SU1632373A3 - Lubricating material for hot plastic working of steel - Google Patents

Lubricating material for hot plastic working of steel Download PDF

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Publication number
SU1632373A3
SU1632373A3 SU874203328A SU4203328A SU1632373A3 SU 1632373 A3 SU1632373 A3 SU 1632373A3 SU 874203328 A SU874203328 A SU 874203328A SU 4203328 A SU4203328 A SU 4203328A SU 1632373 A3 SU1632373 A3 SU 1632373A3
Authority
SU
USSR - Soviet Union
Prior art keywords
lubricant
der
schmierstoff
styrene
thickener
Prior art date
Application number
SU874203328A
Other languages
Russian (ru)
Inventor
Штауб Ганс-Рудольф
Перьяр Жак
Original Assignee
Лонца Аг. (Фирма)
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Publication of SU1632373A3 publication Critical patent/SU1632373A3/en

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    • C—CHEMISTRY; METALLURGY
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    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M111/00—Lubrication compositions characterised by the base-material being a mixture of two or more compounds covered by more than one of the main groups C10M101/00 - C10M109/00, each of these compounds being essential
    • C10M111/04—Lubrication compositions characterised by the base-material being a mixture of two or more compounds covered by more than one of the main groups C10M101/00 - C10M109/00, each of these compounds being essential at least one of them being a macromolecular organic compound
    • C—CHEMISTRY; METALLURGY
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    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M103/00—Lubricating compositions characterised by the base-material being an inorganic material
    • C10M103/04—Metals; Alloys
    • C—CHEMISTRY; METALLURGY
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    • C10M103/00—Lubricating compositions characterised by the base-material being an inorganic material
    • C10M103/06—Metal compounds
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    • C10M107/00—Lubricating compositions characterised by the base-material being a macromolecular compound
    • C10M107/02—Hydrocarbon polymers; Hydrocarbon polymers modified by oxidation
    • C10M107/12—Hydrocarbon polymers; Hydrocarbon polymers modified by oxidation containing aromatic monomer, e.g. styrene
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    • C10M107/00—Lubricating compositions characterised by the base-material being a macromolecular compound
    • C10M107/02—Hydrocarbon polymers; Hydrocarbon polymers modified by oxidation
    • C10M107/14—Hydrocarbon polymers; Hydrocarbon polymers modified by oxidation containing conjugated diens
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    • C10M125/00—Lubricating compositions characterised by the additive being an inorganic material
    • C10M125/02—Carbon; Graphite
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    • C10M125/18—Compounds containing halogen
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    • C10M125/22—Compounds containing sulfur, selenium or tellurium
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    • C10M143/10—Lubricating compositions characterised by the additive being a macromolecular hydrocarbon or such hydrocarbon modified by oxidation containing aromatic monomer, e.g. styrene
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    • C10M143/12—Lubricating compositions characterised by the additive being a macromolecular hydrocarbon or such hydrocarbon modified by oxidation containing conjugated diene
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    • C10M173/00—Lubricating compositions containing more than 10% water
    • C10M173/02—Lubricating compositions containing more than 10% water not containing mineral or fatty oils
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    • C10M2201/042—Carbon; Graphite; Carbon black halogenated, i.e. graphite fluoride
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    • C10M2201/053—Metals; Alloys used as base material
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    • C10M2201/0623—Oxides; Hydroxides; Carbonates or bicarbonates used as base material
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Abstract

Schmierstoff für die Verwendung bei der spanlosen Verformung von Stahl bei hohen Temperaturen und insbesondere bei der Herstellung von nahtlosen Rohren in sogenannten Multiple pipe mills, wobei der Schmierstoff wasserfest auf dem Werkzeug haften muss.
Erreicht wird dies durch einen Schmierstoff, enthaltend neben einem Festschmierstoff und einem Verdickungsmittel einen Binder aus der Reihe der carboxylierten Styrol-Butadienlatices.

Description

Из бретение относитс  к смазочному материалу, предназначенному дл  применени  при гор чей обработке металлов давлением.Binding refers to a lubricant intended for use in the hot working of metals by pressure.

Цель изобретени  - повышен е водостойкости и толщины смазочной пленки материала.The purpose of the invention is to increase the water resistance and thickness of the lubricating film of the material.

Дл  приготовлени  смазочного ма- териала используют в качестве твердого смазочного наполнител  графит и/или дисульфид молибдена, в качестве зл густнтел  - соединение, выбранное группы, включающей полисахариды, полиакриловую кислоту, полнвинилпнрро- лндон, глину, и в качестве св зуте- го - клрбокснлированный стиролбутл- диеновый латекс с содержанием в нем 60-90 мас.Х стирола.For preparing lubricant material, graphite and / or molybdenum disulfide is used as a solid lubricant filler, a compound selected from groups including polysaccharides, polyacrylic acid, polynvinylprondolndon, clay, and as a bond - clrboxed styrene-diene latex with 60-90 wt.X styrene content in it.

Из числа твердых смазочных материалов графит дает особенно хорошие результаты и предпочтительно использование графита с высокой чистотой, например свыше 96Ј и со средним размером зерен не более 300 мкм. Наилучшие результаты достигаютс  применением графита 99,5%. чистоты со средним размером зерен JOO мкм. Смазочный материал представл ет собой 40-60%-ную водную дисперсию. В зкость дисперсии предпочтительно составл ет 500-15000 сП при 10-30°С. Смазочный материал готов т простым смешением компонентов в воде. Состав смазочного материала приведен в табл.1.Among solid lubricants, graphite gives particularly good results and it is preferable to use graphite with high purity, for example over 96Ј and with an average grain size of no more than 300 microns. The best results are achieved using graphite 99.5%. purity with an average grain size JOO microns. The lubricant is a 40-60% aqueous dispersion. The viscosity of the dispersion is preferably 500-15,000 cP at 10-30 ° C. The lubricant is prepared by simply mixing the components in water. The composition of the lubricant is given in table.1.

оэoh

СОWITH

юYu

ОЭOE

1one

соwith

ОABOUT

Дл  сравнительных испытаний был приготовлен СОСТЕВ известного смазочного материала (состав 12), который представл ет собой ЗОХ-ную водную дисперсию смазки, включающей следующие компоненты, мас.%:For comparative tests, a COMPOSITION of a known lubricant (composition 12) was prepared, which is an OOH aqueous lubricant dispersion, comprising the following components, in wt.%:

Графит54Graphite54

Полнфосфат 11Complete phosphate 11

Буру5Buru5

Силикат натри  10Sodium silicate 10

Полиэтилен 1ВPolyethylene 1B

Алкилцеллюлоза 2Alkyl cellulose 2

Водную дисперсию можно наносить на инструмент с температурой 80- 350РС и более. При этом в реэульта- те соприкосновени  с гор чей поверхностью водный носитель дисперсии испар етс  и образуетс  пленка смазочного материала равномерной тол- цины. Пленка смазочного материала  вл етс  гомогенной, а значительной степени водостойкой, так как не смываетс  водой, пленка при этом не набухает. Смазочный материал пригоден дл  смтки инструмента, например оправки, стержн  оправки или матрицы , при их применении при обработке заготовок, например, гильз или Tpy6v в частности при термомеханичес кой обработке стали и прокатке гильз дл  получени  бесшовных труб на трубопрокатных станах с 6-8 клет ми, при необходимости и на пилнгрнмопых станлх, в прессах дл  прессовани  прутков или ковочных прессах,Water dispersion can be applied to the instrument with a temperature of 80-350PC and more. In this case, in contact with the hot surface, the aqueous dispersion carrier evaporates and a lubricant film of uniform thickness is formed. The lubricant film is homogeneous and, to a large extent, waterproof, as it does not wash off with water, and the film does not swell. The lubricant is suitable for disassembling a tool, for example a mandrel, a mandrel bar or a matrix, when used in machining workpieces, for example, liners or Tpy6v, in particular, for thermomechanical treatment of steel and rolling sleeves to produce seamless pipes on tube rolling mills with 6-8 stands , if necessary, on peeler stanlh, in presses for pressing rods or forging presses,

Смлзочнне материалы составов & 1-12 игпытынали на трубопрокатных станлх с 6-8 клет ми. В процессе испытани  оценивали когеэнонные свойства смазочного материала (силу сцеплени  смазочного материала с поверхностью металла), водостойкость, которую определ ли по количеству (%) смлзочной пленки нерастворимой о воде , тлордость пленки, определ емую методом иар панъ  (по Сиккенсу) при 150-260°С, толщину планки и в зкостьSmolzochenn materials of compositions & 1–12 igpitals on pipe rolling stanlhs with 6–8 cages. During the test, the coheenon properties of the lubricant (adhesion of the lubricant to the metal surface), water resistance, which was determined by the amount (%) of the thin film insoluble about water, the trussiness of the film, determined by the Iar Pan method (according to Seekens) at 150-260 ° C, plank thickness and viscosity

водной д:сперсии смазочного материала . Результаты испытаний приведены в табл.2.water d: lubricant sperm. The test results are shown in table 2.

Как видно из данных табл.2, водостойкость предлагаемого смазочного материала в 3 раза превышает известный , при этом толщина смазочной пленки на поверхности металла повы- шаетс  с 15 до 40-60 мкм.As can be seen from the data of Table 2, the resistance of the proposed lubricant is 3 times higher than the known one, and the thickness of the lubricating film on the metal surface increases from 15 to 40-60 microns.

Claims (1)

Формула изобретени Invention Formula Смазочный материал дл  гор чей обработки стали давлением, содержащий воду и смазку, включающую твердый смазочный наполнитель, загуститель и св зующее, отличающийс  тем, что, с целью повыше- 0 ни  водостойкости и толщины смазочной пленки материала, смазка в качестве твердого смазочного наполнител  содержит графит и/или дисульфид молибдена, в качестве загустител  5 соединение, выбранное из группы, ,включающей полисахариды, полиакрило- :вую кислоту, поливинилпирролидон, |глину, и в качестве св зующего - карбоксил ированный стиролбутадненовый 0 латекс с содержанием в нем 60- 90 мас-% стирола при следующем соотношении компонентов в расчете на смазку, мас.%:Lubricant for hot pressurizing steel containing water and lubricant including solid lubricant filler, thickener and binder, characterized in that, in order to increase the water resistance and thickness of the lubricant film, the lubricant contains graphite as a solid lubricant filler. and / or molybdenum disulfide, as a thickener 5, a compound selected from the group consisting of: polysaccharides, polyacrylate acid, polyvinylpyrrolidone, | clay, and carboxylated styrene butane as a binder out of 0 latex with a content of 60-90 wt.% styrene in the following ratio of components in terms of lubricant, wt.%: Графит и/или дн5 сульфид молибдена 50,0-79,8 Карбоксилиров энный стиролбут дненовый латекс с содержанием в нем 60-90 мас.1 0 стирола20-45Graphite and / or dn5 molybdenum sulfide 50.0-79.8 Carboxyl nth styrene buta dna latex containing 60-90 wt. 1 0 styrene 20-45 Загуститель, выбранный из группы, включающей полисахлрнды, полиакриловую кислоту, 5 поливннллпирролидон,A thickener selected from the group consisting of polysachrnds, polyacrylic acid, 5 polyvnpyrrolidone, глину0,2-5,0clay 0.2-5.0 при содержании в смазочном материале 40-60 мас.% см.чзки и до 100 мас.% воды.when the content in the lubricant 40-60 wt.% cm.chzki and up to 100 wt.% water. Т О л   n a IT o l n a I
SU874203328A 1986-09-23 1987-09-16 Lubricating material for hot plastic working of steel SU1632373A3 (en)

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EP0554822B1 (en) * 1992-02-06 1999-12-29 Timcal Ag Mandrel lubricant for the manufacture of seamless tubes
WO1997002334A1 (en) * 1995-07-04 1997-01-23 Timcal Ag Lubricant for pass rollers
JP4996810B2 (en) * 2000-09-29 2012-08-08 ケルサン・テクノロジーズ・コーポレイション Friction control composition
US6759372B2 (en) * 2002-04-12 2004-07-06 Kelsan Technologies Corp. Friction control composition with enhanced retentivity
CN105695076B (en) * 2016-02-26 2018-09-18 常州高特新材料有限公司 A kind of aqueous diamond wire silicon chip cutting fluid
RU2716499C1 (en) * 2019-10-03 2020-03-12 Федеральное государственное бюджетное учреждение науки Ордена Трудового Красного Знамени Институт нефтехимического синтеза им. А.В. Топчиева Российской академии наук (ИНХС РАН) Method of producing biodegradable low-temperature grease based on cellulose
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AR243593A1 (en) 1993-08-31
CH669603A5 (en) 1989-03-31
EP0261438A2 (en) 1988-03-30
JPH0830198B2 (en) 1996-03-27
CN87106375A (en) 1988-04-06
DE3764052D1 (en) 1990-09-06
JPS6389593A (en) 1988-04-20
ATE55145T1 (en) 1990-08-15
ES2016603B3 (en) 1990-11-16
EP0261438B1 (en) 1990-08-01
EP0261438A3 (en) 1988-12-07
CN1011515B (en) 1991-02-06

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