SG11201811500VA - Method for reactivation of a homogeneous oxidation catalyst - Google Patents

Method for reactivation of a homogeneous oxidation catalyst

Info

Publication number
SG11201811500VA
SG11201811500VA SG11201811500VA SG11201811500VA SG11201811500VA SG 11201811500V A SG11201811500V A SG 11201811500VA SG 11201811500V A SG11201811500V A SG 11201811500VA SG 11201811500V A SG11201811500V A SG 11201811500VA SG 11201811500V A SG11201811500V A SG 11201811500VA
Authority
SG
Singapore
Prior art keywords
reactivation
oxidation catalyst
homogeneous oxidation
homogeneous
catalyst
Prior art date
Application number
SG11201811500VA
Inventor
Ralf Meier
Stephanie Bajus
Jens Döring
Original Assignee
Evonik Degussa Gmbh
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Evonik Degussa Gmbh filed Critical Evonik Degussa Gmbh
Publication of SG11201811500VA publication Critical patent/SG11201811500VA/en

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J38/00Regeneration or reactivation of catalysts, in general
    • B01J38/48Liquid treating or treating in liquid phase, e.g. dissolved or suspended
    • B01J38/64Liquid treating or treating in liquid phase, e.g. dissolved or suspended using alkaline material; using salts
    • B01J38/66Liquid treating or treating in liquid phase, e.g. dissolved or suspended using alkaline material; using salts using ammonia or derivatives thereof
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/16Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/24Chromium, molybdenum or tungsten
    • B01J23/30Tungsten
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J38/00Regeneration or reactivation of catalysts, in general
    • B01J38/48Liquid treating or treating in liquid phase, e.g. dissolved or suspended
    • B01J38/64Liquid treating or treating in liquid phase, e.g. dissolved or suspended using alkaline material; using salts
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C249/00Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C249/04Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes
    • C07C249/08Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes by reaction of hydroxylamines with carbonyl compounds
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/56Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds from heterocyclic compounds
    • C07C45/57Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds from heterocyclic compounds with oxygen as the only heteroatom
    • C07C45/58Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds from heterocyclic compounds with oxygen as the only heteroatom in three-membered rings
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D225/00Heterocyclic compounds containing rings of more than seven members having one nitrogen atom as the only ring hetero atom
    • C07D225/02Heterocyclic compounds containing rings of more than seven members having one nitrogen atom as the only ring hetero atom not condensed with other rings
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D301/00Preparation of oxiranes
    • C07D301/02Synthesis of the oxirane ring
    • C07D301/03Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
    • C07D301/12Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with hydrogen peroxide or inorganic peroxides or peracids
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00Systems containing only non-condensed rings
    • C07C2601/18Systems containing only non-condensed rings with a ring being at least seven-membered
    • C07C2601/20Systems containing only non-condensed rings with a ring being at least seven-membered the ring being twelve-membered
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/50Improvements relating to the production of bulk chemicals
    • Y02P20/584Recycling of catalysts

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
SG11201811500VA 2016-06-30 2017-06-28 Method for reactivation of a homogeneous oxidation catalyst SG11201811500VA (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP16177260.3A EP3263557A1 (en) 2016-06-30 2016-06-30 Method for reactivation of a homogeneous oxidation catalyst
PCT/EP2017/065957 WO2018002114A1 (en) 2016-06-30 2017-06-28 Method for reactivating a homogeneous oxidation catalyst

Publications (1)

Publication Number Publication Date
SG11201811500VA true SG11201811500VA (en) 2019-01-30

Family

ID=56292524

Family Applications (2)

Application Number Title Priority Date Filing Date
SG10201912345YA SG10201912345YA (en) 2016-06-30 2017-06-28 Method for reactivation of a homogeneous oxidation catalyst
SG11201811500VA SG11201811500VA (en) 2016-06-30 2017-06-28 Method for reactivation of a homogeneous oxidation catalyst

Family Applications Before (1)

Application Number Title Priority Date Filing Date
SG10201912345YA SG10201912345YA (en) 2016-06-30 2017-06-28 Method for reactivation of a homogeneous oxidation catalyst

Country Status (7)

Country Link
US (1) US10994270B2 (en)
EP (2) EP3263557A1 (en)
JP (1) JP6732971B2 (en)
CN (1) CN109641862B (en)
ES (1) ES2721794T3 (en)
SG (2) SG10201912345YA (en)
WO (1) WO2018002114A1 (en)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP3578539A1 (en) 2018-06-07 2019-12-11 Evonik Operations GmbH Method for the continuous production of ketones from epoxides in a fixed bed
KR102499747B1 (en) * 2018-12-19 2023-02-15 한화솔루션 주식회사 Novel process for producing Laurolactam and synthesis apparatus thereof
KR20220083279A (en) * 2020-12-11 2022-06-20 한화솔루션 주식회사 Recovery and reuse method of homogeneous selective hydrogenation catalyst

Family Cites Families (22)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2869986A (en) * 1955-03-31 1959-01-20 Shell Dev Recovery of tungstic catalysts
US2968527A (en) * 1957-10-03 1961-01-17 Columbia Southern Chem Corp Method of recovering tungstic acid values from aqueous media
GB894592A (en) * 1957-10-03 1962-04-26 Columbia Southern Chem Corp Process for the recovery of tungstic acid catalyst
FR1306120A (en) * 1961-09-01 1962-10-13 Electrochimie Soc Tungstic catalyst recovery process
GB1518338A (en) * 1974-11-18 1978-07-19 Degussa Process for separating epoxidation and hydroxylation catalysts from distillation residues
NL182292C (en) * 1974-11-18 1988-02-16 Degussa PROCESS FOR RECOVERY OF ALKALINE METAL VANADATE, MOLYBDATE AND / OR WOOL FRAME CATALYSTS.
DE2543333C2 (en) * 1975-09-29 1985-06-20 Degussa Ag, 6000 Frankfurt Process for the simultaneous production of pure grape acid and meso-tartaric acid
GB1520920A (en) * 1975-02-26 1978-08-09 Degussa Production of pure racemic acid and mesotartaric acid
NL8004084A (en) 1979-07-19 1981-01-21 Donegani Guido Ist PROCESS FOR THE CATALYTIC EPOXYDATION OF OLEKINS WITH HYDROGEN PEROXIDE.
JPH0720552B2 (en) * 1986-11-20 1995-03-08 三菱レイヨン株式会社 Regeneration method of oxidation catalyst
JPH04190851A (en) * 1990-11-27 1992-07-09 Mitsui Toatsu Chem Inc Regeneration of catalyst for preparing maleimides
FR2789073B1 (en) 1999-01-28 2002-02-15 Novance PREPARATION OF MONOCARBOXYL FATTY ACID DERIVATIVES CARRYING TWO VICINAL HYDROXYL FUNCTIONS OR AN EPOXIDE FUNCTION
DE10247496A1 (en) 2002-10-11 2004-04-22 Degussa Ag Use of a sales accelerator in epoxidation
CA2597120C (en) * 2005-03-07 2013-08-06 Yasuteru Kajikawa Methods for oxidizing organic compounds
KR20080077015A (en) * 2005-12-22 2008-08-20 셀 인터나쵸나아레 레사아치 마아츠샤피 비이부이 A process for the preparation of an olefin oxide or a chemical derivable from an olefin oxide, and a reactor suitable for such a process
EP2537836A1 (en) * 2011-06-22 2012-12-26 Momentive Specialty Chemicals Research Belgium S.A. Apparatus and methods to preserve catalyst activity in an epoxidation process
WO2014175152A1 (en) * 2013-04-23 2014-10-30 株式会社ダイセル Recovery method and reuse method of oxo acid catalyst
DE102014209421A1 (en) * 2014-05-19 2015-11-19 Evonik Degussa Gmbh Membrane-assisted catalyst separation in the epoxidation of cyclic, unsaturated C12 compounds, for example cyclododecene (CDEN)
EP2980069A1 (en) * 2014-08-01 2016-02-03 Evonik Degussa GmbH Method for preparation of cyclododecanone
EP3002058A1 (en) * 2014-10-02 2016-04-06 Evonik Degussa GmbH Catalyst system for the production of ketones from epoxides
EP3330247B1 (en) * 2016-12-02 2019-05-08 Evonik Degussa GmbH Catalytic oxidation of 3,5,5-trimethylcyclohexa-3-ene-1-one (beta-isophorone) with hydrogen peroxide to 2,6,6-trimethyl-2-cyclohexene-1,4-dion (keto isophorone)
CN109516941B (en) * 2017-09-20 2020-08-28 万华化学集团股份有限公司 Production method of laurolactam

Also Published As

Publication number Publication date
ES2721794T3 (en) 2019-08-05
WO2018002114A1 (en) 2018-01-04
EP3374353A1 (en) 2018-09-19
US20190232271A1 (en) 2019-08-01
EP3263557A1 (en) 2018-01-03
EP3374353B1 (en) 2019-02-13
CN109641862A (en) 2019-04-16
CN109641862B (en) 2022-11-18
SG10201912345YA (en) 2020-02-27
US10994270B2 (en) 2021-05-04
JP6732971B2 (en) 2020-07-29
JP2019523121A (en) 2019-08-22

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