SU478835A1 - Method for producing bis-phosphorylated-mercaptoethylamine derivatives - Google Patents
Method for producing bis-phosphorylated-mercaptoethylamine derivativesInfo
- Publication number
- SU478835A1 SU478835A1 SU1944374A SU1944374A SU478835A1 SU 478835 A1 SU478835 A1 SU 478835A1 SU 1944374 A SU1944374 A SU 1944374A SU 1944374 A SU1944374 A SU 1944374A SU 478835 A1 SU478835 A1 SU 478835A1
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- mercaptoethylamine
- phosphorylated
- derivatives
- producing bis
- bis
- Prior art date
Links
Description
1-2 мм pt. ст. Степень их чистоты и строение подтверждены элементным и спектральным анализами, а также с помощью колоночной , тонкослойной и бумансной хроматографии .1-2 mm pt. Art. The degree of their purity and structure is confirmed by elemental and spectral analyzes, as well as by means of column, thin layer and boom chromatography.
Пример 1. Получение N, 5-бис-(5-метил-о-изобутилтифосфорил )-р-меркаптоэтиламина .Example 1. Obtaining N, 5-bis- (5-methyl-o-isobutylphosphonyl) -p-mercaptoethylamine.
К раствору 0,02 г-моль бис-(5-метил-о-изобутилтиофосфорил )-.сульфида в бензоле при перемешивании и температуре 15-20°С прибавл ют раствор 0,02 г-моль этиленимина.To a solution of 0.02 g-mol of bis- (5-methyl-o-isobutylthiophosphoryl) -. Sulfide in benzene with a stirring and a temperature of 15-20 ° C is added a solution of 0.02 g-mol of ethylenimine.
Вычислено, %: N 3,43; Р 15,50; S 23,50.Calculated,%: N 3.43; P 15.50; S 23.50.
В ИК-спбктре полученного соединени обнаружепы следующие характеристические области поглощени , 540, 560 и 610 (Р-S-С), 725 (СН2-ма тниковые), 1035 (Р-О-С), ИЗО (С-N), 1260 (Р 0), 1445The following characteristic absorption regions, 540, 560 and 610 (P-S-C), 725 (CH2-tartar), 1035 (P-O-C), FROM (C-N), 1260 (P 0), 1445
(СН2СН2-деформационные). 2890 - 2980(CH2CH2-deformation). 2890 - 2980
(СНзСНз валентные), 3250(СНзСНз valent), 3250
(N-Н валентные ).(N – H valence).
По примеру 1 получают другие соединени общей формулы 1, перечень и данные анализа которых представлены в таблице.In Example 1, other compounds of general formula 1 are obtained, the list and analysis of which are presented in the table.
ТаблицаTable
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SU1944374A SU478835A1 (en) | 1973-07-02 | 1973-07-02 | Method for producing bis-phosphorylated-mercaptoethylamine derivatives |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SU1944374A SU478835A1 (en) | 1973-07-02 | 1973-07-02 | Method for producing bis-phosphorylated-mercaptoethylamine derivatives |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU478835A1 true SU478835A1 (en) | 1975-07-30 |
Family
ID=20560101
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU1944374A SU478835A1 (en) | 1973-07-02 | 1973-07-02 | Method for producing bis-phosphorylated-mercaptoethylamine derivatives |
Country Status (1)
| Country | Link |
|---|---|
| SU (1) | SU478835A1 (en) |
-
1973
- 1973-07-02 SU SU1944374A patent/SU478835A1/en active
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