SU1099834A3 - Аппарат дл кислотно-каталитического алкилировани - Google Patents
Аппарат дл кислотно-каталитического алкилировани Download PDFInfo
- Publication number
- SU1099834A3 SU1099834A3 SU752127182A SU2127182A SU1099834A3 SU 1099834 A3 SU1099834 A3 SU 1099834A3 SU 752127182 A SU752127182 A SU 752127182A SU 2127182 A SU2127182 A SU 2127182A SU 1099834 A3 SU1099834 A3 SU 1099834A3
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- acid
- alkylation
- heat
- reaction
- reagents
- Prior art date
Links
- 239000002253 acid Substances 0.000 title claims abstract description 14
- 238000005804 alkylation reaction Methods 0.000 title abstract description 12
- 230000029936 alkylation Effects 0.000 title abstract description 7
- 239000003153 chemical reaction reagent Substances 0.000 claims description 15
- 238000005192 partition Methods 0.000 claims description 11
- 239000007795 chemical reaction product Substances 0.000 claims description 5
- 238000000034 method Methods 0.000 claims description 4
- 230000008569 process Effects 0.000 claims description 4
- 238000003442 catalytic alkylation reaction Methods 0.000 claims description 3
- 239000003377 acid catalyst Substances 0.000 abstract description 7
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 abstract description 6
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 abstract description 6
- NNPPMTNAJDCUHE-UHFFFAOYSA-N isobutane Chemical compound CC(C)C NNPPMTNAJDCUHE-UHFFFAOYSA-N 0.000 abstract description 6
- 239000003054 catalyst Substances 0.000 abstract description 5
- AFABGHUZZDYHJO-UHFFFAOYSA-N 2-Methylpentane Chemical compound CCCC(C)C AFABGHUZZDYHJO-UHFFFAOYSA-N 0.000 abstract description 4
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 abstract description 4
- VSCWAEJMTAWNJL-UHFFFAOYSA-K aluminium trichloride Chemical compound Cl[Al](Cl)Cl VSCWAEJMTAWNJL-UHFFFAOYSA-K 0.000 abstract description 4
- 239000007921 spray Substances 0.000 abstract description 4
- 239000001282 iso-butane Substances 0.000 abstract description 3
- 239000000376 reactant Substances 0.000 abstract description 3
- 229910015900 BF3 Inorganic materials 0.000 abstract description 2
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 abstract description 2
- 229910000147 aluminium phosphate Inorganic materials 0.000 abstract description 2
- WTEOIRVLGSZEPR-UHFFFAOYSA-N boron trifluoride Chemical compound FB(F)F WTEOIRVLGSZEPR-UHFFFAOYSA-N 0.000 abstract description 2
- 238000001816 cooling Methods 0.000 abstract description 2
- 239000008096 xylene Substances 0.000 abstract description 2
- QWTDNUCVQCZILF-UHFFFAOYSA-N isopentane Chemical compound CCC(C)C QWTDNUCVQCZILF-UHFFFAOYSA-N 0.000 abstract 2
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 abstract 1
- 229910000040 hydrogen fluoride Inorganic materials 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 description 16
- 229930195733 hydrocarbon Natural products 0.000 description 9
- 150000002430 hydrocarbons Chemical class 0.000 description 9
- 239000004215 Carbon black (E152) Substances 0.000 description 8
- 239000006185 dispersion Substances 0.000 description 8
- 239000000047 product Substances 0.000 description 7
- 150000001336 alkenes Chemical class 0.000 description 4
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 description 4
- -1 2-methylbutak Chemical compound 0.000 description 3
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 description 2
- QQONPFPTGQHPMA-UHFFFAOYSA-N Propene Chemical compound CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 2
- 239000002168 alkylating agent Substances 0.000 description 2
- 229940100198 alkylating agent Drugs 0.000 description 2
- 239000006227 byproduct Substances 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- 125000004432 carbon atom Chemical group C* 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 239000002826 coolant Substances 0.000 description 2
- 238000007599 discharging Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000002347 injection Methods 0.000 description 2
- 239000007924 injection Substances 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 229910019142 PO4 Inorganic materials 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 238000005054 agglomeration Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 150000008051 alkyl sulfates Chemical class 0.000 description 1
- 230000002152 alkylating effect Effects 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- 150000004945 aromatic hydrocarbons Chemical class 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 150000001721 carbon Chemical group 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 150000001896 cresols Chemical class 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 125000001188 haloalkyl group Chemical group 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 150000007522 mineralic acids Chemical class 0.000 description 1
- 150000005673 monoalkenes Chemical class 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 150000002989 phenols Chemical class 0.000 description 1
- 239000010452 phosphate Substances 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 239000003507 refrigerant Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 230000007480 spreading Effects 0.000 description 1
- 125000000383 tetramethylene group Chemical group [H]C([H])([*:1])C([H])([H])C([H])([H])C([H])([H])[*:2] 0.000 description 1
- 229930195735 unsaturated hydrocarbon Natural products 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/26—Nozzle-type reactors, i.e. the distribution of the initial reactants within the reactor is effected by their introduction or injection through nozzles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J14/00—Chemical processes in general for reacting liquids with liquids; Apparatus specially adapted therefor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/0013—Controlling the temperature of the process
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2/00—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms
- C07C2/54—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms by addition of unsaturated hydrocarbons to saturated hydrocarbons or to hydrocarbons containing a six-membered aromatic ring with no unsaturation outside the aromatic ring
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00076—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements inside the reactor
- B01J2219/00081—Tubes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00076—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements inside the reactor
- B01J2219/00083—Coils
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00121—Controlling the temperature by direct heating or cooling
- B01J2219/00123—Controlling the temperature by direct heating or cooling adding a temperature modifying medium to the reactants
- B01J2219/00126—Cryogenic coolants
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US462071A US3914111A (en) | 1974-04-18 | 1974-04-18 | Alkylation reaction chamber |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU1099834A3 true SU1099834A3 (ru) | 1984-06-23 |
Family
ID=23835065
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU752127182A SU1099834A3 (ru) | 1974-04-18 | 1975-04-18 | Аппарат дл кислотно-каталитического алкилировани |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US3914111A (enExample) |
| JP (1) | JPS5542048B2 (enExample) |
| AR (1) | AR210327A1 (enExample) |
| BR (1) | BR7502350A (enExample) |
| CA (1) | CA1051809A (enExample) |
| ES (1) | ES436486A1 (enExample) |
| FR (1) | FR2267996B1 (enExample) |
| GB (1) | GB1503747A (enExample) |
| IN (1) | IN144650B (enExample) |
| IT (1) | IT1035339B (enExample) |
| RO (1) | RO64346A (enExample) |
| SU (1) | SU1099834A3 (enExample) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2700768C1 (ru) * | 2018-06-25 | 2019-09-20 | Общество с ограниченной ответственностью "МилИнвест" (ООО "МилИнвест") | Реактор сернокислотного алкилирования |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3982903A (en) * | 1974-04-18 | 1976-09-28 | Universal Oil Products Company | Alkylation reaction chamber |
| US4024200A (en) * | 1974-12-16 | 1977-05-17 | Uop Inc. | Countercurrent flow reaction chamber for plural stages of HF alkylation |
| US4420462A (en) * | 1982-03-22 | 1983-12-13 | Clyde Robert A | Catalytic heat exchanger |
| US5227556A (en) * | 1990-04-17 | 1993-07-13 | The Dow Chemical Company | Turbulent flow process, monoalkyl aromatic production process and reactor for such process |
| DE102005049457A1 (de) * | 2005-10-15 | 2007-05-16 | Degussa | Vorrichtung zur Durchführung chemischer Reaktionen |
| US7947232B2 (en) * | 2006-12-07 | 2011-05-24 | Exxonmobil Research & Engineering Company | HF alkylation reactor |
| US8747783B2 (en) * | 2009-06-24 | 2014-06-10 | Uop Llc | Acid alkylation system and process for controlling temperature in a settler |
| US20110060178A1 (en) * | 2009-09-04 | 2011-03-10 | Nafis Douglas A | Slurry column gasoline alkylation using gas phase olefin injection |
| FR3008627B1 (fr) | 2013-07-19 | 2017-02-24 | Arkema France | Cuve de conversion thermique utilisee dans un procede d'amidification de cyanohydrine d'acetone |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2855449A (en) * | 1954-03-12 | 1958-10-07 | Phillips Petroleum Co | Method of and apparatus for the acid-catalyzed alkylation of hydrocarbons |
| US3006739A (en) * | 1958-12-03 | 1961-10-31 | Phillips Petroleum Co | Apparatus for contacting immiscible fluids |
| US3150934A (en) * | 1960-01-14 | 1964-09-29 | Texaco Inc | Apparatus for effecting fluidfluid contact |
| US3212860A (en) * | 1962-03-23 | 1965-10-19 | Phillips Petroleum Co | Method of and apparatus for contacting immiscible fluids |
| US3249649A (en) * | 1963-02-28 | 1966-05-03 | Phillips Petroleum Co | Catalytic alkylation |
| US3501536A (en) * | 1969-02-26 | 1970-03-17 | Universal Oil Prod Co | Alkylation with spiralling flow path of reactants and alkylate |
| US3560587A (en) * | 1969-04-14 | 1971-02-02 | Universal Oil Prod Co | Hydrogen fluoride alkylation with reaction cooler and reaction soaker vessels |
| US3607970A (en) * | 1969-04-25 | 1971-09-21 | Universal Oil Prod Co | Process for producing high octane alkylated hydrocarbons substantially free of alkyl fluoride compounds |
| US3705017A (en) * | 1970-11-27 | 1972-12-05 | Universal Oil Prod Co | Apparatus for a catalytic reaction |
-
1974
- 1974-04-18 US US462071A patent/US3914111A/en not_active Expired - Lifetime
-
1975
- 1975-04-09 IN IN715/CAL/75A patent/IN144650B/en unknown
- 1975-04-10 ES ES436486A patent/ES436486A1/es not_active Expired
- 1975-04-16 FR FR7511783A patent/FR2267996B1/fr not_active Expired
- 1975-04-16 IT IT49133/75A patent/IT1035339B/it active
- 1975-04-17 JP JP4588875A patent/JPS5542048B2/ja not_active Expired
- 1975-04-17 RO RO7582011A patent/RO64346A/ro unknown
- 1975-04-17 BR BR2994/75A patent/BR7502350A/pt unknown
- 1975-04-17 CA CA224,831A patent/CA1051809A/en not_active Expired
- 1975-04-17 GB GB15842/75A patent/GB1503747A/en not_active Expired
- 1975-04-18 SU SU752127182A patent/SU1099834A3/ru active
- 1975-04-18 AR AR256419A patent/AR210327A1/es active
Non-Patent Citations (1)
| Title |
|---|
| 1. Патент DE № 2230127, кл. В 01 J 8/06, 1974. 2. Патент US № 3607970, кл. 260-683.48, 1971. * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2700768C1 (ru) * | 2018-06-25 | 2019-09-20 | Общество с ограниченной ответственностью "МилИнвест" (ООО "МилИнвест") | Реактор сернокислотного алкилирования |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS50148302A (enExample) | 1975-11-27 |
| GB1503747A (en) | 1978-03-15 |
| JPS5542048B2 (enExample) | 1980-10-28 |
| AR210327A1 (es) | 1977-07-29 |
| RO64346A (fr) | 1979-05-15 |
| US3914111A (en) | 1975-10-21 |
| CA1051809A (en) | 1979-04-03 |
| FR2267996B1 (enExample) | 1979-07-13 |
| ES436486A1 (es) | 1977-01-01 |
| IT1035339B (it) | 1979-10-20 |
| IN144650B (enExample) | 1978-06-03 |
| FR2267996A1 (enExample) | 1975-11-14 |
| BR7502350A (pt) | 1976-02-17 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| RU2136358C1 (ru) | Способ и устройство для контроля температур (варианты) и способ каталитического дегидрирования углеводородов | |
| US5600053A (en) | Process and apparatus for controlling reaction temperatures | |
| US6106789A (en) | Alkylation reactor with internal acid cooling zones | |
| US5762887A (en) | Apparatus for controlling reaction temperatures | |
| US2491618A (en) | Catalytic contacting apparatus | |
| TWI486213B (zh) | 改良式管狀反應器及其中所使用之牽涉熱交換的觸媒反應之提昇方法 | |
| US3213157A (en) | Catalytic alkylation method and apparatus | |
| US3914111A (en) | Alkylation reaction chamber | |
| US7947232B2 (en) | HF alkylation reactor | |
| US3212860A (en) | Method of and apparatus for contacting immiscible fluids | |
| US3501536A (en) | Alkylation with spiralling flow path of reactants and alkylate | |
| WO2017100493A1 (en) | Reactor system for use with an ionic liquid catalyst | |
| WO2016094241A2 (en) | Ionic liquid reactor with heat exchanger | |
| US3006739A (en) | Apparatus for contacting immiscible fluids | |
| US3108048A (en) | Apparatus for contacting of different density fluids | |
| US3249649A (en) | Catalytic alkylation | |
| CA2007987A1 (en) | Alkylation catalyst isolation | |
| JP3080403B2 (ja) | 乱流プロセスとモノアルキル芳香族炭化水素の製造 | |
| US3982903A (en) | Alkylation reaction chamber | |
| JP2678385B2 (ja) | 自己温度調節流体の使用によるオレフィンの接触二量化、共二量化またはオリゴマー化方法 | |
| EA006358B1 (ru) | Распределитель потока для реактора алкилирования или теплообменника | |
| US3758613A (en) | Hydrogen fluoride-catalyzed alkylation with a venturi-shaped reactor | |
| US4000212A (en) | Unitary acid-hydrocarbon reactor in hydrocarbon alkylation | |
| US3469949A (en) | Alkylation apparatus forming an upwardly spiralling flow path of reactants | |
| US20170189884A1 (en) | Reactor for use with an ionic liquid catalyst |