SU504781A1 - Method for preparing cyclohexylaminophosphonates - Google Patents
Method for preparing cyclohexylaminophosphonatesInfo
- Publication number
- SU504781A1 SU504781A1 SU1446651A SU1446651A SU504781A1 SU 504781 A1 SU504781 A1 SU 504781A1 SU 1446651 A SU1446651 A SU 1446651A SU 1446651 A SU1446651 A SU 1446651A SU 504781 A1 SU504781 A1 SU 504781A1
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- cyclohexyl
- amine
- iso
- chz
- dimethylphosphonyl
- Prior art date
Links
- GLUVSHGBLFDGLO-UHFFFAOYSA-N (cyclohexylamino)phosphonic acid Chemical class OP(O)(=O)NC1CCCCC1 GLUVSHGBLFDGLO-UHFFFAOYSA-N 0.000 title 1
- 239000003960 organic solvent Substances 0.000 claims 1
- 150000001412 amines Chemical class 0.000 description 5
- 125000000113 cyclohexyl group Chemical group [H]C1([H])C([H])([H])C([H])([H])C([H])(*)C([H])([H])C1([H])[H] 0.000 description 5
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 229910021529 ammonia Inorganic materials 0.000 description 1
- AQSJGOWTSHOLKH-UHFFFAOYSA-N phosphite(3-) Chemical class [O-]P([O-])[O-] AQSJGOWTSHOLKH-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N57/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds
- A01N57/18—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-carbon bonds
- A01N57/20—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-carbon bonds containing acyclic or cycloaliphatic radicals
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/38—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)]
- C07F9/40—Esters thereof
- C07F9/4003—Esters thereof the acid moiety containing a substituent or a structure which is considered as characteristic
- C07F9/4018—Esters of cycloaliphatic acids
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Molecular Biology (AREA)
- Agronomy & Crop Science (AREA)
- Biochemistry (AREA)
- Plant Pathology (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Fertilizers (AREA)
- Cultivation Of Plants (AREA)
Description
(54) СПОСОБ ПОЛУЧЕНИЯ ЦИКЛОГЕКСИЛАМИНОФОСФОНАТОВ(54) METHOD FOR PRODUCING CYCLOHEXYLAMINOPHOSPHONATES
N-n-xflop4 eHKn-N- (1- (0,0-диметилфосфонил ) - вдклогексил )-аминN-n-xflop4 eHKn-N- (1- (0,0-dimethylphosphonyl) -doclohexyl) -amine
N-n- метнлфенил- N- (1- (О.О-диметилФОСФОНИЛ ) -1ЩКЛОгвксил )-а1УШнNn-methylphenyl-N- (1- (O.O-dimethylPHOSPHONYL) -1CHClOX)
Ы-л -метилфенил-Ы (1- (0,0-диметилфосфони л) - циклогексил )-аминN-l-methylphenyl-Y (1- (0,0-dimethylphosphonyl l) - cyclohexyl) -amin
N-o-метилфенил- (0,0-диметилфосфонил ) -цнклогексил )-аминN-o-methylphenyl- (0,0-dimethylphosphonyl) -cyclohexyl) -amine
N-фeнил-N-((0,0 диметилфосфонил ) N-phenyl-N - ((0.0 dimethylphosphonyl)
циклогексил)-аминcyclohexyl) -amin
N-n-нитрофенил-N- (1- (0,0 димегилфосфонил ) -циклогексил-аминNn-nitrophenyl-N- (1- (0.0 dimethylphosphonyl) -cyclohexyl-amine
N- циклогексил- N- (1- (0,0-диметилфосфонил ) - циклогексил .аминN-cyclohexyl-N- (1- (0,0-dimethylphosphonyl) -cyclohexyl. Amine
N-6eH3M-N-(l-(0,0-диметилфосфонил ) нциклогексил )-аминN-6eH3M-N- (l- (0,0-dimethylphosphonyl) ncyclohexyl) -amin
N-rt- меток сифенил- N- (I- (0,0-диметилфос фонил )-циклогексил-аминN-rt-labels of siphenyl-N- (I- (0,0-dimethylphos fonyl) -cyclohexyl-amine
N-2,4- дихлорфенил-N- (1 - (0,0-диметилфосфогпш )-циклогексил)-амин Н СНзN-2,4-dichlorophenyl-N- (1 - (0,0-dimethylphosphogpsh) -cyclohexyl) -amine H CH3
Н СНэ СНз С1H CHE CH1 C1
С1 128C1 128
ОABOUT
Н СНз СНз 3H CHZ CHZ 3
9595
СН,CH,
116116
Н СНз СНзH CHZ CHZ
СНзSNS
riri
Н СНз СНзH CHZ CHZ
106106
Н СНз СНзH CHZ CHZ
.-О.-ABOUT
Н СНз СНз НОН СНз СНз НО
191191
Н СН, СНзH CH, CHZ
1,49151.4915
Н СНз СНз (( 1.5260H CHZ CHZ ((1.5260
Н СНз СНз }0 -H CHZ CHZ} 0 -
106106
0101
1,55111.5511
СНзSNS
СWITH
Kl-o- метоксифенил N (1- (0,0-диметилфосфонил ) циклогексил )-а1ишнKl-o-methoxyphenyl N (1- (0,0-dimethylphosphonyl) cyclohexyl) -a1
N-4-пиперидил- N (1- (0,0-диметилфосфонил ) - ЦИК логекси л) ЗМИИN-4-piperidyl-N (1- (0,0-dimethylphosphonyl) - CEC Logix L)
Ы-фенил-Ы(1-(0,0даэтилфосфонил ) -циклогекош ) -аминN-phenyl-N (1- (0,0 daethylphosphonyl) -cyclohexos) -amine
N- о- метилфенил- N (I- (0,0-диэтилфосфонил ) -циклогексил) аминN-o-methylphenyl-N (I- (0,0-diethylphosphonyl) -cyclohexyl) amine
М-л -метилфенил-Ы-(1 (0,0-диэтилфосфонил)циклогексил ) -аминM-l-methylphenyl-L- (1 (0,0-diethylphosphonyl) cyclohexyl) -amine
М-п-метилфенил-N-(I (0,0- да эти лфосфонил ) - циклогексил)аминMn-methylphenyl-N- (I (0,0-yes these lphosphonyl) - cyclohexyl) amine
N- о- хл орфенил- N (1- (0,0-диэтилфосфонил) циклогекснл) -аминN-o-chl orphenyl-N (1- (0,0-diethylphosphonyl) cyclohexnl) -amine
М-л-хлорфенил-Ы- (1 (О.О- диэтилфосфонил) циклогексил ) -аминM-l-chlorophenyl-L- (1 (O.O-diethylphosphonyl) cyclohexyl) -amine
онил) -onil) -
H CICjiUCICiH 3 VОСИ ,H CICjiUCICiH 3 VOSI,
Н СНэ СНэH Sne Sne
1,53781.5378
Н СНз СН, NHH CHZ CH, NH
1,49121.4912
Н CjHj CjHsH CjHj CjHs
9898
CHjCHj
d- d-
Н C,HS CjHsH C, HS CjHs
СН,CH,
103103
Н CjHs СаН,H CjHs SaN,
Н С,Н, CjH,H C, H, CjH,
9292
ClCl
H c,H, c,n, 1,H c, H, c, n, 1,
53005300
, rr
H CjHs QjH|H CjHs QjH |
122122
-У-Y
6868
1,50721.5072
Н ci02H4CiejH4H ci02H4CiejH4
Ы-циклогексил-М- (l- (0,0-диизoпpoпилфocфoшш) циклoгeкcил )-aминН ;Изо- ИзоN-cyclohexyl-M- (l- (0,0-diisopropylphosphol)) cyclohexyl) -aminH; Iso-Iso
1,76901.7690
-СэН, ч:зН, KН Изо- ИзоклоН CjHs CjHs-SeH, h: sN, KN Iso-isocloH CjHs CjHs
N-циклогекси л-N-(1- (0,0-диизобутилфосфонил) чщклогексил ) -аминN-cyclohexy-L-N- (1- (0,0-diisobutylphosphonyl) -cyclohexyl) -amin
N- циклогекси л- N - (1 - (0,0-дипропилфосфонил ) - илклогексил) -аминN-cyclohexyl l-N - (1 - (0,0-dipropylphosphonyl) - ilclohexyl) -amin
N-2-хлорфенилW- (1- (0,0-диизопрогтилфосфошл ) - циклогексил) аминN-2-chlorophenyl W- (1- (0,0-diisoprogtilphostoshl) - cyclohexyl) amine
N-циклогекснл- N- (1- (0,0-ддамилфосфонил)-циклогексил ) -аминN-cyclohexnl-N- (1- (0,0-ddamylphosphonyl) -cyclohexyl) -amine
N-6eH3HH-N-(l (0,0-дихлорэтилфосфонил) -циклогексил )-аминN-6eH3HH-N- (l (0,0-dichloroethylphosphonyl) -cyclohexyl) -amine
N-бензил-N-(1- (0,0-диизобутилфосфонил ) -циклогексил) -аминN-benzyl-N- (1- (0,0-diisobutylphosphonyl) -cyclohexyl) -amine
N-бензил-N-(l- (0,0-диaмилфocфoиил ) -циклогексил) -аминN-benzyl-N- (l- (0,0-diamylphosphoyl) -cyclohexyl) -amine
8 Продолжение таблшоы8 Continuation of the table
С|C |
Н СНэ СНзH SNE SNZ
VV
eHj- 1,5070eHj- 1.5070
И Cj HS Cj Н jAnd Cj HS Cj H j
СН,- 1,4966CH, 1.4966
-03117 СзН7-03117 SzN7
1,48201.4820
1,47681.4768
Н Изо- ИзоС4Нс ) 04119H Izo-IsoS4Ns) 04119
1,47911.4791
СзН7 CjHSzN7 CjH
.Cl.Cl
Изо- Изо-СзН , -СзНтIzo-Iso-SzN, -SzNt
1,44101.4410
1,47751.4775
Н CjHji CsHiiH CjHji CsHii
Н CIC2H4CICiH4 ff V-еНо- 1.5330H CIC2H4CICiH4 ff V-eH-1.5330
Н Изо- Изо- 1,4995N Iso- Iso- 1.4995
С4 Нд С4 Н9 mfC4 Nd C4 H9 mf
Н CsH,, CsH,, Л-CHj- 1,4977H CsH ,, CsH ,, L-CHj- 1.4977
10 Продолжение таблицы 10 Continuation of the table
N-6yTHfl-N-(b (0,0-диметалфосфйнил ) -циклогексил) - мкиN-6yTHfl-N- (b (0,0-dimethylphosphynyl) -cyclohexyl) - mk
М-бутил-Ы- (1- I -(0,0-диэтилфосфонил ) - циклогексил)M-butyl-Y- (1- I - (0,0-diethylphosphonyl) - cyclohexyl)
N-бутил-N-(1 (0,0диизoпpoIшлфoc фонил) -циклогексил) N-butyl-N- (1 (0,0-diisopro-Ishloc fonyl) -cyclohexyl)
4tlVffiH4tlVffiH
N-6ymn-N-(l -(0,0-дкизобутнлфосфонил ) -циклогексил )-амииN-6ymn-N- (l - (0,0-dkisobutnlphosphonyl) -cyclohexyl) -amia
N-6ynui-N-(l (0,0-диамш1фосфонил ) -циклогексил)аминN-6ynui-N- (l (0,0-diamsh1phosphonyl) -cyclohexyl) amine
N- метоксиэтил- N ( 1-0,0-диметилфосфонил ) - циклогекса1л )-аминN-methoxyethyl-N (1-0,0-dimethylphosphonyl) - cyclohexa1l) -amine
N- MeTOkCH3nuj- N- (1- (0,0-диизопропилфосфотш ) -циклогексил )-аминN-MeTOkCH3nuj- N- (1- (0,0-diisopropylphosphoric) -cyclohexyl) -amine
N- метоксипропил- N- (1- (0,0-диизопропилфосфонил ) - циклогекот л)-аминN-methoxypropyl-N- (1- (0,0-diisopropylphosphonyl) -cyclohecot l) -amin
N- метоксипропил- N- (1 - 0,0-диизобутилфосфонил ) - цнклогексн л) амииN-methoxypropyl-N- (1 - 0,0-diisobutylphosphonyl) - cyclohexn l) ammonia
1,47101.4710
Н СНэ СНз С4Н91 .4620H CHE CH3 C4H91 .4620
Н CjHs CjHs 04119H CjHs CjHs 04119
Н Изо- Изо- С4Нв1 ,4565 -СзН7. -CaHiH Iso-Iso-C4Hb1, 4565-SzN7. -CaHi
1,45971,4597
Н Изо- Изо-С4Н94 4 HS С4 9N Izo-Iso-C4H94 4 HS C4 9
Н CsHnCjH,, е4Н9 1,4630H CsHnCjH ,, e4H9 1.4630
Н СНз СН -CjHi-OCHjH CHS CH-CjHi-OCHj
Н Изо- Изо- СрэО-СаН4-1,4545N Iso-Iso-SreO-CaH4-1,44545
-СзН, зН,-SzN, SN,
1,45981,4598
Н Изо- Изо- СНз ОСзН7 СзН7СзН7H Izo-Iso-SNz OSzN7 SzN7SzN7
1,46281.4628
Н Изо- Изо- СНзО-СзН С Hj V4H9N Iso-Iso-СНзО-СзН С Hj V4H9
11eleven
(I- (0,0-диизобутилфосфонил ) -цнклогексил) -амин лоСНз Изо- ИзоСНз Изо- Изо- С4Н9Формула изобретени i. Способ получени пиклогексиламинофосфонатов , отличающийс тем, что диалкилфосфиты подвергают взаимодействию с N-циклогексилиденаминами .(I- (0,0-diisobutylphosphonyl) -cyclohexyl) -amine loCN3 Iso-IsoCH3 Iso-Iso-C4H9 Formula of the invention i. A process for preparing piclohexylaminophosphonates, characterized in that the dialkyl phosphites are reacted with N-cyclohexylidene amines.
12 Продолжение таблицы12 Continuation of the table
Н Изо- Изо- CH30-CjH41 ,4595H Iso-Iso-CH30-CjH41, 4595
4 Н9 G4 Н94 H9 G4 H9
Н СуНц CjHji CHjO-CjH41 ,4625N SUNC CjHji CHjO-CjH41, 4625
1,4650 -CjH7 -СаН1.4650 -CjH7 -SaH
Claims (1)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DD14156069 | 1969-08-04 |
Publications (1)
Publication Number | Publication Date |
---|---|
SU504781A1 true SU504781A1 (en) | 1976-02-28 |
Family
ID=5481515
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
SU1446651A SU504781A1 (en) | 1969-08-04 | 1970-06-23 | Method for preparing cyclohexylaminophosphonates |
SU721446651D SU574195A1 (en) | 1969-08-04 | 1972-06-26 | Plant growth control agent |
Family Applications After (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
SU721446651D SU574195A1 (en) | 1969-08-04 | 1972-06-26 | Plant growth control agent |
Country Status (8)
Country | Link |
---|---|
AT (1) | AT300454B (en) |
CH (1) | CH541278A (en) |
DE (1) | DE2022228C2 (en) |
FR (1) | FR2056340A5 (en) |
HU (1) | HU162750B (en) |
NL (1) | NL164863C (en) |
RO (1) | RO62001A (en) |
SU (2) | SU504781A1 (en) |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3855363A (en) * | 1973-08-08 | 1974-12-17 | Upjohn Co | Cycloalkane, cycloalkene, and cycloalkanone phosphonates |
DE2459491A1 (en) * | 1974-12-17 | 1976-06-24 | Bayer Ag | AGAINST ISOCYANATE-REACTIVE PHOSPHORUS FLAME RETARDANTS |
-
1970
- 1970-04-07 NL NL7004960A patent/NL164863C/en not_active IP Right Cessation
- 1970-05-06 DE DE19702022228 patent/DE2022228C2/en not_active Expired
- 1970-05-11 CH CH694670A patent/CH541278A/en not_active IP Right Cessation
- 1970-05-12 AT AT04268/70A patent/AT300454B/en not_active IP Right Cessation
- 1970-06-11 RO RO6360670A patent/RO62001A/en unknown
- 1970-06-23 SU SU1446651A patent/SU504781A1/en active
- 1970-06-24 FR FR7023412A patent/FR2056340A5/en not_active Expired
- 1970-08-04 HU HUCE000774 patent/HU162750B/hu unknown
-
1972
- 1972-06-26 SU SU721446651D patent/SU574195A1/en active
Also Published As
Publication number | Publication date |
---|---|
NL164863B (en) | 1980-09-15 |
AT300454B (en) | 1972-06-15 |
SU574195A1 (en) | 1977-09-30 |
NL7004960A (en) | 1971-10-11 |
DE2022228A1 (en) | 1971-02-18 |
HU162750B (en) | 1973-04-28 |
RO62001A (en) | 1977-11-15 |
FR2056340A5 (en) | 1971-05-14 |
NL164863C (en) | 1981-02-16 |
CH541278A (en) | 1973-09-15 |
DE2022228C2 (en) | 1982-11-04 |
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