |
| CH589019A5 (enExample) | 1977-06-30 |
| JPS4885544A (enExample) | 1973-11-13 |
| FR2170260B1 (enExample) | 1976-11-05 |
| NL7301297A (enExample) | 1973-08-07 |
| BE794992A (fr) | 1973-08-06 |
| IT978772B (it) | 1974-09-20 |
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