SU465781A3 - Способ получени -диаминоалканов - Google Patents
Способ получени -диаминоалкановInfo
- Publication number
- SU465781A3 SU465781A3 SU1675712A SU1675712A SU465781A3 SU 465781 A3 SU465781 A3 SU 465781A3 SU 1675712 A SU1675712 A SU 1675712A SU 1675712 A SU1675712 A SU 1675712A SU 465781 A3 SU465781 A3 SU 465781A3
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- diamine
- alkanes
- diaminoalkanes
- producing
- yield
- Prior art date
Links
- 238000004519 manufacturing process Methods 0.000 title description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 13
- 238000000034 method Methods 0.000 claims description 6
- 150000001335 aliphatic alkanes Chemical class 0.000 claims description 5
- 239000002904 solvent Substances 0.000 claims description 5
- 229910021529 ammonia Inorganic materials 0.000 claims description 3
- 150000004945 aromatic hydrocarbons Chemical class 0.000 claims description 3
- 125000004432 carbon atom Chemical group C* 0.000 claims description 3
- 150000001924 cycloalkanes Chemical class 0.000 claims description 2
- 239000000203 mixture Substances 0.000 claims description 2
- 238000000926 separation method Methods 0.000 claims 1
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 18
- 150000004985 diamines Chemical class 0.000 description 14
- 238000002329 infrared spectrum Methods 0.000 description 7
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- HOWGUJZVBDQJKV-UHFFFAOYSA-N docosane Chemical compound CCCCCCCCCCCCCCCCCCCCCC HOWGUJZVBDQJKV-UHFFFAOYSA-N 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 150000003839 salts Chemical class 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 238000002844 melting Methods 0.000 description 2
- 230000008018 melting Effects 0.000 description 2
- -1 polymethylene dibromide Polymers 0.000 description 2
- 238000001228 spectrum Methods 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- SWLVFNYSXGMGBS-UHFFFAOYSA-N ammonium bromide Chemical compound [NH4+].[Br-] SWLVFNYSXGMGBS-UHFFFAOYSA-N 0.000 description 1
- 238000005915 ammonolysis reaction Methods 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 125000000950 dibromo group Chemical group Br* 0.000 description 1
- 238000004455 differential thermal analysis Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 229940083124 ganglion-blocking antiadrenergic secondary and tertiary amines Drugs 0.000 description 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 150000003141 primary amines Chemical class 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 238000001953 recrystallisation Methods 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/04—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups
- C07C209/06—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups by substitution of halogen atoms
- C07C209/08—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups by substitution of halogen atoms with formation of amino groups bound to acyclic carbon atoms or to carbon atoms of rings other than six-membered aromatic rings
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR7025506A FR2097517A5 (enExample) | 1970-07-09 | 1970-07-09 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU465781A3 true SU465781A3 (ru) | 1975-03-30 |
Family
ID=9058516
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU1675712A SU465781A3 (ru) | 1970-07-09 | 1971-07-09 | Способ получени -диаминоалканов |
Country Status (8)
| Country | Link |
|---|---|
| BE (1) | BE769721A (enExample) |
| CH (1) | CH528474A (enExample) |
| DE (1) | DE2133650A1 (enExample) |
| FR (1) | FR2097517A5 (enExample) |
| GB (1) | GB1326985A (enExample) |
| LU (1) | LU63482A1 (enExample) |
| NL (1) | NL7109295A (enExample) |
| SU (1) | SU465781A3 (enExample) |
-
1970
- 1970-07-09 FR FR7025506A patent/FR2097517A5/fr not_active Expired
-
1971
- 1971-07-06 NL NL7109295A patent/NL7109295A/xx unknown
- 1971-07-06 DE DE19712133650 patent/DE2133650A1/de active Pending
- 1971-07-06 CH CH990271A patent/CH528474A/fr not_active IP Right Cessation
- 1971-07-06 LU LU63482D patent/LU63482A1/xx unknown
- 1971-07-07 GB GB3193471A patent/GB1326985A/en not_active Expired
- 1971-07-08 BE BE769721A patent/BE769721A/xx unknown
- 1971-07-09 SU SU1675712A patent/SU465781A3/ru active
Also Published As
| Publication number | Publication date |
|---|---|
| FR2097517A5 (enExample) | 1972-03-03 |
| BE769721A (fr) | 1971-11-16 |
| CH528474A (fr) | 1972-09-30 |
| GB1326985A (en) | 1973-08-15 |
| DE2133650A1 (de) | 1972-01-20 |
| LU63482A1 (enExample) | 1971-11-15 |
| NL7109295A (enExample) | 1972-01-11 |
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