SG11201901880SA - Volume change compensated silicon-silicon oxide-lithium composite material having nano silicon particles embedded in a silicon: silicon lithium silicate composite matrix, and cyclical ex-situ manufacturing processes - Google Patents
Volume change compensated silicon-silicon oxide-lithium composite material having nano silicon particles embedded in a silicon: silicon lithium silicate composite matrix, and cyclical ex-situ manufacturing processesInfo
- Publication number
- SG11201901880SA SG11201901880SA SG11201901880SA SG11201901880SA SG11201901880SA SG 11201901880S A SG11201901880S A SG 11201901880SA SG 11201901880S A SG11201901880S A SG 11201901880SA SG 11201901880S A SG11201901880S A SG 11201901880SA SG 11201901880S A SG11201901880S A SG 11201901880SA
- Authority
- SG
- Singapore
- Prior art keywords
- silicon
- sslc material
- volume change
- prelithiated
- sslc
- Prior art date
Links
Classifications
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/362—Composites
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/362—Composites
- H01M4/364—Composites as mixtures
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/04—Processes of manufacture in general
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/04—Processes of manufacture in general
- H01M4/0438—Processes of manufacture in general by electrochemical processing
- H01M4/044—Activating, forming or electrochemical attack of the supporting material
- H01M4/0445—Forming after manufacture of the electrode, e.g. first charge, cycling
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/38—Selection of substances as active materials, active masses, active liquids of elements or alloys
- H01M4/386—Silicon or alloys based on silicon
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
- H01M4/483—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides for non-aqueous cells
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
- H01M4/485—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of mixed oxides or hydroxides for inserting or intercalating light metals, e.g. LiTi2O4 or LiTi2OxFy
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M10/00—Secondary cells; Manufacture thereof
- H01M10/05—Accumulators with non-aqueous electrolyte
- H01M10/052—Li-accumulators
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M10/00—Secondary cells; Manufacture thereof
- H01M10/05—Accumulators with non-aqueous electrolyte
- H01M10/052—Li-accumulators
- H01M10/0525—Rocking-chair batteries, i.e. batteries with lithium insertion or intercalation in both electrodes; Lithium-ion batteries
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M2004/026—Electrodes composed of, or comprising, active material characterised by the polarity
- H01M2004/027—Negative electrodes
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/13—Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
- H01M4/139—Processes of manufacture
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/13—Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
- H01M4/139—Processes of manufacture
- H01M4/1391—Processes of manufacture of electrodes based on mixed oxides or hydroxides, or on mixtures of oxides or hydroxides, e.g. LiCoOx
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/13—Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
- H01M4/139—Processes of manufacture
- H01M4/1395—Processes of manufacture of electrodes based on metals, Si or alloys
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/10—Energy storage using batteries
Abstract
INTERNATIONAL APPLICATION PUBLISHED UNDER THE PATENT COOPERATION TREATY (PCT) (19) World Intellectual Property :::` , Organization 3 MD HIM 01E101011M 3E1 0 1011101fl 0111 00I1011 NH ill OEN International Bureau (10) International Publication Number (43) International Publication Date .....•\"\"- WO 2018/042361 Al 08 March 2018 (08.03.2018) WIP0 I PCT (51) International Patent Classification: CA, CH, CL, CN, CO, CR, CU, CZ, DE, DJ, DK, DM, DO, HO1M 4/36 (2006.01) C01B 33/02 (2006.01) DZ, EC, EE, EG, ES, FI, GB, GD, GE, GH, GM, GT, HN, (21) International Application Number: HR, HU, ID, IL, IN, IR, IS, JO, JP, KE, KG, KH, KN, KP, PCT/IB2017/055236 KR, KW, KZ, LA, LC, LK, LR, LS, LU, LY, MA, MD, ME, MG, MK, MN, MW, MX, MY, MZ, NA, NG, NI, NO, NZ, (22) International Filing Date: OM, PA, PE, PG, PH, PL, PT, QA, RO, RS, RU, RW, SA, 31 August 2017 (31.08.2017) SC, SD, SE, SG, SK, SL, SM, ST, SV, SY, TH, TJ, TM, TN, TR, TT, TZ, UA, UG, US, UZ, VC, VN, ZA, ZM, ZW. (25) Filing Language: English (26) Publication Language: English (84) Designated States (unless otherwise indicated, for every kind of regional protection available): ARIPO (BW, GH, (30) Priority Data: GM, KE, LR, LS, MW, MZ, NA, RW, SD, SL, ST, SZ, TZ, 62/383,372 02 September 2016 (02.09.2016) US UG, ZM, ZW), Eurasian (AM, AZ, BY, KG, KZ, RU, TJ, 62/478,535 29 March 2017 (29.03.2017) US TM), European (AL, AT, BE, BG, CH, CY, CZ, DE, DK, EE, ES, FI, FR, GB, GR, HR, HU, IE, IS, IT, LT, LU, LV, (71) Applicant: EOCELL LIMITED [CN/CN]; Room 804, MC, MK, MT, NL, NO, PL, PT, RO, RS, SE, SI, SK, SM, Lap Fai Building, 6-8 Pottinger Street, Central, Hong Kong, TR), OAPI (BF, BJ, CF, CG, CI, CM, GA, GN, GQ, GW, Hong Kong (CN). KM, ML, MR, NE, SN, TD, TG). (72) Inventors: MATUS, Yuriy; 4025 Rennellwood Way, Pleasanton, California 94566 (US). HAN, Yongbong; 226 Published: Laidley Street, San Francisco, California 94131 (US). PAK, — with international search report (Art. 21(3)) — Michael; 2200 Lake Road, Belmont, California 94002 = (US). = (81) Designated States (unless otherwise indicated, for every _ kind of national protection available): AE, AG, AL, AM, — AO, AT, AU, AZ, BA, BB, BG, BH, BN, BR, BW, BY, BZ, = = = = (54) Title: VOLUME CHANGE COMPENSATED SILICON-SILICON OXIDE-LITHIUM COMPOSITE MATERIAL HAVING _ NANO SILICON PARTICLES EMBEDDED IN A SILICON: SILICON LITHIUM SILICATE COMPOSITE MATRIX, AND CY- _ CLICAL EX-SITU MANUFACTURING PROCESSES = (57) : A method for producing a volume change compensated silicon: silicon ox- 110 = = Produce Prelithiated SSLC Material Exhibiting Enhanced, Substantially Complete or Complete Lithiation ide: lithium composite (SSLC) material is disclosed. The method includes producing an initially prelithiated SSLC material; delithiating the initially prelithiated material to pro- duce delithiated least iteration Produce Partially Lithiated SSLC Material a SSLC material; and performing at one of a volume change compensation process involving: (a) re-prelithiating the delithiated SSLC material to pro- = 2 114 --) duce are-prelithiated SSLC material; and (b) delithiating the re-prelithiated SSLC material = = = Complete Reaction of Unreacted Lithium and SiO in the Partially x Lithiated SSLC Material to Produce Further Lithiated SSLC Material produced in (a), wherein at least one of the following is satisfied: (i) prior to performing the at least one iteration of the volume change compensation process the initially prelithi- ated SSLC material is essentially completely lithiated; and (ii) at least one iteration of the = - 120 -, 1 volume change compensation process produces a re-prelithiated SSLC material that is es- — L = Delithiate the Produced Prelithiated SSLC Material to Produce Completely DelithiatedSSLC Material Having Si Nano Particles Embedded in a Porous Plastically Deformable Li. SLC Matrix sentially completely prelithiated. In a fmal iteration of the volume change compensation process, delithiating the re-prelithiated SSLC material produced in (a) completely delithi- ates the re-prelithiated SSLC material to produce the volume change compensated SSLC material. The aforesaid is to, or ex situ with respect to, the fabri- process performed prior _ 130 i cation of an anode that contains the produced volume change compensated SSLC material. Filter / Wash / Dry the Delithiated SSLC Material Il 140 V; Mechanically Stabilize the Delithiated SSLC Material en el 150 i 71 . © GC Enhance the Electrical Conductivity of the Delithiated SSLC Material with Carbon / Carbon Based Matenal(s) (e g , Graphite) 11 © el FIG. 1 loo
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US201662383372P | 2016-09-02 | 2016-09-02 | |
US201762478535P | 2017-03-29 | 2017-03-29 | |
PCT/IB2017/055236 WO2018042361A1 (en) | 2016-09-02 | 2017-08-31 | Volume change compensated silicon-silicon oxide-lithium composite material having nano silicon particles embedded in a silicon: silicon lithium silicate composite matrix, and cyclical ex-situ manufacturing processes |
Publications (1)
Publication Number | Publication Date |
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SG11201901880SA true SG11201901880SA (en) | 2019-03-28 |
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Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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SG11201901880SA SG11201901880SA (en) | 2016-09-02 | 2017-08-31 | Volume change compensated silicon-silicon oxide-lithium composite material having nano silicon particles embedded in a silicon: silicon lithium silicate composite matrix, and cyclical ex-situ manufacturing processes |
Country Status (11)
Country | Link |
---|---|
US (1) | US10347907B2 (en) |
EP (1) | EP3507845B1 (en) |
JP (1) | JP6940595B2 (en) |
KR (1) | KR102355992B1 (en) |
CN (1) | CN109923706B (en) |
HU (1) | HUE055597T2 (en) |
MY (1) | MY190556A (en) |
PL (1) | PL3507845T3 (en) |
SG (1) | SG11201901880SA (en) |
TW (1) | TWI778974B (en) |
WO (1) | WO2018042361A1 (en) |
Families Citing this family (16)
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KR101766535B1 (en) * | 2014-10-02 | 2017-08-10 | 주식회사 엘지화학 | Negative electrode active material for lithium secondary battery, method for preparing the same, and lithium secondary battery comprising the same |
JP2019160724A (en) * | 2018-03-16 | 2019-09-19 | Tdk株式会社 | Negative electrode and lithium ion secondary battery |
WO2020129652A1 (en) * | 2018-12-21 | 2020-06-25 | パナソニックIpマネジメント株式会社 | Negative electrode active material for secondary batteries, and secondary battery |
US10916763B2 (en) * | 2019-06-03 | 2021-02-09 | Enevate Corporation | Surface-fluorinated silicon-containing electrodes |
CN110311121B (en) * | 2019-07-10 | 2022-05-06 | 洛阳联创锂能科技有限公司 | Lithium-containing silicon oxide negative electrode material for lithium ion battery and preparation method thereof |
EP4107807A1 (en) * | 2020-02-19 | 2022-12-28 | University of Maryland, College Park | High-performance microsized anodes and methods of making and using the same |
JP7268633B2 (en) * | 2020-04-07 | 2023-05-08 | トヨタ自動車株式会社 | Method for producing active material |
CN113809285B (en) * | 2020-06-12 | 2023-08-08 | 比亚迪股份有限公司 | Silicon-based composite anode material, preparation method thereof and all-solid-state lithium battery |
CN113809309B (en) * | 2020-06-12 | 2023-08-08 | 比亚迪股份有限公司 | Silicon-based composite anode material, preparation method thereof and all-solid-state lithium battery |
CN113809330B (en) * | 2020-06-12 | 2023-08-08 | 比亚迪股份有限公司 | Silicon-based composite anode material, preparation method thereof and all-solid-state lithium battery |
GB202012302D0 (en) * | 2020-08-07 | 2020-09-23 | Kings College | Lithiated silicon |
CN112164779B (en) * | 2020-09-24 | 2022-03-08 | 长沙矿冶研究院有限责任公司 | Carbon-coated silicon-based negative electrode material and preparation method thereof |
CN112234160B (en) * | 2020-10-20 | 2022-02-11 | 陕西煤业化工技术研究院有限责任公司 | Lithium supplementing method for lithium ion battery negative electrode active material |
CN112701267B (en) * | 2020-12-30 | 2022-02-08 | 湖州杉杉新能源科技有限公司 | Pre-lithiated silica composite material, negative pole piece, lithium battery and preparation method of pre-lithiated silica composite material |
CN114835131A (en) * | 2022-03-21 | 2022-08-02 | 湖北钛时代新能源有限公司 | Preparation method of lithium silicate cathode material and lithium ion battery |
DE102022205073A1 (en) | 2022-05-20 | 2023-11-23 | Volkswagen Aktiengesellschaft | Method for producing a battery cell |
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KR100686783B1 (en) * | 2006-01-16 | 2007-02-26 | 엘에스전선 주식회사 | Anode material for secondary battery, method for producing of itself and secondary batteries using the same |
JP4985949B2 (en) * | 2006-03-27 | 2012-07-25 | 信越化学工業株式会社 | Method for producing silicon-silicon oxide-lithium composite, and negative electrode material for non-aqueous electrolyte secondary battery |
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KR102592237B1 (en) * | 2015-03-02 | 2023-10-20 | 이오셀 리미티드 | Silicon-silicon oxide-lithium composite material having nano-silicon particles embedded in a silicon:silicon lithium silicate composite matrix and method for manufacturing the same |
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PL3586387T3 (en) * | 2017-02-21 | 2024-03-18 | Tesla, Inc. | Prelithiated energy storage device |
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2017
- 2017-08-31 JP JP2019512256A patent/JP6940595B2/en active Active
- 2017-08-31 EP EP17845639.8A patent/EP3507845B1/en active Active
- 2017-08-31 WO PCT/IB2017/055236 patent/WO2018042361A1/en unknown
- 2017-08-31 PL PL17845639T patent/PL3507845T3/en unknown
- 2017-08-31 US US15/691,780 patent/US10347907B2/en active Active
- 2017-08-31 KR KR1020197008414A patent/KR102355992B1/en active IP Right Grant
- 2017-08-31 SG SG11201901880SA patent/SG11201901880SA/en unknown
- 2017-08-31 CN CN201780054191.1A patent/CN109923706B/en active Active
- 2017-08-31 MY MYPI2019001116A patent/MY190556A/en unknown
- 2017-08-31 HU HUE17845639A patent/HUE055597T2/en unknown
- 2017-09-01 TW TW106129969A patent/TWI778974B/en active
Also Published As
Publication number | Publication date |
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EP3507845B1 (en) | 2021-03-31 |
KR102355992B1 (en) | 2022-01-26 |
EP3507845A4 (en) | 2020-04-01 |
CN109923706B (en) | 2022-01-04 |
TW201817063A (en) | 2018-05-01 |
PL3507845T3 (en) | 2021-07-19 |
KR20190042655A (en) | 2019-04-24 |
HUE055597T2 (en) | 2022-05-28 |
JP2019533878A (en) | 2019-11-21 |
US20180069233A1 (en) | 2018-03-08 |
CN109923706A (en) | 2019-06-21 |
EP3507845A1 (en) | 2019-07-10 |
TWI778974B (en) | 2022-10-01 |
MY190556A (en) | 2022-04-27 |
US10347907B2 (en) | 2019-07-09 |
WO2018042361A1 (en) | 2018-03-08 |
JP6940595B2 (en) | 2021-09-29 |
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