SU405359A1 - Method for producing 6-diethylenimidophosphamido-2-dimethylamino-7-methylpurine - Google Patents
Method for producing 6-diethylenimidophosphamido-2-dimethylamino-7-methylpurineInfo
- Publication number
- SU405359A1 SU405359A1 SU1727401A SU1727401A SU405359A1 SU 405359 A1 SU405359 A1 SU 405359A1 SU 1727401 A SU1727401 A SU 1727401A SU 1727401 A SU1727401 A SU 1727401A SU 405359 A1 SU405359 A1 SU 405359A1
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- producing
- methylpurine
- dimethylamino
- diethylenimidophosphamido
- amino
- Prior art date
Links
Description
Изобретепие относитс к области получени фосфорорганических соединений, содержащих этиленим:идные группы, а именно к способу получени нового 6-диэтиленимидофосфа мидо-2-Д Иметпламино - 7 - метилпурина формулы - v/9fij , №РХт,/(Н. i Чи, ,, Ссн,),в/ЦХ, Это соединение может быть использов )о в качестве физиологически активного вещества . Способ получени 6-диэтиленимидофосфам ,идо-2-днметиламино-7-мети л пурина основан на известной получени полных амидов фосфорБой кислоты. Согласно предлагаемому способу 6-амино2-д ,пметиламиыо-7-.метилпурип формулы t,-f 1 ( СНз)гКЛиА,., подвергают взаимодействию с .хлорокисыо фосфора или п тихлорпстым фосфором :i муравьиной кислотой при нагреваипп, лучше всего npiH кип ченип смеси. Образующийс при этом дихлорангпдрид 2-днметилам)П1о-7метилпуриНИл - 6 - а-мидофосфорной ююлоты формулы ШРССТ , (СЕзЬЛ затем оорабатывают этплеппмнпом. Процесс желательно проводить в с-теде. инертного органического раствор1ггел . например х.тороформа. При обработке этилениммном желательно использовать акцептор хлористого водорода, например карбонат кали . Исходный б- амино-2-димет1Иламино-7-1меThe invention relates to the field of production of organophosphorus compounds containing ethylene: the id groups, namely, to a method for producing a new 6-diethylenimidophosphate mido-2-D Imetplamino-7-methylpurine of the formula v / 9fij, No. РХт, / (N. i Chi, , Ссн,), in / ЦХ, This compound can be used as a physiologically active substance. The method for producing 6-diethylenimidophosphamide, ido-2-dnmethylamino-7-methy l purine is based on the known preparation of complete phosphorus amides. According to the proposed method, 6-amino-2-d, pmethylamino-7-.methylpuripe of the formula t, -f 1 (CH3) hCLiA,., Is reacted with chloro-phosphate or p-phosphorus: i with formic acid when heated, best npiH bake mixes. The resulting dichlorohydrin 2-dimethylamino) Pio-7methylpuriNyl-6-a-midophosphoric yulota of the formula SHRSST, (CEZL is then modified with eplenmpmnom. The process is preferably carried out in a working inert organic solution of silica gel, for example, using the inert organic solution 1 g. hydrogen chloride, for example, potassium carbonate. Original b-amino-2-dimethyl1-amino-7-1me
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SU1727401A SU405359A1 (en) | 1971-12-21 | 1971-12-21 | Method for producing 6-diethylenimidophosphamido-2-dimethylamino-7-methylpurine |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SU1727401A SU405359A1 (en) | 1971-12-21 | 1971-12-21 | Method for producing 6-diethylenimidophosphamido-2-dimethylamino-7-methylpurine |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU405359A1 true SU405359A1 (en) | 1975-11-05 |
Family
ID=20496930
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU1727401A SU405359A1 (en) | 1971-12-21 | 1971-12-21 | Method for producing 6-diethylenimidophosphamido-2-dimethylamino-7-methylpurine |
Country Status (1)
| Country | Link |
|---|---|
| SU (1) | SU405359A1 (en) |
-
1971
- 1971-12-21 SU SU1727401A patent/SU405359A1/en active
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